#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/05/2200577.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200577_Fobs loop_ _publ_author_name 'Ricard, David' 'Richard, Philippe' 'Boitrel, Bernard' _publ_section_title ; (Methanol){\a-5,10,15:\b-20-tetrakis[2-(chloroacetamido)phenyl]porphyrin}zinc(II) chloroform solvate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m404 _journal_page_last m406 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.009 _cell_angle_gamma 90.000 _cell_length_a 13.0780 _cell_length_b 17.8990 _cell_length_c 22.7900 _exptl_crystal_F_000 2440.00 _reflns_d_resolution_high 0.7686 _[local]_cod_data_source_file ya6045Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' XYZN file =3D SHELXL INS file, from DIRDIF output for BB12' _shelx_refln_list_code 4 _shelx_f_calc_maximum 399.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 208.97 327.78 21.49 o 4 0 0 12503.04 11321.92 241.81 o 6 0 0 11252.08 12031.22 306.29 o 8 0 0 4340.98 3761.44 134.34 o 10 0 0 18.75 59.11 85.98 o 12 0 0 1906.90 1821.61 177.32 o 14 0 0 205.18 343.90 139.71 o 16 0 0 1337.29 1891.47 580.34 o 1 1 0 1231.08 684.17 72.54 o 4 1 0 59692.08 57538.89 1198.67 o 5 1 0 638.30 903.34 35.95 o 6 1 0 8641.34 8393.54 207.76 o 7 1 0 69.50 34.93 53.73 o 8 1 0 59.07 18.81 34.20 o 9 1 0 633.70 741.09 56.61 o 10 1 0 4014.54 4421.63 386.89 o 11 1 0 313.65 330.17 83.92 o 12 1 0 3976.53 3906.94 186.18 o 13 1 0 96.93 186.41 96.01 o 14 1 0 13.25 49.48 110.16 o 15 1 0 111.53 358.88 140.63 o 16 1 0 95.56 130.23 123.26 o 0 2 0 27731.37 22595.48 1418.60 o 1 2 0 10895.39 12387.38 224.65 o 2 2 0 229.18 234.04 107.47 o 3 2 0 11606.30 9122.60 134.85 o 4 2 0 66.38 20.90 18.81 o 5 2 0 10478.65 10062.87 212.25 o 6 2 0 11833.10 13242.46 273.57 o 7 2 0 2143.14 2083.96 110.16 o 8 2 0 10204.76 8729.72 239.12 o 9 2 0 3163.33 3112.92 110.98 o 10 2 0 1905.09 1953.22 137.02 o 11 2 0 2.54 2.69 56.99 o 12 2 0 874.63 875.71 117.60 o 13 2 0 1903.02 2199.88 140.67 o 14 2 0 169.44 174.18 98.08 o 15 2 0 523.12 479.59 106.19 o 16 2 0 318.70 610.70 180.01 o 1 3 0 8368.13 9234.41 394.95 o 2 3 0 1560.12 1827.50 49.63 o 3 3 0 10978.35 13098.80 239.01 o 4 3 0 62.07 277.38 48.36 o 5 3 0 14776.05 14562.46 335.84 o 6 3 0 27071.02 25517.88 564.55 o 7 3 0 3122.39 3217.43 96.01 o 8 3 0 1562.12 1699.42 73.22 o 9 3 0 9896.94 10068.73 238.76 o 10 3 0 3727.43 3713.45 169.26 o 11 3 0 3479.77 3665.85 303.60 o 12 3 0 1386.48 1437.21 122.40 o 13 3 0 466.48 446.08 99.25 o 14 3 0 1327.02 1107.65 145.08 o 15 3 0 64.73 215.81 134.34 o 16 3 0 158.90 37.61 155.83 o 1 4 0 157.54 322.70 34.93 o 2 4 0 30066.89 31242.10 550.63 o 3 4 0 2880.18 2449.07 63.26 o 4 4 0 3221.11 2143.13 128.96 o 5 4 0 8045.37 7781.36 233.29 o 6 4 0 1426.27 1445.80 77.92 o 7 4 0 16834.37 17689.05 421.44 o 8 4 0 82.64 96.72 56.42 o 9 4 0 5315.27 5160.33 139.93 o 10 4 0 2542.23 2536.11 354.65 o 11 4 0 265.50 285.50 78.49 o 12 4 0 614.27 604.94 190.76 o 13 4 0 2781.20 2883.86 174.21 o 14 4 0 308.17 736.17 198.82 o 15 4 0 570.58 585.71 155.83 o 16 4 0 72.93 247.18 209.57 o 1 5 0 2412.81 1816.41 37.32 o 2 5 0 2151.14 2145.06 43.73 o 3 5 0 41934.52 40233.88 744.23 o 4 5 0 15982.40 15559.91 383.54 o 5 5 0 8946.85 9844.93 478.24 o 6 5 0 327.91 462.32 53.73 o 7 5 0 4383.61 4250.86 384.20 o 8 5 0 169.80 132.23 48.36 o 9 5 0 6.77 253.20 60.79 o 10 5 0 1320.79 1402.48 150.46 o 11 5 0 876.50 639.44 150.46 o 12 5 0 544.83 623.32 155.83 o 13 5 0 1414.03 1257.39 188.07 o 14 5 0 3.76 -10.75 112.84 o 15 5 0 99.52 16.12 128.96 o 0 6 0 4659.29 4791.15 140.67 o 1 6 0 48085.27 48355.35 838.17 o 2 6 0 1906.05 1544.05 35.95 o 3 6 0 4222.07 4399.54 77.82 o 4 6 0 245.19 438.31 40.30 o 5 6 0 3982.08 3498.27 125.39 o 6 6 0 6447.10 6806.58 199.67 o 7 6 0 7868.87 7423.77 282.11 o 8 6 0 291.91 468.32 52.79 o 9 6 0 114.29 75.23 134.34 o 10 6 0 1072.54 1037.08 112.84 o 11 6 0 1042.61 1123.06 155.83 o 12 6 0 749.54 1219.78 150.46 o 13 6 0 319.32 386.89 118.22 o 14 6 0 227.08 300.91 145.08 o 15 6 0 646.02 832.89 214.94 o 1 7 0 10586.05 9585.94 174.64 o 2 7 0 27826.35 27990.46 585.71 o 3 7 0 4605.23 4615.34 83.33 o 4 7 0 6402.65 7519.55 155.83 o 5 7 0 10759.24 9725.18 235.21 o 6 7 0 221.65 175.83 41.28 o 7 7 0 106.72 116.98 42.74 o 8 7 0 5.13 14.83 47.38 o 9 7 0 1841.64 1700.90 110.89 o 10 7 0 21.25 -42.99 96.72 o 11 7 0 1091.08 977.97 155.83 o 12 7 0 83.75 279.42 177.32 o 13 7 0 81.12 85.98 166.58 o 14 7 0 446.83 446.00 188.07 o 15 7 0 55.14 16.12 209.57 o 0 8 0 71.93 80.66 18.81 o 1 8 0 1541.60 1201.12 30.40 o 2 8 0 4815.98 5212.11 131.65 o 3 8 0 7548.33 7426.88 212.25 o 4 8 0 14.73 18.81 13.82 o 5 8 0 467.93 389.62 28.84 o 6 8 0 135.60 124.23 30.40 o 7 8 0 2065.46 1740.15 87.14 o 8 8 0 88.20 138.18 77.38 o 9 8 0 2370.25 2641.43 117.49 o 10 8 0 1278.06 687.81 139.71 o 11 8 0 1322.83 1311.13 128.96 o 12 8 0 678.04 763.03 139.71 o 13 8 0 1388.44 1504.57 290.17 o 14 8 0 1527.61 1338.00 252.55 o 15 8 0 551.11 306.29 171.95 o 1 9 0 2825.75 2911.82 142.40 o 2 9 0 10895.98 10577.25 239.12 o 3 9 0 6.71 29.55 15.20 o 4 9 0 47.65 167.43 14.82 o 5 9 0 45.38 62.61 19.96 o 6 9 0 5350.12 5543.19 123.44 o 7 9 0 199.68 164.53 85.98 o 8 9 0 989.80 1035.10 74.86 o 9 9 0 110.65 59.11 118.22 o 10 9 0 3489.98 3707.70 343.90 o 11 9 0 76.58 32.24 123.59 o 12 9 0 301.99 96.72 112.84 o 13 9 0 557.89 569.59 145.08 o 14 9 0 59.19 -128.96 134.34 o 15 9 0 73.84 193.45 166.58 o 0 10 0 2381.90 2272.27 83.29 o 1 10 0 492.41 585.71 37.61 o 2 10 0 384.19 248.23 16.12 o 3 10 0 20.20 27.54 13.82 o 4 10 0 263.34 148.27 22.80 o 5 10 0 2227.77 1886.09 62.61 o 6 10 0 212.71 250.95 29.55 o 7 10 0 2029.90 1904.84 131.65 o 8 10 0 8069.71 7821.92 206.34 o 9 10 0 491.12 478.24 75.23 o 10 10 0 1248.96 934.99 96.72 o 11 10 0 1268.89 999.47 112.84 o 12 10 0 195.43 182.70 107.47 o 13 10 0 1151.20 1429.35 182.70 o 14 10 0 730.74 381.52 145.08 o 1 11 0 207.62 292.53 24.18 o 2 11 0 2250.28 2253.88 153.14 o 3 11 0 2541.41 2736.44 65.76 o 4 11 0 6469.85 6295.69 228.37 o 5 11 0 2990.33 2735.23 84.92 o 6 11 0 2236.31 2066.27 81.29 o 7 11 0 1710.44 1757.01 79.52 o 8 11 0 71.74 150.46 59.11 o 9 11 0 1567.77 1504.57 112.84 o 10 11 0 385.22 435.25 96.72 o 11 11 0 1533.73 1617.42 123.59 o 12 11 0 22.10 -59.11 80.60 o 13 11 0 288.31 263.30 112.84 o 14 11 0 30.86 295.54 128.96 o 0 12 0 4174.08 3885.03 177.32 o 1 12 0 1823.89 1838.10 42.59 o 2 12 0 3.95 -26.87 26.87 o 3 12 0 2215.66 2499.00 83.92 o 4 12 0 2025.70 2454.01 81.29 o 5 12 0 823.27 769.05 64.48 o 6 12 0 884.47 732.32 56.62 o 7 12 0 1452.90 1268.14 80.60 o 8 12 0 373.20 462.12 80.60 o 9 12 0 421.40 376.14 80.60 o 10 12 0 535.10 526.60 102.10 o 11 12 0 236.21 343.90 112.84 o 12 12 0 430.91 424.50 102.10 o 13 12 0 116.60 220.31 102.10 o 14 12 0 254.25 123.59 145.08 o 1 13 0 10277.64 10112.89 306.29 o 2 13 0 498.67 453.25 36.61 o 3 13 0 5691.13 5733.50 182.70 o 4 13 0 1695.61 1767.88 102.10 o 5 13 0 18.45 -26.87 64.48 o 6 13 0 2892.47 3256.33 166.58 o 7 13 0 154.57 96.72 80.60 o 8 13 0 630.72 526.60 96.72 o 9 13 0 3307.22 3030.64 145.08 o 10 13 0 411.98 488.99 91.35 o 11 13 0 14.18 171.95 96.72 o 12 13 0 16.36 21.49 96.72 o 13 13 0 650.11 553.47 139.71 o 0 14 0 4232.65 4175.19 204.19 o 1 14 0 45.86 102.10 59.11 o 2 14 0 223.47 408.38 75.23 o 3 14 0 4129.42 4116.09 155.83 o 4 14 0 211.85 354.65 85.98 o 5 14 0 1611.07 1805.49 118.22 o 6 14 0 1183.77 892.00 80.60 o 7 14 0 50.08 -75.23 91.35 o 8 14 0 151.39 -16.12 96.72 o 9 14 0 260.90 188.07 85.98 o 10 14 0 143.46 214.94 118.22 o 11 14 0 0.74 0.00 80.60 o 12 14 0 18.16 118.22 118.22 o 13 14 0 1046.39 961.85 139.71 o 1 15 0 33.23 91.35 53.73 o 2 15 0 941.89 1262.77 102.10 o 3 15 0 1351.40 1171.42 107.47 o 4 15 0 2435.63 2246.11 128.96 o 5 15 0 8101.60 8269.79 257.93 o 6 15 0 18.46 177.32 80.60 o 7 15 0 1131.37 1149.92 102.10 o 8 15 0 19.43 42.99 69.86 o 9 15 0 928.09 811.40 96.72 o 10 15 0 1762.04 1789.37 155.83 o 11 15 0 68.63 53.73 112.84 o 12 15 0 410.80 677.06 112.84 o 0 16 0 118.29 85.98 80.60 o 1 16 0 1599.29 1445.47 91.35 o 2 16 0 111.10 155.83 85.98 o 3 16 0 986.88 908.12 80.60 o 4 16 0 211.74 365.40 80.60 o 5 16 0 498.48 435.25 91.35 o 6 16 0 894.18 870.50 118.22 o 7 16 0 940.91 881.25 118.22 o 8 16 0 876.86 1273.51 145.08 o 9 16 0 17.66 -69.86 107.47 o 10 16 0 13.30 42.99 102.10 o 11 16 0 119.23 102.10 96.72 o 1 17 0 247.44 338.53 91.35 o 2 17 0 1102.51 999.47 85.98 o 3 17 0 2785.73 2751.22 134.34 o 4 17 0 1027.66 897.37 107.47 o 5 17 0 6.04 48.36 69.86 o 6 17 0 419.12 338.53 96.72 o 7 17 0 731.28 1139.18 134.34 o 8 17 0 18.85 -85.98 139.71 o 9 17 0 55.27 -80.60 80.60 o 10 17 0 1309.32 1235.90 123.59 o 11 17 0 44.04 171.95 155.83 o 0 18 0 52.59 -64.48 96.72 o 1 18 0 32.58 -75.23 75.23 o 2 18 0 375.07 155.83 85.98 o 3 18 0 107.66 112.84 64.48 o 4 18 0 1664.61 1612.04 128.96 o 5 18 0 1.78 118.22 85.98 o 6 18 0 318.99 376.14 107.47 o 7 18 0 758.04 956.48 123.59 o 8 18 0 94.62 145.08 107.47 o 9 18 0 0.39 -16.12 112.84 o 10 18 0 225.11 53.73 145.08 o 1 19 0 7.50 102.10 91.35 o 2 19 0 3025.39 3508.88 166.58 o 3 19 0 40.49 -10.75 107.47 o 4 19 0 12.63 -10.75 80.60 o 5 19 0 231.78 155.83 102.10 o 6 19 0 76.72 0.00 85.98 o 7 19 0 78.62 10.75 85.98 o 8 19 0 163.81 284.79 123.59 o 9 19 0 218.10 231.06 96.72 o 0 20 0 13.01 381.52 209.57 o 1 20 0 692.11 886.62 145.08 o 2 20 0 18.60 145.08 91.35 o 3 20 0 1356.27 1483.08 123.59 o 4 20 0 462.74 386.89 107.47 o 5 20 0 216.65 306.29 102.10 o 6 20 0 1140.74 1198.29 150.46 o 7 20 0 111.90 -32.24 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1850.11 333.16 o -13 1 1 1272.24 1227.11 212.25 o -12 1 1 29.67 -60.25 89.23 o -11 1 1 1987.55 1954.25 120.90 o -10 1 1 3904.19 3807.72 370.77 o -9 1 1 528.83 499.94 64.48 o -8 1 1 95.25 132.60 58.80 o -7 1 1 54.35 45.82 35.95 o -6 1 1 5992.34 5484.41 130.99 o -5 1 1 4020.43 4763.39 132.34 o -4 1 1 3925.63 3652.64 96.72 o -3 1 1 16062.05 17277.26 292.25 o -2 1 1 30152.17 31743.38 1265.46 o 2 1 1 352.86 217.66 11.40 o 3 1 1 10147.41 12916.84 191.85 o 4 1 1 26857.29 25032.67 418.30 o 5 1 1 89.52 21.49 37.61 o 6 1 1 9285.28 8879.65 298.23 o 7 1 1 1708.50 1110.57 47.38 o 8 1 1 1158.46 1103.33 61.98 o 9 1 1 6680.75 6443.45 220.31 o 10 1 1 34.65 157.85 60.44 o 11 1 1 4.34 -53.73 107.47 o 12 1 1 370.37 478.48 107.84 o 13 1 1 2178.72 2119.38 136.15 o 14 1 1 95.54 181.96 161.20 o 15 1 1 1660.66 1386.99 155.23 o 16 1 1 672.68 916.77 214.11 o -16 2 1 4.38 82.67 148.04 o -15 2 1 861.37 958.58 134.27 o -14 2 1 52.07 137.02 125.39 o -13 2 1 104.20 118.11 88.47 o -12 2 1 56.89 37.61 139.71 o -11 2 1 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-10 3 1 72.99 155.83 69.53 o -9 3 1 1033.24 1230.62 83.29 o -8 3 1 5449.18 5492.02 174.66 o -7 3 1 630.22 787.99 102.10 o -6 3 1 21931.17 23723.57 550.88 o -5 3 1 181.43 98.87 48.36 o -4 3 1 22891.08 19564.90 398.79 o -3 3 1 2254.79 2434.45 61.80 o -2 3 1 2257.85 2190.64 52.68 o -1 3 1 23187.88 26164.38 478.64 o 0 3 1 1100.25 1238.45 27.65 o 1 3 1 5700.16 6951.46 118.27 o 2 3 1 44.01 96.72 11.40 o 3 3 1 35363.50 38256.33 652.34 o 4 3 1 6188.15 4420.84 113.23 o 5 3 1 2884.25 3353.43 79.52 o 6 3 1 3817.29 3682.30 85.43 o 7 3 1 3322.69 3521.99 89.23 o 8 3 1 10708.96 10825.93 263.30 o 9 3 1 430.50 496.12 65.76 o 10 3 1 2166.98 1988.73 128.96 o 11 3 1 1.90 73.63 64.26 o 12 3 1 142.13 20.55 158.52 o 13 3 1 47.17 75.90 89.07 o 14 3 1 3407.53 3445.36 212.25 o 15 3 1 340.92 478.24 231.06 o 16 3 1 383.11 -26.87 145.08 o -16 4 1 907.92 1112.31 209.57 o -15 4 1 403.78 360.02 134.34 o -14 4 1 211.60 228.27 93.42 o -13 4 1 2.65 -19.34 91.35 o -12 4 1 625.21 1000.88 94.99 o -11 4 1 1664.28 1017.17 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126.28 o -9 2 28 1111.26 1017.89 121.59 o -8 2 28 109.19 13.85 85.43 o -7 2 28 312.79 291.31 142.40 o -6 2 28 1267.22 1186.39 112.04 o -5 2 28 426.87 495.31 166.58 o -4 2 28 1041.71 1140.59 109.99 o -3 2 28 62.78 -59.49 104.57 o -2 2 28 547.08 620.62 126.28 o -1 2 28 445.60 558.27 96.83 o 0 2 28 0.47 42.80 104.57 o -9 3 28 325.60 357.20 111.65 o -8 3 28 2.72 48.36 112.84 o -7 3 28 718.06 617.50 161.20 o -6 3 28 29.12 28.33 82.56 o -5 3 28 1182.30 772.87 109.99 o -4 3 28 274.43 126.22 85.43 o -3 3 28 37.75 -94.18 94.18 o -2 3 28 1067.02 1017.52 134.34 o -1 3 28 356.03 351.96 163.89 o 0 3 28 141.99 93.14 107.47 o -8 4 28 104.36 245.92 96.39 o -7 4 28 810.41 890.53 119.99 o -6 4 28 10.44 -58.51 100.70 o -5 4 28 178.60 224.14 110.16 o -4 4 28 4.88 -96.72 96.72 o -3 4 28 1792.95 1597.05 209.57 o -2 4 28 40.87 228.71 104.44 o -1 4 28 81.49 71.65 102.38 o 0 4 28 232.24 222.91 139.71 o -8 5 28 21.23 55.69 100.36 o -7 5 28 546.71 449.00 128.96 o -6 5 28 283.57 267.91 171.95 o -5 5 28 149.86 -18.85 111.65 o -4 5 28 43.22 251.36 100.70 o -3 5 28 399.22 384.05 150.46 o -2 5 28 81.38 73.51 100.64 o -1 5 28 1194.56 1343.60 427.19 o -7 6 28 1188.10 1276.05 212.25 o -6 6 28 159.44 233.80 260.61 o -5 6 28 9.30 178.07 109.41 o -4 6 28 210.69 251.91 94.76 o -3 6 28 656.86 720.19 121.13 o -2 6 28 17.60 147.06 104.30 o -6 7 28 74.89 110.16 131.65 o -5 7 28 268.68 214.65 106.19 o -4 7 28 714.41 801.58 378.83 o -3 7 28 9.07 169.26 111.88 o -7 0 29 1018.76 1101.56 204.19 o -5 0 29 589.40 467.49 155.83 o -3 0 29 24.49 -48.36 150.46 o -7 1 29 188.58 378.59 104.02 o -6 1 29 707.02 662.59 100.64 o -5 1 29 123.28 156.20 150.46 o -4 1 29 58.31 -76.96 212.25 o -3 1 29 656.21 290.36 101.97 o -2 1 29 627.52 540.79 117.60 o -7 2 29 210.93 312.15 225.69 o -6 2 29 1554.73 1145.35 130.06 o -5 2 29 166.89 177.01 96.39 o -4 2 29 4.39 44.66 85.43 o -3 2 29 531.67 268.93 114.87 o -2 2 29 150.10 207.15 92.57 o -6 3 29 2.56 63.97 303.60 o -5 3 29 18.97 54.13 123.59 o -4 3 29 5.30 2.79 94.08 o -3 3 29 2390.36 2286.24 177.32 o -2 3 29 266.85 142.67 113.80 o -6 4 29 780.71 677.06 300.91 o -5 4 29 333.04 307.43 123.59 o -4 4 29 960.97 578.60 108.24 o -3 4 29 424.54 387.78 290.17 o