#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180922 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/02/2200275.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200275_Fobs loop_ _publ_author_name 'Baddeley, Thomas C.' 'Clow, Simon M.' 'Cox, Philip J.' 'McLaughlin, Anna M.' 'Wardell, James L.' _publ_section_title ; \a,\a-Trehalose octaacetate ethyl acetate solvate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o456 _journal_page_last o457 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1406 _cell_length_b 15.2215 _cell_length_c 17.8879 _exptl_crystal_F_000 1624.00 _reflns_d_resolution_high 0.7704 _cod_data_source_file bt6040Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' trehalose octaacetate - ethyl acetate complex in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 147.93 138.71 5.51 o 4 0 0 37930.51 36748.44 661.51 o 6 0 0 44.00 -1.54 11.66 o 8 0 0 7684.37 7989.02 166.54 o 10 0 0 1857.23 2004.55 63.95 o 12 0 0 6412.17 6880.77 184.52 o 14 0 0 295.45 245.87 40.49 o 16 0 0 716.17 588.85 63.35 o 18 0 0 0.56 -111.03 120.59 o 1 1 0 34839.44 509.30 5433.16 o 2 1 0 12.03 9.60 2.74 o 3 1 0 3349.18 3078.65 43.63 o 4 1 0 12414.96 12400.76 168.09 o 5 1 0 915.84 1010.85 18.48 o 6 1 0 415.92 455.39 13.04 o 7 1 0 6821.19 7122.32 99.19 o 8 1 0 980.16 900.69 31.57 o 9 1 0 1149.39 1164.97 28.06 o 10 1 0 174.83 222.80 15.12 o 11 1 0 2430.77 2281.61 52.52 o 12 1 0 246.65 202.28 17.73 o 13 1 0 462.56 454.36 27.85 o 14 1 0 0.35 0.77 22.80 o 15 1 0 15.32 43.99 35.47 o 16 1 0 6.71 -20.32 45.35 o 17 1 0 24.13 40.13 68.08 o 18 1 0 136.14 -15.41 79.59 o 1 2 0 2128.93 1910.57 34.40 o 2 2 0 9691.52 8940.41 139.10 o 3 2 0 3081.36 2970.33 44.80 o 4 2 0 135.51 126.61 8.39 o 5 2 0 2742.34 2655.52 41.25 o 6 2 0 24336.54 24763.70 319.12 o 7 2 0 166.61 176.14 10.60 o 8 2 0 39.72 45.45 9.66 o 9 2 0 2689.11 2560.64 61.22 o 10 2 0 4667.06 4973.92 92.56 o 11 2 0 989.83 978.26 29.06 o 12 2 0 3776.38 3957.18 88.90 o 13 2 0 526.27 494.98 26.79 o 14 2 0 52.14 50.28 22.29 o 15 2 0 30.49 43.16 42.79 o 16 2 0 133.21 127.07 41.07 o 17 2 0 67.92 66.83 52.38 o 18 2 0 416.31 348.24 138.39 o 1 3 0 802.04 806.95 20.40 o 2 3 0 25564.71 24856.86 421.41 o 3 3 0 0.15 5.17 3.84 o 4 3 0 3064.45 2835.80 42.84 o 5 3 0 605.91 641.61 20.99 o 6 3 0 1086.21 1307.25 26.53 o 7 3 0 3872.16 4559.43 170.55 o 8 3 0 604.90 603.62 19.64 o 9 3 0 385.21 381.22 18.77 o 10 3 0 249.06 248.04 20.16 o 11 3 0 1784.27 1841.25 56.66 o 12 3 0 64.69 53.55 21.37 o 13 3 0 179.94 165.72 26.18 o 14 3 0 5.50 -8.29 22.54 o 15 3 0 9.36 34.25 27.83 o 16 3 0 8.75 59.78 42.33 o 17 3 0 235.54 245.68 56.77 o 18 3 0 40.63 32.41 91.47 o 0 4 0 13986.78 11501.85 483.69 o 1 4 0 177.60 126.53 33.16 o 2 4 0 1073.77 1124.67 26.48 o 3 4 0 14541.87 14458.17 310.43 o 4 4 0 192.01 198.26 10.98 o 5 4 0 237.08 276.75 10.64 o 6 4 0 7520.35 8757.13 151.81 o 7 4 0 697.25 819.60 24.52 o 8 4 0 0.08 19.59 10.93 o 9 4 0 96.19 78.80 14.06 o 10 4 0 491.26 573.36 29.86 o 11 4 0 97.21 121.61 17.14 o 12 4 0 199.66 214.06 21.88 o 13 4 0 8.06 10.05 18.74 o 14 4 0 16.78 24.48 26.60 o 15 4 0 495.05 487.97 39.47 o 16 4 0 3.29 -7.84 41.06 o 17 4 0 554.03 557.16 67.16 o 1 5 0 1158.13 963.44 24.79 o 2 5 0 3751.04 4218.89 83.77 o 3 5 0 2.29 3.09 5.76 o 4 5 0 6078.37 6159.08 98.28 o 5 5 0 8325.53 8220.59 169.00 o 6 5 0 19.48 21.24 8.55 o 7 5 0 1738.71 1693.19 44.39 o 8 5 0 0.17 6.60 10.31 o 9 5 0 119.81 97.24 12.58 o 10 5 0 2889.44 3044.02 89.46 o 11 5 0 1948.32 1906.02 59.92 o 12 5 0 638.86 643.85 30.26 o 13 5 0 342.32 310.67 23.52 o 14 5 0 233.83 266.56 28.70 o 15 5 0 1.54 -19.15 47.12 o 16 5 0 99.50 15.07 39.89 o 17 5 0 357.30 395.92 69.10 o 0 6 0 4259.12 3995.18 159.37 o 1 6 0 19512.10 20198.43 411.38 o 2 6 0 5554.88 5398.58 107.45 o 3 6 0 36.79 46.96 10.09 o 4 6 0 3936.57 4459.16 116.55 o 5 6 0 2651.79 2806.85 69.15 o 6 6 0 767.79 873.20 37.60 o 7 6 0 591.58 625.84 18.08 o 8 6 0 2964.57 3311.91 64.51 o 9 6 0 302.66 316.67 17.37 o 10 6 0 1028.62 1022.96 38.41 o 11 6 0 689.40 679.96 27.55 o 12 6 0 105.48 102.75 20.67 o 13 6 0 8.83 -20.98 20.98 o 14 6 0 500.94 539.47 33.51 o 15 6 0 66.27 52.89 32.63 o 16 6 0 479.55 594.03 63.04 o 17 6 0 145.34 275.71 96.16 o 1 7 0 35.52 7.41 8.00 o 2 7 0 305.45 380.59 14.03 o 3 7 0 625.89 581.86 19.23 o 4 7 0 2517.06 2943.29 64.00 o 5 7 0 7992.78 8541.22 227.81 o 6 7 0 0.57 0.86 9.69 o 7 7 0 26.51 27.27 10.02 o 8 7 0 41.25 61.39 12.61 o 9 7 0 888.39 890.63 26.87 o 10 7 0 1556.26 1649.47 91.55 o 11 7 0 2531.80 2757.99 140.16 o 12 7 0 309.61 260.31 23.35 o 13 7 0 6.70 4.09 24.31 o 14 7 0 74.17 58.06 30.69 o 15 7 0 364.90 345.01 44.12 o 16 7 0 35.69 39.73 80.85 o 17 7 0 523.76 426.14 80.81 o 0 8 0 3625.45 3456.95 121.94 o 1 8 0 7375.64 7679.78 155.60 o 2 8 0 2074.63 2241.89 48.48 o 3 8 0 1039.73 1123.35 29.83 o 4 8 0 3.58 5.32 7.13 o 5 8 0 1450.17 1490.75 37.59 o 6 8 0 209.16 219.61 11.52 o 7 8 0 29.58 28.74 11.02 o 8 8 0 280.97 303.85 17.03 o 9 8 0 58.31 34.09 14.61 o 10 8 0 1264.04 1294.93 40.71 o 11 8 0 3.00 10.46 17.05 o 12 8 0 158.19 169.62 22.34 o 13 8 0 51.24 35.99 22.78 o 14 8 0 105.18 25.78 45.29 o 15 8 0 23.66 -24.45 44.75 o 16 8 0 138.07 91.14 70.14 o 1 9 0 9231.09 9555.73 362.82 o 2 9 0 3.14 -6.48 8.64 o 3 9 0 3328.85 3329.41 78.63 o 4 9 0 6.03 18.46 7.62 o 5 9 0 130.04 161.38 22.95 o 6 9 0 1524.30 1568.38 43.93 o 7 9 0 6.05 5.75 11.11 o 8 9 0 5.42 0.03 12.18 o 9 9 0 893.18 855.41 27.10 o 10 9 0 14.75 3.07 18.63 o 11 9 0 379.36 349.24 23.80 o 12 9 0 309.19 325.43 28.34 o 13 9 0 97.63 69.70 25.86 o 14 9 0 34.65 16.84 31.17 o 15 9 0 54.25 102.46 46.57 o 16 9 0 0.94 94.26 91.97 o 0 10 0 258.22 222.75 18.50 o 1 10 0 482.55 563.01 21.22 o 2 10 0 824.37 842.03 25.98 o 3 10 0 628.74 574.90 18.59 o 4 10 0 6.11 11.62 9.97 o 5 10 0 124.54 103.74 17.14 o 6 10 0 617.79 704.94 48.77 o 7 10 0 95.56 126.68 20.72 o 8 10 0 204.64 202.04 28.21 o 9 10 0 101.70 107.46 12.40 o 10 10 0 1258.45 1230.69 36.67 o 11 10 0 396.76 346.22 21.73 o 12 10 0 5.35 -2.09 21.17 o 13 10 0 1.72 25.15 24.45 o 14 10 0 164.14 167.43 45.15 o 15 10 0 0.05 -49.84 49.84 o 1 11 0 1.52 1.84 13.36 o 2 11 0 14.39 18.92 13.78 o 3 11 0 928.14 942.45 26.53 o 4 11 0 697.49 663.10 27.21 o 5 11 0 17.79 36.95 14.56 o 6 11 0 0.67 1.78 16.23 o 7 11 0 0.01 8.42 18.85 o 8 11 0 21.90 31.60 21.49 o 9 11 0 142.28 98.31 28.36 o 10 11 0 482.45 442.74 34.55 o 11 11 0 184.51 210.70 37.00 o 12 11 0 1.75 27.34 18.29 o 13 11 0 54.09 87.65 41.58 o 14 11 0 29.94 33.95 43.27 o 15 11 0 20.43 34.71 91.94 o 0 12 0 172.28 147.71 19.24 o 1 12 0 126.76 141.07 14.08 o 2 12 0 183.64 154.07 15.57 o 3 12 0 67.06 71.47 15.35 o 4 12 0 68.83 89.90 10.30 o 5 12 0 351.05 354.05 35.34 o 6 12 0 100.80 99.42 21.34 o 7 12 0 163.30 164.28 27.29 o 8 12 0 64.54 84.41 23.62 o 9 12 0 346.99 380.61 36.47 o 10 12 0 523.72 638.49 51.43 o 11 12 0 20.84 52.02 32.43 o 12 12 0 32.92 7.78 33.56 o 13 12 0 12.72 3.51 67.63 o 14 12 0 71.17 -11.09 65.68 o 1 13 0 69.61 49.45 16.04 o 2 13 0 172.21 175.23 16.90 o 3 13 0 26.20 33.30 13.35 o 4 13 0 15.12 5.04 7.21 o 5 13 0 132.41 107.96 20.23 o 6 13 0 61.78 81.01 20.34 o 7 13 0 30.00 23.32 21.89 o 8 13 0 8.18 4.79 21.89 o 9 13 0 209.96 242.20 32.82 o 10 13 0 170.80 217.15 32.94 o 11 13 0 0.70 -5.99 32.15 o 12 13 0 24.69 -6.67 73.18 o 13 13 0 0.00 -16.47 112.09 o 0 14 0 2192.52 2319.32 116.87 o 1 14 0 77.78 97.03 18.26 o 2 14 0 700.62 668.62 35.46 o 3 14 0 313.81 282.55 17.63 o 4 14 0 46.81 51.28 17.50 o 5 14 0 199.78 245.59 20.15 o 6 14 0 398.73 389.74 25.50 o 7 14 0 84.59 108.51 25.49 o 8 14 0 193.69 250.10 41.85 o 9 14 0 0.28 -28.58 28.58 o 10 14 0 530.28 582.41 62.86 o 11 14 0 23.74 43.33 47.26 o 12 14 0 6.09 11.15 66.27 o 1 15 0 205.45 194.28 30.20 o 2 15 0 0.15 3.13 14.56 o 3 15 0 215.61 227.44 21.55 o 4 15 0 26.85 35.14 16.97 o 5 15 0 166.71 169.57 20.55 o 6 15 0 102.94 81.78 24.22 o 7 15 0 1423.83 1420.11 92.06 o 8 15 0 1.24 -34.20 46.35 o 9 15 0 188.77 199.37 72.91 o 10 15 0 5.73 23.82 45.07 o 11 15 0 18.83 -49.94 49.94 o 0 16 0 3290.03 3892.27 251.67 o 1 16 0 0.06 -14.60 15.48 o 2 16 0 390.91 420.96 28.49 o 3 16 0 80.86 96.15 18.91 o 4 16 0 92.56 120.88 34.10 o 5 16 0 8.11 2.29 27.13 o 6 16 0 12.21 -10.35 33.54 o 7 16 0 183.39 156.90 45.53 o 8 16 0 1162.72 1273.06 141.04 o 9 16 0 7.46 17.47 84.60 o 10 16 0 29.49 -0.17 50.63 o 1 17 0 1805.86 1722.51 87.58 o 2 17 0 23.13 44.55 31.49 o 3 17 0 2.40 -15.94 33.78 o 4 17 0 6.06 38.34 31.52 o 5 17 0 7.27 27.36 78.89 o 6 17 0 92.64 152.25 42.01 o 7 17 0 192.85 117.40 71.72 o 2 18 0 326.25 287.13 63.48 o 3 18 0 2.59 24.17 57.11 o 4 18 0 8.21 60.30 78.36 o 5 18 0 2.53 66.67 97.22 o 6 18 0 30.51 67.20 88.72 o 7 18 0 29.92 55.51 98.81 o 2 0 1 1936.13 1977.36 29.85 o 3 0 1 7151.00 6501.37 89.60 o 4 0 1 6291.06 6064.36 102.96 o 5 0 1 4686.31 5059.33 71.10 o 6 0 1 689.74 642.48 15.52 o 7 0 1 4274.41 4799.64 68.88 o 8 0 1 32.48 13.04 9.96 o 9 0 1 3067.81 3244.27 71.46 o 10 0 1 58.94 58.90 13.34 o 11 0 1 637.32 668.14 25.05 o 12 0 1 267.13 271.03 20.81 o 13 0 1 485.04 441.87 25.34 o 14 0 1 481.22 494.30 30.02 o 15 0 1 6.33 22.61 30.49 o 16 0 1 46.31 22.48 50.55 o 17 0 1 2.32 127.04 52.67 o 18 0 1 1.13 -19.71 81.58 o 2 1 1 2974.73 2811.65 28.80 o 3 1 1 8881.53 8147.69 78.90 o 4 1 1 22310.22 22546.68 206.82 o 5 1 1 1822.39 1839.49 20.10 o 6 1 1 2784.07 2957.53 30.87 o 7 1 1 970.40 875.43 13.73 o 8 1 1 2960.46 3303.40 37.49 o 9 1 1 1399.96 1336.26 21.03 o 10 1 1 2006.06 2223.41 30.74 o 11 1 1 86.59 89.72 11.81 o 12 1 1 44.05 14.18 13.20 o 13 1 1 96.05 101.70 15.49 o 14 1 1 40.56 52.41 16.42 o 15 1 1 12.91 19.71 22.81 o 16 1 1 99.52 71.09 31.01 o 17 1 1 29.41 39.73 37.93 o 18 1 1 99.30 -5.56 55.37 o 0 2 1 2354.24 1740.92 79.13 o 1 2 1 8955.77 8150.03 478.05 o 2 2 1 1568.93 1158.66 15.96 o 3 2 1 1179.25 1089.37 12.85 o 4 2 1 8595.30 8324.00 97.74 o 5 2 1 11354.33 11465.84 132.25 o 6 2 1 1905.27 1918.51 24.71 o 7 2 1 1161.10 1204.25 17.48 o 8 2 1 1412.93 1476.63 21.17 o 9 2 1 448.78 440.19 14.88 o 10 2 1 1.92 6.01 8.73 o 11 2 1 39.44 23.20 10.89 o 12 2 1 36.39 29.31 13.12 o 13 2 1 443.88 468.36 18.95 o 14 2 1 47.86 22.39 17.01 o 15 2 1 32.31 -1.02 20.78 o 16 2 1 39.91 28.94 27.21 o 17 2 1 9.04 62.75 42.79 o 18 2 1 8.92 -7.63 52.36 o 0 3 1 13636.48 12979.26 252.28 o 1 3 1 11688.19 10661.49 159.95 o 2 3 1 5257.68 5107.53 56.24 o 3 3 1 4002.98 3868.48 46.77 o 4 3 1 5448.46 5391.45 55.12 o 5 3 1 4647.74 4757.82 54.06 o 6 3 1 4721.26 4806.38 87.30 o 7 3 1 1768.50 2028.26 31.69 o 8 3 1 1148.79 1151.39 19.05 o 9 3 1 78.49 72.55 8.75 o 10 3 1 1.74 5.84 8.86 o 11 3 1 80.35 109.21 11.94 o 12 3 1 363.51 416.57 18.00 o 13 3 1 706.32 706.95 22.92 o 14 3 1 1.84 24.95 18.52 o 15 3 1 47.15 101.16 23.55 o 16 3 1 46.23 66.34 27.34 o 17 3 1 49.57 3.35 33.63 o 18 3 1 178.17 206.43 56.14 o 0 4 1 11299.88 11010.75 264.24 o 1 4 1 226.11 168.71 31.74 o 2 4 1 1240.44 1116.55 21.70 o 3 4 1 1339.73 1374.37 17.51 o 4 4 1 6623.60 6709.67 113.60 o 5 4 1 6146.56 6425.32 79.43 o 6 4 1 6558.46 6876.82 107.22 o 7 4 1 410.97 425.18 11.09 o 8 4 1 324.58 324.57 11.36 o 9 4 1 1186.09 1243.48 21.88 o 10 4 1 819.77 867.15 21.89 o 11 4 1 60.67 40.87 11.45 o 12 4 1 89.47 96.76 15.06 o 13 4 1 199.01 199.80 16.78 o 14 4 1 98.28 73.46 18.83 o 15 4 1 4.41 21.00 23.22 o 16 4 1 175.18 202.94 31.43 o 17 4 1 54.50 30.00 39.24 o 0 5 1 5894.93 5922.07 121.26 o 1 5 1 937.27 979.04 17.95 o 2 5 1 2617.84 2605.90 37.20 o 3 5 1 132.59 145.42 8.53 o 4 5 1 4293.46 4427.70 49.58 o 5 5 1 2805.43 3082.89 38.75 o 6 5 1 2321.23 2622.37 54.13 o 7 5 1 1452.08 1560.19 24.50 o 8 5 1 815.47 812.70 21.76 o 9 5 1 444.99 465.61 13.46 o 10 5 1 357.51 353.23 13.97 o 11 5 1 333.22 329.34 15.05 o 12 5 1 657.85 631.29 21.60 o 13 5 1 76.83 81.93 15.10 o 14 5 1 47.80 56.37 17.59 o 15 5 1 212.42 193.08 23.96 o 16 5 1 46.45 36.38 28.33 o 17 5 1 25.40 39.85 44.74 o 0 6 1 2226.97 1777.36 46.17 o 1 6 1 388.81 384.15 8.96 o 2 6 1 1767.45 1668.52 29.29 o 3 6 1 2713.87 2818.92 46.31 o 4 6 1 3167.21 3261.39 44.87 o 5 6 1 2242.92 2366.99 40.35 o 6 6 1 6812.99 6937.47 119.05 o 7 6 1 446.89 443.66 11.06 o 8 6 1 6.19 12.64 8.20 o 9 6 1 381.92 396.80 13.86 o 10 6 1 435.94 449.87 14.32 o 11 6 1 385.79 340.25 15.18 o 12 6 1 1.31 -8.37 12.54 o 13 6 1 4.37 34.29 16.26 o 14 6 1 109.43 144.28 19.70 o 15 6 1 35.58 14.88 25.10 o 16 6 1 14.50 49.51 32.98 o 17 6 1 89.02 179.28 55.46 o 0 7 1 0.03 4.40 6.96 o 1 7 1 377.38 308.28 7.96 o 2 7 1 6011.01 6095.03 89.72 o 3 7 1 1759.19 1871.30 30.15 o 4 7 1 670.52 592.47 12.49 o 5 7 1 1419.25 1396.59 33.43 o 6 7 1 940.81 1025.45 19.53 o 7 7 1 990.22 1095.03 22.53 o 8 7 1 404.57 420.80 12.63 o 9 7 1 61.80 45.46 10.13 o 10 7 1 1636.99 1564.41 31.68 o 11 7 1 476.54 414.05 16.44 o 12 7 1 155.46 156.27 15.23 o 13 7 1 1.34 1.54 15.79 o 14 7 1 34.27 27.28 20.38 o 15 7 1 4.61 7.80 23.37 o 16 7 1 76.89 26.04 47.30 o 17 7 1 19.30 -22.23 61.16 o 0 8 1 1578.71 1775.63 45.61 o 1 8 1 979.51 982.93 17.41 o 2 8 1 688.30 671.87 14.46 o 3 8 1 7040.42 7301.18 101.02 o 4 8 1 3210.76 3284.15 51.38 o 5 8 1 318.79 331.14 11.50 o 6 8 1 274.57 250.89 11.15 o 7 8 1 247.56 274.02 15.65 o 8 8 1 718.09 754.84 17.99 o 9 8 1 374.69 361.65 13.21 o 10 8 1 702.70 736.71 19.25 o 11 8 1 85.74 101.26 14.70 o 12 8 1 13.26 15.84 14.41 o 13 8 1 50.20 44.64 17.88 o 14 8 1 71.05 53.05 21.42 o 15 8 1 38.85 26.38 30.35 o 16 8 1 153.78 171.29 55.44 o 0 9 1 716.65 824.02 25.54 o 1 9 1 308.73 301.79 9.73 o 2 9 1 1414.60 1510.43 25.80 o 3 9 1 3602.36 3800.10 53.51 o 4 9 1 888.27 881.03 30.85 o 5 9 1 429.57 430.86 15.44 o 6 9 1 410.19 402.57 12.92 o 7 9 1 794.78 786.21 25.36 o 8 9 1 769.58 720.19 15.44 o 9 9 1 839.19 838.02 18.19 o 10 9 1 991.37 976.48 25.69 o 11 9 1 173.01 166.68 14.19 o 12 9 1 2.39 22.39 16.14 o 13 9 1 113.33 107.76 19.71 o 14 9 1 79.85 98.48 25.68 o 15 9 1 271.34 307.35 45.05 o 16 9 1 28.64 18.57 72.04 o 0 10 1 87.50 72.68 12.75 o 1 10 1 401.15 420.37 13.85 o 2 10 1 522.44 497.99 13.77 o 3 10 1 1327.10 1314.17 22.75 o 4 10 1 27.60 38.75 12.65 o 5 10 1 316.75 311.64 12.98 o 6 10 1 500.60 482.80 22.94 o 7 10 1 240.23 259.24 13.11 o 8 10 1 160.65 182.68 13.58 o 9 10 1 413.81 427.67 16.93 o 10 10 1 159.70 163.59 16.27 o 11 10 1 318.26 352.54 15.96 o 12 10 1 21.45 26.86 16.36 o 13 10 1 8.54 13.01 21.11 o 14 10 1 69.84 53.99 30.77 o 15 10 1 3.85 -35.63 35.63 o 0 11 1 233.20 221.56 14.35 o 1 11 1 405.80 433.94 15.19 o 2 11 1 67.19 71.42 10.75 o 3 11 1 87.96 99.35 7.54 o 4 11 1 32.07 32.01 8.77 o 5 11 1 39.61 68.79 10.88 o 6 11 1 91.24 61.20 13.05 o 7 11 1 921.18 942.48 39.49 o 8 11 1 371.81 359.83 19.15 o 9 11 1 262.05 265.91 13.73 o 10 11 1 476.42 463.67 19.53 o 11 11 1 78.00 63.73 16.41 o 12 11 1 117.51 116.86 19.98 o 13 11 1 9.02 27.76 29.11 o 14 11 1 68.02 7.34 35.97 o 15 11 1 145.68 218.44 57.12 o 0 12 1 23.82 17.37 11.62 o 1 12 1 273.34 273.00 13.80 o 2 12 1 61.74 73.89 8.62 o 3 12 1 59.94 79.53 10.65 o 4 12 1 301.74 296.68 13.65 o 5 12 1 220.79 223.75 14.98 o 6 12 1 975.98 982.15 31.84 o 7 12 1 84.36 99.97 19.89 o 8 12 1 148.93 129.37 17.55 o 9 12 1 39.57 25.37 18.29 o 10 12 1 44.11 44.88 19.99 o 11 12 1 45.74 37.74 19.53 o 12 12 1 31.14 15.05 29.76 o 13 12 1 170.12 137.78 43.93 o 14 12 1 110.00 117.41 53.30 o 0 13 1 104.08 137.63 19.63 o 1 13 1 884.01 896.38 23.99 o 2 13 1 110.15 109.62 11.20 o 3 13 1 1129.86 1163.82 23.00 o 4 13 1 264.44 258.40 13.60 o 5 13 1 803.88 740.31 25.05 o 6 13 1 460.56 433.65 20.91 o 7 13 1 335.17 302.01 21.68 o 8 13 1 63.80 63.41 18.09 o 9 13 1 141.53 138.01 22.19 o 10 13 1 81.06 90.06 21.95 o 11 13 1 129.55 136.25 30.51 o 12 13 1 2.54 -29.59 36.29 o 13 13 1 94.13 84.68 54.92 o 0 14 1 478.45 528.26 24.26 o 1 14 1 474.51 492.46 15.50 o 2 14 1 5.84 5.95 8.96 o 3 14 1 469.63 530.14 13.85 o 4 14 1 1099.47 1055.80 22.84 o 5 14 1 277.18 242.16 17.66 o 6 14 1 237.25 257.84 15.76 o 7 14 1 491.37 521.71 25.41 o 8 14 1 652.02 699.74 40.17 o 9 14 1 23.92 -1.09 26.79 o 10 14 1 109.34 81.43 31.80 o 11 14 1 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6 35.53 70.68 62.56 o 14 11 6 12.41 3.17 63.91 o 0 12 6 1643.97 1648.61 62.16 o 1 12 6 775.36 795.16 26.30 o 2 12 6 1103.53 1152.32 25.36 o 3 12 6 1043.99 1022.68 37.79 o 4 12 6 635.79 627.20 24.70 o 5 12 6 501.37 487.53 21.56 o 6 12 6 114.75 151.91 18.59 o 7 12 6 131.92 120.69 21.59 o 8 12 6 510.64 504.82 29.85 o 9 12 6 63.09 64.62 18.92 o 10 12 6 44.88 48.20 26.09 o 11 12 6 115.04 90.67 40.55 o 12 12 6 55.09 62.86 58.17 o 13 12 6 258.20 159.47 73.29 o 0 13 6 334.67 367.23 26.13 o 1 13 6 331.90 317.01 17.86 o 2 13 6 2231.44 2265.33 44.80 o 3 13 6 462.72 473.81 19.85 o 4 13 6 548.51 543.57 26.62 o 5 13 6 721.53 666.19 26.26 o 6 13 6 4.29 1.73 18.50 o 7 13 6 200.67 195.65 25.43 o 8 13 6 44.79 39.41 28.55 o 9 13 6 110.27 107.93 23.28 o 10 13 6 221.10 257.07 42.58 o 11 13 6 254.79 311.24 41.14 o 12 13 6 84.86 198.11 53.89 o 0 14 6 179.96 180.20 25.14 o 1 14 6 393.52 368.63 21.03 o 2 14 6 533.95 528.68 16.23 o 3 14 6 121.92 129.95 20.95 o 4 14 6 265.99 232.63 19.42 o 5 14 6 43.59 26.53 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7 1382.09 1379.12 36.80 o 13 3 7 104.87 92.46 17.47 o 14 3 7 61.30 91.61 20.65 o 15 3 7 66.15 88.55 24.42 o 16 3 7 12.33 -31.66 31.66 o 17 3 7 0.66 19.28 42.75 o 0 4 7 3798.40 4052.88 65.70 o 1 4 7 8332.70 8854.16 99.85 o 2 4 7 2252.04 2431.41 30.16 o 3 4 7 2475.48 2565.64 30.90 o 4 4 7 606.91 529.67 10.40 o 5 4 7 565.02 547.49 12.38 o 6 4 7 2115.62 2071.10 26.46 o 7 4 7 856.88 949.01 19.65 o 8 4 7 371.12 363.83 12.82 o 9 4 7 207.87 208.30 11.14 o 10 4 7 1206.01 1264.65 28.08 o 11 4 7 578.97 608.47 19.91 o 12 4 7 66.44 71.53 15.35 o 13 4 7 41.66 34.35 17.27 o 14 4 7 75.27 32.41 22.89 o 15 4 7 22.77 27.31 26.91 o 16 4 7 119.63 162.23 33.66 o 17 4 7 42.90 94.00 50.97 o 0 5 7 11913.22 12546.71 214.40 o 1 5 7 10449.99 11228.70 136.31 o 2 5 7 4361.58 5018.32 67.20 o 3 5 7 632.60 626.15 15.69 o 4 5 7 1600.42 1428.66 19.05 o 5 5 7 746.90 721.73 13.67 o 6 5 7 463.00 473.63 12.20 o 7 5 7 1276.75 1245.59 20.29 o 8 5 7 299.92 305.26 12.05 o 9 5 7 649.22 661.09 17.15 o 10 5 7 427.99 451.08 16.74 o 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16.65 o 5 12 7 32.02 21.02 14.81 o 6 12 7 194.62 235.90 18.87 o 7 12 7 243.42 192.39 19.81 o 8 12 7 94.69 87.40 14.54 o 9 12 7 46.29 36.18 24.08 o 10 12 7 78.08 52.28 26.23 o 11 12 7 106.17 137.07 33.15 o 12 12 7 25.87 103.63 44.53 o 13 12 7 66.95 107.75 76.10 o 0 13 7 577.04 569.80 33.18 o 1 13 7 556.05 565.44 24.16 o 2 13 7 855.39 867.09 28.29 o 3 13 7 97.57 77.03 14.33 o 4 13 7 381.21 352.42 21.21 o 5 13 7 259.59 291.18 19.92 o 6 13 7 717.35 786.31 34.96 o 7 13 7 92.90 144.04 21.17 o 8 13 7 194.45 188.58 25.51 o 9 13 7 55.99 78.74 31.30 o 10 13 7 41.61 37.84 26.86 o 11 13 7 118.98 133.61 43.60 o 12 13 7 180.24 113.47 88.40 o 0 14 7 552.32 601.65 33.74 o 1 14 7 21.47 31.85 16.88 o 2 14 7 31.62 50.30 9.73 o 3 14 7 419.10 404.52 27.57 o 4 14 7 74.66 87.03 19.09 o 5 14 7 212.65 185.48 23.88 o 6 14 7 66.64 33.35 21.21 o 7 14 7 19.22 24.07 24.37 o 8 14 7 48.66 -22.37 22.37 o 9 14 7 161.68 136.50 34.68 o 10 14 7 41.35 23.94 36.37 o 11 14 7 156.09 195.98 81.62 o 0 15 7 11.68 11.84 22.94 o 1 15 7 34.96 23.39 16.63 o 2 15 7 159.71 160.85 25.79 o 3 15 7 12.19 9.97 23.90 o 4 15 7 347.35 325.72 36.30 o 5 15 7 127.21 128.67 24.68 o 6 15 7 41.51 48.50 25.86 o 7 15 7 76.88 68.19 32.94 o 8 15 7 168.45 116.21 55.01 o 9 15 7 7.72 -19.49 58.03 o 10 15 7 17.56 43.39 66.41 o 0 16 7 191.17 165.26 50.32 o 1 16 7 51.48 94.53 36.76 o 2 16 7 80.77 99.05 27.02 o 3 16 7 17.29 -8.51 27.09 o 4 16 7 73.37 113.75 28.01 o 5 16 7 98.20 121.44 37.88 o 6 16 7 33.84 15.36 39.30 o 7 16 7 144.96 234.81 47.26 o 8 16 7 105.43 96.69 77.00 o 9 16 7 20.37 63.57 76.69 o 0 17 7 127.22 81.71 55.40 o 1 17 7 83.31 38.74 37.29 o 2 17 7 370.79 428.22 42.18 o 3 17 7 70.31 101.37 41.57 o 4 17 7 53.73 34.67 45.48 o 5 17 7 119.49 106.40 42.42 o 6 17 7 71.99 78.52 64.39 o 7 17 7 30.18 2.77 69.26 o 0 18 7 103.01 52.06 66.67 o 1 18 7 75.39 113.72 60.14 o 2 18 7 65.84 50.39 51.25 o 3 18 7 90.61 48.34 93.76 o 4 18 7 311.60 353.33 69.33 o 5 18 7 59.86 -60.56 60.56 o 0 0 8 3969.95 4099.27 101.60 o 1 0 8 112.33 112.02 11.36 o 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o 2 2 8 2680.44 2875.05 31.82 o 3 2 8 60.71 60.61 5.04 o 4 2 8 829.30 818.64 12.42 o 5 2 8 2010.24 2029.95 25.49 o 6 2 8 124.43 141.53 7.94 o 7 2 8 504.03 479.18 11.80 o 8 2 8 315.51 343.67 11.59 o 9 2 8 807.57 731.16 16.59 o 10 2 8 717.11 680.85 16.84 o 11 2 8 51.65 44.80 12.83 o 12 2 8 314.96 328.03 16.91 o 13 2 8 53.84 58.80 16.33 o 14 2 8 6.91 4.86 20.03 o 15 2 8 75.27 75.97 28.17 o 16 2 8 7.87 16.83 34.09 o 17 2 8 223.51 166.33 43.23 o 0 3 8 118.11 110.56 10.66 o 1 3 8 5078.52 5185.87 56.05 o 2 3 8 815.33 952.36 15.48 o 3 3 8 2455.07 2680.54 29.46 o 4 3 8 1006.82 994.49 15.88 o 5 3 8 901.54 878.50 14.54 o 6 3 8 86.38 118.39 7.97 o 7 3 8 1060.15 1123.51 18.41 o 8 3 8 589.70 622.44 18.89 o 9 3 8 1704.84 1702.63 28.34 o 10 3 8 97.44 87.36 11.75 o 11 3 8 265.98 239.09 14.86 o 12 3 8 62.96 61.04 14.02 o 13 3 8 767.48 727.81 24.35 o 14 3 8 39.56 13.09 22.25 o 15 3 8 145.04 115.23 27.50 o 16 3 8 2.34 5.60 31.98 o 17 3 8 72.67 -40.93 40.93 o 0 4 8 4183.79 4517.01 77.31 o 1 4 8 1835.29 2085.16 27.18 o 2 4 8 5065.03 5471.17 63.41 o 3 4 8 12424.23 12894.12 131.18 o 4 4 8 380.61 341.18 9.24 o 5 4 8 261.28 255.66 9.07 o 6 4 8 26.32 21.32 8.27 o 7 4 8 345.72 339.34 11.42 o 8 4 8 730.84 729.31 16.30 o 9 4 8 751.68 724.90 17.50 o 10 4 8 349.52 342.35 14.33 o 11 4 8 49.74 88.35 13.46 o 12 4 8 631.53 677.67 23.04 o 13 4 8 286.63 295.29 19.78 o 14 4 8 71.15 74.81 23.96 o 15 4 8 55.08 43.84 23.54 o 16 4 8 107.55 102.93 42.89 o 0 5 8 190.76 183.83 12.71 o 1 5 8 3778.42 4085.93 48.39 o 2 5 8 120.20 114.78 8.95 o 3 5 8 214.96 205.62 8.58 o 4 5 8 876.99 843.34 16.48 o 5 5 8 739.61 664.07 13.79 o 6 5 8 145.48 123.59 8.77 o 7 5 8 567.74 552.97 14.38 o 8 5 8 379.54 358.69 12.59 o 9 5 8 1474.74 1522.66 34.97 o 10 5 8 491.21 499.32 16.30 o 11 5 8 539.11 464.51 18.86 o 12 5 8 172.81 193.77 18.03 o 13 5 8 424.39 408.06 22.01 o 14 5 8 48.73 59.56 23.18 o 15 5 8 254.36 237.78 26.90 o 16 5 8 200.66 240.89 47.62 o 0 6 8 2027.84 2182.45 38.72 o 1 6 8 183.32 140.34 8.31 o 2 6 8 2835.11 3152.78 48.97 o 3 6 8 2397.00 2424.52 39.88 o 4 6 8 41.22 43.91 7.65 o 5 6 8 40.22 35.54 7.86 o 6 6 8 1600.62 1719.98 26.03 o 7 6 8 87.07 77.83 9.52 o 8 6 8 595.84 616.95 15.61 o 9 6 8 2442.50 2536.25 42.55 o 10 6 8 759.96 796.06 19.92 o 11 6 8 224.52 223.18 15.37 o 12 6 8 239.01 235.39 18.21 o 13 6 8 59.72 50.81 17.83 o 14 6 8 145.64 84.53 24.87 o 15 6 8 88.67 3.09 27.70 o 16 6 8 369.50 432.56 46.97 o 0 7 8 1694.75 1730.07 42.03 o 1 7 8 2643.77 2526.70 33.69 o 2 7 8 446.23 491.18 20.69 o 3 7 8 376.62 358.97 10.88 o 4 7 8 346.14 330.30 11.12 o 5 7 8 3712.57 3834.38 56.24 o 6 7 8 179.43 165.46 9.50 o 7 7 8 830.42 809.15 20.60 o 8 7 8 206.54 195.28 11.75 o 9 7 8 861.12 799.64 20.07 o 10 7 8 163.92 160.26 14.43 o 11 7 8 378.20 359.36 17.01 o 12 7 8 87.93 80.21 17.95 o 13 7 8 45.87 22.41 21.39 o 14 7 8 41.60 6.82 22.50 o 15 7 8 57.74 100.73 35.55 o 0 8 8 3.14 0.30 7.42 o 1 8 8 616.51 619.70 22.32 o 2 8 8 171.41 156.16 11.80 o 3 8 8 662.10 654.84 16.34 o 4 8 8 234.60 259.53 10.60 o 5 8 8 194.94 195.11 12.39 o 6 8 8 1899.43 2004.51 49.14 o 7 8 8 308.14 310.05 11.58 o 8 8 8 1076.02 1055.30 20.76 o 9 8 8 129.25 119.30 12.49 o 10 8 8 509.50 463.82 17.84 o 11 8 8 33.76 21.31 14.11 o 12 8 8 30.70 14.33 17.30 o 13 8 8 4.37 -15.73 20.57 o 14 8 8 37.74 47.28 35.29 o 15 8 8 19.73 4.25 45.96 o 0 9 8 1873.07 1904.56 47.82 o 1 9 8 1280.01 1233.47 38.70 o 2 9 8 1488.20 1499.00 39.28 o 3 9 8 943.50 977.97 22.79 o 4 9 8 767.94 770.69 26.53 o 5 9 8 3080.89 3118.41 69.11 o 6 9 8 283.37 279.07 15.33 o 7 9 8 3695.24 3839.11 65.09 o 8 9 8 123.25 133.48 15.13 o 9 9 8 687.67 739.42 22.24 o 10 9 8 132.49 133.05 11.29 o 11 9 8 41.70 26.50 11.21 o 12 9 8 25.39 45.87 17.59 o 13 9 8 6.21 4.92 29.18 o 14 9 8 27.71 22.93 54.74 o 15 9 8 3.28 54.61 118.60 o 0 10 8 1405.01 1390.02 56.97 o 1 10 8 1349.45 1389.36 35.93 o 2 10 8 1557.72 1579.53 41.44 o 3 10 8 905.85 902.56 24.06 o 4 10 8 81.56 79.75 14.24 o 5 10 8 93.56 108.64 15.89 o 6 10 8 2156.81 2178.46 46.91 o 7 10 8 178.17 198.73 14.91 o 8 10 8 264.63 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