#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/06/2200610.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200610_Fobs loop_ _publ_author_name 'Davies, John E.' 'Kirby, Anthony J.' 'Roussev, Christo D.' _publ_section_title ; Pentacyclohexyloxyphosphorane ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o994 _journal_page_last o995 _journal_volume 57 _journal_year 2001 _space_group_IT_number 1 _symmetry_space_group_name_Hall 'P 1' _symmetry_space_group_name_H-M 'P 1' _cell_angle_alpha 88.403 _cell_angle_beta 88.589 _cell_angle_gamma 90.021 _cell_length_a 10.0853 _cell_length_b 10.0892 _cell_length_c 30.1129 _exptl_crystal_F_000 1160.00 _reflns_d_resolution_high 0.8401 _[local]_cod_data_source_file cf6107Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ak0003 in P1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 153.42 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma 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18.42 o 3 -4 32 20.62 37.41 16.93 o -3 -3 32 2.91 -4.33 12.50 o -2 -3 32 68.17 57.56 14.33 o -1 -3 32 0.95 16.30 13.46 o 0 -3 32 27.33 39.05 12.60 o 1 -3 32 60.55 53.33 14.09 o 2 -3 32 39.13 56.89 12.89 o 3 -3 32 34.98 45.30 13.90 o 4 -3 32 52.46 47.70 11.20 o -1 -4 33 8.51 14.38 16.30 o 0 -4 33 109.26 122.62 18.47 o 1 -4 33 145.47 158.45 20.44 o 2 -4 33 104.43 103.97 18.80 o -1 -3 33 25.58 47.13 12.94 o