#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200580.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200580_Fobs loop_ _publ_author_name 'Niemeyer, Mark' _publ_section_title ; A tetranuclear copper compound containing three different types of anions: trans-(\m-tert-butoxy)bis(\m-2,4,6,2'',4'',6''-hexamethyl-1,1':3',1''-terphenyl-2',2'-diyl)(\m-iodo)tetracopper(I) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m416 _journal_page_last m418 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.734 _cell_angle_beta 80.137 _cell_angle_gamma 72.592 _cell_length_a 12.3307 _cell_length_b 12.6105 _cell_length_c 16.3613 _exptl_crystal_F_000 1096.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ya6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nie29 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7119.73 7024.01 149.93 o 3 0 0 71614.07 73366.41 441.44 o 4 0 0 9629.09 9978.64 220.72 o 5 0 0 930.37 839.40 170.00 o 6 0 0 67.51 74.13 180.03 o 7 0 0 8209.69 7852.27 283.70 o 8 0 0 0.23 137.11 198.42 o 9 0 0 2.17 167.77 241.34 o 10 0 0 171.98 171.67 157.74 o 11 0 0 733.93 957.57 181.70 o 12 0 0 2794.88 2729.45 256.39 o 13 0 0 252.39 192.29 199.54 o 14 0 0 514.80 506.65 212.92 o -13 1 0 1695.96 1746.25 228.52 o -12 1 0 243.42 175.57 182.82 o -11 1 0 114.84 -11.70 173.90 o -10 1 0 32.94 -10.59 157.74 o 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