#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/00/2200076.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200076_Fobs loop_ _publ_author_name 'Batten, Stuart R.' 'Harris, Alexander R.' _publ_section_title ; trans-Tetraaquabis(pyridine-4-carboxylate-\kN)nickel(II) ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m7 _journal_page_last m8 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 96.511 _cell_angle_beta 104.929 _cell_angle_gamma 113.692 _cell_length_a 6.2862 _cell_length_b 6.8598 _cell_length_c 9.2394 _exptl_crystal_F_000 194.00 _reflns_d_resolution_high 0.7507 _[local]_cod_data_source_file ob6007Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ah29 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 84.22 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 148.14 143.84 6.09 o 2 0 0 31.87 33.98 1.42 o 3 0 0 9.29 7.77 0.72 o 4 0 0 423.66 417.34 13.05 o 5 0 0 142.00 152.60 5.69 o 6 0 0 73.27 80.46 3.31 o 7 0 0 31.84 29.79 2.63 o -7 1 0 35.47 28.18 2.71 o -6 1 0 180.63 191.20 8.21 o -5 1 0 490.91 492.16 16.27 o -4 1 0 506.45 522.69 18.64 o -3 1 0 407.06 519.89 17.70 o -2 1 0 812.95 774.19 23.30 o -1 1 0 602.80 580.80 31.96 o 1 1 0 515.26 497.93 20.74 o 2 1 0 16.36 25.34 1.01 o 3 1 0 1016.78 1073.54 42.49 o 4 1 0 273.24 279.51 9.48 o 5 1 0 111.73 115.07 4.62 o 6 1 0 147.12 139.14 4.82 o -7 2 0 39.81 36.75 4.06 o -6 2 0 13.10 21.29 4.11 o -5 2 0 217.46 207.97 6.84 o -4 2 0 348.90 338.47 10.82 o -3 2 0 1511.11 1612.10 55.31 o -2 2 0 1221.07 1230.83 40.31 o -1 2 0 7092.22 7267.99 267.87 o 0 2 0 2194.76 2224.63 72.57 o 1 2 0 663.85 604.07 32.69 o 2 2 0 764.78 744.34 30.72 o 3 2 0 358.57 356.91 15.60 o 4 2 0 1.65 2.08 0.61 o 5 2 0 14.98 13.88 1.37 o 6 2 0 88.88 82.58 4.71 o -7 3 0 92.37 92.71 6.30 o -6 3 0 45.55 42.49 2.66 o -5 3 0 41.28 44.62 2.25 o -4 3 0 5.49 10.30 2.20 o -3 3 0 2111.11 2275.16 71.77 o -2 3 0 155.33 160.14 4.93 o -1 3 0 115.35 109.70 2.17 o 0 3 0 72.87 66.16 1.85 o 1 3 0 90.55 81.18 3.44 o 2 3 0 1032.83 1056.94 39.56 o 3 3 0 274.75 287.67 15.35 o 4 3 0 187.51 190.14 7.34 o 5 3 0 124.84 120.39 9.23 o -7 4 0 52.58 60.73 4.65 o -6 4 0 386.76 380.02 12.96 o -5 4 0 255.23 263.55 9.88 o -4 4 0 278.46 281.01 8.41 o -3 4 0 280.47 277.80 9.06 o -2 4 0 1940.92 2042.72 43.43 o -1 4 0 70.69 91.17 1.86 o 0 4 0 653.36 646.02 18.38 o 1 4 0 12.43 14.67 1.23 o 2 4 0 17.96 16.78 1.52 o 3 4 0 72.18 74.80 3.79 o 4 4 0 166.33 164.96 7.08 o -7 5 0 143.42 152.69 10.75 o -6 5 0 217.01 214.70 15.03 o -5 5 0 17.54 16.11 1.67 o -4 5 0 362.56 394.95 12.88 o -3 5 0 22.17 24.44 0.86 o -2 5 0 351.25 354.20 9.36 o -1 5 0 402.78 399.11 7.46 o 0 5 0 199.94 195.92 6.60 o 1 5 0 355.12 361.84 31.41 o 2 5 0 95.87 101.81 6.53 o 3 5 0 137.51 130.70 5.76 o 4 5 0 50.85 43.97 5.08 o -7 6 0 297.88 287.02 16.38 o -6 6 0 143.44 139.42 8.21 o -5 6 0 161.24 162.34 4.21 o -4 6 0 233.06 229.48 5.54 o -3 6 0 359.29 369.45 10.14 o -2 6 0 124.62 118.98 5.42 o -1 6 0 196.91 185.34 7.93 o 0 6 0 57.51 59.00 2.81 o 1 6 0 164.35 169.64 13.86 o 2 6 0 103.42 111.50 14.08 o 3 6 0 12.76 23.87 6.11 o -7 7 0 3.35 1.89 3.33 o -6 7 0 0.67 -0.11 1.73 o -5 7 0 342.91 320.38 16.32 o -4 7 0 49.96 50.64 2.39 o -3 7 0 287.36 294.09 11.98 o -2 7 0 34.99 32.48 2.54 o -1 7 0 38.16 39.04 1.24 o 0 7 0 281.11 297.35 12.83 o 1 7 0 142.10 146.70 11.84 o -6 8 0 23.40 21.34 4.57 o -5 8 0 90.61 93.41 6.25 o -4 8 0 85.83 81.65 6.83 o -3 8 0 8.81 3.80 1.32 o -2 8 0 200.04 185.04 7.40 o 0 8 0 45.14 48.12 6.91 o 0 -8 1 36.69 35.82 7.08 o 2 -8 1 40.93 25.84 2.68 o 3 -8 1 181.16 178.14 16.03 o 4 -8 1 224.57 207.79 10.49 o 5 -8 1 113.62 120.95 8.16 o 6 -8 1 30.14 25.33 3.97 o -2 -7 1 95.71 98.33 5.25 o -1 -7 1 317.51 297.65 13.13 o 0 -7 1 90.29 99.89 10.83 o 1 -7 1 3.73 4.31 1.35 o 2 -7 1 2.28 4.39 1.10 o 3 -7 1 60.75 63.27 2.55 o 4 -7 1 431.07 433.65 11.57 o 5 -7 1 73.04 75.49 10.13 o 6 -7 1 1.23 0.42 2.21 o 7 -7 1 64.67 49.90 6.72 o -3 -6 1 7.20 4.23 2.51 o -2 -6 1 123.88 134.88 16.45 o -1 -6 1 192.67 190.85 12.14 o 0 -6 1 168.87 168.19 3.65 o 1 -6 1 66.29 66.12 2.38 o 2 -6 1 694.38 714.65 33.02 o 3 -6 1 493.21 490.75 11.72 o 4 -6 1 155.78 151.42 4.15 o 5 -6 1 115.65 122.39 4.20 o 6 -6 1 206.32 218.56 12.18 o 7 -6 1 28.00 25.02 4.10 o -4 -5 1 82.52 81.60 5.96 o -3 -5 1 180.88 181.59 7.44 o -2 -5 1 218.21 211.56 18.46 o -1 -5 1 1.07 1.51 1.03 o 0 -5 1 32.17 31.46 0.92 o 1 -5 1 371.09 374.57 9.26 o 2 -5 1 364.30 364.13 9.33 o 3 -5 1 152.59 159.65 3.69 o 4 -5 1 10.18 11.51 1.55 o 5 -5 1 44.50 46.62 2.75 o 6 -5 1 533.97 561.04 25.57 o 7 -5 1 80.64 68.51 6.07 o -5 -4 1 135.41 123.20 7.57 o -4 -4 1 19.34 18.29 1.96 o -3 -4 1 349.19 356.47 22.52 o -2 -4 1 26.40 27.54 2.00 o -1 -4 1 35.32 35.46 1.70 o 0 -4 1 64.81 48.66 2.04 o 1 -4 1 4406.92 4434.31 105.26 o 2 -4 1 913.12 883.06 21.48 o 3 -4 1 25.49 22.86 1.39 o 4 -4 1 109.60 110.82 4.06 o 5 -4 1 164.84 166.10 6.97 o 6 -4 1 50.20 52.97 6.61 o 7 -4 1 41.18 41.71 4.75 o -5 -3 1 100.25 96.82 5.37 o -4 -3 1 180.03 206.34 10.37 o -3 -3 1 247.40 250.28 14.40 o -2 -3 1 2.92 2.51 0.95 o -1 -3 1 170.45 168.40 8.15 o 0 -3 1 364.66 350.80 10.87 o 1 -3 1 200.35 179.62 4.30 o 2 -3 1 407.13 394.42 11.24 o 3 -3 1 285.92 271.08 8.46 o 4 -3 1 443.28 438.86 13.71 o 5 -3 1 363.05 372.69 12.29 o 6 -3 1 9.28 11.57 1.99 o 7 -3 1 212.01 203.13 11.48 o -6 -2 1 147.40 142.76 8.88 o -5 -2 1 24.28 18.46 1.09 o -4 -2 1 209.19 208.20 6.11 o -3 -2 1 192.19 192.14 4.89 o -2 -2 1 1497.17 1531.27 36.84 o -1 -2 1 1152.07 1171.45 33.10 o 0 -2 1 4229.32 4128.92 115.63 o 1 -2 1 67.75 77.02 2.80 o 2 -2 1 37.41 42.84 1.86 o 3 -2 1 994.91 1000.43 35.56 o 4 -2 1 235.68 252.94 7.84 o 5 -2 1 45.14 51.03 2.72 o 6 -2 1 23.16 28.34 2.08 o 7 -2 1 87.32 86.70 6.94 o -6 -1 1 123.71 127.13 4.62 o -5 -1 1 63.83 66.73 2.42 o -4 -1 1 100.36 107.28 3.90 o -3 -1 1 1.55 8.00 0.65 o -2 -1 1 672.31 680.09 19.94 o -1 -1 1 834.64 875.70 27.62 o 0 -1 1 672.93 617.42 31.05 o 1 -1 1 572.86 585.56 23.54 o 2 -1 1 88.63 78.73 3.10 o 3 -1 1 339.33 346.61 10.17 o 4 -1 1 703.86 710.80 23.45 o 5 -1 1 368.35 369.17 12.92 o 6 -1 1 442.00 446.60 18.26 o 7 -1 1 20.68 25.56 3.17 o -7 0 1 28.28 24.71 2.78 o -6 0 1 2.02 5.82 1.12 o -5 0 1 1046.64 1015.48 33.88 o -4 0 1 419.46 434.69 14.50 o -3 0 1 377.19 380.03 11.99 o -2 0 1 70.26 72.41 2.56 o -1 0 1 5117.66 4723.97 278.58 o 0 0 1 455.74 449.27 26.34 o 1 0 1 335.80 314.91 13.12 o 2 0 1 97.10 82.98 3.05 o 3 0 1 21.93 19.79 1.67 o 4 0 1 225.09 228.82 6.80 o 5 0 1 207.16 199.01 6.64 o 6 0 1 197.17 192.52 10.88 o -7 1 1 52.22 60.63 4.16 o -6 1 1 98.67 95.18 3.96 o -5 1 1 337.31 338.30 9.74 o -4 1 1 34.39 22.93 1.26 o -3 1 1 376.13 373.48 11.09 o -2 1 1 107.95 130.88 5.04 o -1 1 1 441.65 461.17 12.79 o 0 1 1 1002.60 1031.43 27.50 o 1 1 1 370.54 347.13 11.68 o 2 1 1 963.05 974.24 38.57 o 3 1 1 822.05 818.81 26.69 o 4 1 1 263.45 262.35 8.50 o 5 1 1 103.54 106.13 3.88 o 6 1 1 2.77 0.63 1.72 o -8 2 1 50.90 59.83 5.93 o -7 2 1 47.82 60.87 5.95 o -6 2 1 644.95 599.22 20.31 o -5 2 1 73.23 80.88 3.08 o -4 2 1 586.62 564.02 16.94 o -3 2 1 1234.92 1271.25 34.94 o -2 2 1 2318.23 2476.49 72.06 o -1 2 1 524.28 592.10 14.38 o 0 2 1 324.85 330.34 12.01 o 1 2 1 309.65 290.92 9.02 o 2 2 1 432.38 414.06 10.69 o 3 2 1 645.81 639.88 20.45 o 4 2 1 15.50 17.64 1.02 o 5 2 1 39.68 43.63 2.59 o 6 2 1 21.47 16.44 4.25 o -8 3 1 343.69 348.89 13.93 o -7 3 1 97.87 87.16 6.82 o -6 3 1 33.34 28.82 1.92 o -5 3 1 3.97 7.75 1.45 o -4 3 1 571.13 611.42 21.30 o -3 3 1 831.60 883.75 29.68 o -2 3 1 699.44 713.87 24.71 o -1 3 1 425.75 418.58 9.42 o 0 3 1 122.50 107.87 3.47 o 1 3 1 892.17 878.98 31.13 o 2 3 1 580.86 549.89 23.50 o 3 3 1 214.01 218.23 9.13 o 4 3 1 14.97 17.79 3.87 o 5 3 1 3.78 5.06 2.38 o -8 4 1 108.76 108.42 5.64 o -7 4 1 485.95 471.22 23.07 o -6 4 1 85.38 90.89 6.49 o -5 4 1 304.47 306.95 12.59 o -4 4 1 113.94 114.63 3.58 o -3 4 1 99.18 104.17 4.20 o -2 4 1 9.36 16.00 0.81 o -1 4 1 361.93 362.87 8.58 o 0 4 1 623.27 618.27 11.55 o 1 4 1 63.95 59.78 2.67 o 2 4 1 114.46 113.38 4.28 o 3 4 1 10.31 9.99 2.32 o 4 4 1 218.98 230.95 11.68 o -8 5 1 0.67 7.17 3.34 o -7 5 1 84.13 83.72 5.20 o -6 5 1 217.68 214.51 7.87 o -5 5 1 506.52 528.05 14.47 o -4 5 1 53.08 50.49 4.47 o -3 5 1 54.86 55.42 1.83 o -2 5 1 500.34 490.66 12.30 o -1 5 1 472.31 459.63 11.06 o 0 5 1 629.07 637.87 15.54 o 1 5 1 84.37 86.97 3.42 o 2 5 1 28.90 29.84 2.37 o 3 5 1 3.97 7.46 2.37 o -7 6 1 21.81 23.82 4.76 o -6 6 1 115.95 122.64 4.28 o -5 6 1 49.51 48.12 2.25 o -4 6 1 101.23 101.72 3.89 o -3 6 1 34.30 32.73 1.45 o -2 6 1 122.04 128.98 3.53 o -1 6 1 117.56 116.68 3.19 o 0 6 1 102.19 98.26 8.38 o 1 6 1 228.06 229.73 18.11 o 2 6 1 27.81 26.15 2.70 o -7 7 1 26.27 19.63 4.76 o -6 7 1 31.56 25.98 2.42 o -5 7 1 55.35 48.56 2.50 o -4 7 1 360.87 359.83 15.22 o -3 7 1 418.61 416.40 13.28 o -2 7 1 19.46 22.88 1.35 o -1 7 1 63.71 64.54 2.99 o 0 7 1 26.52 25.70 2.46 o 1 7 1 72.80 91.57 98.90 o -6 8 1 2.96 -0.77 2.58 o -5 8 1 77.71 71.71 6.58 o -4 8 1 64.61 52.63 9.88 o -3 8 1 85.60 79.01 3.43 o -2 8 1 88.85 84.05 4.64 o 0 -8 2 9.94 11.60 3.25 o 2 -8 2 342.78 308.85 34.94 o 3 -8 2 170.27 168.42 21.26 o 4 -8 2 110.66 108.57 11.17 o 5 -8 2 13.82 15.11 3.52 o 6 -8 2 98.10 88.22 8.31 o -2 -7 2 78.24 70.80 4.51 o -1 -7 2 10.76 16.43 2.33 o 0 -7 2 109.54 107.47 6.07 o 1 -7 2 5.01 5.98 0.89 o 2 -7 2 130.04 131.39 7.43 o 3 -7 2 23.43 26.75 1.50 o 4 -7 2 232.11 229.52 5.79 o 5 -7 2 126.28 119.49 11.71 o 6 -7 2 55.60 49.84 5.61 o -3 -6 2 31.81 33.11 4.07 o -2 -6 2 159.69 161.96 15.26 o -1 -6 2 107.33 112.48 11.79 o 0 -6 2 235.74 232.19 4.84 o 1 -6 2 489.36 513.40 21.60 o 2 -6 2 169.72 173.12 5.13 o 3 -6 2 85.10 88.49 2.92 o 4 -6 2 29.90 31.88 1.37 o 5 -6 2 149.94 151.67 4.76 o 6 -6 2 18.61 22.47 3.65 o 7 -6 2 41.20 33.03 6.16 o -4 -5 2 77.85 72.61 4.52 o -3 -5 2 87.53 89.05 4.26 o -2 -5 2 1.21 2.73 2.92 o -1 -5 2 54.03 60.45 8.90 o 0 -5 2 66.43 66.17 2.08 o 1 -5 2 892.10 885.36 25.81 o 2 -5 2 175.46 177.28 6.03 o 3 -5 2 228.84 223.57 5.37 o 4 -5 2 6.09 8.78 1.36 o 5 -5 2 154.92 160.94 5.44 o 6 -5 2 452.58 477.81 22.09 o 7 -5 2 229.78 234.56 12.51 o -5 -4 2 0.66 -0.16 4.08 o -4 -4 2 393.14 401.20 22.19 o -3 -4 2 445.36 457.05 17.30 o -2 -4 2 28.85 28.39 3.90 o -1 -4 2 220.15 225.77 7.57 o 0 -4 2 627.33 658.89 21.51 o 1 -4 2 846.40 822.66 17.84 o 2 -4 2 128.06 120.75 3.05 o 3 -4 2 6.69 7.61 0.69 o 4 -4 2 81.95 85.89 3.15 o 5 -4 2 48.72 43.52 3.52 o 6 -4 2 143.52 148.90 9.66 o 7 -4 2 146.38 134.81 10.80 o -5 -3 2 85.06 89.19 6.21 o -4 -3 2 61.73 66.01 3.84 o -3 -3 2 31.41 30.14 2.67 o -2 -3 2 228.20 246.24 6.14 o -1 -3 2 366.39 360.45 6.92 o 0 -3 2 879.84 877.75 16.95 o 1 -3 2 2.50 2.31 0.43 o 2 -3 2 680.36 624.75 16.27 o 3 -3 2 513.98 515.09 16.60 o 4 -3 2 964.84 987.20 30.34 o 5 -3 2 474.23 484.70 16.89 o 6 -3 2 11.10 11.87 2.51 o 7 -3 2 12.82 11.12 3.04 o -6 -2 2 48.57 60.00 6.22 o -5 -2 2 326.76 322.31 8.33 o -4 -2 2 92.74 99.62 3.65 o -3 -2 2 98.02 97.40 2.80 o -2 -2 2 2116.23 2175.14 56.32 o -1 -2 2 1061.33 1073.74 24.06 o 0 -2 2 42.16 36.06 1.19 o 1 -2 2 853.86 835.01 28.90 o 2 -2 2 20.71 17.64 1.99 o 3 -2 2 759.32 765.80 23.72 o 4 -2 2 413.18 407.89 12.48 o 5 -2 2 159.12 161.00 5.83 o 6 -2 2 73.91 78.38 4.61 o 7 -2 2 27.04 15.75 3.65 o -7 -1 2 130.97 143.95 11.32 o -6 -1 2 131.56 130.05 4.12 o -5 -1 2 16.59 16.27 1.80 o -4 -1 2 55.77 56.28 1.84 o -3 -1 2 327.05 343.35 7.78 o -2 -1 2 1039.69 1061.15 27.14 o -1 -1 2 1080.53 1113.41 25.37 o 0 -1 2 218.38 212.78 6.74 o 1 -1 2 1834.12 1720.58 45.06 o 2 -1 2 398.10 394.62 12.58 o 3 -1 2 605.92 587.03 20.61 o 4 -1 2 446.06 434.69 13.58 o 5 -1 2 26.78 27.42 2.92 o 6 -1 2 69.84 70.04 3.27 o 7 -1 2 31.46 20.08 3.70 o -7 0 2 25.80 28.61 2.53 o -6 0 2 412.47 411.79 11.80 o -5 0 2 425.45 442.21 11.47 o -4 0 2 466.70 470.58 11.06 o -3 0 2 456.39 485.87 15.12 o -2 0 2 472.23 512.14 11.80 o -1 0 2 59.74 60.67 1.63 o 0 0 2 185.54 179.26 5.14 o 1 0 2 1546.62 1357.71 38.19 o 2 0 2 397.71 376.13 12.39 o 3 0 2 64.31 61.01 2.42 o 4 0 2 139.34 141.01 4.62 o 5 0 2 259.96 266.27 10.83 o 6 0 2 116.04 104.97 4.16 o -7 1 2 12.77 16.69 1.91 o -6 1 2 56.80 53.71 2.36 o -5 1 2 611.93 633.32 15.65 o -4 1 2 563.89 582.19 14.55 o -3 1 2 540.14 548.68 14.74 o -2 1 2 99.46 112.47 2.79 o -1 1 2 985.33 961.74 30.13 o 0 1 2 2267.24 2200.19 60.33 o 1 1 2 525.14 504.49 15.89 o 2 1 2 721.15 669.16 18.95 o 3 1 2 346.93 339.04 10.34 o 4 1 2 28.23 28.83 1.42 o 5 1 2 25.52 25.81 1.78 o 6 1 2 45.74 42.69 5.56 o -8 2 2 86.99 82.90 4.32 o -7 2 2 401.13 376.21 10.35 o -6 2 2 109.90 113.47 4.13 o -5 2 2 33.18 32.22 1.45 o -4 2 2 113.16 116.98 3.40 o -3 2 2 141.02 143.42 4.28 o -2 2 2 1747.12 1790.66 56.46 o -1 2 2 8.26 12.97 0.69 o 0 2 2 56.80 49.79 1.41 o 1 2 2 432.76 430.58 15.95 o 2 2 2 770.78 747.83 17.99 o 3 2 2 406.31 403.32 11.18 o 4 2 2 103.24 100.17 3.50 o 5 2 2 16.57 14.12 2.38 o -8 3 2 133.97 124.70 5.86 o -7 3 2 204.21 211.90 7.26 o -6 3 2 196.04 194.92 5.29 o -5 3 2 2.45 2.82 1.19 o -4 3 2 444.19 450.57 11.34 o -3 3 2 941.32 939.69 25.05 o -2 3 2 2004.70 2079.74 60.88 o -1 3 2 304.55 301.51 7.28 o 0 3 2 45.10 43.77 1.24 o 1 3 2 370.61 334.70 11.80 o 2 3 2 197.34 208.71 9.43 o 3 3 2 37.15 38.99 1.32 o 4 3 2 137.74 138.80 8.04 o 5 3 2 86.30 77.76 6.82 o -8 4 2 238.00 220.47 9.09 o -7 4 2 36.21 41.22 2.31 o -6 4 2 36.50 37.87 2.18 o -5 4 2 60.35 63.88 2.28 o -4 4 2 85.98 84.97 6.47 o -3 4 2 320.74 335.50 9.49 o -2 4 2 1.16 2.96 0.63 o -1 4 2 844.46 856.12 18.78 o 0 4 2 973.19 959.24 25.85 o 1 4 2 172.04 162.65 5.18 o 2 4 2 16.23 15.95 2.44 o 3 4 2 61.02 50.92 4.27 o 4 4 2 149.37 150.36 7.97 o -8 5 2 17.41 19.75 4.17 o -7 5 2 94.24 93.41 5.21 o -6 5 2 126.76 123.76 5.06 o -5 5 2 742.53 767.90 22.03 o -4 5 2 160.30 167.17 5.29 o -3 5 2 175.81 191.49 5.06 o -2 5 2 17.28 17.62 1.17 o -1 5 2 333.86 348.58 6.95 o 0 5 2 325.27 324.62 6.85 o 1 5 2 14.90 15.64 1.57 o 2 5 2 74.33 73.03 4.17 o 3 5 2 235.57 233.12 9.75 o -7 6 2 12.26 7.36 4.28 o -6 6 2 52.25 50.91 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119.47 115.78 4.41 o -2 -2 9 13.66 12.93 1.61 o -1 -2 9 81.38 79.71 3.41 o 0 -2 9 398.73 406.49 10.64 o 1 -2 9 309.01 306.42 12.64 o 2 -2 9 57.22 55.77 4.50 o 3 -2 9 0.79 -1.17 3.25 o -6 -1 9 2.06 -1.14 3.21 o -5 -1 9 251.62 260.45 12.20 o -4 -1 9 127.24 125.41 4.36 o -3 -1 9 24.47 28.13 2.80 o -2 -1 9 28.54 28.23 2.61 o -1 -1 9 152.33 145.78 5.50 o 0 -1 9 488.24 483.67 12.95 o 1 -1 9 214.83 215.05 9.99 o 2 -1 9 109.15 118.42 9.14 o 3 -1 9 34.94 34.16 4.58 o -6 0 9 68.63 74.98 5.91 o -5 0 9 286.54 262.75 8.98 o -4 0 9 71.26 78.29 3.81 o -3 0 9 116.50 122.06 4.38 o -2 0 9 282.99 293.86 8.12 o -1 0 9 185.55 190.50 5.45 o 0 0 9 47.37 45.84 2.24 o 1 0 9 39.23 37.64 4.11 o 2 0 9 70.14 72.64 6.88 o -6 1 9 54.00 44.62 5.20 o -5 1 9 0.86 2.36 1.90 o -4 1 9 49.04 58.44 5.62 o -3 1 9 170.76 175.29 5.46 o -2 1 9 432.94 432.66 10.35 o -1 1 9 247.99 253.18 7.23 o 0 1 9 39.56 42.47 2.17 o 1 1 9 93.92 93.18 7.17 o 2 1 9 72.38 63.39 6.05 o -6 2 9 148.40 121.84 9.19 o -5 2 9 31.70 42.61 5.69 o -4 2 9 102.74 112.90 6.41 o -3 2 9 205.74 212.87 12.05 o -2 2 9 99.67 98.57 4.40 o -1 2 9 91.67 90.43 5.64 o 0 2 9 52.62 43.81 3.17 o 1 2 9 16.54 14.82 3.49 o -6 3 9 81.14 77.44 6.60 o -5 3 9 194.00 202.82 22.43 o -4 3 9 76.24 73.05 7.85 o -3 3 9 65.52 65.44 3.18 o -2 3 9 178.77 192.80 11.21 o -1 3 9 178.90 187.08 11.64 o 0 3 9 135.00 126.79 8.10 o -6 4 9 92.52 100.39 8.60 o -5 4 9 126.27 121.08 7.23 o -4 4 9 96.74 108.93 6.73 o -3 4 9 8.88 6.77 3.82 o -2 4 9 41.59 41.06 5.18 o -1 4 9 24.00 18.10 3.54 o -5 5 9 69.01 64.14 6.80 o -4 5 9 146.46 154.18 10.49 o -3 5 9 208.96 204.80 11.39 o -2 -5 10 3.84 12.35 3.90 o -1 -5 10 9.34 13.73 3.46 o 0 -5 10 21.15 20.64 3.58 o 1 -5 10 103.59 104.08 6.82 o 2 -5 10 185.61 195.56 13.66 o -3 -4 10 40.50 39.36 4.68 o -2 -4 10 105.54 100.11 9.68 o -1 -4 10 97.42 95.09 6.20 o 0 -4 10 202.39 222.67 11.30 o 1 -4 10 0.77 4.93 3.30 o 2 -4 10 45.33 51.21 5.04 o -4 -3 10 17.66 16.26 3.74 o -3 -3 10 2.36 6.24 2.99 o -2 -3 10 181.72 191.71 9.24 o -1 -3 10 99.65 98.36 6.46 o 0 -3 10 214.86 225.94 11.47 o 1 -3 10 190.11 227.75 9.93 o 2 -3 10 39.24 46.52 5.60 o -5 -2 10 102.58 94.13 7.43 o -4 -2 10 121.38 120.81 7.12 o -3 -2 10 58.20 49.86 4.37 o -2 -2 10 38.10 42.22 4.19 o -1 -2 10 127.04 119.29 4.71 o 0 -2 10 49.15 48.40 3.92 o 1 -2 10 211.77 213.94 10.64 o 2 -2 10 31.23 43.82 5.04 o -5 -1 10 127.70 121.02 9.23 o -4 -1 10 104.65 106.29 6.64 o -3 -1 10 224.90 242.81 12.02 o -2 -1 10 8.94 6.12 1.62 o -1 -1 10 266.77 268.97 8.64 o 0 -1 10 304.90 320.68 11.69 o 1 -1 10 70.30 60.54 5.30 o 2 -1 10 54.19 50.40 4.86 o -6 0 10 52.43 49.64 6.91 o -5 0 10 110.02 109.33 8.03 o -4 0 10 44.18 47.44 8.21 o -3 0 10 158.83 169.15 9.30 o -2 0 10 124.59 125.98 3.99 o -1 0 10 19.60 21.17 2.02 o 0 0 10 53.06 55.11 6.69 o 1 0 10 9.35 8.08 5.51 o -6 1 10 58.41 55.14 6.37 o -5 1 10 30.04 35.85 2.52 o -4 1 10 191.68 179.57 6.57 o -3 1 10 100.23 93.66 7.81 o -2 1 10 544.20 543.67 13.89 o -1 1 10 111.84 113.85 5.17 o 0 1 10 2.66 4.70 2.11 o 1 1 10 31.72 23.41 4.74 o -6 2 10 114.21 117.91 8.76 o -5 2 10 13.41 8.01 3.87 o -4 2 10 112.01 109.66 4.62 o -3 2 10 19.70 16.57 2.13 o -1 2 10 114.08 105.37 8.84 o 0 2 10 41.42 43.72 4.51 o -5 3 10 243.71 225.56 12.09 o -4 3 10 14.57 11.62 3.80 o -3 3 10 126.03 134.70 8.50 o -2 3 10 17.89 13.85 3.81 o -1 3 10 19.98 9.95 4.10 o -4 4 10 2.52 1.55 4.09 o -3 4 10 56.41 56.20 5.80 o -2 -4 11 96.30 94.03 8.01 o -1 -4 11 114.77 106.06 7.40 o 0 -4 11 44.54 55.61 5.49 o 1 -4 11 6.45 2.99 3.65 o -3 -3 11 89.21 77.51 5.94 o -2 -3 11 117.60 115.92 7.29 o -1 -3 11 173.15 167.57 9.66 o 0 -3 11 267.03 329.04 16.59 o 1 -3 11 2.85 6.56 3.61 o -4 -2 11 80.47 76.71 6.63 o -3 -2 11 95.81 98.15 6.27 o -2 -2 11 5.64 13.22 3.31 o -1 -2 11 19.03 11.64 3.55 o 0 -2 11 86.57 81.24 5.74 o 1 -2 11 160.17 168.11 14.54 o -4 -1 11 240.51 221.98 14.61 o -3 -1 11 65.27 60.07 5.03 o -2 -1 11 39.81 39.64 4.10 o -1 -1 11 132.46 130.12 10.07 o 0 -1 11 1.10 1.78 2.83 o 1 -1 11 148.63 168.29 11.46 o -5 0 11 54.56 55.92 6.31 o -4 0 11 52.94 69.21 14.55 o -3 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