#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180922 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/02/2200251.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200251_Fobs loop_ _publ_author_name 'Bond, Andrew D.' 'Jones, William' _publ_section_title ; Bis[3-hydroxy-4-methyl-2(3H)-thiazolethiolato-S^2^,O]bis(methanol-O)cobalt(II) ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m140 _journal_page_last m142 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.349 _cell_angle_gamma 90.000 _cell_length_a 5.0414 _cell_length_b 18.8777 _cell_length_c 8.6814 _exptl_crystal_F_000 426.00 _reflns_d_resolution_high 0.8401 _cod_data_source_file ya6012Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' wj9917 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 147.32 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6430.07 5632.19 187.21 o 2 0 0 1111.47 1159.22 35.98 o 3 0 0 204.19 195.49 23.28 o 4 0 0 999.25 1085.83 82.25 o 5 0 0 364.07 344.28 42.13 o 1 1 0 1917.95 1813.21 43.37 o 2 1 0 162.00 144.19 14.92 o 3 1 0 1523.70 1568.94 43.12 o 4 1 0 556.81 575.15 45.62 o 5 1 0 228.66 241.99 30.73 o 1 2 0 247.71 252.34 6.87 o 2 2 0 834.50 899.48 17.14 o 3 2 0 1588.14 1585.92 40.33 o 4 2 0 3235.16 3536.23 141.30 o 5 2 0 540.90 500.60 51.05 o 1 3 0 473.94 504.66 15.08 o 2 3 0 1283.45 1306.54 25.25 o 3 3 0 1687.99 1906.90 38.34 o 4 3 0 47.07 56.29 6.90 o 5 3 0 338.63 345.64 32.20 o 0 4 0 454.02 493.65 31.84 o 1 4 0 3440.37 3221.26 97.08 o 2 4 0 4222.79 4192.26 85.05 o 3 4 0 2253.52 2361.65 47.09 o 4 4 0 57.73 72.84 8.57 o 5 4 0 95.40 81.43 50.91 o 1 5 0 9474.53 9335.08 245.74 o 2 5 0 1083.16 1013.68 18.61 o 3 5 0 208.31 222.54 6.47 o 4 5 0 1.74 3.24 2.82 o 5 5 0 29.51 24.13 24.13 o 0 6 0 107.12 100.24 11.42 o 1 6 0 186.26 181.47 7.78 o 2 6 0 2186.08 2281.46 54.12 o 3 6 0 1506.75 1538.49 32.56 o 4 6 0 1189.44 1219.20 39.55 o 5 6 0 406.94 396.55 46.69 o 1 7 0 2059.49 2073.41 65.40 o 2 7 0 284.00 307.44 13.28 o 3 7 0 1509.02 1474.09 40.55 o 4 7 0 326.39 314.15 13.42 o 5 7 0 2.47 -27.13 27.13 o 0 8 0 16969.16 17243.56 992.44 o 1 8 0 4596.53 4443.40 125.95 o 2 8 0 320.82 312.72 11.99 o 3 8 0 33.02 28.42 5.57 o 4 8 0 127.22 97.24 9.00 o 5 8 0 301.60 254.32 46.98 o 1 9 0 848.42 895.76 24.85 o 2 9 0 89.02 81.54 6.85 o 3 9 0 242.31 227.33 10.28 o 4 9 0 482.60 465.52 19.56 o 5 9 0 187.03 184.06 43.12 o 0 10 0 14.82 76.82 18.56 o 1 10 0 114.04 105.67 7.00 o 2 10 0 86.70 75.54 7.28 o 3 10 0 635.21 616.31 20.71 o 4 10 0 598.27 577.61 21.85 o 5 10 0 725.21 660.29 75.68 o 1 11 0 881.84 855.49 24.28 o 2 11 0 1355.62 1371.42 39.13 o 3 11 0 537.46 493.65 18.42 o 4 11 0 105.20 108.81 11.85 o 5 11 0 26.92 38.41 34.13 o 0 12 0 34.30 22.70 15.42 o 1 12 0 1850.96 1846.08 48.69 o 2 12 0 4846.39 5133.26 162.50 o 3 12 0 680.81 648.73 24.99 o 4 12 0 3.29 4.28 10.00 o 5 12 0 2.53 29.99 34.41 o 1 13 0 303.55 286.59 14.14 o 2 13 0 495.57 436.67 22.13 o 3 13 0 39.40 28.42 10.00 o 4 13 0 4.41 10.14 12.99 o 0 14 0 100.71 114.38 21.85 o 1 14 0 76.72 75.54 8.57 o 2 14 0 1939.88 1888.49 75.54 o 3 14 0 466.08 441.38 23.85 o 4 14 0 121.19 104.10 14.71 o 1 15 0 184.27 152.65 11.14 o 2 15 0 20.66 17.28 10.00 o 3 15 0 6.47 14.28 10.00 o 4 15 0 280.32 261.60 24.42 o 0 16 0 1544.83 1800.81 99.39 o 1 16 0 1551.02 1637.88 67.26 o 2 16 0 28.76 8.43 11.42 o 3 16 0 12.79 25.70 11.42 o 4 16 0 85.81 64.12 18.71 o 1 17 0 28.59 28.42 10.00 o 2 17 0 97.65 85.68 11.14 o 3 17 0 11.18 5.71 12.71 o 0 18 0 790.21 767.25 66.97 o 1 18 0 105.20 92.82 13.14 o 2 18 0 8.66 1.43 10.14 o 3 18 0 159.47 164.07 27.13 o 1 19 0 349.55 390.55 32.84 o 2 19 0 222.35 295.59 29.84 o 3 19 0 4.44 48.41 25.70 o 0 20 0 97.77 138.08 34.70 o 1 20 0 333.51 351.28 36.84 o 2 20 0 900.22 1000.43 86.11 o 1 21 0 11.13 -2.86 25.85 o 2 21 0 102.13 104.10 30.13 o 0 22 0 59.61 80.25 29.84 o 1 22 0 24.97 35.70 28.42 o -5 1 1 927.40 875.49 89.39 o -4 1 1 1284.17 1362.86 31.39 o -3 1 1 384.53 380.28 9.39 o -2 1 1 34.51 34.58 4.21 o -1 1 1 5900.85 5906.50 128.15 o 1 1 1 5244.46 4856.59 117.58 o 2 1 1 14.00 14.25 12.21 o 3 1 1 160.68 107.34 22.99 o 4 1 1 1309.40 1387.80 65.34 o 5 1 1 330.55 298.04 31.73 o -5 2 1 164.60 141.65 29.70 o -4 2 1 987.04 1017.14 24.64 o -3 2 1 6.21 9.89 6.43 o -2 2 1 883.45 900.12 17.42 o -1 2 1 46.46 53.42 3.13 o 1 2 1 1027.41 1024.11 25.48 o 2 2 1 505.80 479.57 14.71 o 3 2 1 500.21 514.92 24.42 o 4 2 1 1147.11 1126.78 51.09 o 5 2 1 0.26 2.27 17.92 o -5 3 1 8.04 17.28 22.99 o -4 3 1 923.47 939.19 24.13 o -3 3 1 1970.19 1990.57 37.96 o -2 3 1 1149.73 1136.44 22.45 o -1 3 1 1300.26 1299.29 27.89 o 0 3 1 868.65 811.98 24.33 o 1 3 1 1998.94 1868.79 58.64 o 2 3 1 1627.30 1569.27 33.08 o 3 3 1 3238.10 3307.89 72.35 o 4 3 1 364.59 379.51 48.69 o 5 3 1 232.55 218.61 38.27 o -5 4 1 25.44 45.69 27.13 o -4 4 1 16.20 22.90 5.01 o -3 4 1 252.26 260.34 7.87 o -2 4 1 115.30 125.85 10.21 o -1 4 1 149.60 170.47 6.43 o 0 4 1 2011.61 1941.65 61.11 o 1 4 1 10.32 16.56 7.14 o 2 4 1 1078.32 1174.48 57.55 o 3 4 1 7.09 8.37 1.28 o 4 4 1 66.93 64.76 8.71 o 5 4 1 6.77 12.85 21.23 o -5 5 1 45.59 4.28 25.70 o -4 5 1 452.21 432.96 15.17 o -3 5 1 5728.26 5982.84 108.06 o -2 5 1 2449.08 2411.80 44.54 o -1 5 1 990.64 981.92 27.89 o 0 5 1 1255.95 1209.33 41.02 o 1 5 1 913.93 838.34 23.03 o 2 5 1 2948.01 2979.40 78.52 o 3 5 1 837.97 833.81 28.63 o 4 5 1 178.07 173.95 11.78 o 5 5 1 42.63 31.44 28.49 o -5 6 1 0.06 -17.28 25.70 o -4 6 1 66.84 70.15 8.78 o -3 6 1 189.00 175.50 7.82 o -2 6 1 316.03 360.53 12.14 o -1 6 1 971.41 990.19 25.09 o 0 6 1 28.37 15.88 6.93 o 1 6 1 2219.66 2176.48 54.15 o 2 6 1 1179.67 1206.45 31.47 o 3 6 1 344.38 361.20 9.62 o 4 6 1 913.10 947.87 35.89 o 5 6 1 1.10 3.84 21.30 o -5 7 1 971.14 1010.00 110.52 o -4 7 1 224.17 224.17 10.33 o -3 7 1 208.06 216.05 10.00 o -2 7 1 609.11 571.08 14.56 o -1 7 1 1948.91 1986.37 49.83 o 0 7 1 4859.42 4788.61 111.75 o 1 7 1 2792.75 2832.96 61.47 o 2 7 1 194.64 208.96 12.85 o 3 7 1 476.93 493.28 16.64 o 4 7 1 1254.30 1296.64 33.83 o 5 7 1 359.08 379.81 39.98 o -5 8 1 2.77 -22.99 22.99 o -4 8 1 59.06 45.69 7.14 o -3 8 1 67.34 69.78 30.84 o -2 8 1 81.75 84.25 7.00 o -1 8 1 505.00 544.59 14.00 o 0 8 1 194.82 190.71 15.07 o 1 8 1 134.48 125.95 6.85 o 2 8 1 138.34 163.07 10.78 o 3 8 1 237.19 244.91 11.01 o 4 8 1 33.39 24.11 5.50 o 5 8 1 88.16 64.12 38.70 o -5 9 1 547.63 487.08 54.98 o -4 9 1 326.88 323.58 16.28 o -3 9 1 5.40 7.69 9.21 o -2 9 1 769.34 774.93 18.65 o -1 9 1 4048.68 4142.46 88.17 o 0 9 1 4421.38 4414.40 108.04 o 1 9 1 1348.20 1310.59 30.13 o 2 9 1 31.58 32.99 7.00 o 3 9 1 36.72 38.41 5.57 o 4 9 1 660.42 633.45 22.85 o 5 9 1 792.47 807.52 83.82 o -5 10 1 77.93 59.97 29.84 o -4 10 1 776.96 732.12 30.70 o -3 10 1 5.83 3.20 8.43 o -2 10 1 137.88 126.15 7.97 o -1 10 1 88.09 79.05 19.42 o 0 10 1 864.19 950.13 26.99 o 1 10 1 3.25 2.86 5.71 o 2 10 1 233.99 227.33 11.42 o 3 10 1 64.70 57.12 6.85 o 4 10 1 217.11 195.49 11.57 o 5 10 1 1.84 15.71 31.42 o -5 11 1 89.63 80.25 33.13 o -4 11 1 172.02 178.92 13.14 o -3 11 1 471.54 467.40 15.46 o -2 11 1 960.70 951.05 21.53 o -1 11 1 239.79 287.89 27.77 o 0 11 1 6.44 5.05 5.00 o 1 11 1 1947.04 2042.56 51.26 o 2 11 1 1711.83 1823.37 38.70 o 3 11 1 1367.94 1433.68 54.41 o 4 11 1 422.48 414.82 23.13 o 5 11 1 299.19 295.59 55.83 o -5 12 1 24.36 28.42 42.70 o -4 12 1 28.56 25.70 11.42 o -3 12 1 76.76 67.26 8.71 o -2 12 1 82.75 79.82 7.01 o -1 12 1 6.33 9.45 5.25 o 0 12 1 923.89 955.45 23.42 o 1 12 1 150.43 121.81 8.28 o 2 12 1 1001.72 1019.57 31.42 o 3 12 1 50.35 42.70 9.85 o 4 12 1 79.47 75.54 13.14 o -4 13 1 107.67 71.68 14.14 o -3 13 1 4432.54 4730.00 140.37 o -2 13 1 3198.81 3277.47 95.25 o -1 13 1 829.69 848.78 21.99 o 0 13 1 66.89 59.97 5.85 o 1 13 1 1182.35 1213.91 39.55 o 2 13 1 2188.04 2328.59 72.97 o 3 13 1 29.47 31.27 8.43 o 4 13 1 13.19 19.85 11.42 o -4 14 1 30.74 36.98 15.56 o -3 14 1 83.69 87.11 11.28 o -2 14 1 68.29 68.54 6.85 o -1 14 1 105.25 85.68 7.00 o 0 14 1 159.41 145.37 8.14 o 1 14 1 1427.94 1474.09 43.55 o 2 14 1 1880.32 2001.87 67.69 o 3 14 1 84.53 64.12 12.71 o 4 14 1 499.75 492.08 33.56 o -4 15 1 98.31 65.40 22.56 o -3 15 1 22.02 41.27 11.14 o -2 15 1 54.06 57.12 8.57 o -1 15 1 4.52 10.14 5.71 o 0 15 1 184.13 190.21 10.42 o 1 15 1 963.64 1000.43 38.27 o 2 15 1 756.60 781.95 29.56 o 3 15 1 501.77 455.81 22.56 o 4 15 1 266.70 279.02 34.13 o -4 16 1 68.41 65.40 20.13 o -3 16 1 19.69 22.70 12.99 o -2 16 1 122.03 120.09 11.57 o -1 16 1 69.88 58.26 5.71 o 0 16 1 1009.65 911.61 31.99 o 1 16 1 91.49 67.26 8.71 o 2 16 1 198.44 169.93 12.85 o 3 16 1 112.88 97.24 14.14 o 4 16 1 115.53 75.54 24.28 o -3 17 1 25.54 17.28 15.71 o -2 17 1 406.00 424.11 23.28 o -1 17 1 1999.37 2167.37 84.39 o 0 17 1 1804.48 2059.70 144.08 o 1 17 1 215.44 218.34 15.56 o 2 17 1 40.31 41.27 15.56 o 3 17 1 5.75 4.28 17.28 o -3 18 1 123.88 105.67 41.13 o -2 18 1 189.30 192.35 24.13 o -1 18 1 451.41 462.38 48.69 o 0 18 1 10.20 38.41 25.70 o 1 18 1 0.59 -8.43 18.42 o 2 18 1 4.87 2.86 20.13 o 3 18 1 92.21 78.82 20.13 o -3 19 1 41.67 -39.98 39.98 o -2 19 1 9.79 -10.14 29.99 o -1 19 1 191.36 148.08 33.13 o 0 19 1 34.77 -8.43 28.42 o 1 19 1 106.73 144.37 24.56 o 2 19 1 839.79 948.46 72.11 o 3 19 1 725.19 779.81 75.97 o -2 20 1 119.89 178.92 35.41 o -1 20 1 0.01 8.43 29.84 o 0 20 1 139.06 175.93 41.13 o 1 20 1 611.23 707.70 62.26 o 2 20 1 134.05 138.08 28.42 o -2 21 1 1052.54 868.78 122.52 o -1 21 1 573.53 552.48 81.68 o 0 21 1 74.17 44.27 31.13 o 1 21 1 18.86 34.27 25.70 o -1 22 1 4.49 -1.43 28.84 o 0 22 1 173.39 188.21 34.27 o -5 0 2 1231.13 1402.41 73.54 o -4 0 2 1041.16 1118.38 37.98 o -3 0 2 358.31 366.99 15.99 o -2 0 2 7803.51 7805.55 207.06 o -1 0 2 21702.80 20870.17 677.00 o 0 0 2 92.54 92.82 7.28 o 1 0 2 42.95 49.98 5.85 o 2 0 2 203.11 209.48 9.85 o 3 0 2 1.36 11.28 15.56 o 4 0 2 55.31 15.71 24.28 o 5 0 2 1011.26 957.88 112.24 o -5 1 2 169.12 171.85 11.56 o -4 1 2 361.53 346.52 12.38 o -3 1 2 4.86 -2.86 4.04 o -2 1 2 477.12 442.28 8.99 o -1 1 2 20941.42 19867.89 474.39 o 0 1 2 1085.53 1018.97 27.14 o 1 1 2 199.05 207.10 6.48 o 2 1 2 0.23 0.71 2.14 o 3 1 2 6.93 -5.94 19.21 o 4 1 2 67.56 40.30 17.14 o 5 1 2 261.89 252.58 63.69 o -5 2 2 209.95 234.19 16.14 o -4 2 2 78.62 74.04 6.16 o -3 2 2 38.73 38.69 4.14 o -2 2 2 946.45 883.44 17.47 o -1 2 2 1077.53 1041.54 28.13 o 0 2 2 2643.64 2537.63 75.23 o 1 2 2 3171.38 2923.27 77.57 o 2 2 2 9054.63 9368.61 226.65 o 3 2 2 1894.51 2015.75 72.26 o 4 2 2 320.84 329.32 46.27 o 5 2 2 311.54 323.87 36.74 o -5 3 2 166.86 158.36 13.28 o -4 3 2 1.53 -2.15 5.10 o -3 3 2 831.13 874.98 18.74 o -2 3 2 29.01 27.88 4.28 o -1 3 2 796.75 793.79 28.84 o 0 3 2 1112.84 1081.96 28.63 o 1 3 2 6730.67 6804.53 164.54 o 2 3 2 254.36 272.19 9.99 o 3 3 2 1945.08 2127.25 60.32 o 4 3 2 1201.74 1194.07 71.96 o 5 3 2 3.20 -16.94 22.93 o -5 4 2 30.23 25.71 8.29 o -4 4 2 1059.71 1177.17 46.77 o -3 4 2 5634.78 5826.82 95.29 o -2 4 2 7820.17 7504.98 147.58 o -1 4 2 351.19 370.42 10.50 o 0 4 2 582.17 664.64 18.25 o 1 4 2 2065.04 2013.72 59.79 o 2 4 2 1076.36 1073.26 36.86 o 3 4 2 224.52 208.98 5.26 o 4 4 2 434.49 407.09 27.41 o 5 4 2 53.55 9.53 23.80 o -5 5 2 2.67 2.86 10.10 o -4 5 2 82.61 79.98 6.65 o -3 5 2 105.82 112.27 7.14 o -2 5 2 24.55 22.63 4.39 o -1 5 2 659.88 595.71 15.51 o 0 5 2 2091.02 2220.13 63.21 o 1 5 2 67.30 55.18 4.90 o 2 5 2 26.84 40.32 5.00 o 3 5 2 393.51 350.20 23.92 o 4 5 2 913.55 918.73 40.55 o 5 5 2 48.48 12.96 47.69 o -5 6 2 58.26 65.34 24.35 o -4 6 2 191.84 198.24 9.95 o -3 6 2 661.32 711.84 16.90 o -2 6 2 358.67 342.16 10.35 o -1 6 2 207.36 224.14 7.85 o 0 6 2 3344.09 3226.79 85.54 o 1 6 2 9953.19 9914.66 259.83 o 2 6 2 2156.19 2102.10 62.17 o 3 6 2 1044.23 1090.25 31.20 o 4 6 2 306.08 336.61 17.39 o 5 6 2 136.88 105.55 27.53 o -5 7 2 241.26 157.36 30.27 o -4 7 2 213.24 208.96 19.21 o -3 7 2 3.04 4.70 6.26 o -2 7 2 1292.06 1288.17 27.76 o -1 7 2 2659.69 2673.04 85.96 o 0 7 2 163.83 162.76 8.47 o 1 7 2 123.57 137.91 11.07 o 2 7 2 246.67 275.97 10.71 o 3 7 2 26.74 18.46 6.43 o 4 7 2 30.44 36.69 13.49 o 5 7 2 42.39 22.12 28.56 o -5 8 2 731.26 715.84 72.83 o -4 8 2 899.01 923.04 33.54 o -3 8 2 581.91 618.54 16.66 o -2 8 2 843.47 913.81 29.77 o -1 8 2 3891.35 3896.70 85.01 o 0 8 2 3171.89 3089.04 77.03 o 1 8 2 262.97 286.05 11.26 o 2 8 2 426.32 385.96 24.78 o 3 8 2 91.31 82.46 7.28 o 4 8 2 369.95 387.37 14.22 o 5 8 2 1162.29 1317.88 137.30 o -5 9 2 59.24 50.59 17.14 o -4 9 2 254.02 242.26 14.48 o -3 9 2 3.46 0.71 10.15 o -2 9 2 673.99 686.94 16.63 o -1 9 2 3446.99 3723.84 82.73 o 0 9 2 257.52 257.70 20.49 o 1 9 2 0.37 -3.38 10.00 o 2 9 2 9.89 4.66 7.27 o 3 9 2 4.39 4.39 12.21 o 4 9 2 30.90 34.55 10.00 o 5 9 2 132.95 77.78 31.31 o -5 10 2 106.72 52.69 30.13 o -4 10 2 20.56 20.60 12.07 o -3 10 2 1.51 -6.38 6.38 o -2 10 2 7.61 3.24 11.35 o -1 10 2 295.71 274.84 14.02 o 0 10 2 3383.77 3391.67 96.54 o 1 10 2 2401.70 2536.68 74.16 o 2 10 2 2037.54 2178.69 65.87 o 3 10 2 721.97 715.13 28.56 o 4 10 2 791.99 799.93 37.35 o -4 11 2 1.86 8.59 10.23 o -3 11 2 391.82 370.87 13.49 o -2 11 2 101.17 89.75 17.99 o -1 11 2 0.57 0.53 7.91 o 0 11 2 2206.33 2262.73 63.03 o 1 11 2 2501.22 2630.30 59.29 o 2 11 2 0.76 2.86 10.00 o 3 11 2 454.20 439.81 22.13 o 4 11 2 270.39 265.32 20.99 o -4 12 2 986.81 950.62 38.51 o -3 12 2 3989.63 4188.56 115.16 o -2 12 2 1907.72 2023.23 60.22 o -1 12 2 21.36 5.37 9.75 o 0 12 2 41.47 45.90 10.01 o 1 12 2 435.30 426.46 16.47 o 2 12 2 188.20 170.93 13.85 o 3 12 2 304.35 290.45 16.71 o 4 12 2 111.01 97.24 18.56 o -4 13 2 13.88 15.19 12.92 o -3 13 2 1.66 0.28 20.06 o -2 13 2 218.01 215.96 15.42 o -1 13 2 31.24 15.03 9.75 o 0 13 2 78.04 65.40 10.76 o 1 13 2 339.71 331.72 16.56 o 2 13 2 144.23 101.10 15.99 o 3 13 2 128.17 101.10 11.42 o 4 13 2 466.08 452.67 41.84 o -4 14 2 196.50 166.07 18.56 o -3 14 2 405.45 351.81 23.42 o -2 14 2 338.44 310.54 21.63 o -1 14 2 106.50 129.14 12.71 o 0 14 2 447.89 426.42 19.18 o 1 14 2 2348.02 2443.11 93.39 o 2 14 2 720.19 701.70 39.98 o 3 14 2 858.83 794.66 42.55 o 4 14 2 274.95 299.59 33.99 o -4 15 2 6.37 21.28 17.14 o -3 15 2 135.45 121.56 14.35 o -2 15 2 232.28 214.43 17.77 o -1 15 2 609.13 610.17 27.63 o 0 15 2 298.27 268.04 22.49 o 1 15 2 544.22 467.23 29.42 o 2 15 2 538.89 392.12 34.41 o 3 15 2 139.89 111.10 14.28 o 4 15 2 60.29 62.97 26.99 o -4 16 2 69.24 39.84 28.56 o -3 16 2 56.77 61.12 20.13 o -2 16 2 178.71 219.31 43.55 o -1 16 2 1144.46 1256.43 71.76 o 0 16 2 1419.20 1453.81 74.97 o 1 16 2 21.62 47.27 15.56 o 2 16 2 8.72 12.85 17.14 o 3 16 2 30.69 31.27 18.56 o -3 17 2 2.61 -15.71 20.13 o -2 17 2 412.14 413.25 32.27 o -1 17 2 8.09 -8.43 21.28 o 0 17 2 0.08 2.86 22.99 o 1 17 2 4.80 0.00 14.28 o 2 17 2 17.74 8.43 24.13 o 3 17 2 5.90 0.00 14.28 o -3 18 2 56.56 11.28 31.27 o -2 18 2 27.10 27.13 20.13 o -1 18 2 993.88 1043.84 97.67 o 0 18 2 586.87 577.61 61.69 o 1 18 2 238.30 298.16 40.41 o 2 18 2 301.59 299.59 30.13 o 3 18 2 369.47 349.85 38.13 o -3 19 2 73.09 31.27 39.70 o 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