#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/08/2200854.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200854_Fobs loop_ _publ_author_name 'Bond, Andrew D.' _publ_section_title ; A 1:2 complex of pyromellitic diimide and dimethyl sulfoxide ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o194 _journal_page_last o195 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 114.533 _cell_angle_gamma 90.000 _cell_length_a 12.4152 _cell_length_b 5.3266 _cell_length_c 13.8046 _exptl_crystal_F_000 388.00 _reflns_d_resolution_high 0.7698 _[local]_cod_data_source_file cf6143Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ab0103 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 136.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 313.52 223.97 105.45 o 3 0 0 76.50 97.08 4.24 o 4 0 0 963.22 889.16 25.63 o 5 0 0 184.49 148.76 7.06 o 6 0 0 2940.65 2911.43 87.41 o 7 0 0 195.42 204.19 10.04 o 8 0 0 689.15 713.67 50.69 o 9 0 0 115.88 122.77 11.29 o 10 0 0 145.20 145.81 14.56 o 11 0 0 0.35 0.68 8.56 o 12 0 0 233.28 220.31 22.54 o 13 0 0 83.18 80.33 17.14 o 14 0 0 90.42 92.11 23.06 o 1 1 0 0.03 2.14 0.37 o 2 1 0 2410.29 2176.16 38.01 o 3 1 0 3234.39 3132.74 60.20 o 4 1 0 5.71 5.53 1.46 o 5 1 0 805.36 817.47 16.57 o 6 1 0 801.92 839.01 18.84 o 7 1 0 583.82 589.24 14.93 o 8 1 0 171.74 150.98 6.70 o 9 1 0 351.49 333.10 13.23 o 10 1 0 165.22 180.17 10.57 o 11 1 0 53.25 44.69 8.19 o 12 1 0 32.01 25.28 9.18 o 13 1 0 9.25 -4.12 8.62 o 14 1 0 1.65 0.59 10.69 o 0 2 0 1136.49 944.67 257.39 o 1 2 0 164.31 167.55 9.54 o 2 2 0 376.98 397.78 6.72 o 3 2 0 23.79 28.15 1.63 o 4 2 0 56.80 61.66 2.94 o 5 2 0 280.30 290.08 6.90 o 6 2 0 70.67 59.23 3.46 o 7 2 0 2.22 1.66 3.00 o 8 2 0 307.51 287.64 11.86 o 9 2 0 37.09 38.00 5.85 o 10 2 0 7.64 9.03 5.39 o 11 2 0 46.99 39.32 13.04 o 12 2 0 0.14 0.65 9.06 o 13 2 0 10.57 6.00 13.39 o 14 2 0 7.24 0.68 16.95 o 1 3 0 345.79 378.46 10.70 o 2 3 0 57.35 52.26 2.83 o 3 3 0 936.23 1009.17 18.50 o 4 3 0 183.80 178.22 4.86 o 5 3 0 45.60 43.64 2.73 o 6 3 0 64.33 55.32 3.59 o 7 3 0 0.62 2.84 2.42 o 8 3 0 837.62 846.49 46.89 o 9 3 0 60.77 67.43 6.52 o 10 3 0 148.83 165.86 11.91 o 11 3 0 72.60 66.66 9.42 o 12 3 0 13.23 11.92 11.32 o 13 3 0 12.09 18.37 11.81 o 0 4 0 1375.67 1353.60 60.22 o 1 4 0 652.67 653.22 15.13 o 2 4 0 2.28 3.37 1.96 o 3 4 0 132.00 134.73 5.86 o 4 4 0 410.39 376.15 17.71 o 5 4 0 200.45 213.30 6.82 o 6 4 0 363.88 379.76 16.91 o 7 4 0 83.68 89.12 6.32 o 8 4 0 26.98 15.39 6.03 o 9 4 0 2.64 0.13 5.67 o 10 4 0 115.78 143.63 21.52 o 11 4 0 21.37 12.08 14.73 o 1 5 0 123.52 127.84 16.99 o 2 5 0 194.79 214.76 7.09 o 3 5 0 7.35 11.93 3.52 o 4 5 0 505.94 542.35 26.59 o 5 5 0 1.58 0.00 6.10 o 6 5 0 3.28 -5.42 8.75 o 7 5 0 1.58 3.39 8.75 o 8 5 0 158.55 180.82 22.33 o 9 5 0 55.07 77.53 16.89 o 10 5 0 16.96 24.95 14.17 o 0 6 0 240.37 195.29 27.54 o 1 6 0 90.40 88.07 14.55 o 2 6 0 2.32 11.09 9.76 o 3 6 0 5.21 -6.47 15.09 o 4 6 0 2.25 -5.85 11.70 o 5 6 0 34.86 61.13 22.99 o 6 6 0 1.61 -0.68 13.92 o 7 6 0 48.56 42.15 18.06 o -14 1 1 26.41 55.40 15.34 o -13 1 1 288.07 317.20 26.72 o -12 1 1 13.87 14.07 8.90 o -11 1 1 9.63 3.48 8.52 o -10 1 1 12.89 3.95 5.83 o -9 1 1 28.00 37.37 5.18 o -8 1 1 664.74 666.68 18.23 o -7 1 1 32.10 26.84 3.35 o -6 1 1 165.68 167.87 7.84 o -5 1 1 81.32 68.55 2.96 o -4 1 1 91.69 103.63 3.31 o -3 1 1 1585.34 1525.25 28.41 o -2 1 1 2047.21 2151.98 33.61 o -1 1 1 71.61 76.22 1.63 o 0 1 1 1857.43 1751.22 29.81 o 1 1 1 6683.41 6446.09 201.84 o 2 1 1 66.23 73.39 2.15 o 3 1 1 2598.99 2513.51 45.23 o 4 1 1 1738.46 1722.27 32.66 o 5 1 1 27.54 27.90 2.52 o 6 1 1 681.63 701.89 17.31 o 7 1 1 237.42 256.10 8.33 o 8 1 1 23.18 20.65 3.94 o 9 1 1 269.42 285.21 15.08 o 10 1 1 179.21 208.33 12.02 o 11 1 1 3.60 9.05 9.51 o 12 1 1 1.18 -6.94 8.18 o 13 1 1 15.16 24.43 11.18 o 14 1 1 75.92 100.73 20.59 o -14 2 1 33.16 52.91 16.59 o -13 2 1 3.53 4.82 8.75 o -12 2 1 45.75 47.80 16.05 o -11 2 1 310.81 341.41 15.42 o -10 2 1 715.58 759.62 32.16 o -9 2 1 1.40 2.00 4.22 o -8 2 1 183.59 155.31 6.19 o -7 2 1 25.08 17.73 5.04 o -6 2 1 1926.03 1985.16 38.54 o -5 2 1 1733.39 1776.91 32.69 o -4 2 1 64.15 56.86 2.22 o -3 2 1 466.28 516.50 8.36 o -2 2 1 1169.42 1197.61 19.30 o -1 2 1 23.18 20.95 1.06 o 0 2 1 10.80 7.51 0.56 o 1 2 1 111.09 94.61 2.34 o 2 2 1 2448.21 2596.60 39.58 o 3 2 1 143.93 140.16 3.57 o 4 2 1 415.60 409.25 8.63 o 5 2 1 67.05 58.70 2.98 o 6 2 1 1192.84 1237.90 29.16 o 7 2 1 930.03 931.29 25.14 o 8 2 1 74.37 67.57 6.96 o 9 2 1 194.71 200.98 11.58 o 10 2 1 7.52 5.03 9.30 o 11 2 1 374.92 392.01 34.90 o 12 2 1 119.69 156.98 15.30 o 13 2 1 52.98 43.83 13.69 o -13 3 1 56.91 63.52 13.10 o -12 3 1 24.41 17.60 8.82 o -11 3 1 7.06 10.00 7.08 o -10 3 1 0.06 -6.34 6.34 o -9 3 1 23.57 20.62 4.80 o -8 3 1 84.11 72.94 5.99 o -7 3 1 62.77 54.10 4.86 o -6 3 1 273.66 254.14 7.55 o -5 3 1 8.72 6.51 1.80 o -4 3 1 104.24 100.80 3.13 o -3 3 1 374.18 394.42 7.45 o -2 3 1 340.18 362.47 8.28 o -1 3 1 1.68 4.39 1.40 o 0 3 1 296.19 332.67 8.99 o 1 3 1 354.41 395.87 9.78 o 2 3 1 370.78 348.69 7.23 o 3 3 1 543.31 544.46 11.27 o 4 3 1 445.74 456.72 11.45 o 5 3 1 69.30 68.00 6.45 o 6 3 1 21.15 13.83 3.11 o 7 3 1 346.22 326.21 14.52 o 8 3 1 10.49 7.38 3.98 o 9 3 1 84.42 85.99 8.14 o 10 3 1 108.47 129.73 11.10 o 11 3 1 10.54 6.52 9.88 o 12 3 1 7.62 5.18 8.94 o -12 4 1 11.85 29.39 15.40 o -11 4 1 7.62 2.65 15.34 o -10 4 1 54.40 54.79 13.37 o -9 4 1 69.49 60.36 10.26 o -8 4 1 0.61 1.29 3.91 o -7 4 1 26.19 26.86 6.76 o -6 4 1 4.78 2.86 2.29 o -5 4 1 86.78 89.24 3.60 o -4 4 1 68.43 73.94 4.63 o -3 4 1 141.63 148.23 10.25 o -2 4 1 104.45 105.23 4.29 o -1 4 1 77.35 92.33 8.08 o 0 4 1 60.36 58.13 6.10 o 1 4 1 53.77 56.93 3.57 o 2 4 1 10.71 11.01 3.68 o 3 4 1 41.89 42.18 3.76 o 4 4 1 15.01 15.28 1.77 o 5 4 1 617.25 624.69 16.95 o 6 4 1 104.88 116.48 9.10 o 7 4 1 35.75 33.33 10.38 o 8 4 1 0.00 -3.13 6.14 o 9 4 1 23.66 13.89 8.29 o 10 4 1 0.01 -2.03 11.46 o 11 4 1 5.17 1.36 14.79 o -10 5 1 6.75 -17.50 17.50 o -9 5 1 160.60 175.57 21.59 o -8 5 1 52.71 52.39 12.08 o -7 5 1 10.43 6.04 7.39 o -6 5 1 11.48 16.82 8.75 o -5 5 1 0.01 0.04 6.31 o -4 5 1 44.26 42.19 5.01 o -3 5 1 518.17 540.59 18.73 o -2 5 1 403.98 391.36 18.19 o -1 5 1 577.62 565.30 23.82 o 0 5 1 58.66 66.28 12.14 o 1 5 1 429.03 419.20 18.97 o 2 5 1 25.47 25.68 3.04 o 3 5 1 256.84 275.98 14.33 o 4 5 1 100.07 130.73 13.57 o 5 5 1 14.14 23.66 8.81 o 6 5 1 10.07 10.84 6.78 o 7 5 1 13.27 23.66 13.49 o 8 5 1 3.90 -7.45 10.84 o 9 5 1 10.86 36.53 14.23 o -7 6 1 130.72 165.04 26.03 o -6 6 1 214.09 202.01 28.45 o -5 6 1 103.08 121.59 25.53 o -4 6 1 113.79 85.82 12.32 o -3 6 1 0.01 1.33 13.15 o -2 6 1 20.47 16.89 8.32 o -1 6 1 88.66 101.30 11.83 o 0 6 1 142.53 139.12 14.62 o 1 6 1 115.86 145.05 36.57 o 2 6 1 55.53 50.09 11.08 o 3 6 1 40.27 51.25 11.06 o 4 6 1 6.01 0.68 12.44 o 5 6 1 16.19 -1.97 17.19 o 6 6 1 145.23 171.53 24.73 o -15 0 2 43.14 49.12 20.28 o -14 0 2 63.10 47.83 15.10 o -13 0 2 108.24 116.12 20.35 o -12 0 2 588.07 635.93 36.01 o -11 0 2 146.87 141.98 13.20 o -10 0 2 559.29 583.13 26.86 o -9 0 2 133.50 118.16 7.92 o -8 0 2 145.24 117.96 8.91 o -7 0 2 390.22 407.75 17.15 o -6 0 2 9.03 4.39 3.00 o -5 0 2 12.22 4.62 2.99 o -4 0 2 13938.71 14396.85 369.33 o -3 0 2 12803.66 13321.47 345.16 o -2 0 2 846.70 657.55 293.52 o 1 0 2 18744.42 17010.58 462.65 o 2 0 2 3.06 2.65 1.58 o 3 0 2 250.22 245.11 9.01 o 4 0 2 496.64 485.74 27.90 o 5 0 2 37.87 36.94 6.66 o 6 0 2 583.22 590.99 22.94 o 7 0 2 181.99 178.74 10.70 o 8 0 2 12.35 18.55 9.92 o 9 0 2 104.88 99.36 11.29 o 10 0 2 390.21 336.03 28.77 o 11 0 2 89.40 107.16 17.26 o 12 0 2 17.76 -9.92 11.89 o 13 0 2 111.48 90.58 18.56 o -15 1 2 14.07 3.94 15.09 o -14 1 2 2.45 5.18 10.24 o -13 1 2 171.85 152.84 18.63 o -12 1 2 30.72 37.01 7.39 o -11 1 2 22.29 23.69 14.45 o -10 1 2 9.95 12.75 5.68 o -9 1 2 1292.87 1261.82 41.93 o -8 1 2 243.86 236.03 10.84 o -7 1 2 528.92 473.53 18.24 o -6 1 2 1502.02 1613.52 31.95 o -5 1 2 2027.93 2088.83 38.52 o -4 1 2 104.55 103.34 3.35 o -3 1 2 1449.19 1453.52 24.89 o -2 1 2 1814.19 1659.77 25.77 o -1 1 2 4068.74 3819.75 58.46 o 0 1 2 905.90 845.37 13.21 o 1 1 2 5325.94 5159.03 119.02 o 2 1 2 8237.99 8334.95 145.76 o 3 1 2 1429.77 1348.77 26.63 o 4 1 2 19.81 12.91 2.02 o 5 1 2 446.89 445.44 10.25 o 6 1 2 589.54 592.80 15.26 o 7 1 2 252.76 243.35 12.88 o 8 1 2 49.75 48.59 7.11 o 9 1 2 459.21 518.09 21.05 o 10 1 2 66.92 84.11 12.95 o 11 1 2 69.71 70.77 13.99 o 12 1 2 11.70 14.99 13.25 o 13 1 2 59.45 65.84 13.38 o -14 2 2 35.74 42.59 12.86 o -13 2 2 43.51 49.00 14.70 o -12 2 2 11.76 13.02 16.82 o -11 2 2 33.56 27.26 7.91 o -10 2 2 0.93 3.28 5.71 o -9 2 2 0.33 2.09 5.30 o -8 2 2 13.25 15.55 3.02 o -7 2 2 63.76 59.64 3.73 o -6 2 2 936.22 975.76 20.53 o -5 2 2 371.51 376.99 11.12 o -4 2 2 51.74 60.56 2.44 o -3 2 2 231.16 237.44 4.58 o -2 2 2 127.56 143.98 3.07 o -1 2 2 3.41 3.43 0.73 o 0 2 2 79.27 89.21 2.19 o 1 2 2 386.99 445.89 9.35 o 2 2 2 4.18 1.03 0.98 o 3 2 2 7.79 4.71 1.25 o 4 2 2 393.98 422.09 9.83 o 5 2 2 73.11 68.51 3.82 o 6 2 2 37.81 37.23 3.52 o 7 2 2 8.01 4.82 3.16 o 8 2 2 132.13 125.56 8.43 o 9 2 2 37.49 30.13 14.27 o 10 2 2 12.52 21.80 7.96 o 11 2 2 1.23 5.58 8.44 o 12 2 2 0.03 3.82 10.34 o 13 2 2 4.49 -1.36 16.70 o -13 3 2 140.99 146.79 18.16 o -12 3 2 59.19 74.83 13.56 o -11 3 2 39.79 43.64 10.90 o -10 3 2 4.44 3.30 8.96 o -9 3 2 55.97 55.31 6.46 o -8 3 2 26.98 26.63 4.47 o -7 3 2 1772.08 1763.22 43.41 o -6 3 2 7.33 2.34 2.41 o -5 3 2 245.05 271.26 6.81 o -4 3 2 732.85 770.73 14.54 o -3 3 2 47.45 49.82 1.84 o -2 3 2 863.60 898.64 16.52 o -1 3 2 6.71 3.95 0.54 o 0 3 2 19.23 17.49 1.87 o 1 3 2 21.43 23.52 1.90 o 2 3 2 165.28 156.55 3.99 o 3 3 2 3.79 7.08 1.38 o 4 3 2 593.60 639.11 16.19 o 5 3 2 146.35 149.47 5.84 o 6 3 2 230.54 238.36 8.72 o 7 3 2 235.97 237.30 14.61 o 8 3 2 136.77 134.73 18.15 o 9 3 2 25.53 21.67 6.72 o 10 3 2 162.63 151.96 14.14 o 11 3 2 35.22 24.35 14.30 o 12 3 2 15.78 1.75 10.28 o -12 4 2 17.92 19.96 13.31 o -11 4 2 158.73 141.40 21.41 o -10 4 2 102.16 96.76 9.96 o -9 4 2 93.60 95.68 9.41 o -8 4 2 1.47 0.68 6.99 o -7 4 2 59.07 69.66 4.95 o -6 4 2 48.23 36.08 2.81 o -5 4 2 865.94 945.59 27.77 o -4 4 2 309.06 296.58 10.05 o -3 4 2 369.35 352.76 10.57 o -2 4 2 23.87 18.13 2.19 o -1 4 2 318.25 335.41 8.32 o 0 4 2 517.68 502.76 13.07 o 1 4 2 1611.37 1700.03 39.91 o 2 4 2 79.78 81.90 5.63 o 3 4 2 71.59 72.16 3.45 o 4 4 2 163.15 161.25 5.62 o 5 4 2 653.58 684.02 31.36 o 6 4 2 24.67 34.75 4.59 o 7 4 2 174.08 208.81 11.77 o 8 4 2 46.48 27.95 14.42 o 9 4 2 6.78 0.00 8.81 o 10 4 2 1.57 -2.03 12.14 o 11 4 2 91.34 88.59 23.00 o -10 5 2 0.65 -6.04 11.40 o -9 5 2 70.74 94.50 14.79 o -8 5 2 134.69 172.34 17.52 o -7 5 2 137.33 148.85 14.80 o -6 5 2 2.26 1.36 8.01 o -5 5 2 14.22 12.11 4.32 o -4 5 2 0.67 0.14 3.76 o -3 5 2 441.67 459.48 13.93 o -2 5 2 81.46 103.70 8.94 o -1 5 2 66.08 69.36 8.93 o 0 5 2 0.56 5.89 5.95 o 1 5 2 46.12 50.59 8.13 o 2 5 2 216.21 225.31 14.41 o 3 5 2 19.16 16.71 6.44 o 4 5 2 28.24 31.18 8.81 o 5 5 2 151.67 177.87 17.03 o 6 5 2 14.21 27.79 10.84 o 7 5 2 8.26 0.68 12.20 o 8 5 2 48.34 53.62 14.24 o 9 5 2 23.65 37.34 13.56 o -7 6 2 0.74 23.10 20.45 o -6 6 2 0.17 -3.27 13.74 o -5 6 2 42.28 24.03 13.62 o -4 6 2 38.80 51.86 11.83 o -3 6 2 5.39 2.28 10.04 o -2 6 2 132.40 143.25 15.68 o -1 6 2 60.81 56.59 11.74 o 0 6 2 7.49 12.45 8.48 o 1 6 2 93.13 79.66 11.80 o 2 6 2 0.19 -5.40 8.12 o 3 6 2 0.15 -5.24 13.68 o 4 6 2 108.11 118.58 19.79 o 5 6 2 4.37 -18.61 25.26 o -15 1 3 48.89 64.37 21.54 o -14 1 3 9.67 3.06 13.09 o -13 1 3 71.37 74.15 9.91 o -12 1 3 251.54 258.67 24.15 o -11 1 3 5.69 -6.90 6.90 o -10 1 3 29.78 34.11 10.20 o -9 1 3 62.53 55.51 6.05 o -8 1 3 0.75 -0.22 3.11 o -7 1 3 499.08 509.44 12.36 o -6 1 3 84.43 68.08 3.66 o -5 1 3 444.93 459.99 10.08 o -4 1 3 292.91 311.43 6.22 o -3 1 3 502.99 442.40 7.41 o -2 1 3 523.25 472.53 7.97 o -1 1 3 614.31 622.86 10.51 o 0 1 3 4348.09 4195.16 88.52 o 1 1 3 327.25 345.00 7.62 o 2 1 3 7185.13 7166.71 127.93 o 3 1 3 674.66 699.85 15.10 o 4 1 3 367.56 376.52 8.98 o 5 1 3 155.13 150.13 5.98 o 6 1 3 86.23 94.37 5.91 o 7 1 3 121.96 109.49 11.65 o 8 1 3 81.93 85.64 10.17 o 9 1 3 14.28 12.10 7.49 o 10 1 3 58.57 62.33 22.93 o 11 1 3 51.42 46.51 10.08 o 12 1 3 3.38 -1.57 10.25 o 13 1 3 5.72 5.98 16.57 o -14 2 3 0.28 2.84 11.68 o -13 2 3 29.42 35.58 10.49 o -12 2 3 102.06 84.69 9.68 o -11 2 3 3.19 6.28 6.03 o -10 2 3 496.52 485.58 20.06 o -9 2 3 1291.32 1324.88 74.04 o -8 2 3 3.69 3.96 3.01 o -7 2 3 32.94 31.45 3.08 o -6 2 3 1684.69 1738.81 34.06 o -5 2 3 2173.97 2204.31 40.17 o -4 2 3 90.55 80.17 2.56 o -3 2 3 194.39 193.56 3.97 o -2 2 3 181.98 197.39 3.96 o -1 2 3 1810.79 1874.94 29.30 o 0 2 3 358.46 335.06 6.09 o 1 2 3 918.97 953.86 17.67 o 2 2 3 4.42 3.31 1.41 o 3 2 3 3472.40 3726.10 67.16 o 4 2 3 402.56 439.74 10.66 o 5 2 3 435.66 448.35 18.48 o 6 2 3 54.52 45.62 4.30 o 7 2 3 705.25 729.63 24.50 o 8 2 3 132.75 141.89 18.66 o 9 2 3 253.76 254.50 15.79 o 10 2 3 95.83 99.18 10.36 o 11 2 3 49.84 50.84 11.34 o 12 2 3 123.45 130.87 17.71 o -14 3 3 77.20 52.81 15.25 o -13 3 3 37.55 31.09 24.74 o -12 3 3 14.86 14.45 7.97 o -11 3 3 4.95 8.84 8.35 o -10 3 3 10.03 14.35 4.88 o -9 3 3 2.24 3.30 3.77 o -8 3 3 121.69 121.50 6.54 o -7 3 3 189.24 197.74 7.28 o -6 3 3 98.54 111.95 4.36 o -5 3 3 2.16 2.56 1.84 o -4 3 3 83.68 90.36 3.86 o -3 3 3 266.80 290.21 6.41 o -2 3 3 275.19 267.26 5.51 o -1 3 3 772.45 816.34 14.50 o 0 3 3 137.60 121.18 3.11 o 1 3 3 100.21 116.34 3.18 o 2 3 3 760.06 784.26 17.32 o 3 3 3 1121.40 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