#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200739.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200739_Fobs loop_ _publ_author_name 'Batsanov, Andrei S.' 'Howard, Judith A. K.' 'Moore, Nichola S.' 'Kilner, Melvyn' _publ_section_title ; Hexaaquanickel(II) bis(p-tolylsulfonate) ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m485 _journal_page_last m487 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.719 _cell_angle_gamma 90.000 _cell_length_a 6.9140 _cell_length_b 6.2990 _cell_length_c 24.9330 _exptl_crystal_F_000 532.00 _reflns_d_resolution_high 0.7331 _[local]_cod_data_source_file om6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 97srv116 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.86 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 30991.83 29696.04 561.50 o 4 0 0 15242.49 15331.82 396.50 o 6 0 0 5065.33 5123.49 148.33 o 8 0 0 739.29 742.75 42.67 o 1 1 0 34173.78 33702.20 423.54 o 2 1 0 4856.88 4901.35 64.71 o 3 1 0 2058.37 1941.55 44.51 o 4 1 0 1510.29 1595.67 26.16 o 5 1 0 5607.30 5502.96 90.57 o 6 1 0 822.99 860.14 27.40 o 7 1 0 993.35 1041.34 33.55 o 8 1 0 209.77 204.78 20.10 o 9 1 0 243.50 365.89 31.05 o 0 2 0 4915.91 5264.71 97.83 o 1 2 0 274.49 323.20 11.58 o 2 2 0 189.73 247.86 6.90 o 3 2 0 1467.80 1556.56 24.08 o 4 2 0 901.25 876.85 19.70 o 5 2 0 187.56 195.63 13.61 o 6 2 0 1832.85 1741.30 31.54 o 7 2 0 524.53 449.86 22.96 o 8 2 0 352.46 281.33 29.93 o 9 2 0 10.11 -17.17 23.65 o 1 3 0 2297.02 2396.39 35.02 o 2 3 0 94.44 123.00 19.26 o 3 3 0 302.83 301.25 8.83 o 4 3 0 24.59 16.92 6.98 o 5 3 0 1714.47 1727.51 30.20 o 6 3 0 86.85 94.35 19.11 o 7 3 0 912.38 847.36 19.39 o 8 3 0 81.72 94.51 19.79 o 0 4 0 46.75 30.06 6.33 o 1 4 0 6.63 6.52 7.19 o 2 4 0 4.06 7.10 4.27 o 3 4 0 2.29 31.39 19.61 o 4 4 0 27.56 26.72 7.54 o 5 4 0 33.88 52.11 7.13 o 6 4 0 162.21 144.55 13.32 o 7 4 0 75.28 108.84 11.87 o 8 4 0 4.71 -20.55 13.70 o 1 5 0 32.66 64.67 13.90 o 2 5 0 15.80 22.00 17.19 o 3 5 0 218.93 239.01 24.57 o 4 5 0 61.61 76.22 12.11 o 5 5 0 69.17 31.75 8.11 o 6 5 0 11.19 69.93 23.09 o 7 5 0 17.10 -31.11 26.49 o 0 6 0 325.59 332.64 23.23 o 1 6 0 0.02 27.72 9.16 o 2 6 0 316.18 315.36 33.26 o 3 6 0 40.68 59.20 9.02 o 4 6 0 14.73 16.97 15.61 o 5 6 0 2.88 11.88 23.09 o 6 6 0 152.82 116.03 18.10 o 1 7 0 370.70 329.24 18.69 o 2 7 0 11.17 -1.60 21.78 o 3 7 0 74.91 39.93 14.44 o 4 7 0 0.29 35.07 25.47 o 5 7 0 202.98 179.60 27.03 o 0 8 0 558.37 588.61 35.96 o 1 8 0 0.58 -27.70 20.55 o 2 8 0 92.85 56.74 27.25 o 3 8 0 29.52 40.43 28.82 o -9 0 1 44.97 37.75 23.01 o -7 0 1 93.16 164.41 20.77 o -5 0 1 47.94 50.04 12.06 o -3 0 1 321.02 291.73 10.42 o -1 0 1 176.30 201.08 5.66 o 1 0 1 70.99 108.63 16.08 o 3 0 1 795.25 893.14 47.92 o 5 0 1 20.65 22.78 10.72 o 7 0 1 15.78 32.39 16.98 o 9 0 1 38.15 28.37 26.81 o -9 1 1 35.72 47.70 22.78 o -8 1 1 111.84 99.73 25.47 o -7 1 1 18.50 14.75 11.20 o -6 1 1 29.51 22.52 14.07 o -5 1 1 625.36 637.19 17.82 o -4 1 1 920.71 960.39 22.87 o -3 1 1 18.91 24.89 4.72 o -2 1 1 126.29 165.18 5.26 o -1 1 1 27.10 35.44 2.55 o 0 1 1 90.40 89.82 8.25 o 1 1 1 77.05 75.18 4.48 o 2 1 1 37.96 24.00 4.66 o 3 1 1 16.58 10.96 5.26 o 4 1 1 856.08 959.94 17.85 o 5 1 1 0.10 22.47 13.06 o 6 1 1 83.05 67.83 11.19 o 7 1 1 81.74 119.25 16.98 o 8 1 1 80.11 143.66 17.46 o 9 1 1 0.94 54.08 20.22 o -9 2 1 37.49 88.11 29.62 o -8 2 1 21.37 -10.68 10.52 o -7 2 1 103.90 117.38 10.96 o -6 2 1 138.29 109.18 15.28 o -5 2 1 174.19 180.34 10.22 o -4 2 1 540.42 542.58 34.43 o -3 2 1 2598.70 2550.95 29.75 o -2 2 1 56.75 66.69 7.69 o -1 2 1 246.13 231.70 8.09 o 0 2 1 813.69 793.42 20.34 o 1 2 1 22.70 31.95 2.79 o 2 2 1 11.09 18.43 7.77 o 3 2 1 1045.50 1080.27 35.85 o 4 2 1 61.83 64.49 18.31 o 5 2 1 22.70 37.09 13.12 o 6 2 1 1.75 9.81 8.36 o 7 2 1 8.53 -15.51 10.34 o 8 2 1 1.77 50.27 16.05 o 9 2 1 117.22 155.45 18.75 o -8 3 1 191.34 220.95 16.56 o -7 3 1 7.06 45.02 21.75 o -6 3 1 188.74 207.38 16.92 o -5 3 1 878.52 863.33 22.31 o -4 3 1 1136.72 1105.00 18.59 o -3 3 1 81.56 100.15 9.98 o -2 3 1 3928.04 3731.67 124.23 o -1 3 1 1756.31 1805.94 27.47 o 0 3 1 60.03 26.53 5.19 o 1 3 1 1030.11 1120.29 18.82 o 2 3 1 3902.08 3928.23 54.77 o 3 3 1 356.99 371.55 17.02 o 4 3 1 979.16 977.22 28.85 o 5 3 1 25.83 10.47 21.87 o 6 3 1 66.53 89.37 9.48 o 7 3 1 1.84 12.47 8.16 o 8 3 1 349.61 352.16 18.77 o -8 4 1 8.54 -1.44 18.35 o -7 4 1 397.13 470.51 20.89 o -6 4 1 65.84 87.32 14.57 o -5 4 1 416.90 442.00 13.31 o -4 4 1 194.57 224.73 18.31 o -3 4 1 3969.15 4136.69 59.72 o -2 4 1 67.41 80.55 9.93 o -1 4 1 1637.21 1590.93 26.24 o 0 4 1 971.81 1108.91 19.79 o 1 4 1 2468.26 2369.24 46.69 o 2 4 1 357.50 388.42 10.77 o 3 4 1 8107.52 8016.41 186.49 o 4 4 1 109.35 126.81 17.09 o 5 4 1 976.01 945.75 18.75 o 6 4 1 34.60 31.76 7.51 o 7 4 1 1021.52 1064.15 28.55 o 8 4 1 7.42 50.21 18.11 o -7 5 1 0.04 -15.80 10.53 o -6 5 1 271.61 311.79 21.73 o -5 5 1 1.28 11.22 9.43 o -4 5 1 633.81 688.34 19.12 o -3 5 1 85.07 76.10 12.09 o -2 5 1 2534.24 2648.23 41.85 o -1 5 1 15.78 22.28 5.20 o 0 5 1 39.37 49.75 7.09 o 1 5 1 30.74 40.40 11.90 o 2 5 1 4791.88 4687.82 67.71 o 3 5 1 0.00 -2.52 9.16 o 4 5 1 1510.74 1568.07 29.30 o 5 5 1 12.59 24.47 7.49 o 6 5 1 590.93 555.34 32.24 o 7 5 1 18.87 94.57 11.68 o -6 6 1 11.15 65.55 17.64 o -5 6 1 267.61 304.01 38.37 o -4 6 1 13.01 -11.27 7.51 o -3 6 1 1568.10 1618.01 38.72 o -2 6 1 6.97 24.53 7.77 o -1 6 1 420.41 461.56 15.07 o 0 6 1 53.73 49.17 7.24 o 1 6 1 431.62 445.50 15.23 o 2 6 1 61.46 82.45 10.38 o 3 6 1 1862.56 1929.97 34.74 o 4 6 1 0.04 -17.12 11.41 o 5 6 1 142.42 144.07 27.34 o 6 6 1 0.00 48.41 71.26 o -5 7 1 69.44 72.82 23.90 o -4 7 1 682.32 609.39 39.54 o -3 7 1 4.12 95.83 20.55 o -2 7 1 1422.86 1453.84 81.42 o -1 7 1 11.83 10.47 22.78 o 0 7 1 282.59 316.57 18.86 o 1 7 1 18.23 94.32 16.53 o 2 7 1 1395.91 1550.13 44.35 o 3 7 1 16.38 66.78 50.71 o 4 7 1 552.51 610.06 41.55 o 5 7 1 5.81 -28.82 19.21 o -3 8 1 214.36 174.91 31.27 o -2 8 1 26.49 7.59 24.57 o -1 8 1 84.31 75.28 21.00 o 0 8 1 71.44 -25.02 21.22 o 1 8 1 78.82 54.06 21.89 o 2 8 1 46.14 7.82 21.89 o 3 8 1 239.89 205.29 31.05 o -8 0 2 369.29 384.89 30.83 o -6 0 2 846.68 834.78 38.42 o -4 0 2 1320.48 1323.76 44.90 o -2 0 2 770.62 890.72 19.89 o 0 0 2 7207.92 5946.96 106.30 o 2 0 2 1993.60 2172.54 43.04 o 4 0 2 4697.14 4607.03 128.44 o 6 0 2 4324.99 4119.16 123.53 o 8 0 2 1156.15 1116.69 54.51 o -9 1 2 61.87 97.16 49.93 o -8 1 2 256.90 221.07 19.18 o -7 1 2 288.87 274.26 18.54 o -6 1 2 333.92 345.26 20.36 o -5 1 2 410.91 412.04 16.50 o -4 1 2 97.74 98.06 7.48 o -3 1 2 40.59 73.13 8.14 o -2 1 2 2670.17 2598.26 67.84 o -1 1 2 273.28 296.42 4.91 o 0 1 2 3790.48 3714.25 68.26 o 1 1 2 400.49 403.62 6.75 o 2 1 2 10654.54 10900.82 185.39 o 3 1 2 445.38 584.40 18.77 o 4 1 2 3859.52 3941.84 62.90 o 5 1 2 2869.67 2858.68 52.72 o 6 1 2 918.56 960.42 44.34 o 7 1 2 552.51 533.12 37.42 o 8 1 2 157.96 144.78 17.12 o 9 1 2 242.33 233.47 46.13 o -9 2 2 13.68 26.29 14.54 o -8 2 2 57.69 106.12 57.92 o -7 2 2 154.38 157.72 10.55 o -6 2 2 125.61 135.92 14.11 o -5 2 2 109.00 106.48 18.25 o -4 2 2 237.38 228.82 9.32 o -3 2 2 363.81 376.98 14.44 o -2 2 2 228.60 180.88 6.15 o -1 2 2 71.33 69.15 5.87 o 0 2 2 7960.95 8296.55 107.09 o 1 2 2 1842.99 1698.17 32.44 o 2 2 2 58.71 53.60 7.64 o 3 2 2 2143.03 2264.52 86.11 o 4 2 2 289.27 250.09 7.12 o 5 2 2 1629.40 1703.70 29.66 o 6 2 2 439.29 441.46 13.74 o 7 2 2 275.94 281.63 27.05 o 8 2 2 4.08 -36.14 45.79 o 9 2 2 171.17 204.55 22.84 o -8 3 2 102.02 146.09 17.77 o -7 3 2 209.24 245.41 15.11 o -6 3 2 293.50 270.38 12.46 o -5 3 2 890.82 861.37 21.42 o -4 3 2 268.61 254.86 15.14 o -3 3 2 1913.88 1849.24 31.40 o -2 3 2 2857.37 2780.39 75.19 o -1 3 2 6749.59 6740.38 246.62 o 0 3 2 776.16 819.25 17.86 o 1 3 2 7352.44 7640.61 100.80 o 2 3 2 1459.90 1630.52 39.34 o 3 3 2 1230.38 1301.39 43.33 o 4 3 2 758.99 706.31 17.77 o 5 3 2 1020.16 959.83 18.33 o 6 3 2 310.65 294.76 16.00 o 7 3 2 193.09 196.25 12.36 o 8 3 2 179.05 200.58 29.76 o -8 4 2 202.50 230.38 28.63 o -7 4 2 530.00 527.43 16.06 o -6 4 2 580.52 582.56 37.53 o -5 4 2 604.73 587.91 32.66 o -4 4 2 806.67 852.12 23.54 o -3 4 2 2048.72 2125.20 34.22 o -2 4 2 1421.25 1471.82 43.60 o -1 4 2 1708.43 1829.44 41.35 o 0 4 2 1316.21 1395.53 29.28 o 1 4 2 1115.11 1188.01 21.08 o 2 4 2 841.33 945.88 25.92 o 3 4 2 294.73 336.17 16.80 o 4 4 2 18.89 51.69 25.44 o 5 4 2 195.76 152.35 8.29 o 6 4 2 307.05 315.70 35.66 o 7 4 2 26.37 51.62 19.60 o 8 4 2 2.83 -2.49 11.45 o -7 5 2 159.60 196.75 45.11 o -6 5 2 18.48 38.95 14.87 o -5 5 2 329.87 301.78 19.57 o -4 5 2 1.74 -9.10 6.07 o -3 5 2 177.16 217.61 17.89 o -2 5 2 14.06 8.06 5.42 o -1 5 2 73.30 73.61 15.93 o 0 5 2 26.91 54.67 17.85 o 1 5 2 49.57 35.34 11.69 o 2 5 2 83.97 80.44 6.99 o 3 5 2 7.94 27.76 6.35 o 4 5 2 21.67 24.62 11.58 o 5 5 2 4.03 1.16 9.14 o 6 5 2 7.48 12.18 18.73 o 7 5 2 35.75 68.89 13.08 o -6 6 2 228.18 203.81 19.66 o -5 6 2 18.25 72.98 14.83 o -4 6 2 200.07 227.99 14.22 o -3 6 2 481.75 423.94 16.08 o -2 6 2 408.83 475.06 17.20 o -1 6 2 143.14 144.22 17.73 o 0 6 2 296.93 307.49 11.21 o 1 6 2 124.12 116.74 15.90 o 2 6 2 509.73 445.02 19.73 o 3 6 2 119.83 139.96 25.25 o 4 6 2 26.85 43.17 17.34 o 5 6 2 17.24 3.95 16.46 o 6 6 2 302.41 326.05 39.94 o -5 7 2 214.47 251.53 30.83 o -4 7 2 23.35 13.40 24.13 o -3 7 2 216.03 209.62 30.49 o -2 7 2 275.82 305.93 50.04 o -1 7 2 467.49 470.10 35.62 o 0 7 2 0.68 8.37 42.04 o 1 7 2 547.90 495.37 48.46 o 2 7 2 140.89 162.18 28.70 o 3 7 2 192.02 195.11 14.25 o 4 7 2 40.62 -22.95 15.30 o 5 7 2 247.11 159.49 31.27 o -3 8 2 395.97 359.64 32.39 o -2 8 2 108.29 92.03 25.47 o -1 8 2 79.47 48.25 23.68 o 0 8 2 377.87 385.78 33.06 o 1 8 2 139.09 29.71 22.56 o 2 8 2 100.00 74.61 23.46 o 3 8 2 185.92 178.04 33.95 o -9 0 3 273.09 358.30 39.09 o -7 0 3 1302.77 1376.70 55.62 o -5 0 3 1920.91 2125.48 68.58 o -3 0 3 5938.80 5937.61 116.72 o -1 0 3 17095.61 16236.96 409.01 o 1 0 3 11952.52 11369.41 143.97 o 3 0 3 4816.28 5014.24 184.96 o 5 0 3 1411.33 1500.68 53.16 o 7 0 3 48.66 95.16 19.66 o 9 0 3 265.06 332.17 36.41 o -9 1 3 86.36 125.69 32.73 o -8 1 3 476.10 453.41 41.21 o -7 1 3 21.11 41.99 22.11 o -6 1 3 1122.19 1159.86 28.29 o -5 1 3 325.51 358.92 12.51 o -4 1 3 1555.17 1570.73 34.27 o -3 1 3 71.27 61.16 4.54 o -2 1 3 1967.41 1944.61 54.68 o -1 1 3 1778.17 1837.71 43.15 o 0 1 3 6212.12 5921.59 119.11 o 1 1 3 3173.42 3232.74 65.68 o 2 1 3 1306.71 1377.94 57.56 o 3 1 3 1910.04 2004.08 26.95 o 4 1 3 3451.37 3467.06 50.08 o 5 1 3 1001.26 1114.57 25.05 o 6 1 3 74.18 73.68 8.99 o 7 1 3 326.80 327.69 44.12 o 8 1 3 231.35 217.30 19.53 o 9 1 3 55.47 70.56 17.77 o -9 2 3 269.25 268.41 36.98 o -8 2 3 214.49 191.14 15.18 o -7 2 3 819.93 864.22 25.88 o -6 2 3 410.98 378.43 16.12 o -5 2 3 1013.76 969.52 38.53 o -4 2 3 762.33 790.93 13.91 o -3 2 3 814.80 731.80 11.80 o -2 2 3 83.02 118.91 6.06 o -1 2 3 532.63 556.41 12.40 o 0 2 3 4824.19 4653.75 66.84 o 1 2 3 498.77 516.65 9.61 o 2 2 3 35.75 44.16 11.42 o 3 2 3 2169.58 2177.76 38.20 o 4 2 3 906.19 1001.18 17.16 o 5 2 3 739.11 757.58 20.93 o 6 2 3 554.73 530.39 28.50 o 7 2 3 263.78 247.80 14.26 o 8 2 3 151.87 184.57 18.88 o 9 2 3 287.86 304.25 35.52 o -8 3 3 344.01 343.91 24.67 o -7 3 3 387.30 405.43 25.99 o -6 3 3 1346.47 1344.38 26.74 o -5 3 3 2428.31 2567.62 66.52 o -4 3 3 1779.94 1765.91 29.29 o -3 3 3 307.75 331.73 11.12 o -2 3 3 2794.96 2745.26 39.85 o -1 3 3 2887.73 2936.62 41.78 o 0 3 3 1851.88 1762.70 38.50 o 1 3 3 1146.47 1278.12 30.76 o 2 3 3 3501.95 3467.36 68.35 o 3 3 3 343.09 289.86 22.08 o 4 3 3 1631.00 1633.01 28.19 o 5 3 3 780.37 777.83 25.39 o 6 3 3 633.00 638.43 20.73 o 7 3 3 520.00 525.62 36.34 o 8 3 3 796.08 775.69 30.76 o -8 4 3 33.38 -27.91 36.96 o -7 4 3 101.30 77.12 15.44 o -6 4 3 331.60 330.32 13.35 o -5 4 3 915.06 939.22 26.72 o -4 4 3 789.61 796.51 20.37 o -3 4 3 1283.26 1275.17 23.79 o -2 4 3 149.66 154.59 13.03 o -1 4 3 1401.39 1384.75 25.76 o 0 4 3 1863.81 2052.32 37.40 o 1 4 3 1260.38 1235.71 21.88 o 2 4 3 81.07 71.13 13.25 o 3 4 3 2260.99 2331.07 40.53 o 4 4 3 291.31 310.88 16.53 o 5 4 3 189.24 176.91 10.97 o 6 4 3 269.21 279.68 15.48 o 7 4 3 687.06 672.29 24.29 o 8 4 3 125.28 158.24 15.83 o -7 5 3 40.44 71.34 19.10 o -6 5 3 81.79 110.43 33.84 o -5 5 3 0.49 -2.09 11.34 o -4 5 3 215.56 220.61 10.22 o -3 5 3 44.66 38.70 8.58 o -2 5 3 711.89 714.16 22.92 o -1 5 3 4.33 27.01 5.53 o 0 5 3 140.43 132.10 12.32 o 1 5 3 2.49 11.50 12.70 o 2 5 3 1498.36 1489.48 38.20 o 3 5 3 97.27 106.49 12.80 o 4 5 3 138.12 143.04 14.06 o 5 5 3 30.53 41.35 21.92 o 6 5 3 109.54 127.74 18.15 o 7 5 3 32.69 12.42 23.22 o -6 6 3 36.81 28.24 28.70 o -5 6 3 186.42 135.92 33.95 o -4 6 3 104.18 121.43 15.68 o -3 6 3 284.13 274.05 13.35 o -2 6 3 30.44 18.16 8.38 o -1 6 3 518.34 519.39 16.42 o 0 6 3 33.15 14.44 16.39 o 1 6 3 781.65 789.19 21.38 o 2 6 3 30.83 14.95 8.25 o 3 6 3 1322.23 1339.73 39.46 o 4 6 3 60.69 89.42 29.19 o 5 6 3 114.64 122.65 13.11 o 6 6 3 54.43 131.00 25.21 o -5 7 3 272.73 297.57 30.72 o -4 7 3 161.91 167.17 18.31 o -3 7 3 187.59 143.62 18.92 o -2 7 3 356.38 386.57 21.60 o -1 7 3 410.00 427.32 22.01 o 0 7 3 310.94 246.63 13.76 o 1 7 3 194.21 199.45 13.15 o 2 7 3 924.20 893.97 25.01 o 3 7 3 113.35 104.15 22.81 o 4 7 3 436.49 370.87 68.41 o 5 7 3 29.47 30.57 15.01 o -3 8 3 182.65 155.25 31.05 o -2 8 3 406.92 411.92 36.19 o -1 8 3 153.27 207.75 27.92 o 0 8 3 784.18 887.05 47.13 o 1 8 3 93.61 58.97 23.68 o 2 8 3 348.47 343.78 34.85 o 3 8 3 144.15 279.23 38.42 o -8 0 4 21.77 15.64 18.54 o -6 0 4 272.11 249.74 20.33 o -4 0 4 2.77 1.07 5.13 o -2 0 4 1345.16 1388.54 40.43 o 0 0 4 2779.80 2501.60 93.31 o 2 0 4 221.57 262.18 9.15 o 4 0 4 1455.66 1452.68 35.52 o 6 0 4 69.35 40.21 14.07 o 8 0 4 2.02 2.46 19.43 o -9 1 4 26.31 68.24 16.69 o -8 1 4 39.42 1.52 35.74 o -7 1 4 121.44 132.76 31.72 o -6 1 4 223.18 250.29 12.23 o -5 1 4 29.30 49.61 10.17 o 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