#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/04/2200404.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200404_Fobs loop_ _publ_author_name 'Bond, Andrew D.' 'Feeder, Neil' 'Redman, James E.' 'Sanders, Jeremy K. M.' _publ_section_title ; 4,4'-Bipyridine-3,3'-dicarboxylic acid dihydrate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o869 _journal_page_last o871 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.770 _cell_angle_gamma 90.000 _cell_length_a 8.5200 _cell_length_b 15.9700 _cell_length_c 9.6700 _exptl_crystal_F_000 584.00 _reflns_d_resolution_high 0.8345 _[local]_cod_data_source_file bt6080Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' js9928 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 192.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6126.51 6430.63 202.32 o 4 0 0 118.92 117.00 12.50 o 6 0 0 935.29 1051.95 61.16 o 8 0 0 121.81 126.92 20.20 o 1 1 0 115.32 118.84 12.10 o 2 1 0 7.25 12.51 9.02 o 3 1 0 1793.82 1769.14 59.88 o 4 1 0 59.09 50.59 22.42 o 5 1 0 6.67 10.09 17.36 o 6 1 0 79.69 82.33 20.64 o 7 1 0 37.82 46.16 23.54 o 9 1 0 7.76 23.54 23.27 o 0 2 0 6927.81 4094.71 920.62 o 1 2 0 853.05 857.27 13.33 o 2 2 0 37179.99 31710.65 503.67 o 3 2 0 8535.79 9385.69 393.11 o 4 2 0 4492.26 4720.01 342.89 o 5 2 0 394.50 386.78 18.35 o 6 2 0 100.99 106.88 27.93 o 7 2 0 76.40 66.17 33.03 o 9 2 0 147.50 114.37 21.19 o 1 3 0 809.82 800.87 39.72 o 2 3 0 949.79 883.94 7.82 o 3 3 0 5.79 16.94 18.21 o 4 3 0 236.28 245.49 33.69 o 5 3 0 416.84 415.87 43.24 o 6 3 0 4.34 20.81 15.23 o 7 3 0 319.11 321.28 15.75 o 8 3 0 272.13 281.85 32.82 o 9 3 0 59.45 74.68 34.49 o 0 4 0 677.45 651.50 18.85 o 1 4 0 4716.41 4788.34 125.04 o 2 4 0 5204.92 5795.95 79.85 o 3 4 0 2344.81 2300.16 115.01 o 4 4 0 1237.15 1287.19 77.53 o 5 4 0 302.15 290.90 28.76 o 6 4 0 219.50 259.02 32.12 o 7 4 0 730.63 856.95 76.36 o 8 4 0 77.13 69.67 24.03 o 9 4 0 309.45 293.31 54.37 o 1 5 0 84.98 79.85 5.92 o 2 5 0 234.95 232.35 18.43 o 3 5 0 55.73 48.16 11.79 o 4 5 0 498.15 503.12 61.35 o 5 5 0 778.74 782.14 19.50 o 6 5 0 245.16 236.84 30.65 o 7 5 0 500.68 532.96 61.76 o 8 5 0 18.87 36.06 39.13 o 9 5 0 395.80 312.90 51.38 o 0 6 0 57.29 43.06 7.45 o 1 6 0 405.49 384.56 26.15 o 2 6 0 42.79 43.71 20.87 o 3 6 0 7.73 11.84 6.93 o 4 6 0 562.76 603.52 83.88 o 5 6 0 1294.26 1338.30 163.77 o 6 6 0 1194.98 1202.46 162.19 o 7 6 0 82.07 66.93 37.10 o 8 6 0 178.44 177.37 22.07 o 9 6 0 350.57 287.65 36.91 o 1 7 0 125.40 128.48 10.61 o 2 7 0 9.56 16.06 5.52 o 3 7 0 0.32 6.19 11.45 o 4 7 0 151.87 165.71 46.26 o 5 7 0 24.29 39.48 43.94 o 6 7 0 654.87 657.21 51.44 o 7 7 0 909.20 889.65 81.25 o 8 7 0 140.08 106.64 38.71 o 0 8 0 15.46 13.16 3.63 o 1 8 0 89.55 94.75 9.57 o 2 8 0 828.39 816.29 21.85 o 3 8 0 174.27 188.21 23.53 o 4 8 0 853.81 922.38 47.03 o 5 8 0 4.42 19.03 52.28 o 6 8 0 815.91 867.66 54.37 o 7 8 0 582.98 561.20 151.32 o 8 8 0 205.95 151.68 45.67 o 1 9 0 691.90 658.71 23.43 o 2 9 0 106.18 110.33 15.77 o 3 9 0 32.64 25.06 16.58 o 4 9 0 745.42 778.43 49.46 o 5 9 0 258.64 239.94 62.14 o 6 9 0 405.91 425.86 51.04 o 7 9 0 42.33 54.06 35.25 o 8 9 0 491.31 440.70 88.67 o 0 10 0 66.37 70.05 13.27 o 1 10 0 16.36 7.71 8.86 o 2 10 0 319.98 302.69 9.82 o 3 10 0 827.37 827.30 45.99 o 4 10 0 0.42 7.40 14.93 o 5 10 0 375.50 360.02 43.27 o 6 10 0 242.64 263.95 26.88 o 7 10 0 11.89 13.24 23.50 o 8 10 0 593.31 481.21 37.06 o 1 11 0 95.24 103.42 13.78 o 2 11 0 433.00 429.77 52.66 o 3 11 0 65.31 51.97 26.07 o 4 11 0 83.76 104.19 18.82 o 5 11 0 0.03 40.04 26.08 o 6 11 0 760.95 769.49 98.40 o 7 11 0 4.54 14.82 26.58 o 0 12 0 10.40 3.54 7.93 o 1 12 0 1338.64 1293.76 87.24 o 2 12 0 201.42 228.42 13.92 o 3 12 0 493.49 416.05 55.96 o 4 12 0 310.81 322.82 40.69 o 5 12 0 146.40 93.82 44.64 o 6 12 0 2.63 30.47 24.92 o 7 12 0 4.13 11.61 30.74 o 1 13 0 351.11 353.82 14.40 o 2 13 0 5.25 6.58 9.08 o 3 13 0 14.41 15.69 10.60 o 4 13 0 204.96 196.87 53.47 o 0 14 0 758.91 790.40 13.51 o 1 14 0 3415.45 3558.61 179.69 o 2 14 0 102.75 103.86 12.53 o 3 14 0 182.51 220.38 15.14 o 4 14 0 154.87 147.80 53.61 o 5 14 0 118.01 125.86 33.42 o 6 14 0 0.46 49.00 36.89 o 1 15 0 50.89 59.05 15.94 o 2 15 0 0.88 28.68 13.19 o 3 15 0 200.73 187.91 41.90 o 4 15 0 144.41 119.37 34.73 o 5 15 0 7.38 18.71 24.14 o 0 16 0 234.46 223.07 21.74 o 1 16 0 1020.88 1103.53 104.58 o 2 16 0 52.71 75.82 16.43 o 3 16 0 1274.52 1298.79 36.63 o 4 16 0 0.43 27.96 30.89 o 5 16 0 15.09 33.76 18.26 o 1 17 0 344.61 362.23 84.34 o 2 17 0 13.98 19.98 27.32 o 3 17 0 38.68 48.43 54.21 o 4 17 0 1.21 13.82 28.29 o 0 18 0 300.79 231.67 84.97 o 1 18 0 474.88 432.24 21.58 o 2 18 0 14.35 24.63 17.88 o 3 18 0 128.59 71.69 17.04 o 1 19 0 72.55 61.54 14.11 o -7 0 1 37.03 39.62 17.33 o -5 0 1 26.08 28.94 8.98 o -3 0 1 1.48 23.22 12.92 o -1 0 1 7433.36 5851.44 1627.47 o 1 0 1 483.60 490.97 53.71 o 3 0 1 25.37 16.84 10.95 o 5 0 1 140.03 139.40 13.40 o 7 0 1 171.31 187.18 13.68 o 9 0 1 30.62 26.36 29.53 o -9 1 1 9.16 39.59 31.37 o -8 1 1 6.61 13.89 24.65 o -7 1 1 73.82 78.10 27.02 o -6 1 1 177.30 185.44 11.76 o -5 1 1 569.33 661.89 51.36 o -4 1 1 282.17 264.20 32.87 o -3 1 1 1676.17 1650.40 24.27 o -2 1 1 8.31 9.16 9.66 o -1 1 1 118.71 124.62 20.43 o 0 1 1 412.44 351.63 26.08 o 1 1 1 898.69 807.70 26.40 o 2 1 1 2590.44 2766.63 85.31 o 3 1 1 311.54 338.35 42.78 o 4 1 1 107.67 155.85 24.05 o 5 1 1 1955.40 2079.66 149.76 o 6 1 1 3.40 13.14 17.04 o 7 1 1 171.84 150.16 23.18 o 8 1 1 22.91 34.28 20.78 o 9 1 1 134.73 121.88 30.09 o -9 2 1 16.02 52.67 19.29 o -7 2 1 66.20 66.26 25.62 o -6 2 1 575.58 597.99 27.61 o -5 2 1 718.85 765.40 46.31 o -4 2 1 411.04 393.76 17.20 o -3 2 1 307.90 262.04 11.30 o -2 2 1 5903.72 6231.85 111.09 o -1 2 1 563.75 522.20 17.37 o 0 2 1 1899.27 1865.28 165.85 o 1 2 1 1109.36 1175.19 44.42 o 2 2 1 24463.87 21975.71 1309.34 o 3 2 1 431.52 385.53 28.53 o 4 2 1 120.14 136.74 24.77 o 5 2 1 55.69 63.24 36.37 o 6 2 1 96.20 77.69 47.27 o 7 2 1 31.03 45.10 21.80 o 8 2 1 90.90 88.22 19.55 o 9 2 1 38.87 57.23 17.20 o -9 3 1 38.39 50.98 23.00 o -8 3 1 22.91 53.99 40.86 o -7 3 1 599.84 676.99 41.35 o -5 3 1 1355.74 1567.40 110.95 o -4 3 1 26.23 25.41 7.55 o -3 3 1 366.02 397.35 19.85 o -2 3 1 43.58 34.48 10.86 o -1 3 1 323.50 299.24 13.52 o 0 3 1 63.08 28.83 16.19 o 1 3 1 163.11 144.77 15.98 o 2 3 1 2652.53 2606.34 138.93 o 3 3 1 14.02 24.77 15.64 o 4 3 1 1400.98 1349.20 101.40 o 5 3 1 1.08 12.75 26.37 o 6 3 1 173.46 184.74 45.84 o 7 3 1 0.31 24.00 15.77 o 8 3 1 48.04 57.74 15.09 o 9 3 1 24.47 30.14 17.75 o -9 4 1 0.04 17.19 29.82 o -8 4 1 26.70 35.65 26.12 o -7 4 1 9.99 35.63 30.92 o -6 4 1 508.16 547.79 36.54 o -5 4 1 36.59 27.69 9.71 o -4 4 1 4842.56 5248.88 223.77 o -3 4 1 7621.38 8323.84 488.87 o -2 4 1 1462.76 1426.03 29.77 o -1 4 1 7575.97 8262.11 134.16 o 0 4 1 450.93 411.17 26.28 o 1 4 1 110.71 81.85 16.22 o 2 4 1 796.33 835.73 45.69 o 3 4 1 515.37 489.29 28.30 o 4 4 1 4276.73 4378.33 207.96 o 5 4 1 1493.18 1515.27 142.08 o 6 4 1 404.98 426.31 28.09 o 7 4 1 155.83 177.81 48.41 o 8 4 1 0.76 38.26 56.94 o -9 5 1 40.85 60.14 17.86 o -8 5 1 6.88 24.12 22.18 o -7 5 1 46.99 44.08 24.68 o -6 5 1 121.56 137.12 21.57 o -5 5 1 591.94 650.16 36.93 o -4 5 1 469.76 473.30 40.59 o -3 5 1 1584.26 1619.31 85.02 o -2 5 1 3334.35 3235.87 197.42 o -1 5 1 831.86 797.16 22.06 o 0 5 1 885.11 756.08 47.10 o 1 5 1 135.41 151.89 16.76 o 2 5 1 92.85 111.33 10.98 o 3 5 1 20.34 19.25 11.50 o 4 5 1 1629.14 1578.19 89.44 o 5 5 1 37.86 48.22 28.56 o 6 5 1 45.41 52.76 42.03 o 7 5 1 21.79 27.85 35.06 o 8 5 1 292.59 246.19 16.49 o -9 6 1 14.54 43.93 34.93 o -8 6 1 16.96 36.09 18.89 o -7 6 1 6.31 22.10 16.42 o -6 6 1 85.56 91.13 21.23 o -5 6 1 7.79 47.89 18.05 o -4 6 1 2328.60 2414.70 145.95 o -3 6 1 744.16 830.94 59.22 o -2 6 1 3048.26 3230.60 118.98 o -1 6 1 3318.82 3328.95 116.45 o 0 6 1 1931.08 1987.45 101.30 o 1 6 1 1425.85 1500.21 47.89 o 2 6 1 144.31 117.26 25.25 o 3 6 1 1154.78 1062.15 55.62 o 4 6 1 601.51 660.43 86.55 o 5 6 1 701.70 738.93 97.22 o 6 6 1 466.86 461.45 60.53 o 7 6 1 10.82 16.12 14.17 o 8 6 1 0.71 86.27 41.83 o -9 7 1 6.59 14.07 25.91 o -8 7 1 10.71 20.42 32.07 o -7 7 1 52.07 62.86 31.06 o -6 7 1 459.03 464.84 66.14 o -5 7 1 4.51 10.70 14.14 o -4 7 1 134.33 125.05 19.54 o -3 7 1 18.04 11.78 9.37 o -2 7 1 329.35 273.69 32.91 o -1 7 1 1058.12 1060.15 55.89 o 0 7 1 1232.27 1140.93 27.56 o 1 7 1 1686.89 1680.44 158.33 o 2 7 1 79.33 88.66 35.44 o 3 7 1 104.91 93.45 18.79 o 4 7 1 8.14 7.21 9.29 o 5 7 1 12.78 24.74 14.59 o 6 7 1 7.67 14.16 45.85 o 7 7 1 59.34 50.62 22.51 o 8 7 1 147.37 157.29 81.21 o -8 8 1 85.56 66.62 41.86 o -7 8 1 62.37 60.80 20.84 o -6 8 1 379.91 445.07 60.57 o -5 8 1 1.87 13.41 20.41 o -4 8 1 64.99 64.44 23.09 o -3 8 1 372.06 371.30 24.55 o -2 8 1 5.67 9.31 10.70 o -1 8 1 74.52 77.21 9.52 o 0 8 1 2086.05 2029.34 66.33 o 1 8 1 371.45 376.86 32.16 o 3 8 1 27.27 35.79 24.20 o 5 8 1 545.21 565.03 77.25 o 6 8 1 6.29 35.93 21.82 o 7 8 1 304.56 251.83 99.77 o -8 9 1 57.84 41.40 40.96 o -7 9 1 41.45 49.59 49.14 o -6 9 1 53.10 50.80 13.74 o -5 9 1 149.77 136.70 15.22 o -4 9 1 109.30 127.40 39.88 o -3 9 1 176.01 179.33 17.32 o -2 9 1 0.00 25.82 12.64 o -1 9 1 10.52 14.68 6.62 o 0 9 1 225.33 188.44 17.74 o 1 9 1 652.93 639.13 27.96 o 2 9 1 18.50 15.50 10.37 o 3 9 1 468.69 501.65 59.76 o 4 9 1 2.85 16.13 8.12 o 5 9 1 76.63 85.35 30.42 o 6 9 1 26.39 46.77 22.06 o 7 9 1 3.93 7.22 26.63 o 8 9 1 89.97 66.10 14.86 o -8 10 1 17.73 29.27 21.39 o -7 10 1 52.09 46.91 21.75 o -6 10 1 28.76 48.59 16.33 o -5 10 1 347.93 325.37 51.60 o -4 10 1 0.66 20.41 20.80 o -3 10 1 4.52 10.61 8.94 o -2 10 1 379.85 374.47 45.72 o -1 10 1 17.60 22.44 9.21 o 0 10 1 685.51 699.74 55.77 o 1 10 1 50.35 61.66 18.12 o 2 10 1 91.32 94.12 15.17 o 3 10 1 2026.94 2092.41 179.06 o 4 10 1 548.26 576.66 73.93 o 5 10 1 906.14 915.79 73.52 o 6 10 1 14.34 17.86 11.92 o 7 10 1 132.28 122.34 32.15 o -8 11 1 1.01 12.46 13.77 o -7 11 1 55.64 44.32 29.61 o -6 11 1 0.62 28.61 13.03 o -5 11 1 89.53 77.00 20.95 o -4 11 1 147.15 146.84 12.37 o -3 11 1 84.27 83.86 12.33 o -2 11 1 388.49 371.09 26.68 o -1 11 1 1.55 15.78 15.47 o 0 11 1 51.10 38.15 27.37 o 1 11 1 20.78 24.38 8.81 o 2 11 1 0.11 5.68 3.48 o 3 11 1 20.39 11.25 12.33 o 4 11 1 176.42 205.48 29.98 o 6 11 1 50.05 25.68 16.39 o 7 11 1 2.77 31.59 32.85 o -7 12 1 5.36 25.44 25.02 o -6 12 1 38.99 56.72 22.54 o -5 12 1 148.98 154.15 22.21 o -4 12 1 215.65 249.93 22.07 o -3 12 1 14.45 16.80 13.49 o -2 12 1 96.48 89.88 11.61 o -1 12 1 96.24 98.88 13.16 o 0 12 1 162.52 145.19 22.24 o 1 12 1 1756.44 1809.36 89.44 o 2 12 1 302.63 301.71 30.95 o 3 12 1 2217.94 2256.58 111.45 o 4 12 1 248.87 213.39 17.39 o 5 12 1 156.85 114.39 38.62 o 6 12 1 1.75 42.12 19.85 o 7 12 1 240.30 223.87 22.08 o -7 13 1 18.30 24.87 18.59 o -6 13 1 22.58 79.96 30.00 o -5 13 1 79.16 76.10 29.11 o -4 13 1 417.59 447.77 74.55 o -3 13 1 97.67 106.26 34.54 o -2 13 1 278.78 277.08 18.15 o -1 13 1 32.45 28.79 21.71 o 0 13 1 157.00 175.31 22.58 o 1 13 1 418.03 436.46 36.67 o 2 13 1 97.73 75.85 20.52 o 4 13 1 0.06 14.73 38.04 o 5 13 1 17.11 53.63 24.16 o 6 13 1 178.86 130.99 67.06 o -6 14 1 2.05 38.36 23.90 o -5 14 1 77.24 83.95 27.52 o -4 14 1 13.64 20.89 16.31 o -3 14 1 23.30 46.01 49.75 o -2 14 1 290.20 282.84 17.03 o -1 14 1 345.89 368.00 95.04 o 0 14 1 49.78 57.10 13.27 o 1 14 1 936.97 1026.74 41.95 o 2 14 1 238.02 251.69 12.91 o 3 14 1 112.50 113.98 20.69 o 4 14 1 12.44 18.33 13.66 o 5 14 1 311.52 260.38 30.24 o 6 14 1 12.52 47.85 38.71 o -6 15 1 0.30 31.37 24.58 o -4 15 1 175.76 176.10 46.41 o -3 15 1 389.80 423.74 24.89 o -2 15 1 0.03 7.80 13.90 o -1 15 1 76.56 81.20 13.65 o 0 15 1 0.51 10.71 13.27 o 1 15 1 681.90 710.80 15.79 o 2 15 1 62.27 41.91 27.24 o 3 15 1 510.56 593.24 35.71 o 4 15 1 48.66 67.64 29.11 o 5 15 1 80.36 91.12 20.91 o -5 16 1 0.89 6.76 24.87 o -4 16 1 8.81 28.44 25.57 o -3 16 1 278.62 290.55 21.56 o -2 16 1 21.38 27.52 14.32 o -1 16 1 949.53 973.30 23.91 o 0 16 1 22.33 26.63 7.77 o 1 16 1 0.87 11.31 10.54 o 2 16 1 262.76 282.14 28.09 o 4 16 1 10.65 14.56 23.99 o -4 17 1 151.54 123.18 22.74 o -3 17 1 2.27 18.29 16.67 o -2 17 1 27.63 49.47 27.56 o -1 17 1 117.93 131.31 45.66 o 0 17 1 214.53 183.84 20.44 o 1 17 1 45.11 52.45 13.46 o 2 17 1 4.00 19.32 17.51 o 3 17 1 42.82 59.97 18.39 o -3 18 1 591.19 561.32 31.34 o -2 18 1 33.11 37.84 51.18 o -1 18 1 17.65 20.24 14.21 o 0 18 1 0.64 2.14 2.92 o 1 18 1 2.68 10.50 10.46 o 2 18 1 65.60 46.95 17.18 o 0 19 1 117.84 88.93 120.25 o -10 0 2 166.84 201.95 32.29 o -8 0 2 2.85 9.82 17.76 o -6 0 2 39.63 60.53 20.53 o -4 0 2 480.15 458.42 20.65 o -2 0 2 469.27 370.85 18.63 o 0 0 2 3248.49 3279.01 71.75 o 2 0 2 9994.18 10956.79 293.87 o 4 0 2 3611.26 3645.08 122.94 o 6 0 2 249.57 280.82 20.23 o 8 0 2 52.25 39.47 37.28 o -10 1 2 124.55 63.98 61.37 o -9 1 2 262.85 210.55 28.46 o -7 1 2 550.58 627.44 43.80 o -6 1 2 220.34 233.16 23.57 o -5 1 2 166.01 186.83 14.91 o -4 1 2 400.29 383.52 16.91 o -3 1 2 748.86 692.31 56.02 o -2 1 2 974.92 850.58 68.21 o -1 1 2 276.48 192.47 23.43 o 0 1 2 327.21 303.16 14.67 o 1 1 2 1076.01 1013.16 29.09 o 2 1 2 44.04 37.95 11.13 o 3 1 2 53.17 44.57 18.82 o 4 1 2 644.55 670.21 67.42 o 5 1 2 13.53 18.88 16.03 o 6 1 2 56.47 51.00 17.95 o 7 1 2 187.35 194.27 35.16 o 8 1 2 22.32 37.62 37.67 o -9 2 2 309.36 274.89 35.14 o -8 2 2 53.54 45.02 17.97 o -7 2 2 31.84 35.83 24.28 o -6 2 2 248.40 276.59 24.78 o -5 2 2 6.98 11.99 12.92 o -4 2 2 197.79 210.58 13.90 o -3 2 2 90.75 79.96 10.65 o -2 2 2 4586.88 4909.11 93.29 o -1 2 2 2880.55 2849.99 164.73 o 0 2 2 1096.86 1043.96 66.61 o 1 2 2 3577.02 3649.17 205.98 o 2 2 2 1118.54 988.51 41.91 o 3 2 2 229.49 234.64 30.23 o 4 2 2 166.75 108.65 24.78 o 5 2 2 112.41 116.05 25.16 o 6 2 2 102.73 97.29 44.20 o 7 2 2 31.52 50.52 88.62 o 8 2 2 182.33 147.63 65.62 o -9 3 2 274.83 273.22 15.82 o -8 3 2 88.96 110.63 38.13 o -7 3 2 20.06 50.13 32.57 o -6 3 2 158.50 143.24 20.72 o -5 3 2 42.43 48.21 14.34 o -4 3 2 717.29 709.03 18.59 o -3 3 2 383.46 414.43 13.78 o -2 3 2 3.15 7.53 11.32 o -1 3 2 410.58 414.03 22.93 o 0 3 2 667.02 624.29 19.90 o 1 3 2 381.70 419.07 16.50 o 2 3 2 1640.61 1765.88 72.82 o 3 3 2 218.18 242.54 27.45 o 4 3 2 364.95 374.98 21.34 o 5 3 2 109.31 114.95 24.32 o 6 3 2 468.29 558.90 85.52 o 7 3 2 200.56 213.56 33.68 o 8 3 2 7.60 62.00 36.25 o -9 4 2 4.27 62.76 35.68 o -8 4 2 56.91 62.75 39.61 o -7 4 2 229.52 207.02 20.49 o -6 4 2 36.22 80.20 23.94 o -5 4 2 175.10 189.18 20.32 o -4 4 2 2.95 12.92 15.52 o -3 4 2 1159.08 1065.49 57.70 o -2 4 2 588.50 574.06 39.93 o -1 4 2 101.58 74.99 36.60 o 0 4 2 112.43 84.41 7.98 o 1 4 2 56.50 31.73 11.01 o 2 4 2 110.50 128.53 25.35 o 3 4 2 249.60 258.25 25.21 o 4 4 2 64.22 58.63 25.93 o 5 4 2 275.99 281.94 14.13 o 6 4 2 7.30 25.66 19.94 o 7 4 2 43.87 56.27 47.05 o 8 4 2 21.01 24.67 21.56 o -9 5 2 47.85 67.19 27.73 o -8 5 2 3.36 28.96 45.91 o -7 5 2 140.50 152.72 26.02 o -6 5 2 2.23 24.32 16.68 o -5 5 2 186.31 229.40 24.61 o -4 5 2 15.30 23.07 11.31 o -3 5 2 320.55 316.54 13.79 o -2 5 2 20.89 18.47 21.25 o -1 5 2 130.28 172.21 12.91 o 0 5 2 407.33 421.54 12.66 o 1 5 2 102.95 93.82 20.43 o 2 5 2 582.76 539.58 43.80 o 3 5 2 363.18 387.35 55.96 o 4 5 2 509.03 513.84 48.21 o 5 5 2 90.12 83.63 34.95 o 6 5 2 113.69 106.76 62.86 o 7 5 2 55.22 63.03 31.53 o 8 5 2 241.10 215.07 50.13 o -9 6 2 26.82 28.88 21.17 o -8 6 2 10.97 21.28 35.86 o -7 6 2 6.34 31.71 22.91 o -6 6 2 215.02 212.42 19.51 o -5 6 2 398.99 372.98 26.69 o -4 6 2 707.08 710.70 67.55 o -3 6 2 836.54 776.84 37.01 o -2 6 2 826.53 851.09 68.68 o -1 6 2 3416.26 3642.74 142.22 o 0 6 2 727.04 782.81 39.62 o 1 6 2 293.39 285.72 32.43 o 2 6 2 694.04 743.22 75.91 o 3 6 2 74.22 103.52 22.98 o 4 6 2 101.49 101.55 45.59 o 5 6 2 1.56 14.17 13.79 o 6 6 2 0.45 20.88 22.22 o 7 6 2 488.55 498.15 98.42 o 8 6 2 52.81 57.95 53.89 o -8 7 2 5.31 16.30 11.10 o -7 7 2 58.02 47.94 15.96 o -6 7 2 60.54 59.97 15.66 o -5 7 2 2.89 16.73 12.49 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