#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:51:37 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180922 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/02/2200290.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200290_Fobs loop_ _publ_author_name 'Camus, Fabrice' 'Norberg, Bernadette' 'Bourry, Anne' 'Rigo, Beno\?\^it' 'Durant, Fran\,cois' _publ_section_title ; 1,1'-(4-Methylbenzylidene)bis(5-oxopyrrolidine-2-carboxylic acid) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o439 _journal_page_last o440 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.0770 _cell_length_b 11.0650 _cell_length_c 17.1060 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.8110 _cod_data_source_file ci6021Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lilled - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 95.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3049.53 3220.55 31.86 o 4 0 0 165.57 177.34 2.84 o 6 0 0 2272.06 2248.10 35.54 o 8 0 0 2255.22 2251.18 15.25 o 10 0 0 31.37 34.66 1.20 o 1 1 0 7411.57 6803.93 243.84 o 2 1 0 1143.74 1153.32 49.09 o 3 1 0 360.70 350.37 17.27 o 4 1 0 1477.13 1590.18 39.83 o 5 1 0 3801.60 4212.88 90.17 o 6 1 0 146.98 171.11 5.38 o 7 1 0 30.39 30.37 1.80 o 8 1 0 194.26 200.80 3.30 o 9 1 0 28.27 26.45 1.09 o 10 1 0 28.07 29.93 1.09 o 11 1 0 12.83 17.93 0.76 o 0 2 0 2154.22 2397.74 21.18 o 1 2 0 8858.14 8290.46 287.50 o 2 2 0 268.00 281.19 4.43 o 3 2 0 2566.06 2652.35 101.18 o 4 2 0 965.67 1023.35 43.51 o 5 2 0 1.24 1.45 0.94 o 6 2 0 31.94 33.31 0.70 o 7 2 0 36.41 38.31 2.00 o 8 2 0 35.55 32.04 0.86 o 9 2 0 97.07 87.72 2.52 o 10 2 0 5.96 6.70 0.66 o 11 2 0 0.00 0.22 0.77 o 1 3 0 22.96 23.14 0.66 o 2 3 0 47.24 48.30 2.58 o 3 3 0 2370.10 2440.39 97.47 o 4 3 0 132.51 119.35 4.40 o 5 3 0 45.24 43.41 1.72 o 6 3 0 402.18 415.42 6.75 o 7 3 0 104.87 94.80 6.64 o 8 3 0 266.54 254.52 7.42 o 9 3 0 9.59 8.19 0.66 o 10 3 0 53.73 48.14 1.55 o 0 4 0 11.49 13.66 0.72 o 1 4 0 1270.09 1347.00 10.88 o 2 4 0 129.67 131.98 2.39 o 3 4 0 2046.26 2099.26 46.14 o 4 4 0 69.81 73.94 1.57 o 5 4 0 1190.66 1203.72 17.84 o 6 4 0 1.93 1.56 0.31 o 7 4 0 31.11 31.66 0.82 o 8 4 0 48.57 38.51 1.33 o 9 4 0 7.60 8.33 0.66 o 10 4 0 50.39 54.66 1.67 o 1 5 0 307.63 315.60 3.91 o 2 5 0 427.26 490.02 6.43 o 3 5 0 382.71 351.13 4.69 o 4 5 0 412.90 405.24 5.47 o 5 5 0 0.23 0.22 0.31 o 6 5 0 51.28 54.86 2.57 o 7 5 0 35.84 33.47 1.39 o 8 5 0 92.14 83.92 2.56 o 9 5 0 18.51 15.45 0.89 o 10 5 0 39.40 43.04 1.22 o 0 6 0 2307.90 2605.57 27.15 o 1 6 0 410.08 470.55 6.29 o 2 6 0 2.53 3.20 0.36 o 3 6 0 9.70 9.37 0.77 o 4 6 0 358.94 381.47 5.69 o 5 6 0 29.30 31.84 0.70 o 6 6 0 255.62 247.82 5.14 o 7 6 0 146.70 149.91 4.11 o 8 6 0 1.06 0.22 0.56 o 9 6 0 226.02 242.01 6.43 o 10 6 0 2.59 1.99 0.44 o 1 7 0 11.70 12.18 0.39 o 2 7 0 14.74 12.59 0.69 o 3 7 0 0.46 5.01 1.73 o 4 7 0 64.14 59.46 1.22 o 5 7 0 347.84 299.20 5.56 o 6 7 0 87.28 81.70 1.79 o 7 7 0 0.00 0.00 0.89 o 8 7 0 91.51 97.34 2.99 o 9 7 0 8.14 11.07 0.66 o 0 8 0 79.37 76.48 1.55 o 1 8 0 15.02 12.56 0.47 o 2 8 0 208.52 226.42 4.62 o 3 8 0 51.55 53.54 1.50 o 4 8 0 462.10 444.16 6.78 o 5 8 0 4.90 4.45 0.47 o 6 8 0 4.36 2.55 0.66 o 7 8 0 25.99 25.46 0.99 o 8 8 0 15.32 13.51 0.78 o 9 8 0 49.75 45.34 1.21 o 1 9 0 43.55 47.54 1.53 o 2 9 0 58.32 58.77 1.16 o 3 9 0 262.13 247.79 5.86 o 4 9 0 30.87 24.21 1.11 o 5 9 0 45.77 37.85 1.21 o 6 9 0 43.81 41.81 1.33 o 7 9 0 2.38 2.32 0.55 o 8 9 0 23.03 25.38 0.89 o 0 10 0 737.60 725.43 12.57 o 1 10 0 296.07 293.65 8.91 o 2 10 0 0.07 0.77 0.55 o 3 10 0 18.52 15.90 0.89 o 4 10 0 32.74 32.01 1.21 o 5 10 0 258.09 239.25 6.96 o 6 10 0 24.64 28.57 1.11 o 7 10 0 2.07 1.10 0.44 o 1 11 0 12.20 12.47 0.89 o 2 11 0 61.15 55.40 1.54 o 3 11 0 6.23 5.41 0.55 o 4 11 0 8.70 8.81 0.66 o 5 11 0 244.60 249.35 6.27 o 6 11 0 4.83 3.29 0.44 o 0 12 0 133.38 150.26 3.75 o 1 12 0 8.94 11.45 0.88 o 2 12 0 81.27 84.40 2.75 o 3 12 0 10.46 8.59 0.66 o 4 12 0 6.92 8.36 0.66 o 5 12 0 5.27 4.50 0.44 o 1 13 0 12.23 12.40 0.66 o 2 13 0 75.10 81.00 2.30 o 3 13 0 0.45 1.20 0.33 o 1 0 1 194.30 178.00 1.38 o 2 0 1 5461.28 5257.24 10.39 o 3 0 1 1933.03 2044.75 8.06 o 4 0 1 215.86 243.66 3.36 o 5 0 1 3.88 2.02 0.27 o 6 0 1 52.31 58.84 3.26 o 7 0 1 90.11 89.77 3.47 o 8 0 1 101.51 88.39 3.03 o 9 0 1 21.36 20.16 0.98 o 10 0 1 8.32 7.55 0.66 o 11 0 1 63.38 75.59 2.08 o -11 1 1 4.89 7.05 0.54 o -10 1 1 7.25 8.92 0.76 o -9 1 1 111.05 116.65 3.60 o -8 1 1 289.86 265.96 7.55 o -7 1 1 166.67 162.58 4.06 o -6 1 1 149.89 147.36 3.53 o -5 1 1 77.16 71.99 2.22 o -4 1 1 127.47 126.18 3.56 o -3 1 1 464.11 467.47 5.65 o -2 1 1 5408.52 5213.86 15.26 o -1 1 1 5395.67 4709.36 48.37 o 0 1 1 2563.91 2671.26 110.85 o 1 1 1 5433.78 5211.03 51.27 o 2 1 1 5405.33 5577.61 15.85 o 3 1 1 465.65 486.06 5.76 o 4 1 1 127.96 121.69 3.44 o 5 1 1 77.01 80.45 2.33 o 6 1 1 148.41 159.46 3.66 o 7 1 1 164.86 177.71 4.21 o 8 1 1 287.59 277.46 7.86 o -11 2 1 40.74 50.60 1.66 o -10 2 1 6.16 7.30 0.66 o -9 2 1 45.35 40.93 1.33 o -8 2 1 158.77 149.46 4.10 o -7 2 1 16.55 15.52 0.89 o -6 2 1 233.88 231.08 6.22 o -5 2 1 481.77 444.82 7.67 o -4 2 1 1128.22 1164.30 10.80 o -3 2 1 4904.76 5105.14 19.59 o -2 2 1 5638.55 5460.79 17.23 o -1 2 1 2418.67 2264.97 9.55 o 0 2 1 5551.83 5699.66 173.08 o 1 2 1 2408.29 2421.62 9.91 o 2 2 1 5642.46 5977.60 18.13 o 3 2 1 4896.65 5591.22 20.48 o 4 2 1 1127.97 1296.28 11.40 o 5 2 1 479.68 476.36 7.97 o 6 2 1 234.72 239.05 6.30 o 7 2 1 16.14 18.11 0.77 o 8 2 1 158.92 158.16 4.30 o -10 3 1 100.15 109.97 3.00 o -9 3 1 26.55 23.65 1.00 o -8 3 1 81.10 77.80 2.44 o -7 3 1 79.34 79.75 2.44 o -6 3 1 131.40 148.08 3.68 o -5 3 1 262.00 256.45 6.00 o -4 3 1 481.46 475.30 7.34 o -3 3 1 1441.33 1427.83 11.12 o -2 3 1 115.56 115.04 2.89 o -1 3 1 2453.77 2310.83 11.32 o 0 3 1 418.37 421.83 4.35 o 1 3 1 2453.91 2409.39 11.68 o 2 3 1 115.93 109.69 2.76 o 3 3 1 1449.49 1564.03 11.72 o 4 3 1 477.30 513.78 7.61 o 5 3 1 259.75 257.61 6.07 o 6 3 1 130.22 148.61 3.64 o 7 3 1 79.46 89.75 2.53 o -10 4 1 23.61 23.14 0.89 o -9 4 1 138.02 142.49 3.89 o -8 4 1 123.97 123.85 3.78 o -7 4 1 71.98 66.42 2.34 o -6 4 1 176.50 167.37 4.00 o -5 4 1 482.20 492.65 8.79 o -4 4 1 743.64 725.91 9.67 o -3 4 1 18.47 16.67 0.56 o -2 4 1 943.86 948.85 8.99 o -1 4 1 1071.32 1031.64 8.77 o 0 4 1 668.73 697.27 17.19 o 1 4 1 1083.49 1073.59 9.03 o 2 4 1 940.10 994.81 9.23 o 3 4 1 18.53 17.62 0.55 o 4 4 1 739.41 796.63 10.14 o 5 4 1 480.62 516.24 9.02 o 6 4 1 175.87 163.88 3.96 o 7 4 1 73.23 72.32 2.31 o -10 5 1 13.03 14.74 0.66 o -9 5 1 22.01 25.20 1.11 o -8 5 1 246.24 242.54 5.10 o -7 5 1 247.36 216.40 4.89 o -6 5 1 48.63 42.87 1.22 o -5 5 1 75.51 80.85 2.22 o -4 5 1 341.65 316.87 6.88 o -3 5 1 953.98 912.04 10.65 o -2 5 1 486.92 460.29 7.10 o -1 5 1 552.05 536.08 7.21 o 0 5 1 13.36 17.28 0.90 o 1 5 1 552.84 551.05 7.36 o 2 5 1 489.17 476.05 7.14 o 3 5 1 951.68 948.80 10.88 o 4 5 1 343.50 335.78 7.01 o 5 5 1 75.21 79.18 2.19 o 6 5 1 47.16 44.47 1.43 o 7 5 1 247.84 227.67 4.92 o -10 6 1 52.51 55.95 1.76 o -9 6 1 26.40 25.14 1.00 o -8 6 1 163.73 157.08 4.10 o -7 6 1 5.76 7.09 0.56 o -6 6 1 232.57 216.32 4.77 o -5 6 1 27.50 28.16 1.00 o -4 6 1 31.51 31.96 1.00 o -3 6 1 29.09 35.07 1.11 o -2 6 1 590.74 559.96 8.55 o -1 6 1 262.80 282.23 5.99 o 0 6 1 0.90 1.22 0.18 o 1 6 1 263.38 293.93 6.01 o 2 6 1 592.62 565.16 8.64 o 3 6 1 28.96 34.81 0.98 o 4 6 1 30.41 30.97 1.10 o 5 6 1 27.00 30.75 0.98 o 6 6 1 233.96 227.56 4.92 o -9 7 1 14.41 15.22 0.66 o -8 7 1 6.26 9.52 0.66 o -7 7 1 348.12 342.12 8.64 o -6 7 1 145.54 152.34 4.21 o -5 7 1 46.89 47.46 1.55 o -4 7 1 43.26 40.87 1.22 o -3 7 1 295.30 276.13 6.98 o -2 7 1 483.54 502.19 8.97 o -1 7 1 327.35 320.36 6.98 o 0 7 1 934.93 993.57 8.59 o 1 7 1 326.88 336.48 7.08 o 2 7 1 486.78 529.73 9.15 o 3 7 1 294.86 274.50 6.86 o 4 7 1 42.73 41.71 1.31 o 5 7 1 46.19 48.00 1.52 o 6 7 1 145.63 152.47 4.14 o -9 8 1 43.45 44.97 1.21 o -8 8 1 75.91 78.37 2.53 o -7 8 1 52.06 52.19 1.55 o -6 8 1 27.85 24.12 1.11 o -5 8 1 137.60 130.39 3.87 o -4 8 1 355.34 312.26 8.07 o -3 8 1 157.40 146.51 3.87 o -2 8 1 253.90 263.05 6.97 o -1 8 1 40.75 44.45 1.33 o 0 8 1 227.29 218.79 4.43 o 1 8 1 39.89 42.23 1.30 o 2 8 1 251.03 256.33 6.97 o 3 8 1 157.76 148.55 3.91 o 4 8 1 353.88 322.57 8.17 o 5 8 1 138.15 122.64 3.69 o -8 9 1 17.23 19.66 0.77 o -7 9 1 15.65 19.18 0.89 o -6 9 1 49.20 47.91 1.66 o -5 9 1 136.08 154.05 4.19 o -4 9 1 96.76 96.31 2.75 o -3 9 1 158.91 158.38 4.19 o -2 9 1 19.83 19.39 1.10 o -1 9 1 27.12 32.39 1.10 o 0 9 1 9.37 8.43 0.77 o 1 9 1 26.80 33.02 1.20 o 2 9 1 20.02 18.47 0.87 o 3 9 1 157.97 158.53 4.13 o -7 10 1 21.03 19.99 0.77 o -6 10 1 12.41 12.23 0.77 o -5 10 1 11.70 12.68 0.77 o -4 10 1 23.64 22.49 0.99 o -3 10 1 66.29 66.68 1.98 o -2 10 1 10.22 13.44 0.89 o -1 10 1 13.98 15.76 0.89 o 0 10 1 1195.88 1153.41 15.87 o 1 10 1 14.21 14.54 0.87 o -6 11 1 30.43 29.12 0.99 o -5 11 1 100.05 96.24 2.75 o -4 11 1 4.46 5.29 0.66 o -3 11 1 4.69 5.28 0.55 o -2 11 1 5.20 6.93 0.66 o -1 11 1 211.23 193.72 4.50 o 0 11 1 17.37 16.47 0.88 o -5 12 1 15.16 16.96 0.77 o -4 12 1 25.04 27.65 0.98 o -3 12 1 103.92 112.41 3.07 o -2 12 1 32.04 29.67 1.10 o -1 12 1 39.25 41.98 1.32 o 0 12 1 97.45 94.16 2.97 o -3 13 1 15.70 16.62 0.76 o -2 13 1 57.49 64.76 1.98 o -1 13 1 20.69 20.41 0.77 o 0 13 1 17.83 22.72 0.88 o 0 0 2 4195.98 4000.40 27.24 o 1 0 2 298.37 277.72 4.59 o 2 0 2 2414.83 2427.36 13.74 o 3 0 2 603.02 548.28 4.29 o 4 0 2 591.52 550.17 5.04 o 5 0 2 6.72 13.02 0.44 o 6 0 2 10.97 10.90 0.46 o 7 0 2 121.22 133.89 2.56 o 8 0 2 362.99 362.97 7.24 o 9 0 2 130.54 131.90 3.77 o 10 0 2 102.10 101.18 3.11 o 11 0 2 0.81 1.99 0.44 o -11 1 2 11.46 12.43 0.66 o -10 1 2 14.40 14.91 0.89 o -9 1 2 217.49 214.68 4.89 o -8 1 2 338.14 322.76 8.39 o -7 1 2 57.41 56.79 1.54 o -6 1 2 58.16 66.42 1.98 o -5 1 2 429.72 382.52 6.89 o -4 1 2 188.37 159.44 3.93 o -3 1 2 3500.64 3439.99 15.40 o -2 1 2 3254.68 3121.77 12.23 o -1 1 2 4032.17 3762.81 11.03 o 0 1 2 2103.82 2129.70 84.72 o 1 1 2 4022.92 3917.77 11.35 o 2 1 2 3242.66 3262.37 12.66 o 3 1 2 3502.57 3630.91 15.95 o 4 1 2 188.20 171.55 4.06 o 5 1 2 426.14 413.51 7.24 o 6 1 2 58.10 64.51 1.98 o 7 1 2 57.36 63.57 1.88 o 8 1 2 338.26 342.72 8.85 o -11 2 2 48.04 54.52 1.67 o -10 2 2 120.74 125.62 3.22 o -9 2 2 15.68 19.70 0.89 o -8 2 2 40.03 39.59 1.34 o -7 2 2 43.44 41.99 1.34 o -6 2 2 48.50 46.71 1.33 o -5 2 2 165.98 164.78 4.76 o -4 2 2 75.72 80.87 2.10 o -3 2 2 1508.68 1368.98 10.27 o -2 2 2 1424.66 1389.26 8.94 o -1 2 2 6488.24 6418.71 16.82 o 0 2 2 619.32 639.86 26.47 o 1 2 2 6496.57 7037.89 17.63 o 2 2 2 1428.92 1511.56 9.41 o 3 2 2 1512.60 1499.23 10.87 o 4 2 2 75.65 83.99 2.09 o 5 2 2 167.02 171.63 4.84 o 6 2 2 48.54 47.84 1.55 o 7 2 2 43.47 45.34 1.33 o 8 2 2 39.68 43.98 1.33 o -10 3 2 0.40 0.34 1.11 o -9 3 2 71.17 64.80 1.89 o -8 3 2 37.07 37.80 1.22 o -7 3 2 287.85 282.91 7.66 o -6 3 2 198.26 184.38 4.11 o -5 3 2 1.05 -0.66 1.00 o -4 3 2 1050.15 1083.13 11.11 o -3 3 2 64.43 65.34 1.77 o -2 3 2 459.16 456.55 5.77 o -1 3 2 3830.60 3669.24 14.74 o 0 3 2 2277.06 2190.58 61.44 o 1 3 2 3822.41 3885.73 15.23 o 2 3 2 461.16 481.41 5.92 o 3 3 2 65.53 75.85 1.87 o 4 3 2 1048.93 1155.84 11.45 o 5 3 2 1.09 -1.21 1.21 o 6 3 2 199.98 189.47 4.18 o 7 3 2 288.51 287.14 7.82 o -10 4 2 40.69 43.19 1.11 o -9 4 2 10.82 9.20 0.66 o -8 4 2 10.00 11.21 0.89 o -7 4 2 62.18 70.83 2.00 o -6 4 2 94.84 93.25 2.55 o -5 4 2 111.22 115.46 3.11 o -4 4 2 117.67 118.71 2.89 o -3 4 2 528.81 506.54 7.32 o -2 4 2 491.06 528.77 6.87 o -1 4 2 290.63 290.26 4.76 o 0 4 2 1990.89 2035.72 39.99 o 1 4 2 289.22 299.02 4.93 o 2 4 2 487.69 568.79 7.12 o 3 4 2 533.02 558.35 7.79 o 4 4 2 116.21 121.10 2.86 o 5 4 2 112.65 125.09 3.19 o 6 4 2 92.78 95.80 3.07 o 7 4 2 62.20 68.64 1.98 o -10 5 2 100.62 109.39 2.66 o -9 5 2 248.10 246.85 6.76 o -8 5 2 10.47 10.09 0.78 o -7 5 2 579.52 567.26 11.09 o -6 5 2 128.97 120.29 3.55 o -5 5 2 265.24 271.13 6.99 o -4 5 2 375.80 392.59 7.76 o -3 5 2 135.31 128.16 2.88 o -2 5 2 130.54 122.69 2.66 o -1 5 2 467.68 495.74 7.09 o 0 5 2 947.73 1108.48 20.06 o 1 5 2 468.78 505.02 7.12 o 2 5 2 132.43 128.33 3.83 o 3 5 2 136.89 135.87 2.95 o 4 5 2 371.39 377.03 7.55 o 5 5 2 263.42 268.32 6.90 o 6 5 2 127.47 131.74 3.72 o 7 5 2 577.87 593.29 11.25 o -9 6 2 25.79 31.88 1.11 o -8 6 2 7.18 7.18 0.66 o -7 6 2 34.61 29.89 1.22 o -6 6 2 4.27 5.65 0.78 o -5 6 2 123.53 122.56 3.54 o -4 6 2 745.33 752.85 11.41 o -3 6 2 153.30 141.03 3.32 o -2 6 2 996.98 1013.23 11.63 o -1 6 2 26.11 29.47 0.89 o 0 6 2 1601.82 1650.62 16.87 o 1 6 2 26.70 32.88 0.98 o 2 6 2 1003.51 1035.97 11.80 o 3 6 2 153.71 147.01 3.38 o 4 6 2 747.07 753.42 11.23 o 5 6 2 122.95 136.27 3.70 o 6 6 2 4.15 5.55 0.66 o -9 7 2 7.83 8.05 0.55 o -8 7 2 94.99 95.74 2.98 o -7 7 2 29.34 25.64 1.11 o -6 7 2 133.32 128.26 3.76 o -5 7 2 204.19 202.46 4.53 o -4 7 2 8.51 6.43 0.66 o -3 7 2 517.32 535.43 9.75 o -2 7 2 186.03 184.05 3.99 o -1 7 2 278.13 273.59 6.54 o 0 7 2 39.99 44.59 1.95 o 1 7 2 277.16 261.07 6.31 o 2 7 2 188.41 194.74 4.03 o 3 7 2 520.37 545.01 9.69 o 4 7 2 8.49 5.88 0.54 o 5 7 2 202.75 207.48 4.69 o -9 8 2 36.14 40.06 1.20 o -8 8 2 15.69 18.30 0.89 o -7 8 2 147.27 141.94 3.75 o -6 8 2 425.12 436.64 9.59 o -5 8 2 271.30 245.00 7.39 o -4 8 2 138.02 134.68 3.75 o -3 8 2 110.10 110.65 3.31 o -2 8 2 182.30 187.15 4.30 o -1 8 2 376.38 386.00 8.39 o 0 8 2 11.43 9.87 0.42 o 1 8 2 375.79 379.47 8.26 o 2 8 2 182.13 192.72 4.24 o 3 8 2 110.55 108.04 3.37 o 4 8 2 138.07 137.50 3.80 o 5 8 2 270.99 255.78 7.49 o -8 9 2 17.24 18.01 0.77 o -7 9 2 13.37 13.76 0.77 o -6 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