#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/07/2200782.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200782_Fobs loop_ _publ_author_name 'Blake, Alexander J.' 'Cooke, Paul A.' 'Hubberstey, Peter' 'Sampson, Claire L.' _publ_section_title ; Zinc(II) sulfate tetrahydrate ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i109 _journal_page_last i111 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.260 _cell_angle_gamma 90.000 _cell_length_a 5.9040 _cell_length_b 13.5190 _cell_length_c 7.8830 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.8418 _[local]_cod_data_source_file wn6062Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' znptpd in P 21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 177.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 145.30 217.40 61.30 o 4 0 0 527.89 576.97 91.82 o 6 0 0 1100.84 1096.36 136.77 o 1 1 0 11802.49 12063.90 158.53 o 2 1 0 3432.13 3862.27 134.47 o 3 1 0 172.19 180.38 68.88 o 4 1 0 109.81 9.98 56.21 o 5 1 0 94.11 124.46 68.79 o 6 1 0 882.92 913.07 141.44 o 7 1 0 1556.43 1250.02 178.59 o 0 2 0 2258.81 2400.39 70.32 o 1 2 0 11629.30 12744.66 171.58 o 2 2 0 1604.46 1640.82 100.72 o 3 2 0 5673.36 6456.63 205.24 o 4 2 0 179.58 122.44 66.32 o 5 2 0 1131.61 1348.91 141.22 o 6 2 0 234.00 164.00 77.78 o 1 3 0 3342.28 3095.61 111.53 o 2 3 0 58.09 93.52 52.34 o 3 3 0 1376.61 1757.03 121.42 o 4 3 0 2415.77 2319.76 159.49 o 5 3 0 39.93 74.83 69.71 o 6 3 0 2771.94 2953.20 233.27 o 0 4 0 29141.00 29248.21 290.02 o 1 4 0 8760.89 8479.84 184.51 o 2 4 0 145.57 203.13 60.15 o 3 4 0 599.42 638.14 86.48 o 4 4 0 144.04 59.22 60.60 o 5 4 0 988.95 1067.18 135.14 o 6 4 0 1750.10 2192.62 197.34 o 1 5 0 5625.80 5069.07 158.46 o 2 5 0 80.45 72.11 55.41 o 3 5 0 108.28 208.34 68.31 o 4 5 0 149.27 121.96 75.50 o 5 5 0 22.13 56.56 60.24 o 6 5 0 0.57 27.13 79.12 o 0 6 0 28408.31 29612.27 372.76 o 1 6 0 62.88 186.46 60.50 o 2 6 0 107.63 18.17 49.49 o 3 6 0 1043.91 1076.55 106.28 o 4 6 0 351.09 425.42 92.49 o 5 6 0 789.16 960.70 129.86 o 6 6 0 405.33 431.05 107.75 o 1 7 0 5.25 10.59 53.01 o 2 7 0 3918.03 4086.29 177.02 o 3 7 0 542.72 580.01 91.50 o 4 7 0 269.27 403.18 90.51 o 5 7 0 1.01 -18.08 64.31 o 6 7 0 2595.46 2805.65 231.76 o 0 8 0 3311.57 3090.46 153.99 o 1 8 0 9461.90 9944.32 263.56 o 2 8 0 59.66 -33.72 48.69 o 3 8 0 2737.37 3163.27 175.07 o 4 8 0 99.08 44.06 66.96 o 5 8 0 649.41 866.20 121.00 o 6 8 0 113.70 -28.06 89.26 o 1 9 0 4781.12 4633.38 197.69 o 2 9 0 176.65 200.50 73.81 o 3 9 0 972.71 985.76 125.06 o 4 9 0 428.30 659.90 107.79 o 5 9 0 134.11 209.21 78.74 o 0 10 0 6668.91 6452.89 241.14 o 1 10 0 105.77 68.08 58.16 o 2 10 0 656.82 494.97 92.81 o 3 10 0 51.41 49.11 63.16 o 4 10 0 968.69 895.12 126.12 o 5 10 0 0.56 -9.57 55.00 o 1 11 0 56.74 33.31 66.61 o 2 11 0 2690.11 2754.52 191.61 o 3 11 0 67.48 151.36 74.71 o 4 11 0 193.07 435.21 106.57 o 5 11 0 6.35 -45.85 78.93 o 0 12 0 3.79 -51.54 56.69 o 1 12 0 2259.88 2364.23 174.69 o 2 12 0 58.12 39.61 69.81 o 3 12 0 1254.50 1134.56 146.24 o 4 12 0 15.93 104.62 82.74 o 1 13 0 2214.45 2266.78 181.72 o 2 13 0 1314.21 1211.31 147.27 o 3 13 0 152.38 36.41 70.55 o 4 13 0 149.81 33.21 63.83 o 0 14 0 3017.47 2869.00 213.08 o 1 14 0 348.16 260.91 88.40 o 2 14 0 406.15 398.10 111.47 o 3 14 0 623.36 532.09 113.83 o 1 15 0 1276.50 1443.94 170.72 o 2 15 0 561.19 642.11 121.96 o 0 16 0 446.84 410.83 119.94 o -5 0 1 3475.77 3553.31 360.78 o -3 0 1 2998.06 3152.22 133.27 o -1 0 1 775.66 632.48 58.55 o 1 0 1 2780.59 2922.43 82.70 o 3 0 1 11281.84 10603.96 211.70 o 5 0 1 1377.92 1352.79 119.50 o -6 1 1 24.20 -0.91 108.52 o -5 1 1 849.27 1013.14 93.94 o -4 1 1 13211.64 14706.40 442.92 o -3 1 1 1.76 54.41 41.43 o -2 1 1 150.41 78.87 130.87 o -1 1 1 330.75 310.95 54.93 o 0 1 1 1528.12 1774.56 72.18 o 1 1 1 5908.00 6206.57 116.90 o 2 1 1 4067.03 3906.29 114.89 o 3 1 1 1131.14 1043.18 81.78 o 4 1 1 2514.75 2570.11 140.64 o 5 1 1 823.73 1059.15 113.42 o 6 1 1 171.23 92.88 65.46 o -6 2 1 2290.80 2397.08 147.07 o -5 2 1 42.37 112.39 80.75 o -4 2 1 532.08 514.43 68.11 o -3 2 1 1426.64 1572.94 82.48 o -2 2 1 21.98 121.29 42.34 o -1 2 1 23.19 54.97 52.79 o 0 2 1 2110.66 2470.10 92.81 o 1 2 1 103.04 102.86 48.79 o 2 2 1 15596.16 14065.32 211.51 o 3 2 1 1042.34 969.31 81.58 o 4 2 1 48.29 152.71 57.43 o 5 2 1 134.61 128.58 66.00 o 6 2 1 2812.98 2860.23 198.52 o -6 3 1 10.29 -2.16 55.81 o -5 3 1 8364.36 9090.71 234.21 o -4 3 1 2396.58 2516.51 120.01 o -3 3 1 1739.45 1734.04 88.45 o -2 3 1 285.25 357.47 47.87 o -1 3 1 1342.55 1440.96 87.41 o 0 3 1 641.88 543.51 66.61 o 1 3 1 7154.86 7665.25 179.07 o 2 3 1 353.66 317.63 58.58 o 3 3 1 974.45 991.00 83.79 o 4 3 1 1055.44 1029.17 105.20 o 5 3 1 2959.95 3377.12 195.70 o 6 3 1 3.36 134.73 69.55 o -6 4 1 764.36 697.75 307.27 o -5 4 1 2759.50 2800.42 159.50 o -4 4 1 863.02 884.94 89.28 o -3 4 1 6068.26 6658.47 388.82 o -2 4 1 4.20 -47.06 37.02 o -1 4 1 856.09 932.49 76.46 o 0 4 1 641.39 502.24 64.44 o 1 4 1 1775.40 1818.90 107.91 o 2 4 1 1726.22 1659.06 99.21 o 3 4 1 7881.80 7491.50 207.48 o 4 4 1 737.30 810.78 97.13 o 5 4 1 699.39 700.69 101.90 o 6 4 1 387.87 452.13 100.24 o -6 5 1 72.09 -52.69 52.42 o -5 5 1 20.30 36.77 49.64 o -4 5 1 14035.50 15630.09 409.18 o -3 5 1 81.34 84.80 41.22 o -2 5 1 1764.67 1501.02 145.09 o -1 5 1 2444.72 2270.68 110.95 o 0 5 1 294.01 266.92 61.84 o 1 5 1 226.64 171.90 62.16 o 2 5 1 6077.28 6299.58 201.88 o 3 5 1 2947.57 2821.36 140.48 o 4 5 1 4079.98 4463.01 206.10 o 5 5 1 418.06 343.58 83.57 o 6 5 1 52.71 146.98 78.10 o -6 6 1 1118.31 1268.07 118.34 o -5 6 1 596.83 671.19 215.68 o -4 6 1 129.95 183.00 53.95 o -3 6 1 1040.02 945.21 238.38 o -2 6 1 1692.79 1721.80 137.08 o -1 6 1 3031.05 2778.55 126.05 o 0 6 1 5308.51 5337.75 167.52 o 1 6 1 1.64 17.50 55.13 o 2 6 1 6611.15 6673.20 222.84 o 3 6 1 3300.18 3216.35 152.42 o 4 6 1 4.32 -12.61 56.69 o 5 6 1 993.86 821.21 120.36 o 6 6 1 513.00 492.51 107.08 o -6 7 1 18.42 17.29 57.85 o -5 7 1 2268.73 2203.09 247.53 o -4 7 1 144.31 317.91 146.83 o -3 7 1 640.67 596.68 144.05 o -2 7 1 8.88 30.24 62.26 o -1 7 1 4225.81 3916.63 155.27 o 0 7 1 108.48 79.76 55.35 o 1 7 1 14117.54 15358.92 306.98 o 2 7 1 0.43 8.61 52.89 o 3 7 1 1857.02 1632.70 125.70 o 4 7 1 154.58 222.52 75.86 o 5 7 1 1484.59 1476.03 149.03 o 6 7 1 245.60 146.05 89.10 o -6 8 1 1173.27 1148.20 122.81 o -5 8 1 1085.29 1270.72 249.37 o -4 8 1 15.93 75.76 50.47 o -3 8 1 863.99 647.96 67.98 o -2 8 1 1060.76 982.97 214.90 o -1 8 1 16.57 65.49 51.93 o 0 8 1 710.89 714.77 86.64 o 1 8 1 7.32 -75.03 44.31 o 2 8 1 9873.84 10981.68 294.69 o 3 8 1 1171.73 925.03 112.49 o 4 8 1 13.52 -67.25 49.08 o 5 8 1 4.37 -97.10 56.12 o 6 8 1 530.60 540.66 118.98 o -5 9 1 1347.14 1343.92 255.13 o -4 9 1 4193.73 4010.93 394.35 o -3 9 1 2479.44 2077.78 301.00 o -2 9 1 716.69 692.41 68.57 o -1 9 1 44.54 -80.53 47.29 o 0 9 1 247.02 177.98 65.49 o 1 9 1 1150.16 1009.75 106.63 o 2 9 1 588.39 456.36 87.82 o 3 9 1 114.73 30.91 65.65 o 4 9 1 5047.38 5286.15 246.54 o 5 9 1 30.73 41.27 75.63 o -5 10 1 1753.65 1724.16 194.51 o -4 10 1 4.95 -42.58 53.59 o -3 10 1 2300.98 2077.44 147.83 o -2 10 1 63.39 -10.55 42.12 o -1 10 1 46.21 135.05 64.66 o 0 10 1 10.13 23.74 53.05 o 1 10 1 883.61 798.50 102.51 o 2 10 1 795.45 827.03 105.96 o 3 10 1 3510.25 3814.31 217.43 o 4 10 1 9.20 -78.58 58.93 o 5 10 1 2379.41 2277.18 200.57 o -5 11 1 944.02 1058.36 106.64 o -4 11 1 1470.08 1058.94 349.72 o -3 11 1 479.34 333.89 84.46 o -2 11 1 1588.17 1306.88 192.67 o -1 11 1 249.95 274.51 77.04 o 0 11 1 17.60 72.02 57.91 o 1 11 1 2431.07 2402.14 167.68 o 2 11 1 774.07 679.61 106.28 o 3 11 1 2947.11 3242.68 209.46 o 4 11 1 1587.90 1542.57 173.63 o 5 11 1 2024.71 2009.93 207.57 o -4 12 1 2.46 51.50 54.38 o -3 12 1 2.90 1.47 48.42 o -2 12 1 1630.31 1551.75 206.79 o -1 12 1 1009.33 1163.26 128.45 o 0 12 1 783.74 677.21 102.99 o 1 12 1 298.86 256.24 77.04 o 2 12 1 5382.00 5693.30 264.52 o 3 12 1 12.64 -36.60 51.67 o 4 12 1 81.27 173.05 89.33 o -4 13 1 728.20 353.81 112.59 o -3 13 1 348.88 304.60 68.10 o -2 13 1 215.01 246.88 64.81 o -1 13 1 1887.14 1771.36 156.00 o 0 13 1 19.34 -31.00 54.23 o 1 13 1 3385.05 3332.55 216.21 o 2 13 1 21.12 -14.72 63.12 o 3 13 1 42.61 44.25 74.51 o 4 13 1 1484.30 1708.40 198.39 o -3 14 1 1616.75 1523.93 254.65 o -2 14 1 211.88 118.94 58.65 o -1 14 1 213.49 -34.81 65.27 o 0 14 1 337.47 410.80 96.27 o 1 14 1 0.46 13.12 59.09 o 2 14 1 197.15 29.98 71.44 o 3 14 1 1684.38 1625.15 183.93 o -2 15 1 1482.86 1269.88 118.47 o -1 15 1 41.46 181.60 86.03 o 0 15 1 92.40 63.54 68.24 o 1 15 1 329.09 305.22 105.74 o 2 15 1 516.61 524.15 118.44 o -6 0 2 19.50 85.53 61.84 o -4 0 2 5697.25 5593.21 165.35 o -2 0 2 3216.90 3216.70 92.75 o 0 0 2 26638.20 28676.13 297.48 o 2 0 2 9072.12 9868.59 192.12 o 4 0 2 596.41 461.54 71.95 o 6 0 2 462.60 459.08 94.00 o -6 1 2 18.53 -27.51 216.10 o -5 1 2 142.78 184.60 55.55 o -4 1 2 738.15 780.81 78.77 o -3 1 2 302.40 311.27 51.42 o -2 1 2 9045.96 8907.49 244.97 o -1 1 2 11670.93 11090.04 192.79 o 0 1 2 167.82 103.76 61.94 o 1 1 2 1062.47 1239.24 76.72 o 2 1 2 4347.61 4836.38 141.48 o 3 1 2 4942.97 5202.90 167.20 o 4 1 2 30.33 -68.37 39.64 o 5 1 2 564.80 406.35 80.56 o 6 1 2 1652.06 1665.94 149.25 o -6 2 2 2.41 73.29 82.99 o -5 2 2 23.09 60.70 52.26 o -4 2 2 105.27 110.72 49.22 o -3 2 2 14133.38 15174.75 224.72 o -2 2 2 1047.88 1205.49 98.59 o -1 2 2 10456.42 9460.74 196.44 o 0 2 2 194.64 67.31 65.65 o 1 2 2 6603.24 6041.51 158.27 o 2 2 2 4926.23 5570.92 154.63 o 3 2 2 3627.18 3687.07 144.71 o 4 2 2 210.97 163.17 54.39 o 5 2 2 2271.92 2539.97 149.19 o 6 2 2 232.65 164.22 66.58 o -6 3 2 52.45 227.60 66.37 o -5 3 2 151.81 139.31 59.84 o -4 3 2 2012.87 2275.28 115.57 o -3 3 2 1248.74 1506.84 84.36 o -2 3 2 6992.29 6140.85 447.99 o -1 3 2 1428.76 1473.40 100.65 o 0 3 2 132.66 -6.72 64.12 o 1 3 2 181.62 295.78 69.27 o 2 3 2 22.17 -82.86 41.43 o 3 3 2 560.11 526.39 66.35 o 4 3 2 2194.94 2390.85 131.08 o 5 3 2 7.86 -9.09 41.78 o 6 3 2 3820.63 4132.39 214.52 o -6 4 2 98.28 118.95 66.30 o -5 4 2 68.52 56.40 58.95 o -4 4 2 3398.26 3567.95 280.95 o -3 4 2 2743.07 2608.49 186.25 o -2 4 2 1032.04 835.97 108.19 o -1 4 2 1412.11 1417.29 102.41 o 0 4 2 1661.74 1690.96 110.41 o 1 4 2 401.18 426.38 77.97 o 2 4 2 3697.77 3615.09 154.08 o 3 4 2 3052.93 2989.61 139.27 o 4 4 2 1426.73 1323.22 109.77 o 5 4 2 1059.78 1067.79 114.28 o 6 4 2 2169.35 1989.75 159.46 o -6 5 2 30.19 17.64 58.06 o -5 5 2 214.80 189.99 63.69 o -4 5 2 218.86 247.31 57.76 o -3 5 2 1236.56 1308.09 84.17 o -2 5 2 48.43 61.75 41.14 o -1 5 2 3663.33 3276.82 142.37 o 0 5 2 261.22 405.49 76.11 o 1 5 2 1848.40 1873.42 125.80 o 2 5 2 187.73 208.57 68.75 o 3 5 2 5007.28 4909.10 187.99 o 4 5 2 63.41 6.33 42.71 o 5 5 2 205.30 118.79 60.37 o 6 5 2 24.51 0.00 57.11 o -6 6 2 146.48 139.70 65.85 o -5 6 2 197.28 191.79 56.16 o -4 6 2 1552.36 1586.78 101.45 o -3 6 2 2451.96 2377.79 246.16 o -2 6 2 178.77 205.41 47.09 o -1 6 2 4525.96 4055.57 162.21 o 0 6 2 10680.78 10880.17 248.91 o 1 6 2 1964.42 2171.60 133.32 o 2 6 2 2296.64 2659.12 162.72 o 3 6 2 169.02 165.89 67.79 o 4 6 2 2.93 33.59 45.33 o 5 6 2 2204.78 2385.86 163.14 o 6 6 2 198.55 157.79 73.97 o -6 7 2 128.23 171.23 66.99 o -5 7 2 239.87 285.66 67.83 o -4 7 2 454.97 541.85 117.43 o -3 7 2 361.12 403.50 60.62 o -2 7 2 10884.01 9924.85 231.23 o -1 7 2 977.88 818.94 92.65 o 0 7 2 29.01 1.06 51.99 o 1 7 2 365.69 415.73 79.98 o 2 7 2 1162.89 1374.93 128.93 o 3 7 2 216.17 264.72 75.41 o 4 7 2 831.99 821.40 102.67 o 5 7 2 324.85 257.61 77.30 o 6 7 2 2709.25 2593.27 200.28 o -5 8 2 41.47 47.33 45.73 o -4 8 2 363.54 337.34 63.80 o -3 8 2 7935.27 7378.74 441.78 o -2 8 2 320.55 327.06 59.09 o -1 8 2 2640.26 2556.29 149.03 o 0 8 2 1364.06 1455.68 115.05 o 1 8 2 1102.33 1180.98 110.22 o 2 8 2 186.61 110.57 63.41 o 3 8 2 1303.68 1124.32 129.80 o 4 8 2 815.36 853.62 111.59 o 5 8 2 1431.45 1388.81 143.20 o -5 9 2 624.13 509.70 83.43 o -4 9 2 245.84 337.60 93.93 o -3 9 2 1689.20 1645.76 121.58 o -2 9 2 708.13 716.72 85.33 o -1 9 2 2584.73 2562.94 149.15 o 0 9 2 195.47 155.55 61.97 o 1 9 2 1033.14 1284.19 123.56 o 2 9 2 625.78 716.31 104.14 o 3 9 2 442.15 604.52 115.24 o 4 9 2 604.49 650.53 115.94 o 5 9 2 19.49 -106.41 53.21 o -5 10 2 74.45 140.19 60.11 o -4 10 2 2424.71 2057.52 131.26 o -3 10 2 419.58 443.72 68.04 o -2 10 2 386.07 495.61 68.88 o -1 10 2 297.54 282.63 72.56 o 0 10 2 4981.72 5097.80 218.07 o 1 10 2 1650.04 1597.60 142.85 o 2 10 2 175.44 401.74 89.26 o 3 10 2 405.71 388.69 99.28 o 4 10 2 252.17 230.64 95.12 o 5 10 2 147.61 152.87 75.12 o -4 11 2 488.87 447.64 225.68 o -3 11 2 126.22 213.77 60.73 o -2 11 2 5048.03 4973.91 399.36 o -1 11 2 240.05 211.38 73.81 o 0 11 2 143.81 290.21 78.70 o 1 11 2 500.51 280.04 88.24 o 2 11 2 175.80 95.12 69.01 o 3 11 2 68.08 155.43 83.18 o 4 11 2 773.89 911.40 155.01 o -4 12 2 29.68 -6.62 48.93 o -3 12 2 3615.65 3550.36 198.79 o -2 12 2 134.80 136.98 52.31 o -1 12 2 2286.41 2058.66 157.63 o 0 12 2 16.48 -12.73 54.52 o 1 12 2 926.47 945.09 117.90 o 2 12 2 142.44 78.99 66.83 o 3 12 2 65.72 39.42 64.95 o 4 12 2 734.37 704.24 136.77 o -3 13 2 319.39 162.17 165.50 o -2 13 2 2011.95 1930.31 128.05 o -1 13 2 963.66 1150.78 138.98 o 0 13 2 199.62 188.76 78.32 o 1 13 2 903.68 912.27 123.56 o 2 13 2 4.19 112.39 70.51 o 3 13 2 364.56 215.41 96.56 o -3 14 2 152.26 72.72 57.85 o -2 14 2 2.87 -49.22 51.11 o -1 14 2 221.97 238.10 83.12 o 0 14 2 4461.87 4512.09 252.14 o 1 14 2 33.40 27.13 56.53 o 2 14 2 73.49 151.17 79.18 o 3 14 2 375.83 342.24 111.43 o -2 15 2 1068.17 877.19 100.96 o -1 15 2 1074.48 1026.61 135.40 o 0 15 2 6.82 -41.30 51.00 o 1 15 2 1366.26 1384.65 165.95 o 2 15 2 114.47 78.35 80.94 o -5 0 3 1421.41 1395.01 184.76 o -3 0 3 167.24 169.41 45.60 o -1 0 3 31505.25 31990.42 346.14 o 1 0 3 3312.66 3097.72 122.63 o 3 0 3 8644.51 8473.45 223.06 o 5 0 3 1970.71 2133.17 149.70 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