#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/01/2200158.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200158_Fobs loop_ _publ_author_name 'Koskimies, Jorma' 'N\"as\"akk\"al\"a, Matti' 'Mutikainen, Ilpo' _publ_section_title ; 1,8-Dioxa-4,11-dithiacyclotetradecane-2,9-dione ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o261 _journal_page_last o263 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 71.880 _cell_angle_beta 74.040 _cell_angle_gamma 85.410 _cell_length_a 5.3920 _cell_length_b 6.8580 _cell_length_c 8.9600 _exptl_crystal_F_000 140.00 _reflns_d_resolution_high 0.8334 _[local]_cod_data_source_file cv6004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dioxa in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 72.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 45.00 44.20 0.74 o 2 0 0 1361.19 1318.26 22.97 o 3 0 0 359.75 398.43 6.97 o 4 0 0 103.80 107.07 3.26 o 5 0 0 45.02 37.29 1.79 o 6 0 0 1.70 1.77 0.29 o -6 1 0 56.42 50.31 4.37 o -5 1 0 27.16 27.00 2.25 o -4 1 0 1.98 2.57 0.19 o -3 1 0 255.55 267.43 8.47 o -2 1 0 130.19 125.75 5.04 o -1 1 0 5266.09 4128.10 183.41 o 0 1 0 13.09 12.46 0.25 o 1 1 0 1269.48 1191.84 56.37 o 2 1 0 505.28 560.46 26.90 o 3 1 0 392.21 392.38 23.48 o 4 1 0 10.64 8.26 0.42 o 5 1 0 4.01 3.80 0.40 o 6 1 0 0.15 0.28 0.26 o -5 2 0 61.92 60.37 5.15 o -4 2 0 15.83 15.26 1.74 o -3 2 0 234.94 214.74 10.01 o -2 2 0 133.67 133.68 4.96 o -1 2 0 9.80 11.90 0.57 o 0 2 0 54.97 57.98 0.95 o 1 2 0 19.10 19.77 1.66 o 2 2 0 806.87 822.53 40.27 o 3 2 0 0.62 0.44 0.21 o 4 2 0 50.07 49.05 5.34 o 5 2 0 71.91 65.08 4.60 o -5 3 0 0.12 0.38 0.32 o -4 3 0 143.68 121.87 7.36 o -3 3 0 18.77 17.35 0.58 o -2 3 0 6.09 5.49 0.30 o -1 3 0 20.85 24.90 1.03 o 0 3 0 26.52 26.43 0.88 o 1 3 0 402.12 445.42 16.46 o 2 3 0 63.95 60.30 2.42 o 3 3 0 30.74 28.91 1.49 o 4 3 0 216.80 196.70 13.77 o 5 3 0 33.09 29.29 3.85 o -5 4 0 14.38 13.63 0.65 o -4 4 0 32.66 32.78 1.07 o -3 4 0 12.77 11.84 0.50 o -2 4 0 36.63 37.96 2.92 o -1 4 0 104.52 105.64 1.80 o 0 4 0 0.94 0.82 0.19 o 1 4 0 149.16 156.54 4.35 o 2 4 0 1.08 1.16 0.15 o 3 4 0 235.80 216.96 13.01 o 4 4 0 9.84 9.46 0.82 o 5 4 0 41.12 38.65 3.11 o -4 5 0 1.60 1.93 0.24 o -3 5 0 29.60 24.73 1.62 o -2 5 0 39.48 33.16 0.93 o -1 5 0 46.03 39.77 2.12 o 0 5 0 127.63 123.09 2.21 o 1 5 0 21.72 23.37 1.24 o 2 5 0 146.41 137.47 10.15 o 3 5 0 0.87 0.80 0.21 o 4 5 0 77.82 71.98 3.89 o -3 6 0 0.52 0.45 0.23 o -2 6 0 44.13 40.75 1.11 o -1 6 0 18.09 16.40 0.65 o 0 6 0 3.49 3.43 0.25 o 1 6 0 58.40 60.67 3.19 o 2 6 0 8.10 7.39 0.36 o 3 6 0 84.75 74.52 6.35 o -2 7 0 0.56 0.68 0.16 o -1 7 0 0.08 0.00 0.30 o 0 7 0 1.40 2.15 0.48 o 1 7 0 6.38 5.87 0.53 o 2 7 0 16.94 15.22 2.19 o -2 -7 1 5.94 6.14 0.38 o -1 -7 1 131.83 133.31 9.27 o 0 -7 1 3.60 3.93 0.29 o 1 -7 1 9.02 10.38 0.50 o 2 -7 1 4.99 4.98 0.44 o -3 -6 1 16.58 18.41 2.33 o -2 -6 1 243.79 234.55 13.70 o -1 -6 1 1.82 2.54 0.25 o 0 -6 1 77.75 81.16 4.35 o 1 -6 1 0.07 0.00 0.25 o 2 -6 1 64.80 63.94 1.50 o 3 -6 1 40.05 38.48 1.13 o -4 -5 1 22.63 23.48 0.92 o -3 -5 1 141.74 135.10 15.53 o -2 -5 1 12.18 10.66 1.22 o -1 -5 1 185.54 175.29 12.82 o 0 -5 1 4.72 4.74 0.32 o 1 -5 1 399.87 379.27 8.24 o 2 -5 1 0.00 0.04 0.22 o 3 -5 1 38.81 38.57 1.04 o 4 -5 1 7.17 7.16 0.37 o -4 -4 1 26.79 26.30 2.71 o -3 -4 1 30.16 28.59 2.33 o -2 -4 1 142.24 132.75 14.55 o -1 -4 1 40.76 38.37 0.91 o 0 -4 1 794.75 879.39 31.23 o 1 -4 1 66.15 65.85 1.29 o 2 -4 1 23.23 22.34 1.11 o 3 -4 1 123.58 111.14 2.05 o 4 -4 1 3.02 3.03 0.25 o 5 -4 1 0.07 0.00 0.28 o -5 -3 1 3.76 4.50 0.69 o -4 -3 1 0.92 1.17 0.21 o -3 -3 1 31.48 28.05 1.58 o -2 -3 1 224.85 224.68 20.39 o -1 -3 1 384.80 409.40 35.71 o 0 -3 1 242.64 272.78 12.78 o 1 -3 1 3.66 5.29 0.31 o 2 -3 1 422.39 416.36 7.34 o 3 -3 1 10.50 9.02 0.41 o 4 -3 1 16.34 13.92 0.71 o 5 -3 1 2.19 2.43 0.53 o -5 -2 1 11.10 12.05 2.35 o -4 -2 1 8.72 8.07 0.45 o -3 -2 1 229.86 225.62 25.64 o -2 -2 1 4.20 3.26 0.18 o -1 -2 1 321.96 331.27 38.11 o 0 -2 1 349.70 383.44 34.24 o 1 -2 1 560.29 614.65 8.32 o 2 -2 1 7.09 6.65 0.36 o 3 -2 1 87.92 81.19 5.21 o 4 -2 1 0.00 0.00 0.22 o 5 -2 1 75.19 74.69 2.27 o 6 -2 1 15.28 16.13 0.74 o -5 -1 1 53.28 50.17 2.63 o -4 -1 1 33.79 30.59 2.02 o -3 -1 1 176.70 167.91 15.72 o -2 -1 1 29.29 26.72 2.67 o -1 -1 1 246.04 242.76 25.50 o 0 -1 1 723.29 700.79 92.25 o 1 -1 1 2.69 2.73 0.15 o 2 -1 1 298.51 289.73 6.87 o 3 -1 1 73.81 77.27 4.67 o 4 -1 1 114.10 107.00 7.86 o 5 -1 1 3.53 3.69 0.28 o 6 -1 1 2.04 2.17 0.67 o -5 0 1 7.04 7.03 0.24 o -4 0 1 124.79 111.77 5.04 o -3 0 1 3.71 3.02 0.13 o -2 0 1 7.05 5.86 0.18 o -1 0 1 457.96 446.50 15.95 o 1 0 1 851.50 827.64 10.47 o 2 0 1 265.49 266.88 3.56 o 3 0 1 151.12 153.32 2.88 o 4 0 1 35.62 33.62 1.29 o 5 0 1 0.06 0.09 0.17 o 6 0 1 1.98 1.87 0.21 o -5 1 1 71.56 66.97 6.22 o -4 1 1 28.43 22.39 2.27 o -3 1 1 4.31 2.76 0.29 o -2 1 1 60.00 57.99 2.21 o -1 1 1 26.54 24.75 1.22 o 0 1 1 220.97 231.14 10.87 o 1 1 1 17.30 17.71 0.46 o 2 1 1 90.11 99.96 1.53 o 3 1 1 121.03 121.19 1.95 o 4 1 1 17.54 20.49 1.83 o 5 1 1 103.86 97.27 4.79 o 6 1 1 4.33 3.36 0.34 o -5 2 1 16.86 13.80 0.88 o -4 2 1 10.03 7.56 0.43 o -3 2 1 367.38 358.55 15.13 o -2 2 1 0.03 0.00 0.18 o -1 2 1 239.95 253.80 8.05 o 0 2 1 1005.22 1028.65 21.61 o 1 2 1 7.13 7.84 0.27 o 2 2 1 103.01 110.06 3.05 o 3 2 1 49.99 59.20 1.14 o 4 2 1 256.60 231.16 12.11 o 5 2 1 36.04 31.08 2.50 o 6 2 1 108.34 103.86 5.49 o -5 3 1 0.41 0.32 0.23 o -4 3 1 199.52 179.82 9.40 o -3 3 1 1.59 0.90 0.23 o -2 3 1 310.65 318.24 11.85 o -1 3 1 280.63 312.51 7.23 o 0 3 1 626.76 683.22 13.56 o 1 3 1 37.06 39.65 0.79 o 2 3 1 14.87 14.90 0.46 o 3 3 1 98.70 88.64 1.85 o 4 3 1 124.60 120.27 5.42 o 5 3 1 124.40 112.37 4.33 o -5 4 1 27.13 24.71 1.77 o -4 4 1 1.50 1.39 0.21 o -3 4 1 87.69 76.98 3.13 o -2 4 1 16.58 17.94 0.67 o -1 4 1 713.42 716.93 12.40 o 0 4 1 26.18 26.70 0.68 o 1 4 1 374.96 398.10 5.65 o 2 4 1 24.77 26.40 0.71 o 3 4 1 246.54 239.65 9.88 o 4 4 1 18.85 19.17 0.73 o 5 4 1 1.76 2.38 0.50 o -4 5 1 7.18 6.80 0.36 o -3 5 1 0.81 1.05 0.19 o -2 5 1 321.01 275.83 4.27 o -1 5 1 2.32 2.76 0.19 o 0 5 1 398.16 389.94 17.87 o 1 5 1 198.79 188.91 5.15 o 2 5 1 230.93 219.04 8.55 o 3 5 1 7.82 7.33 0.63 o 4 5 1 0.23 0.04 0.25 o -3 6 1 70.44 60.10 1.77 o -2 6 1 20.32 18.85 0.73 o -1 6 1 61.37 60.06 2.88 o 0 6 1 172.49 159.20 2.73 o 1 6 1 57.01 52.84 1.26 o 2 6 1 24.84 22.42 1.64 o 3 6 1 0.01 1.01 0.27 o 4 6 1 14.56 12.97 0.84 o -2 7 1 3.91 3.43 0.30 o -1 7 1 77.77 75.72 1.75 o 0 7 1 1.75 1.20 0.25 o 1 7 1 16.84 17.28 0.70 o 2 7 1 0.03 0.56 0.40 o 3 7 1 37.23 36.18 3.70 o 0 8 1 25.72 23.32 2.21 o -1 -7 2 13.96 10.62 1.16 o 0 -7 2 40.07 41.00 3.34 o 1 -7 2 34.14 34.19 2.67 o -2 -6 2 32.14 31.05 1.79 o -1 -6 2 42.33 40.02 2.92 o 0 -6 2 87.25 84.92 5.74 o 1 -6 2 15.63 15.76 0.67 o 2 -6 2 17.12 18.04 1.11 o 3 -6 2 0.02 0.43 0.16 o -3 -5 2 12.13 10.66 1.09 o -2 -5 2 2.74 2.89 0.53 o -1 -5 2 23.60 18.91 2.21 o 0 -5 2 20.71 20.64 2.04 o 1 -5 2 73.63 74.52 6.12 o 2 -5 2 0.12 0.15 0.27 o 3 -5 2 64.65 68.83 1.68 o 4 -5 2 11.36 12.11 0.90 o -4 -4 2 1.45 1.07 0.25 o -3 -4 2 45.30 39.83 4.90 o -2 -4 2 11.09 12.12 1.74 o -1 -4 2 10.36 9.43 1.14 o 0 -4 2 32.75 27.26 4.60 o 1 -4 2 3.36 3.43 0.22 o 2 -4 2 149.32 148.56 5.02 o 3 -4 2 44.31 42.87 1.05 o 4 -4 2 58.37 59.85 1.41 o 5 -4 2 21.62 21.50 0.82 o -5 -3 2 1.42 1.49 0.27 o -4 -3 2 125.39 111.04 14.90 o -3 -3 2 44.37 40.33 5.80 o -2 -3 2 355.21 349.86 44.22 o -1 -3 2 3.24 4.73 0.53 o 0 -3 2 109.86 124.54 13.07 o 1 -3 2 5.50 3.82 0.23 o 2 -3 2 98.14 110.65 3.34 o 3 -3 2 167.17 160.07 2.63 o 4 -3 2 18.24 18.45 0.67 o 5 -3 2 98.13 101.96 2.05 o -5 -2 2 75.63 70.87 9.58 o -4 -2 2 37.62 34.26 4.58 o -3 -2 2 754.21 737.65 89.31 o -2 -2 2 56.97 58.25 6.35 o -1 -2 2 416.92 441.23 55.51 o 0 -2 2 549.62 583.50 70.83 o 1 -2 2 214.79 218.60 24.07 o 2 -2 2 194.41 226.73 5.76 o 3 -2 2 5.91 6.51 0.34 o 4 -2 2 156.96 148.95 3.83 o 5 -2 2 80.55 74.60 4.29 o 6 -2 2 50.09 48.33 2.40 o -5 -1 2 47.75 42.22 3.70 o -4 -1 2 398.37 362.23 31.30 o -3 -1 2 71.37 68.80 5.74 o -2 -1 2 181.83 176.20 17.00 o -1 -1 2 837.19 871.41 100.03 o 0 -1 2 613.22 571.93 82.23 o 1 -1 2 134.51 136.31 18.79 o 2 -1 2 16.57 16.04 1.35 o 3 -1 2 26.12 25.74 0.95 o 4 -1 2 253.37 242.39 12.34 o 5 -1 2 11.95 10.52 0.52 o 6 -1 2 22.30 23.84 0.86 o -5 0 2 51.62 43.78 2.71 o -4 0 2 32.99 26.04 1.69 o -3 0 2 14.51 14.33 0.79 o -2 0 2 254.64 234.17 9.68 o -1 0 2 873.51 889.88 37.53 o 0 0 2 131.52 118.26 11.05 o 1 0 2 642.72 526.70 67.26 o 2 0 2 424.76 465.02 5.94 o 3 0 2 554.99 572.78 7.33 o 4 0 2 28.52 27.74 0.55 o 5 0 2 10.59 10.97 0.36 o 6 0 2 26.55 27.25 1.29 o -5 1 2 13.98 12.16 1.11 o -4 1 2 4.65 3.45 0.24 o -3 1 2 114.03 102.85 8.68 o -2 1 2 381.46 400.64 22.30 o -1 1 2 138.27 135.20 9.19 o 0 1 2 137.03 131.40 8.37 o 1 1 2 2698.28 2452.49 37.06 o 2 1 2 313.45 349.02 4.82 o 3 1 2 110.77 112.80 1.83 o 4 1 2 0.02 0.41 0.38 o 5 1 2 84.01 87.06 2.12 o 6 1 2 58.59 58.12 3.24 o -5 2 2 3.98 3.19 0.25 o -4 2 2 90.01 79.75 5.25 o -3 2 2 29.91 27.91 1.79 o -2 2 2 561.85 559.41 29.24 o -1 2 2 306.53 340.61 20.43 o 0 2 2 3097.39 2991.20 148.39 o 1 2 2 82.63 87.28 1.35 o 2 2 2 75.29 71.94 1.20 o 3 2 2 56.24 68.67 1.62 o 4 2 2 94.97 101.48 2.46 o 5 2 2 152.33 141.26 6.16 o 6 2 2 12.27 12.47 0.63 o -5 3 2 30.87 26.43 0.89 o -4 3 2 1.78 2.61 0.21 o -3 3 2 320.30 298.75 30.33 o -2 3 2 269.57 270.18 11.14 o -1 3 2 1435.24 1529.33 54.73 o 0 3 2 425.55 485.62 10.87 o 1 3 2 165.76 180.87 2.67 o 2 3 2 198.50 229.34 3.36 o 3 3 2 137.48 148.00 2.38 o 4 3 2 59.51 52.63 1.17 o 5 3 2 8.62 9.45 1.28 o 6 3 2 17.93 16.92 0.73 o -5 4 2 20.36 20.00 0.80 o -4 4 2 38.37 36.14 1.85 o -3 4 2 85.34 77.91 4.10 o -2 4 2 193.86 190.28 12.36 o -1 4 2 81.89 91.63 1.95 o 0 4 2 310.48 328.66 9.00 o 1 4 2 208.80 235.48 3.49 o 2 4 2 192.16 206.63 3.14 o 3 4 2 18.89 19.11 0.62 o 4 4 2 0.69 1.04 0.21 o 5 4 2 0.99 0.74 0.42 o -4 5 2 12.96 11.98 0.61 o -3 5 2 0.08 0.15 0.24 o -2 5 2 1.41 1.32 0.23 o -1 5 2 84.11 77.31 3.78 o 0 5 2 41.42 38.03 0.92 o 1 5 2 127.08 133.80 3.78 o 2 5 2 128.25 125.08 2.15 o 3 5 2 0.02 0.27 0.27 o 4 5 2 56.74 55.44 1.35 o 5 5 2 0.83 0.70 0.19 o -3 6 2 0.10 0.00 0.12 o -2 6 2 0.57 0.69 0.25 o -1 6 2 0.85 1.09 0.22 o 0 6 2 0.95 1.27 0.19 o 1 6 2 49.44 45.95 1.14 o 2 6 2 0.04 0.16 0.25 o 3 6 2 76.01 73.50 1.77 o 4 6 2 2.15 2.27 0.57 o -2 7 2 1.45 0.44 0.31 o -1 7 2 47.89 46.24 1.25 o 0 7 2 0.40 0.39 0.32 o 1 7 2 2.31 2.53 0.27 o 2 7 2 24.27 23.36 0.86 o 3 7 2 3.51 3.37 0.30 o 0 8 2 14.76 14.16 0.70 o 1 8 2 4.18 4.45 0.44 o -2 -6 3 12.08 12.62 0.67 o -1 -6 3 15.77 15.41 2.29 o 0 -6 3 37.09 39.83 6.73 o 1 -6 3 13.54 13.90 1.51 o 2 -6 3 0.04 0.00 0.26 o 3 -6 3 1.98 2.68 0.55 o -3 -5 3 40.59 36.65 7.15 o -2 -5 3 11.43 10.68 0.47 o -1 -5 3 78.07 77.46 10.68 o 0 -5 3 5.65 4.77 0.97 o 1 -5 3 0.23 0.74 0.20 o 2 -5 3 21.05 22.20 0.77 o 3 -5 3 32.60 36.05 1.20 o 4 -5 3 56.03 64.02 2.75 o -4 -4 3 48.97 45.22 7.82 o -3 -4 3 97.59 96.69 12.72 o -2 -4 3 114.54 112.34 20.75 o -1 -4 3 6.49 11.09 1.95 o 0 -4 3 2.58 2.32 0.22 o 1 -4 3 5.66 4.80 0.57 o 2 -4 3 148.85 156.76 13.79 o 3 -4 3 92.46 101.08 1.96 o 4 -4 3 80.53 91.52 2.90 o 5 -4 3 4.75 4.83 0.38 o -4 -3 3 64.48 60.38 4.71 o -3 -3 3 135.29 121.06 17.68 o -2 -3 3 9.60 11.36 1.93 o -1 -3 3 119.87 115.43 16.82 o 0 -3 3 79.85 86.33 12.65 o 1 -3 3 349.60 385.12 35.04 o 2 -3 3 16.63 17.74 0.58 o 3 -3 3 36.81 38.34 0.95 o 4 -3 3 2.36 2.21 0.22 o 5 -3 3 36.22 37.83 1.10 o -5 -2 3 4.69 4.64 0.34 o -4 -2 3 92.98 86.55 9.56 o -3 -2 3 0.70 0.29 0.26 o -2 -2 3 383.39 377.70 47.59 o -1 -2 3 382.98 385.41 59.40 o 0 -2 3 739.08 796.11 110.79 o 1 -2 3 154.45 170.47 22.49 o 2 -2 3 11.67 16.74 2.46 o 3 -2 3 21.04 21.67 0.90 o 4 -2 3 5.78 5.57 0.26 o 5 -2 3 43.28 44.92 1.16 o 6 -2 3 3.42 4.38 0.31 o -5 -1 3 11.42 11.66 1.87 o -4 -1 3 0.14 0.00 0.23 o -3 -1 3 165.67 162.59 25.14 o -2 -1 3 299.54 304.77 35.08 o -1 -1 3 377.81 426.53 55.13 o 0 -1 3 547.72 565.45 83.00 o 1 -1 3 123.28 119.96 22.47 o 2 -1 3 255.49 256.82 26.00 o 3 -1 3 25.31 28.59 1.72 o 4 -1 3 2.61 1.93 0.19 o 5 -1 3 8.71 9.06 0.49 o 6 -1 3 0.09 0.22 0.28 o -5 0 3 2.07 2.87 0.27 o -4 0 3 0.43 0.29 0.15 o -3 0 3 17.88 15.76 0.69 o -2 0 3 0.04 0.39 0.12 o -1 0 3 107.03 112.51 5.70 o 0 0 3 14.83 12.80 1.19 o 1 0 3 548.18 449.24 68.63 o 2 0 3 140.97 153.41 10.87 o 3 0 3 128.25 144.25 2.15 o 4 0 3 111.28 113.57 1.40 o 5 0 3 25.19 27.69 0.60 o 6 0 3 1.72 1.60 0.16 o -5 1 3 47.59 44.82 1.28 o -4 1 3 11.57 12.33 1.43 o -3 1 3 128.92 116.88 10.66 o -2 1 3 0.40 0.88 0.13 o -1 1 3 30.65 33.74 1.85 o 0 1 3 100.51 94.55 9.56 o 1 1 3 201.04 197.90 5.84 o 2 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9.18 9.37 1.89 o 1 -2 8 30.79 35.65 10.30 o 2 -2 8 0.36 0.57 0.42 o 3 -2 8 18.40 19.69 4.48 o 4 -2 8 0.00 0.00 0.31 o -2 -1 8 3.61 5.49 0.82 o -1 -1 8 61.89 80.12 15.43 o 0 -1 8 13.23 17.96 3.53 o 1 -1 8 10.08 10.14 2.98 o 2 -1 8 9.34 9.08 2.75 o 3 -1 8 20.09 21.39 4.22 o 4 -1 8 31.95 27.23 7.46 o -2 0 8 100.80 135.10 10.53 o -1 0 8 7.52 10.04 0.80 o 0 0 8 109.91 112.25 15.07 o 1 0 8 4.51 5.35 0.95 o 2 0 8 163.11 155.38 22.61 o 3 0 8 3.47 3.68 0.36 o 4 0 8 13.62 9.93 0.84 o 5 0 8 2.40 4.01 0.79 o -2 1 8 3.72 4.93 0.50 o -1 1 8 190.36 249.58 33.90 o 0 1 8 35.45 30.67 4.39 o 1 1 8 395.01 305.76 59.95 o 2 1 8 20.08 16.22 1.56 o 3 1 8 17.05 15.46 1.18 o 4 1 8 3.32 2.33 0.38 o 5 1 8 2.97 3.12 0.42 o -2 2 8 99.07 126.72 10.57 o -1 2 8 51.29 68.18 6.14 o 0 2 8 301.96 258.15 45.42 o 1 2 8 30.53 22.72 4.14 o 2 2 8 42.76 28.46 4.20 o 3 2 8 25.61 21.89 1.79 o 4 2 8 24.69 22.06 0.76 o 5 2 8 17.87 18.48 1.43 o -2 3 8 44.32 57.87 5.78 o -1 3 8 46.35 58.41 3.87 o 0 3 8 4.16 5.77 0.44 o 1 3 8 43.75 39.51 4.77 o 2 3 8 25.72 20.27 0.68 o 3 3 8 101.39 64.33 10.13 o 4 3 8 2.89 3.34 0.46 o 5 3 8 3.56 4.32 0.38 o -2 4 8 4.04 6.94 0.38 o -1 4 8 0.34 0.17 0.26 o 0 4 8 5.02 5.48 0.34 o 1 4 8 11.27 14.20 0.86 o 2 4 8 92.96 91.22 4.01 o 3 4 8 38.57 27.75 4.65 o 4 4 8 2.73 2.66 0.65 o 5 4 8 59.08 48.16 1.89 o -2 5 8 0.01 0.73 0.32 o -1 5 8 3.34 4.51 0.36 o 0 5 8 18.35 24.61 2.50 o 1 5 8 1.91 2.77 0.40 o 2 5 8 47.15 47.89 3.74 o 3 5 8 2.59 3.12 0.30 o 4 5 8 60.97 58.53 1.46 o -1 6 8 18.61 21.65 1.64 o 0 6 8 28.62 29.75 1.20 o 1 6 8 29.16 31.41 3.62 o 2 6 8 28.01 31.13 4.14 o 3 6 8 25.04 22.64 1.43 o 1 7 8 21.72 25.28 0.94 o 2 7 8 7.71 10.01 0.45 o 1 -2 9 18.51 24.68 6.60 o 2 -2 9 5.43 5.56 1.93 o 0 -1 9 3.78 7.16 1.72 o 1 -1 9 14.50 18.83 4.25 o 2 -1 9 12.90 10.91 3.05 o 3 -1 9 1.11 1.37 0.82 o -1 0 9 0.02 0.03 0.20 o 0 0 9 21.71 27.34 3.82 o 1 0 9 20.14 19.55 3.02 o 2 0 9 0.65 0.73 0.14 o 3 0 9 20.67 14.03 2.98 o 4 0 9 6.14 4.79 0.63 o -1 1 9 12.67 20.17 3.89 o 0 1 9 21.62 19.77 4.10 o 1 1 9 18.86 9.85 3.30 o 2 1 9 24.40 10.62 3.51 o 3 1 9 40.10 24.39 5.57 o 4 1 9 5.92 4.01 0.67 o -1 2 9 1.16 2.19 0.23 o 0 2 9 19.16 11.94 2.48 o 1 2 9 7.87 4.08 0.42 o 2 2 9 44.40 26.15 4.71 o 3 2 9 0.00 0.19 0.24 o 4 2 9 25.25 18.31 3.47 o -1 3 9 2.12 3.00 0.30 o 0 3 9 5.46 6.04 0.90 o 1 3 9 2.10 2.26 0.25 o 2 3 9 4.44 3.30 0.80 o 3 3 9 38.75 33.32 1.56 o 4 3 9 9.06 5.16 1.05 o -1 4 9 43.02 59.43 7.59 o 0 4 9 12.26 14.23 1.98 o 1 4 9 35.64 37.32 3.78 o 2 4 9 8.79 9.44 2.21 o 3 4 9 15.49 12.92 0.62 o 4 4 9 22.50 17.90 2.71 o -1 5 9 16.94 22.03 1.93 o 0 5 9 97.36 127.73 15.15 o 1 5 9 2.83 2.62 0.32 o 2 5 9 45.18 40.54 3.93 o 3 5 9 1.16 0.87 0.34 o 0 6 9 14.52 19.01 2.59 o 1 6 9 60.38 67.63 6.56 o 2 6 9 39.92 37.55 1.18 o 1 0 10 28.33 32.96 5.98 o 2 0 10 3.86 3.67 0.70 o 0 1 10 39.15 37.57 7.00 o 1 1 10 3.79 3.03 0.80 o 2 1 10 14.83 7.71 1.95 o 3 1 10 13.62 10.95 3.15 o 0 2 10 25.97 17.49 1.43 o 1 2 10 1.48 1.00 0.48 o 2 2 10 67.53 36.49 9.08 o 3 2 10 1.98 0.99 0.36 o 0 3 10 16.73 16.44 2.29 o 1 3 10 69.24 54.97 10.26 o 2 3 10 3.72 2.29 0.63 o 3 3 10 3.90 3.09 0.32 o 0 4 10 29.24 40.64 5.17 o 1 4 10 20.41 22.41 3.70 o 2 4 10 1.79 1.89 0.29 o 3 4 10 0.20 0.00 0.28 o 1 5 10 6.36 6.59 1.20 o 2 5 10 6.86 7.72 0.88 o