#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180922 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/02/2200201.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200201_Fobs loop_ _publ_author_name 'Lynch, Daniel E.' 'McClenaghan, Ian' 'Coles, Simon J.' _publ_section_title ; 2-Chloro-3-[4-(ethoxycarbonyl)-1-piperidyl]-1,4-naphthoquinone ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o125 _journal_page_last o126 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.846 _cell_angle_gamma 90.000 _cell_length_a 12.7804 _cell_length_b 16.9310 _cell_length_c 7.8532 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file ob6020Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 2-Chloro-3-(4'-carbethoxypiperidyl)-1,4-naphthaquinone _shelx_refln_list_code 4 _shelx_f_calc_maximum 218.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1920.19 1647.41 92.31 o 3 0 0 0.13 0.00 17.90 o 4 0 0 1257.51 1065.40 64.06 o 5 0 0 1438.19 1211.65 82.32 o 6 0 0 1829.43 1548.86 139.95 o 7 0 0 264.17 237.77 36.11 o 8 0 0 739.25 628.55 51.42 o 9 0 0 802.56 863.37 78.20 o 10 0 0 591.45 585.25 71.72 o 11 0 0 8.06 -11.76 50.51 o 12 0 0 132.73 165.46 53.19 o 14 0 0 0.93 -2.94 73.22 o 1 1 0 1261.04 574.22 247.10 o 2 1 0 303.61 320.48 9.58 o 3 1 0 4314.44 4038.39 79.83 o 4 1 0 1712.70 1585.45 40.18 o 5 1 0 25.19 28.17 4.81 o 6 1 0 266.09 254.80 26.49 o 7 1 0 91.46 53.39 30.56 o 8 1 0 481.26 514.01 41.78 o 9 1 0 41.31 45.35 26.30 o 10 1 0 22.40 0.63 34.21 o 11 1 0 71.95 38.86 30.38 o 12 1 0 121.72 170.62 42.78 o 0 2 0 7736.58 7776.69 322.63 o 1 2 0 883.55 947.44 30.15 o 2 2 0 330.64 373.16 9.52 o 3 2 0 1298.04 1233.16 24.17 o 4 2 0 3336.29 3251.46 58.17 o 5 2 0 243.49 240.11 7.82 o 6 2 0 39.94 38.43 9.95 o 7 2 0 49.48 50.52 16.19 o 8 2 0 106.58 109.71 13.11 o 9 2 0 0.26 -7.00 23.92 o 10 2 0 41.16 40.29 38.62 o 11 2 0 4.76 -20.84 44.63 o 12 2 0 47.23 -14.43 49.44 o 13 2 0 15.47 28.19 45.36 o 1 3 0 1418.85 1328.33 34.70 o 2 3 0 514.28 543.13 16.00 o 3 3 0 757.03 834.91 19.93 o 4 3 0 533.95 511.20 12.61 o 5 3 0 127.18 129.87 7.97 o 6 3 0 950.53 1024.20 23.71 o 7 3 0 12.47 1.76 7.70 o 8 3 0 63.27 72.36 20.14 o 9 3 0 6.38 8.45 13.38 o 10 3 0 179.39 246.22 49.19 o 11 3 0 66.11 35.28 53.19 o 12 3 0 29.83 37.41 60.40 o 13 3 0 0.15 2.94 63.06 o 0 4 0 22300.77 23411.05 698.38 o 1 4 0 4016.93 3525.90 74.12 o 2 4 0 3060.45 2861.32 65.83 o 3 4 0 228.46 232.61 10.17 o 4 4 0 262.02 262.87 12.51 o 5 4 0 114.04 113.60 8.73 o 6 4 0 1.92 -4.83 5.07 o 7 4 0 65.61 65.72 7.13 o 8 4 0 0.06 4.31 5.82 o 9 4 0 0.45 3.11 15.53 o 10 4 0 16.14 9.65 5.21 o 12 4 0 0.11 -35.27 49.97 o 13 4 0 5.48 11.49 68.14 o 14 4 0 2.66 82.31 68.14 o 1 5 0 139.80 159.10 11.12 o 2 5 0 19.89 6.81 12.88 o 3 5 0 462.05 410.26 17.29 o 4 5 0 506.10 543.75 18.12 o 5 5 0 253.37 248.91 13.82 o 6 5 0 620.33 622.70 21.33 o 7 5 0 0.48 2.76 5.57 o 8 5 0 53.67 48.68 6.99 o 9 5 0 123.96 141.38 9.57 o 10 5 0 14.13 21.57 11.62 o 11 5 0 120.18 143.01 16.25 o 0 6 0 414.33 422.01 26.61 o 1 6 0 30.00 19.08 11.33 o 2 6 0 850.76 874.72 24.92 o 3 6 0 40.77 32.88 12.50 o 4 6 0 390.27 422.98 25.92 o 5 6 0 1365.64 1431.17 39.22 o 6 6 0 65.82 70.08 9.92 o 7 6 0 40.81 32.29 8.58 o 8 6 0 26.15 17.19 8.11 o 9 6 0 55.83 38.20 7.50 o 10 6 0 2.31 6.51 6.61 o 11 6 0 0.20 -17.48 11.66 o 12 6 0 82.62 71.94 15.18 o 1 7 0 239.30 237.57 15.76 o 2 7 0 177.80 154.03 14.26 o 3 7 0 1047.43 1036.99 31.44 o 4 7 0 346.82 381.40 18.57 o 5 7 0 8.21 -13.95 9.30 o 6 7 0 106.59 118.05 12.28 o 7 7 0 39.59 54.24 10.44 o 8 7 0 123.49 121.62 11.68 o 9 7 0 145.87 134.15 13.06 o 10 7 0 242.90 289.77 19.20 o 11 7 0 131.63 149.44 12.48 o 12 7 0 45.10 51.86 19.24 o 0 8 0 8183.28 9209.27 242.88 o 1 8 0 2443.87 2581.84 64.79 o 2 8 0 3970.35 4233.88 99.43 o 3 8 0 0.08 -13.80 15.30 o 4 8 0 102.53 105.02 16.98 o 5 8 0 806.75 854.82 28.96 o 6 8 0 290.27 286.68 17.46 o 7 8 0 175.05 198.50 24.05 o 8 8 0 393.30 445.34 23.13 o 9 8 0 223.45 219.76 19.01 o 10 8 0 1.22 9.60 11.07 o 11 8 0 116.09 109.80 12.78 o 12 8 0 66.41 80.54 18.30 o 1 9 0 2930.20 3114.90 81.10 o 2 9 0 271.87 238.20 19.87 o 3 9 0 411.72 402.90 21.47 o 4 9 0 6.09 -1.83 14.68 o 5 9 0 3.15 15.74 14.71 o 6 9 0 109.64 107.47 13.56 o 7 9 0 98.56 83.59 14.15 o 8 9 0 389.42 418.62 25.07 o 9 9 0 679.53 812.45 39.56 o 10 9 0 5.60 4.59 13.03 o 11 9 0 0.03 -8.72 15.47 o 12 9 0 4.04 -9.26 22.95 o 0 10 0 337.76 345.66 47.35 o 1 10 0 9.52 4.31 18.59 o 2 10 0 510.24 547.98 27.14 o 3 10 0 0.01 9.45 13.84 o 4 10 0 643.39 612.18 34.79 o 5 10 0 13.79 12.28 14.50 o 6 10 0 17.54 18.29 12.82 o 7 10 0 1.82 -19.56 13.14 o 8 10 0 177.94 188.66 18.90 o 9 10 0 11.19 1.95 12.70 o 10 10 0 0.08 27.20 15.67 o 11 10 0 0.05 9.84 15.39 o 12 10 0 6.79 23.11 35.14 o 1 11 0 0.61 -12.43 13.57 o 2 11 0 10.83 13.22 14.69 o 3 11 0 7.31 8.14 14.37 o 4 11 0 8.55 -29.28 19.52 o 5 11 0 23.96 20.77 15.98 o 6 11 0 6.26 16.97 16.52 o 7 11 0 0.49 3.59 14.48 o 8 11 0 0.48 4.58 18.00 o 9 11 0 50.33 22.89 15.02 o 10 11 0 8.84 36.25 19.98 o 11 11 0 0.26 -3.37 15.88 o 12 11 0 8.25 5.56 20.13 o 0 12 0 30.22 11.43 22.39 o 1 12 0 97.32 79.62 18.44 o 2 12 0 82.36 41.66 21.14 o 3 12 0 220.10 237.85 28.48 o 4 12 0 1.74 -2.28 16.75 o 5 12 0 28.46 16.07 18.73 o 6 12 0 2.34 15.12 18.40 o 7 12 0 15.13 7.96 22.03 o 8 12 0 4.14 -16.00 17.71 o 9 12 0 0.46 -7.25 17.83 o 10 12 0 2.15 10.09 22.67 o 11 12 0 0.89 -36.39 24.26 o 1 13 0 326.40 326.61 32.32 o 2 13 0 22.04 37.36 20.20 o 3 13 0 297.60 247.06 25.10 o 4 13 0 114.00 58.84 21.85 o 5 13 0 0.12 -5.66 19.35 o 6 13 0 2.43 3.12 19.92 o 7 13 0 19.61 15.11 18.53 o 8 13 0 1.54 14.15 22.16 o 9 13 0 13.46 20.48 25.93 o 10 13 0 0.58 8.56 24.98 o 11 13 0 0.04 -36.65 29.26 o 0 14 0 4.52 -37.73 27.33 o 1 14 0 5.99 -19.95 19.49 o 2 14 0 57.32 60.97 22.42 o 3 14 0 119.59 111.65 24.57 o 4 14 0 121.01 105.70 25.29 o 5 14 0 68.93 76.17 23.56 o 6 14 0 19.97 31.55 24.38 o 7 14 0 3.22 1.75 28.39 o 8 14 0 14.71 2.04 24.66 o 9 14 0 9.68 -15.78 25.40 o 10 14 0 1.43 12.41 32.91 o 1 15 0 73.69 87.18 24.52 o 2 15 0 62.81 36.29 23.80 o 3 15 0 80.89 90.30 33.02 o 4 15 0 36.16 25.80 25.00 o 5 15 0 44.64 75.32 30.37 o 6 15 0 1.65 19.63 27.65 o 7 15 0 5.33 -15.79 23.98 o 8 15 0 62.56 54.47 28.44 o 9 15 0 5.51 16.74 29.12 o 0 16 0 79.52 119.11 49.24 o 1 16 0 1.39 -7.48 30.29 o 2 16 0 3.77 21.82 29.87 o 3 16 0 48.10 47.09 33.68 o 4 16 0 87.00 86.97 30.29 o 5 16 0 39.84 28.92 29.85 o 6 16 0 5.50 -40.81 56.10 o 7 16 0 32.83 79.00 48.41 o 8 16 0 73.63 45.77 39.47 o 9 16 0 19.58 44.59 42.26 o 1 17 0 25.62 7.25 49.71 o 2 17 0 40.93 67.12 42.84 o 3 17 0 0.06 5.89 40.01 o 4 17 0 76.95 72.50 43.62 o 5 17 0 17.64 0.00 56.92 o 6 17 0 4.18 -49.62 44.03 o 7 17 0 0.64 -65.20 55.98 o 0 18 0 129.81 68.16 70.83 o 1 18 0 20.62 59.24 46.87 o 2 18 0 5.90 -30.99 43.14 o 3 18 0 0.01 9.86 40.15 o 4 18 0 0.43 0.00 56.92 o 5 18 0 0.25 -50.36 51.00 o 6 18 0 1.99 -36.66 87.52 o 1 19 0 24.44 46.18 58.12 o 2 19 0 0.18 108.41 66.71 o 3 19 0 6.52 68.11 60.60 o 4 19 0 7.95 0.82 49.01 o 0 20 0 7.93 25.39 70.82 o 1 20 0 0.05 11.22 93.26 o -13 1 1 4.90 26.46 59.06 o -12 1 1 7.24 5.88 50.77 o -11 1 1 7.24 23.88 32.27 o -10 1 1 792.70 845.05 59.64 o -9 1 1 0.18 -6.95 27.14 o -8 1 1 0.16 9.39 15.58 o -7 1 1 1515.34 1615.95 34.78 o -6 1 1 199.38 180.98 6.78 o -5 1 1 74.77 80.63 8.38 o -4 1 1 1072.60 1048.84 22.37 o -3 1 1 594.26 590.75 15.44 o -2 1 1 579.08 502.50 11.08 o -1 1 1 4355.61 3893.18 84.69 o 0 1 1 5655.21 5192.89 110.91 o 1 1 1 17.40 32.25 4.88 o 2 1 1 13027.37 12445.53 230.44 o 3 1 1 12728.01 12465.29 199.59 o 4 1 1 1876.95 1766.30 33.17 o 5 1 1 58.31 55.38 5.16 o 6 1 1 52.96 49.69 6.15 o 7 1 1 9.38 11.84 6.74 o 8 1 1 46.03 39.30 28.36 o 9 1 1 41.39 14.70 44.10 o 10 1 1 21.22 63.26 27.53 o 11 1 1 57.45 81.25 55.32 o 12 1 1 29.90 55.59 61.47 o 13 1 1 0.02 5.88 57.45 o -14 2 1 0.80 -61.56 48.62 o -13 2 1 1.28 2.94 55.58 o -12 2 1 79.33 119.20 56.66 o -11 2 1 204.67 235.90 38.82 o -10 2 1 9.84 28.37 25.68 o -9 2 1 490.82 529.15 26.03 o -8 2 1 350.64 390.50 27.60 o -7 2 1 3001.86 3244.29 80.01 o -6 2 1 557.26 549.75 15.13 o -5 2 1 8.05 12.54 4.46 o -4 2 1 463.31 435.84 13.72 o -3 2 1 2178.18 1986.30 37.43 o -2 2 1 56.45 61.18 10.24 o -1 2 1 8.12 23.51 7.00 o 0 2 1 4368.45 3832.84 88.88 o 1 2 1 8590.27 8183.58 165.40 o 2 2 1 47609.35 56440.90 950.24 o 3 2 1 8578.16 8662.18 145.26 o 4 2 1 885.39 926.59 18.37 o 5 2 1 367.56 385.78 12.32 o 6 2 1 175.64 159.90 9.34 o 7 2 1 266.06 288.98 18.64 o 8 2 1 47.92 46.37 6.66 o 9 2 1 36.96 44.20 19.17 o 10 2 1 2.72 26.19 29.93 o 11 2 1 98.60 94.88 57.47 o 12 2 1 33.90 143.78 64.67 o 14 2 1 3.69 45.16 67.88 o -14 3 1 2.93 -17.37 69.48 o -12 3 1 4.52 47.30 56.38 o -11 3 1 3.57 55.58 43.83 o -10 3 1 357.42 357.60 24.32 o -9 3 1 257.17 235.37 21.88 o -8 3 1 64.17 67.83 6.42 o -7 3 1 288.10 298.09 13.01 o -6 3 1 2375.33 2464.16 67.72 o -5 3 1 464.85 425.03 12.92 o -4 3 1 2109.64 2126.49 38.53 o -3 3 1 2415.85 2310.20 46.69 o -2 3 1 3250.17 3124.73 69.46 o -1 3 1 2859.74 2815.73 69.54 o 0 3 1 117.95 120.34 10.63 o 1 3 1 37.25 31.07 10.96 o 2 3 1 2796.79 2623.62 62.31 o 3 3 1 4687.52 4463.61 107.00 o 4 3 1 866.89 864.32 26.58 o 5 3 1 806.22 826.40 25.10 o 6 3 1 811.21 866.15 25.05 o 7 3 1 23.22 29.86 8.12 o 8 3 1 327.31 323.83 11.67 o 9 3 1 8.10 6.78 8.54 o 10 3 1 61.33 62.95 8.14 o 11 3 1 19.08 65.21 45.43 o 12 3 1 10.10 -8.55 50.77 o 13 3 1 26.02 -40.89 70.28 o -14 4 1 20.51 -66.01 71.89 o -13 4 1 30.30 -29.40 62.00 o -12 4 1 68.49 43.30 57.73 o -11 4 1 13.89 19.67 10.42 o -10 4 1 0.90 2.92 8.68 o -9 4 1 12.07 7.82 4.64 o -8 4 1 180.40 173.48 13.76 o -7 4 1 25.90 18.17 9.30 o -6 4 1 77.35 89.32 8.93 o -5 4 1 551.63 536.72 17.45 o -4 4 1 428.56 408.53 13.83 o -3 4 1 174.97 163.86 12.88 o -2 4 1 1731.48 1583.43 40.50 o -1 4 1 8000.40 7572.39 161.17 o 0 4 1 3546.32 3216.02 67.08 o 1 4 1 82.88 80.16 9.98 o 2 4 1 1350.86 1264.76 34.04 o 3 4 1 2053.13 2193.47 45.65 o 4 4 1 364.07 379.89 14.39 o 5 4 1 28.44 35.92 10.95 o 6 4 1 489.10 472.61 17.85 o 7 4 1 1419.40 1653.54 50.46 o 8 4 1 3.13 5.87 4.13 o 9 4 1 7.76 0.67 5.08 o 10 4 1 0.20 -7.16 10.53 o 11 4 1 1.11 6.10 14.19 o 12 4 1 9.57 16.84 61.46 o -12 5 1 72.26 65.82 11.73 o -11 5 1 109.95 114.35 15.41 o -10 5 1 30.37 12.91 8.13 o -9 5 1 234.45 232.98 13.67 o -8 5 1 76.12 79.90 9.25 o -7 5 1 427.85 450.77 18.71 o -6 5 1 80.16 81.59 10.25 o -5 5 1 1921.40 1868.39 45.71 o -4 5 1 242.58 249.11 13.10 o -3 5 1 1702.93 1657.43 44.19 o -2 5 1 225.39 210.78 20.04 o -1 5 1 5683.69 5323.21 126.64 o 0 5 1 140.82 175.05 20.54 o 1 5 1 81.69 56.81 12.27 o 2 5 1 883.30 844.18 26.10 o 3 5 1 2361.68 2295.63 55.88 o 4 5 1 32.43 28.62 7.65 o 5 5 1 0.08 3.22 8.64 o 6 5 1 17.68 8.98 7.74 o 7 5 1 12.54 4.03 7.91 o 8 5 1 44.92 47.83 7.49 o 9 5 1 2.58 -0.35 6.56 o 10 5 1 9.41 6.68 11.71 o 11 5 1 5.47 -1.19 16.03 o 12 5 1 25.78 -29.13 58.26 o -13 6 1 7.62 5.61 11.22 o -12 6 1 0.32 -12.75 14.07 o -11 6 1 2.18 2.72 5.01 o -10 6 1 12.40 -2.17 7.92 o -9 6 1 205.24 207.25 12.31 o -8 6 1 6.71 17.12 10.50 o -7 6 1 112.27 115.18 12.40 o -6 6 1 10.42 -2.22 11.07 o -5 6 1 61.41 62.72 11.41 o -4 6 1 1166.97 1211.89 34.19 o -3 6 1 296.25 302.10 16.21 o -2 6 1 1834.76 1693.63 49.16 o -1 6 1 56.78 36.51 14.39 o 0 6 1 2383.97 2372.69 61.17 o 1 6 1 578.72 503.39 20.32 o 2 6 1 469.83 512.35 22.84 o 3 6 1 3490.35 3564.39 90.52 o 4 6 1 3243.22 3555.32 88.33 o 5 6 1 64.07 48.63 11.36 o 6 6 1 8.62 5.44 9.37 o 7 6 1 16.98 2.18 7.71 o 8 6 1 10.20 2.11 8.63 o 9 6 1 123.29 127.79 12.65 o 10 6 1 19.39 25.24 7.00 o 11 6 1 125.56 131.30 20.41 o 12 6 1 20.32 -6.66 10.18 o -13 7 1 0.40 -19.51 22.45 o -12 7 1 0.00 -14.72 21.04 o -11 7 1 4.21 14.42 10.32 o -10 7 1 0.73 -13.65 15.28 o -9 7 1 562.48 561.35 30.08 o -8 7 1 182.65 154.85 14.42 o -7 7 1 328.65 343.92 18.58 o -6 7 1 97.18 93.20 18.40 o -5 7 1 83.30 73.00 13.08 o -4 7 1 118.73 90.15 17.63 o -3 7 1 383.71 370.56 20.34 o -2 7 1 1.02 4.60 11.11 o -1 7 1 4.41 14.38 11.87 o 0 7 1 34.30 20.41 12.26 o 1 7 1 216.39 228.58 16.42 o 2 7 1 3391.07 3742.89 99.45 o 3 7 1 701.85 767.94 29.16 o 4 7 1 585.73 602.44 26.94 o 5 7 1 40.80 19.99 10.81 o 6 7 1 11.00 0.56 10.77 o 7 7 1 1.26 -3.43 14.51 o 8 7 1 12.05 10.07 9.44 o 9 7 1 4.58 13.61 8.50 o 10 7 1 77.83 75.48 11.13 o 11 7 1 182.78 210.68 25.58 o 12 7 1 13.64 14.43 25.92 o -13 8 1 8.31 36.34 25.12 o -12 8 1 8.70 6.63 9.61 o -11 8 1 3.16 4.72 14.25 o -10 8 1 179.03 178.36 16.50 o -9 8 1 214.80 218.51 16.52 o -8 8 1 2.55 -14.06 10.06 o -7 8 1 405.17 462.91 22.89 o -6 8 1 6.19 -6.23 21.48 o -5 8 1 0.07 2.26 11.87 o -4 8 1 146.18 144.75 17.59 o -3 8 1 388.11 377.50 25.56 o -2 8 1 13.53 7.91 12.82 o -1 8 1 14.04 3.20 11.33 o 0 8 1 19.63 -4.53 11.81 o 1 8 1 549.72 597.88 34.42 o 2 8 1 1463.11 1710.04 65.46 o 3 8 1 636.87 686.50 32.19 o 4 8 1 6.49 2.24 15.18 o 5 8 1 88.72 77.53 13.19 o 6 8 1 18.22 30.80 10.76 o 7 8 1 43.88 27.53 11.35 o 8 8 1 16.00 18.77 10.95 o 9 8 1 18.31 4.55 9.99 o 10 8 1 42.30 23.12 12.98 o 11 8 1 39.74 28.12 9.71 o 12 8 1 55.52 22.98 28.60 o -12 9 1 10.82 24.63 16.70 o -11 9 1 32.73 9.62 11.87 o -10 9 1 8.90 12.44 12.06 o -9 9 1 238.64 230.92 23.31 o -8 9 1 29.52 15.41 12.78 o -7 9 1 85.43 89.88 14.23 o -6 9 1 80.34 69.68 12.78 o -5 9 1 0.17 -5.43 15.91 o -4 9 1 165.32 142.94 18.77 o -3 9 1 0.40 -9.50 14.78 o -2 9 1 121.31 107.36 20.00 o -1 9 1 1689.23 1913.28 72.68 o 0 9 1 67.39 63.76 17.18 o 1 9 1 18.56 -19.69 13.12 o 2 9 1 432.69 484.48 26.06 o 3 9 1 78.95 98.22 16.41 o 4 9 1 18.19 9.21 23.53 o 5 9 1 2.34 7.78 12.05 o 6 9 1 12.58 -0.26 11.83 o 7 9 1 7.95 11.15 12.61 o 8 9 1 17.02 23.40 14.02 o 9 9 1 9.91 15.02 12.08 o 10 9 1 26.67 51.51 15.59 o 11 9 1 32.69 56.72 14.23 o 12 9 1 2.83 11.50 17.27 o -12 10 1 5.18 2.99 14.20 o -11 10 1 1.89 -2.60 14.90 o -10 10 1 10.34 10.27 14.19 o -9 10 1 527.98 566.87 34.72 o -8 10 1 0.24 -22.61 15.22 o -7 10 1 544.02 605.83 30.47 o -6 10 1 644.13 592.51 30.81 o -5 10 1 4.55 -14.90 21.21 o -4 10 1 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