#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200165.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200165_Fobs loop_ _publ_author_name 'Parvez, Masood' 'Simion, Dan V.' 'Sorensen, Ted S.' _publ_section_title ; A novel chiral C~2~ axially symmetric acenaphthoquinone diketal ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o366 _journal_page_last o367 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.7990 _cell_length_b 19.3310 _cell_length_c 9.0540 _exptl_crystal_F_000 696.00 _reflns_d_resolution_high 0.8395 _[local]_cod_data_source_file cv6011Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TSS - Dan -6' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.80 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6829.69 6939.01 116.98 o 4 0 0 3635.44 3743.31 70.19 o 6 0 0 1801.55 1824.49 46.35 o 8 0 0 99.09 59.25 31.80 o 10 0 0 207.54 232.82 22.14 o 1 1 0 73.42 72.80 6.89 o 2 1 0 426.06 390.12 16.24 o 3 1 0 1763.91 1747.11 37.63 o 4 1 0 604.48 598.36 23.84 o 5 1 0 401.65 383.16 24.06 o 6 1 0 900.16 1012.78 35.12 o 7 1 0 134.84 137.67 14.14 o 8 1 0 139.13 142.07 16.20 o 9 1 0 52.22 39.24 33.11 o 10 1 0 11.20 -10.68 36.53 o 11 1 0 56.34 23.13 40.65 o 0 2 0 23653.18 23022.81 376.31 o 1 2 0 252.55 263.63 10.49 o 2 2 0 5566.00 5511.69 94.64 o 3 2 0 311.22 289.78 19.40 o 4 2 0 6.87 12.12 18.25 o 5 2 0 72.76 67.04 10.49 o 6 2 0 422.58 371.49 27.08 o 7 2 0 3.97 5.70 26.84 o 8 2 0 193.31 235.50 23.71 o 9 2 0 57.14 42.52 23.54 o 10 2 0 53.34 56.56 36.63 o 11 2 0 150.29 174.68 20.43 o 1 3 0 2788.56 2665.81 47.77 o 2 3 0 453.69 450.07 19.58 o 3 3 0 0.18 -17.75 17.75 o 4 3 0 150.54 144.89 13.82 o 5 3 0 459.40 479.01 25.81 o 6 3 0 70.97 65.78 12.14 o 7 3 0 23.24 57.10 13.73 o 8 3 0 11.44 -9.62 31.24 o 9 3 0 340.91 311.34 26.17 o 10 3 0 89.23 45.79 36.85 o 11 3 0 0.20 37.80 38.34 o 0 4 0 3524.90 3212.29 57.15 o 1 4 0 7212.81 6788.24 115.27 o 2 4 0 4240.15 3964.73 71.40 o 3 4 0 6.13 -2.73 17.53 o 4 4 0 17.51 6.74 18.80 o 5 4 0 332.87 325.56 24.49 o 6 4 0 151.45 156.02 14.98 o 7 4 0 423.52 377.32 32.35 o 8 4 0 5.96 37.04 31.17 o 9 4 0 1.42 56.63 32.49 o 10 4 0 0.61 6.88 35.22 o 11 4 0 39.05 46.98 19.75 o 1 5 0 5190.80 5107.67 89.34 o 2 5 0 151.22 134.05 12.84 o 3 5 0 62.83 61.20 9.18 o 4 5 0 877.26 886.88 29.32 o 5 5 0 1229.84 1367.10 38.30 o 6 5 0 1414.97 1365.23 41.53 o 7 5 0 136.40 126.10 15.53 o 8 5 0 52.50 79.91 16.17 o 9 5 0 143.02 142.64 17.25 o 10 5 0 28.35 67.71 36.22 o 11 5 0 61.42 115.39 19.99 o 0 6 0 285.61 271.77 19.20 o 1 6 0 27.95 -22.89 22.89 o 2 6 0 1084.12 1129.46 29.37 o 3 6 0 302.60 346.11 21.20 o 4 6 0 2117.68 2109.28 47.35 o 5 6 0 164.23 180.43 17.51 o 6 6 0 280.74 299.85 28.99 o 7 6 0 1002.59 1034.43 42.80 o 8 6 0 28.26 18.23 32.51 o 9 6 0 124.30 156.70 17.98 o 10 6 0 1.45 -26.31 36.59 o 11 6 0 72.65 -7.37 42.51 o 1 7 0 647.64 263.50 21.33 o 2 7 0 2363.35 2552.04 51.51 o 3 7 0 441.33 395.27 23.32 o 4 7 0 7.13 -6.98 21.12 o 5 7 0 739.93 733.74 31.85 o 6 7 0 593.56 552.35 32.94 o 7 7 0 38.07 44.26 30.67 o 8 7 0 7.69 2.36 31.92 o 9 7 0 0.05 8.24 33.53 o 10 7 0 18.42 34.54 36.39 o 11 7 0 4.92 27.53 41.41 o 0 8 0 7028.46 6915.38 120.96 o 1 8 0 311.74 -33.31 33.31 o 2 8 0 2.46 -19.16 19.16 o 3 8 0 3.45 8.20 19.79 o 4 8 0 236.50 218.14 17.14 o 5 8 0 24.38 24.73 24.44 o 6 8 0 30.77 44.77 28.29 o 7 8 0 54.49 15.17 31.85 o 8 8 0 4.46 29.22 31.84 o 9 8 0 56.53 17.16 35.22 o 10 8 0 29.76 15.31 38.75 o 1 9 0 0.62 -33.58 33.58 o 2 9 0 235.71 299.04 22.21 o 3 9 0 368.35 342.28 24.64 o 4 9 0 256.91 271.36 25.47 o 5 9 0 1.76 -16.16 25.44 o 6 9 0 49.34 48.87 29.66 o 7 9 0 31.45 2.32 31.62 o 8 9 0 36.91 38.56 32.32 o 9 9 0 1.24 -35.63 35.63 o 10 9 0 0.13 34.49 37.35 o 0 10 0 954.70 972.01 30.43 o 1 10 0 394.77 464.81 24.69 o 2 10 0 0.01 -38.01 38.01 o 3 10 0 29.82 32.86 22.48 o 4 10 0 178.23 195.96 18.34 o 5 10 0 8.28 42.25 26.37 o 6 10 0 0.04 -30.49 30.49 o 7 10 0 396.63 378.35 36.19 o 8 10 0 135.63 116.23 17.66 o 9 10 0 23.46 59.97 35.91 o 10 10 0 67.94 95.17 20.00 o 1 11 0 0.01 -25.28 25.28 o 2 11 0 675.49 467.95 36.40 o 3 11 0 1804.35 1792.16 47.60 o 4 11 0 20.86 37.44 26.40 o 5 11 0 1.50 36.36 27.89 o 6 11 0 191.66 205.72 18.94 o 7 11 0 1.23 -10.67 31.96 o 8 11 0 42.70 47.24 17.44 o 9 11 0 89.18 116.39 18.87 o 10 11 0 36.66 26.03 40.60 o 0 12 0 82.05 82.17 11.38 o 1 12 0 551.55 563.05 28.67 o 2 12 0 259.70 -47.84 47.84 o 3 12 0 626.04 521.09 38.73 o 4 12 0 429.23 444.30 32.76 o 5 12 0 1.40 20.45 29.73 o 6 12 0 0.20 -7.61 31.20 o 7 12 0 18.46 37.53 32.97 o 8 12 0 4.90 -13.77 34.81 o 9 12 0 23.46 27.75 38.58 o 1 13 0 10.76 -25.75 25.75 o 2 13 0 165.80 -38.65 38.65 o 3 13 0 513.64 430.81 38.07 o 4 13 0 136.32 95.81 15.67 o 5 13 0 254.58 196.78 19.53 o 6 13 0 373.86 330.43 25.38 o 7 13 0 64.90 89.08 17.36 o 8 13 0 71.02 74.90 37.71 o 9 13 0 204.64 210.75 20.88 o 0 14 0 282.48 292.89 20.90 o 1 14 0 32.82 41.56 26.76 o 2 14 0 63.75 -32.75 32.75 o 3 14 0 90.91 -38.14 38.14 o 4 14 0 23.34 1.10 32.26 o 5 14 0 0.76 -21.64 32.72 o 6 14 0 129.63 125.91 17.17 o 7 14 0 95.98 115.37 18.01 o 8 14 0 6.69 29.20 36.77 o 9 14 0 14.30 -23.36 39.95 o 1 15 0 252.80 206.34 17.72 o 2 15 0 82.91 -34.14 34.14 o 3 15 0 20.46 -35.66 35.66 o 4 15 0 483.64 497.75 39.82 o 5 15 0 2.34 -17.25 32.15 o 6 15 0 8.98 -24.52 34.01 o 7 15 0 20.37 12.49 35.79 o 8 15 0 4.86 31.90 37.88 o 0 16 0 569.88 530.76 36.20 o 1 16 0 22.45 -31.25 31.25 o 2 16 0 603.10 622.99 39.11 o 3 16 0 239.55 226.26 19.61 o 4 16 0 255.66 234.36 21.90 o 5 16 0 124.23 130.65 17.39 o 6 16 0 61.72 63.59 17.74 o 7 16 0 26.90 -38.16 38.16 o 8 16 0 31.86 35.18 38.70 o 1 17 0 564.81 549.95 37.25 o 2 17 0 22.33 -35.76 35.76 o 3 17 0 9.39 -36.87 36.87 o 4 17 0 3.44 -37.57 37.57 o 5 17 0 142.58 121.45 18.43 o 6 17 0 59.27 74.58 18.36 o 7 17 0 1.29 -25.85 37.83 o 0 18 0 10.36 52.79 31.19 o 1 18 0 0.02 -6.52 33.07 o 2 18 0 203.58 219.81 20.56 o 3 18 0 21.47 -35.20 35.20 o 4 18 0 171.92 173.22 18.53 o 5 18 0 107.26 126.75 18.62 o 6 18 0 4.02 9.74 36.65 o 7 18 0 67.04 74.45 19.86 o 1 19 0 41.44 34.41 33.28 o 2 19 0 39.80 40.39 34.53 o 3 19 0 76.52 76.73 17.50 o 4 19 0 6.73 -39.06 39.06 o 5 19 0 0.02 -36.86 36.86 o 6 19 0 7.10 55.49 37.79 o 0 20 0 35.47 19.73 34.45 o 1 20 0 20.95 -19.45 34.18 o 2 20 0 50.59 51.43 34.38 o 3 20 0 4.82 12.60 35.28 o 4 20 0 22.32 -6.08 36.00 o 5 20 0 2.92 -10.62 38.06 o 1 21 0 3.67 36.91 17.57 o 2 21 0 5.65 20.89 35.56 o 3 21 0 2.55 -36.52 37.58 o 4 21 0 15.89 -19.28 38.07 o 0 22 0 32.32 45.40 36.24 o 1 22 0 0.58 -28.58 36.87 o 2 22 0 3.08 14.74 37.40 o 3 22 0 38.99 75.33 37.85 o 1 0 1 68.60 81.13 6.77 o 2 0 1 10233.02 10359.14 173.13 o 3 0 1 171.60 168.96 13.19 o 4 0 1 191.95 204.74 19.90 o 5 0 1 81.64 71.33 10.56 o 6 0 1 161.01 166.79 14.40 o 7 0 1 1.56 -9.55 26.67 o 8 0 1 15.88 25.94 30.45 o 9 0 1 91.15 78.50 17.02 o 10 0 1 196.14 202.92 19.65 o 11 0 1 151.50 178.37 20.55 o 0 1 1 67.60 73.67 7.43 o 1 1 1 15209.00 15939.52 262.17 o 2 1 1 7031.58 7042.27 119.54 o 3 1 1 582.68 591.94 22.79 o 4 1 1 401.14 403.91 21.90 o 5 1 1 799.22 862.93 29.38 o 6 1 1 35.30 31.70 23.65 o 7 1 1 77.06 84.02 13.95 o 8 1 1 59.38 55.51 31.42 o 9 1 1 50.70 23.90 34.00 o 10 1 1 238.32 257.52 23.33 o 11 1 1 6.31 10.21 38.98 o 0 2 1 26.77 31.29 4.63 o 1 2 1 784.86 762.62 18.84 o 2 2 1 3335.17 3197.86 58.41 o 3 2 1 908.02 853.85 25.64 o 4 2 1 258.92 238.37 20.51 o 5 2 1 253.75 277.48 22.76 o 6 2 1 562.38 552.77 29.71 o 7 2 1 59.47 66.68 13.93 o 8 2 1 8.80 -4.23 31.20 o 9 2 1 241.20 275.90 20.94 o 10 2 1 129.65 122.67 19.01 o 11 2 1 24.53 31.42 23.10 o 0 3 1 8191.64 8600.43 143.56 o 1 3 1 193.32 187.08 14.86 o 2 3 1 10169.11 9957.16 167.62 o 3 3 1 504.99 511.85 21.83 o 4 3 1 396.76 372.42 22.15 o 5 3 1 444.75 418.61 25.47 o 6 3 1 379.25 368.32 28.09 o 7 3 1 64.93 41.91 28.41 o 8 3 1 61.90 57.91 16.18 o 9 3 1 83.66 11.77 35.51 o 10 3 1 45.06 88.72 18.36 o 11 3 1 3.77 7.92 38.86 o 0 4 1 300.54 300.98 17.04 o 1 4 1 1915.12 1813.80 37.24 o 2 4 1 399.94 427.00 20.58 o 3 4 1 446.92 447.51 21.58 o 4 4 1 1034.77 1110.15 31.85 o 5 4 1 876.07 850.66 30.84 o 6 4 1 1029.95 987.62 35.96 o 7 4 1 149.92 129.04 15.16 o 8 4 1 2.74 -0.27 31.94 o 9 4 1 49.22 6.76 34.29 o 10 4 1 29.60 5.37 37.15 o 11 4 1 66.67 79.51 20.23 o 0 5 1 84.75 80.04 8.56 o 1 5 1 56.67 47.00 8.79 o 2 5 1 420.57 420.56 20.54 o 3 5 1 86.70 85.97 9.52 o 4 5 1 383.36 413.31 23.49 o 5 5 1 272.60 243.62 24.60 o 6 5 1 374.47 356.99 28.88 o 7 5 1 86.35 69.20 14.97 o 8 5 1 87.04 71.99 16.49 o 9 5 1 140.51 162.95 17.78 o 10 5 1 54.65 44.37 37.52 o 11 5 1 15.80 65.61 38.60 o 0 6 1 100.78 73.57 8.74 o 1 6 1 1106.51 1114.89 29.06 o 2 6 1 551.25 535.80 22.05 o 3 6 1 715.10 803.82 26.71 o 4 6 1 1553.12 1579.31 40.12 o 5 6 1 479.05 522.55 27.74 o 6 6 1 175.54 213.98 19.83 o 7 6 1 162.16 160.03 15.87 o 8 6 1 36.79 16.73 32.47 o 9 6 1 82.65 75.55 17.47 o 10 6 1 14.03 -29.35 37.05 o 11 6 1 52.98 38.37 41.04 o 0 7 1 0.66 14.34 17.36 o 1 7 1 217.81 244.72 19.54 o 2 7 1 656.45 669.99 24.74 o 3 7 1 1145.88 1232.85 34.30 o 4 7 1 608.07 661.24 28.11 o 5 7 1 34.03 33.35 23.51 o 6 7 1 18.20 41.82 27.05 o 7 7 1 328.50 360.42 33.71 o 8 7 1 281.25 261.87 25.16 o 9 7 1 12.40 31.53 34.28 o 10 7 1 114.18 134.75 19.73 o 11 7 1 5.42 -41.65 41.65 o 0 8 1 9.85 6.32 18.17 o 1 8 1 1214.81 1283.19 33.05 o 2 8 1 250.03 240.34 21.14 o 3 8 1 458.09 426.48 24.35 o 4 8 1 74.78 91.01 11.64 o 5 8 1 89.94 108.23 12.93 o 6 8 1 151.69 151.30 15.04 o 7 8 1 11.36 18.15 31.34 o 8 8 1 9.82 5.16 32.72 o 9 8 1 42.01 75.56 17.51 o 10 8 1 8.28 10.35 38.70 o 0 9 1 121.82 144.74 14.38 o 1 9 1 469.65 474.57 23.63 o 2 9 1 1439.04 1605.91 40.25 o 3 9 1 321.09 337.26 24.44 o 4 9 1 411.95 403.47 27.37 o 5 9 1 217.72 215.57 20.28 o 6 9 1 174.45 199.72 17.63 o 7 9 1 118.09 129.83 16.61 o 8 9 1 133.53 113.90 17.58 o 9 9 1 25.45 23.87 36.21 o 10 9 1 5.22 38.96 38.74 o 0 10 1 0.19 17.49 11.51 o 1 10 1 247.97 344.35 23.35 o 2 10 1 661.54 646.90 27.65 o 3 10 1 831.83 935.50 33.08 o 4 10 1 64.45 44.83 24.76 o 5 10 1 82.49 70.03 14.15 o 6 10 1 9.46 -8.71 30.51 o 7 10 1 271.77 252.62 20.63 o 8 10 1 61.81 59.91 17.15 o 9 10 1 58.82 72.65 18.42 o 10 10 1 32.10 -1.33 41.01 o 0 11 1 27.48 36.07 20.67 o 1 11 1 231.07 245.74 23.77 o 2 11 1 53.39 55.13 11.45 o 3 11 1 33.23 37.17 24.36 o 4 11 1 224.48 302.69 29.10 o 5 11 1 2.13 24.29 27.75 o 6 11 1 34.40 42.80 15.85 o 7 11 1 116.18 87.48 16.93 o 8 11 1 5.90 27.75 33.95 o 9 11 1 9.09 2.82 36.34 o 10 11 1 0.86 -39.73 39.73 o 0 12 1 187.77 182.77 17.36 o 1 12 1 36.62 53.77 11.87 o 2 12 1 264.36 292.09 27.07 o 3 12 1 283.58 321.50 29.29 o 4 12 1 156.66 134.56 14.81 o 5 12 1 493.40 619.69 36.53 o 6 12 1 393.43 368.31 36.85 o 7 12 1 365.91 351.10 26.69 o 8 12 1 204.41 228.50 21.93 o 9 12 1 39.97 49.36 37.88 o 0 13 1 162.94 149.45 15.03 o 1 13 1 628.96 689.51 32.68 o 2 13 1 202.83 197.70 16.67 o 3 13 1 114.22 151.37 15.01 o 4 13 1 293.00 352.13 33.13 o 5 13 1 126.26 124.54 16.54 o 6 13 1 85.00 39.05 34.34 o 7 13 1 191.85 218.90 20.93 o 8 13 1 5.82 -11.75 36.70 o 9 13 1 17.13 67.71 39.32 o 0 14 1 1.44 -26.91 26.91 o 1 14 1 48.42 45.82 27.28 o 2 14 1 220.94 205.38 17.91 o 3 14 1 380.74 433.14 35.10 o 4 14 1 67.95 -11.26 31.62 o 5 14 1 358.33 325.23 25.53 o 6 14 1 143.33 155.13 17.64 o 7 14 1 5.66 -35.98 35.98 o 8 14 1 44.58 29.84 37.27 o 9 14 1 49.00 26.27 40.55 o 0 15 1 302.85 300.84 22.78 o 1 15 1 100.29 89.26 14.84 o 2 15 1 53.48 5.16 29.98 o 3 15 1 305.53 355.74 35.18 o 4 15 1 4.05 21.73 31.74 o 5 15 1 24.25 13.54 32.80 o 6 15 1 38.85 37.30 33.20 o 7 15 1 151.84 74.83 38.71 o 8 15 1 113.78 72.51 40.80 o 0 16 1 186.60 171.94 16.02 o 1 16 1 27.09 40.33 21.52 o 2 16 1 87.54 55.96 32.60 o 3 16 1 102.30 112.07 16.68 o 4 16 1 17.84 37.80 31.32 o 5 16 1 4.60 16.58 32.51 o 6 16 1 5.97 65.38 33.98 o 7 16 1 12.76 7.43 37.15 o 8 16 1 55.49 -7.07 41.59 o 0 17 1 360.71 306.85 25.38 o 1 17 1 338.29 305.48 24.96 o 2 17 1 152.67 140.41 16.86 o 3 17 1 442.22 417.57 38.31 o 4 17 1 121.97 144.99 17.34 o 5 17 1 5.53 -1.81 33.67 o 6 17 1 107.33 57.62 38.09 o 7 17 1 2.79 29.30 37.28 o 0 18 1 218.53 258.98 24.34 o 1 18 1 88.58 103.85 16.60 o 2 18 1 204.27 197.35 17.83 o 3 18 1 6.80 -34.83 34.83 o 4 18 1 12.04 45.71 33.29 o 5 18 1 24.57 -9.35 36.13 o 6 18 1 20.23 66.58 37.05 o 7 18 1 0.82 51.01 38.45 o 0 19 1 13.82 24.26 32.61 o 1 19 1 28.72 56.47 33.18 o 2 19 1 59.12 66.94 34.23 o 3 19 1 12.77 33.62 33.93 o 4 19 1 41.63 67.86 36.69 o 5 19 1 10.71 -9.52 37.41 o 6 19 1 31.76 4.00 39.74 o 0 20 1 0.06 27.01 32.50 o 1 20 1 238.09 300.29 26.58 o 2 20 1 0.61 27.43 34.47 o 3 20 1 14.17 -19.37 35.74 o 4 20 1 28.64 19.43 36.74 o 5 20 1 69.76 56.75 39.52 o 0 21 1 31.49 65.13 34.34 o 1 21 1 0.24 -11.15 35.02 o 2 21 1 11.48 12.61 35.57 o 3 21 1 45.86 36.50 37.82 o 4 21 1 19.63 -22.41 37.75 o 0 22 1 8.14 32.73 36.34 o 1 22 1 16.26 48.23 36.86 o 2 22 1 14.01 48.23 37.16 o 3 22 1 7.27 32.32 37.36 o 0 0 2 43.02 53.23 7.19 o 1 0 2 5570.40 5607.56 96.51 o 2 0 2 631.32 693.27 23.06 o 3 0 2 8238.08 8535.58 146.52 o 4 0 2 1199.27 1213.14 32.90 o 5 0 2 1.20 -1.04 21.51 o 6 0 2 75.94 86.87 12.43 o 7 0 2 52.19 43.96 28.98 o 8 0 2 16.14 47.60 31.88 o 9 0 2 139.36 127.11 17.78 o 10 0 2 40.97 17.08 37.35 o 11 0 2 141.64 142.40 20.59 o 0 1 2 1404.93 1278.86 28.24 o 1 1 2 1494.98 1495.87 32.37 o 2 1 2 1587.03 1490.32 34.01 o 3 1 2 368.38 363.52 20.82 o 4 1 2 507.88 554.57 24.40 o 5 1 2 342.14 358.47 24.78 o 6 1 2 5.16 45.98 24.28 o 7 1 2 7.97 10.27 28.80 o 8 1 2 26.64 -8.10 32.33 o 9 1 2 377.61 377.67 27.95 o 10 1 2 33.71 43.90 37.00 o 11 1 2 43.34 6.50 40.72 o 0 2 2 79.67 92.27 9.28 o 1 2 2 13626.82 13974.79 232.49 o 2 2 2 2804.25 2734.06 52.61 o 3 2 2 1286.12 1273.17 32.21 o 4 2 2 320.94 370.36 22.23 o 5 2 2 21.98 15.76 21.42 o 6 2 2 53.41 53.25 12.61 o 7 2 2 121.21 124.80 15.03 o 8 2 2 310.24 316.85 25.48 o 9 2 2 98.22 40.30 35.99 o 10 2 2 33.97 29.50 37.83 o 11 2 2 48.64 65.16 40.08 o 0 3 2 2715.69 2530.41 48.43 o 1 3 2 870.98 814.26 24.34 o 2 3 2 342.54 326.03 19.96 o 3 3 2 2797.45 2803.29 55.43 o 4 3 2 75.69 39.60 20.32 o 5 3 2 67.01 62.76 11.14 o 6 3 2 95.56 103.48 13.08 o 7 3 2 350.02 358.21 32.73 o 8 3 2 7.72 -0.82 31.98 o 9 3 2 100.28 56.38 36.42 o 10 3 2 43.24 36.57 37.47 o 11 3 2 44.11 -15.96 41.24 o 0 4 2 254.02 285.45 18.83 o 1 4 2 1226.52 1199.96 29.94 o 2 4 2 521.48 537.12 22.32 o 3 4 2 2181.85 2177.34 46.22 o 4 4 2 1499.93 1449.11 38.04 o 5 4 2 475.05 542.17 28.05 o 6 4 2 336.94 363.93 28.66 o 7 4 2 161.77 145.31 15.71 o 8 4 2 42.54 16.25 32.35 o 9 4 2 54.10 -23.29 35.42 o 10 4 2 63.71 76.47 38.29 o 11 4 2 22.28 4.62 40.78 o 0 5 2 1100.89 1163.76 29.39 o 1 5 2 72.51 80.57 9.03 o 2 5 2 2001.13 2074.87 43.87 o 3 5 2 951.20 962.02 29.18 o 4 5 2 66.47 72.29 10.58 o 5 5 2 889.75 934.22 33.67 o 6 5 2 261.30 257.19 20.95 o 7 5 2 216.86 246.74 22.94 o 8 5 2 49.02 54.34 32.51 o 9 5 2 101.33 119.64 17.90 o 10 5 2 4.00 8.03 36.93 o 11 5 2 20.58 52.94 40.92 o 0 6 2 104.06 134.44 13.14 o 1 6 2 601.52 636.61 23.49 o 2 6 2 1418.29 1415.07 34.70 o 3 6 2 999.05 1002.63 30.92 o 4 6 2 355.67 358.12 24.60 o 5 6 2 48.42 45.21 23.77 o 6 6 2 271.76 250.33 21.29 o 7 6 2 71.39 76.91 15.59 o 8 6 2 104.06 32.99 34.24 o 9 6 2 25.06 58.52 34.68 o 10 6 2 11.04 63.76 36.97 o 11 6 2 13.10 23.72 41.07 o 0 7 2 2221.06 2519.76 51.08 o 1 7 2 102.49 104.34 9.77 o 2 7 2 219.22 209.77 20.81 o 3 7 2 876.94 987.03 31.71 o 4 7 2 43.06 58.24 11.16 o 5 7 2 415.29 412.81 28.91 o 6 7 2 251.95 247.31 21.78 o 7 7 2 161.48 162.47 16.61 o 8 7 2 45.00 31.92 32.71 o 9 7 2 181.69 179.81 19.08 o 10 7 2 13.61 70.42 37.24 o 0 8 2 1435.26 1382.67 35.36 o 1 8 2 361.12 396.60 22.41 o 2 8 2 375.80 364.88 23.69 o 3 8 2 851.14 917.32 31.19 o 4 8 2 49.56 41.73 11.35 o 5 8 2 37.64 49.20 13.07 o 6 8 2 204.32 200.46 18.29 o 7 8 2 45.33 -15.30 32.97 o 8 8 2 347.11 318.37 26.35 o 9 8 2 1.88 7.35 35.58 o 10 8 2 10.00 36.75 38.35 o 0 9 2 2.10 -17.24 19.79 o 1 9 2 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