#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/02/2200217.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200217_Fobs loop_ _publ_author_name 'Liu, He' 'Du, Miao' 'Ge, Xiao-Jing' 'Bu, Xian-He' 'Yang, Ming' _publ_section_title ; A novel heptacoordinated cobalt(II) complex of 6,7-dicyanodipyridoquinoxaline (dcdpq): [Co(NO~3~)~2~(CH~3~CN)(dcdpq)] ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m100 _journal_page_last m102 _journal_volume 57 _journal_year 2001 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 115.154 _cell_angle_gamma 90.000 _cell_length_a 8.3141 _cell_length_b 14.6625 _cell_length_c 9.0670 _exptl_crystal_F_000 510.00 _reflns_d_resolution_high 0.7990 _[local]_cod_data_source_file om6006Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' OA1115 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -18 0 122.71 139.20 10.02 o 1 -18 0 6.02 4.68 4.01 o 1 -17 0 80.50 85.91 5.57 o 2 -17 0 27.96 32.86 6.55 o 3 -17 0 32.75 35.00 6.28 o 0 -16 0 151.02 159.51 9.35 o 1 -16 0 39.43 51.08 9.55 o 2 -16 0 104.33 112.08 8.68 o 3 -16 0 53.65 59.58 6.95 o 4 -16 0 1.67 0.53 4.01 o 1 -15 0 300.80 312.13 10.09 o 2 -15 0 26.28 32.86 5.88 o 3 -15 0 127.82 129.18 8.95 o 4 -15 0 90.13 82.43 7.61 o 5 -15 0 0.93 0.94 3.87 o 0 -14 0 389.43 393.30 12.69 o 1 -14 0 115.51 119.65 5.46 o 2 -14 0 176.16 179.13 13.63 o 3 -14 0 191.96 194.64 10.42 o 4 -14 0 14.13 15.10 4.54 o 5 -14 0 125.83 121.03 8.82 o 6 -14 0 27.26 33.43 4.49 o 1 -13 0 248.31 255.65 8.48 o 2 -13 0 216.50 225.50 6.71 o 3 -13 0 392.56 395.03 13.89 o 4 -13 0 229.70 231.12 11.22 o 5 -13 0 3.04 -0.40 3.34 o 6 -13 0 18.74 19.92 3.54 o 0 -12 0 694.65 686.93 10.29 o 1 -12 0 61.13 68.45 2.69 o 2 -12 0 871.80 907.08 32.73 o 3 -12 0 252.27 244.61 10.69 o 4 -12 0 31.94 33.13 5.61 o 5 -12 0 246.92 251.29 11.62 o 6 -12 0 88.21 90.70 5.52 o 7 -12 0 2.83 2.77 2.79 o 1 -11 0 804.26 815.97 8.95 o 2 -11 0 725.87 703.22 8.27 o 3 -11 0 51.22 55.44 3.87 o 4 -11 0 77.16 84.30 4.54 o 5 -11 0 95.44 95.25 7.48 o 6 -11 0 213.22 230.45 7.93 o 7 -11 0 65.94 69.51 5.09 o 0 -10 0 858.43 866.35 10.55 o 1 -10 0 135.18 126.69 3.48 o 2 -10 0 656.78 654.66 7.64 o 3 -10 0 474.11 473.32 13.43 o 4 -10 0 53.97 53.17 3.74 o 5 -10 0 199.59 204.66 6.68 o 6 -10 0 60.20 58.33 3.59 o 7 -10 0 76.12 73.98 5.04 o 1 -9 0 1353.21 1368.47 10.63 o 2 -9 0 263.01 264.63 14.03 o 3 -9 0 223.11 229.57 4.33 o 4 -9 0 379.71 371.92 8.02 o 5 -9 0 9.46 9.75 2.40 o 6 -9 0 181.27 185.07 5.46 o 7 -9 0 184.55 184.30 9.42 o 8 -9 0 10.03 12.85 3.21 o 0 -8 0 2009.14 2110.76 17.77 o 1 -8 0 32.98 31.28 1.88 o 2 -8 0 264.87 256.72 4.27 o 3 -8 0 420.34 413.25 17.50 o 4 -8 0 80.50 92.45 4.41 o 5 -8 0 310.89 319.29 7.88 o 6 -8 0 68.05 67.18 3.56 o 7 -8 0 135.97 144.41 6.08 o 8 -8 0 68.31 66.40 6.48 o 1 -7 0 1784.54 1814.05 13.89 o 2 -7 0 1670.90 1730.02 14.43 o 3 -7 0 124.34 119.30 4.27 o 4 -7 0 91.90 93.25 4.27 o 5 -7 0 17.39 18.97 2.81 o 6 -7 0 275.62 274.00 14.76 o 7 -7 0 185.89 187.15 11.09 o 8 -7 0 53.17 48.73 9.28 o 0 -6 0 463.23 488.01 8.42 o 1 -6 0 983.12 1013.17 9.35 o 2 -6 0 1475.64 1460.17 12.42 o 3 -6 0 343.36 343.87 6.41 o 4 -6 0 193.49 195.45 5.61 o 5 -6 0 166.28 161.25 5.61 o 6 -6 0 236.32 232.54 5.64 o 7 -6 0 46.40 48.89 3.91 o 8 -6 0 115.42 117.27 5.90 o 1 -5 0 418.58 403.58 9.22 o 2 -5 0 400.20 405.85 6.15 o 3 -5 0 2718.24 2785.94 19.37 o 4 -5 0 925.20 947.71 11.36 o 5 -5 0 21.13 20.88 2.10 o 6 -5 0 66.73 65.30 3.47 o 7 -5 0 379.91 409.63 9.78 o 8 -5 0 57.73 58.50 4.43 o 9 -5 0 38.88 46.33 9.28 o 1 -4 0 56.83 52.23 2.14 o 2 -4 0 4113.45 4262.67 23.38 o 3 -4 0 362.41 312.21 5.74 o 4 -4 0 7.84 4.41 1.60 o 5 -4 0 438.09 447.41 18.30 o 6 -4 0 143.61 142.21 4.33 o 7 -4 0 175.34 167.02 6.35 o 8 -4 0 118.07 118.29 5.61 o 9 -4 0 4.50 -0.42 2.87 o 1 -3 0 5901.59 5978.67 28.72 o 2 -3 0 2153.04 2201.74 19.64 o 3 -3 0 1687.28 1716.66 13.36 o 4 -3 0 678.27 631.83 6.92 o 5 -3 0 251.84 247.08 9.89 o 6 -3 0 159.74 166.58 5.08 o 7 -3 0 176.00 174.29 6.25 o 8 -3 0 18.54 19.51 5.14 o 9 -3 0 99.51 113.69 9.22 o 1 -2 0 1829.05 1711.72 14.70 o 2 -2 0 2121.40 2046.51 13.09 o 3 -2 0 1347.11 1351.29 11.22 o 4 -2 0 372.58 401.36 5.34 o 5 -2 0 1969.94 1919.02 17.77 o 6 -2 0 101.93 111.55 5.14 o 7 -2 0 55.94 63.80 5.21 o 8 -2 0 287.40 294.67 8.41 o 9 -2 0 4.45 0.94 3.87 o 2 -1 0 380.00 384.08 4.68 o 3 -1 0 36.23 41.46 4.94 o 4 -1 0 1746.98 1844.25 39.41 o 5 -1 0 487.52 521.22 6.50 o 6 -1 0 376.74 387.12 8.08 o 7 -1 0 66.04 64.34 4.14 o 8 -1 0 6.60 10.15 4.27 o 9 -1 0 143.99 159.91 10.55 o 1 0 0 349.53 350.01 4.54 o 2 0 0 488.79 520.73 14.16 o 3 0 0 6.24 7.88 0.96 o 4 0 0 64.16 67.57 2.31 o 5 0 0 88.91 70.87 3.21 o 6 0 0 126.43 118.57 4.78 o 7 0 0 161.82 159.74 5.81 o 8 0 0 125.48 133.73 9.22 o 9 0 0 53.23 62.52 7.48 o 1 1 0 2193.63 2321.29 14.02 o 2 1 0 437.05 449.56 12.49 o 3 1 0 59.92 66.36 2.47 o 4 1 0 1572.65 1691.00 43.35 o 5 1 0 473.73 504.33 8.02 o 6 1 0 400.61 404.30 7.96 o 7 1 0 74.19 78.69 7.21 o 8 1 0 7.31 12.56 4.54 o 9 1 0 127.14 133.06 9.89 o 0 2 0 1369.14 1372.00 12.29 o 1 2 0 1722.22 1639.31 23.11 o 2 2 0 1956.82 1908.24 13.09 o 3 2 0 1330.82 1339.40 42.01 o 4 2 0 394.28 401.51 10.22 o 5 2 0 1934.97 1930.05 44.22 o 6 2 0 120.13 126.83 5.54 o 7 2 0 52.72 57.98 6.41 o 8 2 0 320.55 345.20 14.16 o 9 2 0 4.18 1.20 4.01 o 1 3 0 5579.66 5722.31 39.28 o 2 3 0 2354.18 2321.87 18.17 o 3 3 0 1656.98 1664.80 14.16 o 4 3 0 554.31 542.90 6.14 o 5 3 0 237.25 247.12 5.63 o 6 3 0 205.73 205.60 9.89 o 7 3 0 167.96 176.61 9.89 o 8 3 0 15.88 11.76 5.08 o 9 3 0 106.43 131.19 9.75 o 0 4 0 1470.91 1639.45 14.96 o 1 4 0 53.53 51.30 1.75 o 2 4 0 4173.36 4199.65 22.49 o 3 4 0 422.52 359.80 13.16 o 4 4 0 5.46 4.85 2.94 o 5 4 0 462.44 454.48 11.69 o 6 4 0 128.99 144.01 8.82 o 7 4 0 160.71 170.46 10.02 o 8 4 0 123.02 136.26 9.22 o 9 4 0 4.05 8.02 4.54 o 1 5 0 381.91 431.47 24.51 o 2 5 0 338.03 353.47 22.64 o 3 5 0 2716.19 2759.87 17.29 o 4 5 0 972.30 994.66 9.62 o 5 5 0 19.47 12.56 3.61 o 6 5 0 48.66 51.43 5.74 o 8 5 0 57.98 56.78 6.68 o 9 5 0 35.99 43.42 7.21 o 0 6 0 562.34 542.12 8.55 o 1 6 0 912.59 925.89 46.96 o 2 6 0 1548.80 1521.42 11.18 o 3 6 0 419.00 409.87 6.55 o 4 6 0 181.36 167.53 7.35 o 5 6 0 199.48 187.30 5.88 o 6 6 0 236.13 210.41 9.89 o 7 6 0 55.76 57.04 6.28 o 8 6 0 109.84 114.62 8.95 o 1 7 0 1798.96 1820.87 20.64 o 2 7 0 1629.31 1667.41 23.91 o 3 7 0 106.63 103.29 3.05 o 4 7 0 113.61 107.54 6.15 o 5 7 0 20.45 29.66 4.68 o 0 8 0 2049.48 2182.90 22.31 o 1 8 0 27.89 26.42 2.05 o 2 8 0 271.77 263.71 4.79 o 3 8 0 425.57 435.51 11.76 o 4 8 0 76.11 84.83 5.88 o 5 8 0 377.07 378.60 12.56 o 1 9 0 1376.22 1382.29 14.03 o 2 9 0 301.81 308.32 5.51 o 3 9 0 212.54 221.23 8.82 o 4 9 0 353.53 367.25 11.76 o 5 9 0 11.40 17.37 4.27 o 0 10 0 885.60 884.12 14.56 o 1 10 0 156.51 156.46 10.55 o 2 10 0 635.92 647.79 14.29 o 3 10 0 504.84 510.72 13.49 o 4 10 0 57.75 58.25 5.34 o 5 10 0 179.23 164.45 8.95 o 1 11 0 760.57 778.65 24.71 o 2 11 0 773.77 789.67 16.57 o 3 11 0 35.78 38.34 4.68 o 4 11 0 102.98 98.06 6.81 o 5 11 0 90.85 96.19 7.35 o 0 12 0 658.59 658.48 13.76 o 1 12 0 75.09 90.98 5.88 o 2 12 0 865.83 884.65 17.90 o 3 12 0 193.98 205.33 9.62 o 4 12 0 29.17 30.99 5.21 o 5 12 0 237.91 236.33 11.36 o 1 13 0 235.11 239.53 9.35 o 2 13 0 198.23 207.07 9.08 o 3 13 0 431.65 430.57 13.89 o 4 13 0 241.41 228.84 10.95 o 5 13 0 3.17 2.27 3.47 o 1 14 0 120.48 142.41 7.75 o 2 14 0 153.27 150.29 8.42 o 3 14 0 185.11 187.96 9.75 o 4 14 0 16.05 9.22 3.87 o 5 14 0 127.32 137.60 9.75 o 1 15 0 270.97 268.25 10.55 o 2 15 0 30.31 26.72 4.94 o 3 15 0 132.56 120.90 8.02 o 4 15 0 103.40 85.63 7.48 o 5 15 0 1.02 4.14 3.47 o 2 16 0 107.88 106.74 7.75 o 3 16 0 66.28 68.40 6.68 o 4 16 0 1.00 -3.47 3.47 o 3 17 0 27.82 20.04 5.21 o -2 -18 1 47.19 51.83 7.48 o -1 -18 1 69.28 74.00 5.48 o 0 -18 1 180.26 200.09 8.02 o 1 -18 1 7.55 8.15 4.41 o -3 -17 1 53.14 60.55 4.77 o -2 -17 1 11.86 9.08 4.14 o -1 -17 1 97.23 102.45 5.80 o 0 -17 1 0.92 2.26 2.74 o 1 -17 1 122.36 148.02 9.89 o 2 -17 1 51.20 55.71 7.75 o 3 -17 1 72.89 86.84 8.28 o -4 -16 1 10.91 12.36 3.17 o -3 -16 1 101.35 112.22 8.82 o -2 -16 1 104.29 114.14 5.70 o -1 -16 1 129.29 133.19 6.09 o 0 -16 1 217.74 224.96 7.74 o 1 -16 1 18.61 20.17 4.94 o 2 -16 1 0.41 -0.27 3.47 o 3 -16 1 89.44 90.71 8.02 o 4 -16 1 3.39 7.08 4.41 o -5 -15 1 1.29 -1.13 2.68 o -4 -15 1 65.30 76.43 5.13 o -3 -15 1 122.65 126.11 8.82 o -2 -15 1 299.72 302.99 9.28 o -1 -15 1 294.35 307.74 8.59 o 0 -15 1 9.43 9.89 2.74 o 1 -15 1 311.55 325.72 8.65 o 2 -15 1 51.73 51.57 6.15 o 3 -15 1 36.10 31.80 5.74 o 4 -15 1 110.43 109.41 8.68 o -6 -14 1 14.43 12.89 3.30 o -5 -14 1 191.32 218.35 14.76 o -4 -14 1 26.12 23.00 3.26 o -3 -14 1 15.10 7.48 3.47 o -2 -14 1 178.95 189.50 5.34 o -1 -14 1 178.88 195.17 11.56 o 0 -14 1 169.39 178.15 5.14 o 1 -14 1 119.42 115.89 10.09 o 2 -14 1 254.82 245.81 11.49 o 3 -14 1 97.92 90.98 7.61 o 4 -14 1 4.55 1.34 3.07 o 5 -14 1 65.01 60.78 8.02 o -6 -13 1 65.51 67.24 4.98 o -5 -13 1 17.60 16.16 3.11 o -3 -13 1 20.49 18.84 4.81 o -2 -13 1 118.17 128.53 5.42 o -1 -13 1 353.62 347.44 14.23 o 0 -13 1 27.42 28.34 2.57 o 1 -13 1 101.79 101.67 5.14 o 2 -13 1 39.63 37.67 3.47 o 3 -13 1 71.93 67.20 4.27 o 4 -13 1 344.61 361.23 14.03 o 5 -13 1 24.66 25.38 5.34 o 6 -13 1 28.66 23.38 5.74 o -7 -12 1 24.43 26.02 6.88 o -6 -12 1 206.78 197.37 7.60 o -5 -12 1 290.80 296.50 8.76 o -4 -12 1 142.83 134.93 8.55 o -3 -12 1 424.54 422.29 13.76 o -2 -12 1 844.01 899.48 19.24 o -1 -12 1 23.17 25.16 3.61 o 0 -12 1 311.02 330.69 6.25 o 1 -12 1 31.31 37.26 2.77 o 2 -12 1 61.50 68.63 3.67 o 3 -12 1 74.08 74.14 4.41 o 4 -12 1 101.97 101.80 5.34 o 5 -12 1 182.08 187.03 7.08 o 6 -12 1 46.44 41.15 6.41 o -7 -11 1 41.87 41.40 4.33 o -6 -11 1 15.26 15.48 3.21 o -5 -11 1 6.16 4.34 3.87 o -4 -11 1 230.48 243.81 10.42 o -3 -11 1 358.63 364.84 12.16 o -2 -11 1 242.82 254.36 10.15 o -1 -11 1 254.69 239.84 4.63 o 0 -11 1 62.48 54.21 9.95 o 1 -11 1 212.57 225.57 4.96 o 2 -11 1 342.63 342.97 5.93 o 3 -11 1 419.36 415.07 8.95 o 4 -11 1 354.17 360.30 8.82 o 5 -11 1 22.51 22.71 3.47 o 6 -11 1 48.94 51.83 4.41 o 7 -11 1 22.29 21.57 3.73 o -8 -10 1 43.23 38.07 4.53 o -7 -10 1 150.45 152.01 6.60 o -6 -10 1 31.50 28.46 3.64 o -5 -10 1 269.31 249.30 8.35 o -4 -10 1 28.30 23.51 4.27 o -3 -10 1 551.61 547.33 8.68 o -2 -10 1 882.52 866.21 10.29 o -1 -10 1 151.88 153.53 3.64 o 0 -10 1 642.49 681.32 9.69 o 1 -10 1 95.70 97.26 5.14 o 2 -10 1 204.82 214.00 7.35 o 3 -10 1 1379.91 1322.43 21.24 o 4 -10 1 124.81 128.78 5.48 o 5 -10 1 234.24 239.26 7.48 o 6 -10 1 28.41 27.79 3.74 o 7 -10 1 27.07 22.00 2.91 o -8 -9 1 42.12 44.00 8.22 o -7 -9 1 34.50 34.86 4.11 o -6 -9 1 111.91 112.04 4.32 o -5 -9 1 153.56 149.67 4.60 o -4 -9 1 116.57 123.04 4.81 o -3 -9 1 348.51 328.24 6.55 o -2 -9 1 384.94 396.77 6.55 o -1 -9 1 3300.28 3427.62 54.77 o 0 -9 1 2.91 3.41 1.37 o 1 -9 1 217.78 209.00 12.89 o 2 -9 1 242.06 237.13 4.88 o 3 -9 1 212.13 227.24 6.55 o 4 -9 1 265.55 247.15 6.95 o 5 -9 1 98.56 94.98 5.08 o 6 -9 1 235.19 262.78 8.15 o 7 -9 1 79.28 84.43 9.15 o -8 -8 1 139.62 143.49 6.37 o -7 -8 1 184.13 188.95 5.68 o -6 -8 1 96.44 92.32 6.28 o -5 -8 1 163.75 171.85 8.28 o -4 -8 1 15.55 15.22 1.83 o -3 -8 1 434.96 428.16 7.21 o -2 -8 1 1427.63 1522.69 12.96 o -1 -8 1 951.68 973.22 10.15 o 0 -8 1 1104.56 1081.68 24.51 o 1 -8 1 221.88 234.22 4.94 o 2 -8 1 190.71 174.03 3.67 o 3 -8 1 907.62 873.70 11.62 o 4 -8 1 342.83 341.73 7.88 o 5 -8 1 379.22 384.61 8.82 o 6 -8 1 57.47 64.12 4.68 o 7 -8 1 168.91 189.82 9.02 o 8 -8 1 56.13 68.75 12.62 o -9 -7 1 135.04 144.78 7.41 o -8 -7 1 1.06 1.34 2.46 o -7 -7 1 63.55 80.28 9.02 o -6 -7 1 652.25 627.80 28.79 o -5 -7 1 139.83 134.48 4.27 o -4 -7 1 264.22 281.44 6.15 o -3 -7 1 503.63 496.16 7.35 o -2 -7 1 907.68 897.61 8.95 o -1 -7 1 689.93 596.62 6.68 o 0 -7 1 0.50 0.46 1.54 o 1 -7 1 429.74 394.37 9.55 o 2 -7 1 472.47 456.34 6.18 o 3 -7 1 140.60 139.34 4.81 o 4 -7 1 468.25 433.78 8.55 o 5 -7 1 216.88 207.74 6.68 o 6 -7 1 349.53 346.94 8.68 o 7 -7 1 84.41 85.42 11.76 o 8 -7 1 27.05 25.68 7.95 o -9 -6 1 15.01 13.87 5.88 o -8 -6 1 127.82 138.98 13.56 o -7 -6 1 84.60 84.08 4.68 o -6 -6 1 146.74 145.30 7.21 o -5 -6 1 376.35 349.09 6.88 o -4 -6 1 520.49 558.36 7.28 o -3 -6 1 1413.48 1425.97 12.56 o -2 -6 1 1454.81 1531.77 11.89 o -1 -6 1 734.37 762.55 7.21 o 0 -6 1 961.75 904.36 17.70 o 1 -6 1 104.54 108.25 5.54 o 2 -6 1 3343.63 3335.31 25.85 o 3 -6 1 452.32 472.52 7.88 o 4 -6 1 206.09 216.82 6.15 o 5 -6 1 355.75 358.03 8.02 o 6 -6 1 152.25 152.24 4.78 o 7 -6 1 21.30 32.04 8.95 o 8 -6 1 116.09 130.37 6.39 o -9 -5 1 41.68 53.83 9.62 o -8 -5 1 14.81 15.43 4.41 o -7 -5 1 134.07 131.88 13.16 o -6 -5 1 119.61 125.04 4.24 o -5 -5 1 274.82 274.27 7.01 o -4 -5 1 2980.29 2921.88 28.05 o -3 -5 1 278.98 254.22 4.68 o -2 -5 1 1173.81 1132.20 9.35 o -1 -5 1 18.65 21.51 2.67 o 0 -5 1 165.64 169.88 4.34 o 1 -5 1 934.40 863.00 7.73 o 2 -5 1 3210.47 3348.69 31.06 o 3 -5 1 381.68 364.57 6.95 o 4 -5 1 826.38 839.23 11.49 o 5 -5 1 32.65 35.40 3.47 o 6 -5 1 602.69 582.38 8.65 o 7 -5 1 171.32 169.02 6.64 o 8 -5 1 44.36 50.37 4.33 o -9 -4 1 2.02 5.46 7.01 o -8 -4 1 337.08 344.98 9.21 o -7 -4 1 16.06 11.47 3.41 o -6 -4 1 79.88 82.61 5.08 o -5 -4 1 500.63 492.19 11.09 o -4 -4 1 435.82 410.36 5.66 o -3 -4 1 2711.84 2806.62 16.10 o -2 -4 1 824.67 807.17 7.48 o -1 -4 1 2484.21 2647.40 22.58 o 0 -4 1 826.10 815.63 16.23 o 1 -4 1 5445.32 5761.34 52.10 o 2 -4 1 919.56 876.50 13.63 o 3 -4 1 1905.39 1876.98 15.50 o 4 -4 1 62.02 61.32 3.47 o 5 -4 1 372.53 387.28 8.02 o 6 -4 1 315.15 309.93 8.01 o 7 -4 1 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