#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:53:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180929 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/09/2200906.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200906_Fobs loop_ _publ_author_name 'Barnes, John C.' 'Brimacombe, John S.' 'Connolly, Lisa M. C.' 'Dix, Alexander P.' _publ_section_title ; Methyl (2'R,3'R)-2-azido-2,6-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-\a-L-glucopyranoside ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o227 _journal_page_last o228 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 10.0648 _cell_length_b 10.5118 _cell_length_c 30.6961 _exptl_crystal_F_000 1360.00 _reflns_d_resolution_high 0.8417 _cod_data_source_file dn6016Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LISA2 in P212121 F pairs merged' _shelx_refln_list_code 4 _shelx_f_calc_maximum 271.18 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2902.86 2480.89 189.20 o 4 0 0 2494.49 2183.54 240.30 o 6 0 0 540.83 550.76 183.67 o 8 0 0 74.47 110.35 165.12 o 10 0 0 220.68 281.73 207.15 o 1 1 0 56.87 52.69 11.77 o 2 1 0 9516.40 9076.32 332.98 o 3 1 0 339.97 323.85 80.03 o 4 1 0 78.25 58.23 69.46 o 5 1 0 5231.11 4859.72 282.12 o 6 1 0 4362.64 4433.38 304.86 o 7 1 0 8.70 18.33 49.87 o 8 1 0 879.73 939.35 128.40 o 9 1 0 223.46 251.25 117.65 o 10 1 0 1.66 0.00 82.95 o 0 2 0 28.40 53.36 13.30 o 1 2 0 10509.33 10738.45 144.73 o 2 2 0 36130.96 37149.06 641.98 o 3 2 0 1298.27 1163.71 90.83 o 4 2 0 1124.88 1164.28 104.23 o 5 2 0 3530.08 3457.79 176.29 o 6 2 0 511.71 527.58 90.71 o 7 2 0 2.21 17.58 110.35 o 8 2 0 417.24 417.96 94.70 o 9 2 0 103.15 122.76 86.82 o 10 2 0 15.00 21.48 126.46 o 1 3 0 448.56 427.72 29.33 o 2 3 0 1390.66 1323.97 86.98 o 3 3 0 143.18 104.36 40.40 o 4 3 0 886.99 808.01 92.84 o 5 3 0 1420.06 1471.36 155.91 o 6 3 0 270.82 296.49 80.87 o 7 3 0 85.81 89.78 75.88 o 8 3 0 8.38 26.62 52.75 o 9 3 0 190.59 179.73 137.85 o 10 3 0 9.77 51.27 111.32 o 0 4 0 1888.77 1853.08 57.04 o 1 4 0 277.51 294.52 26.82 o 2 4 0 306.48 314.57 49.26 o 3 4 0 0.98 9.13 41.36 o 4 4 0 27.38 26.70 50.52 o 5 4 0 2363.73 2377.51 167.33 o 6 4 0 0.78 0.00 51.00 o 7 4 0 1010.16 1093.96 144.69 o 8 4 0 352.74 342.35 99.76 o 9 4 0 807.80 882.70 218.33 o 10 4 0 14.06 0.00 99.61 o 1 5 0 1705.11 1669.02 54.40 o 2 5 0 1068.24 1009.03 75.34 o 3 5 0 941.89 932.53 90.08 o 4 5 0 503.67 495.07 86.33 o 5 5 0 454.66 479.41 91.38 o 6 5 0 829.79 855.64 127.61 o 7 5 0 465.85 486.27 113.90 o 8 5 0 668.78 635.70 133.67 o 9 5 0 616.34 598.21 178.69 o 10 5 0 322.41 398.26 147.92 o 0 6 0 87.82 145.41 97.59 o 1 6 0 5043.83 5221.33 194.33 o 2 6 0 724.35 734.59 65.71 o 3 6 0 542.91 530.43 68.54 o 4 6 0 153.72 151.52 57.12 o 5 6 0 79.24 108.54 70.38 o 6 6 0 205.95 184.05 72.91 o 7 6 0 245.75 275.98 95.13 o 8 6 0 69.57 29.98 66.47 o 9 6 0 44.35 25.03 85.27 o 10 6 0 11.04 0.00 78.88 o 1 7 0 190.87 175.67 35.82 o 2 7 0 3969.11 3938.84 148.02 o 3 7 0 131.71 136.67 46.80 o 4 7 0 17.63 21.31 46.35 o 5 7 0 532.92 510.13 104.12 o 6 7 0 311.27 256.24 90.69 o 7 7 0 21.15 21.69 60.42 o 8 7 0 3.71 3.85 60.58 o 9 7 0 557.28 577.74 189.44 o 0 8 0 47.50 64.94 125.41 o 1 8 0 82.31 78.48 88.16 o 2 8 0 114.98 113.70 90.41 o 3 8 0 812.98 869.05 96.22 o 4 8 0 49.53 63.01 58.89 o 5 8 0 354.89 336.36 79.52 o 6 8 0 9.98 14.53 35.48 o 7 8 0 108.10 67.15 87.69 o 8 8 0 0.04 9.28 83.98 o 1 9 0 16.14 36.40 68.34 o 2 9 0 688.75 687.43 150.13 o 3 9 0 228.45 267.90 141.68 o 4 9 0 377.15 413.48 156.49 o 5 9 0 138.28 138.89 137.76 o 6 9 0 2.71 10.74 99.61 o 7 9 0 88.23 110.35 155.37 o 8 9 0 4.35 0.00 81.54 o 1 10 0 28.35 0.00 95.70 o 2 10 0 0.01 0.00 73.90 o 3 10 0 318.41 427.95 203.36 o 4 10 0 488.87 466.48 187.34 o 5 10 0 8.96 0.76 78.26 o 6 10 0 121.40 172.25 143.30 o 1 11 0 1.11 2.04 70.92 o 2 11 0 59.22 87.40 123.64 o 3 11 0 30.69 83.00 118.72 o 4 11 0 27.31 0.00 104.98 o 1 0 1 1574.67 1455.66 86.59 o 2 0 1 4255.40 3580.46 313.71 o 3 0 1 1999.96 1755.48 134.75 o 4 0 1 8.46 0.00 116.70 o 5 0 1 428.02 444.59 111.92 o 6 0 1 320.12 303.87 104.50 o 7 0 1 936.63 1013.79 171.56 o 8 0 1 41.94 60.06 61.46 o 9 0 1 296.19 302.61 133.94 o 10 0 1 37.32 24.95 87.18 o -10 1 1 123.84 127.44 179.53 o -9 1 1 159.49 96.88 110.03 o -8 1 1 171.10 157.13 54.36 o -7 1 1 575.89 606.08 97.07 o -6 1 1 432.81 436.92 84.65 o -5 1 1 1052.46 1069.01 104.48 o -4 1 1 793.54 736.87 85.41 o -3 1 1 2064.10 1962.49 187.89 o -2 1 1 12532.50 11795.86 350.06 o -1 1 1 25938.02 27816.79 1007.72 o 0 1 1 917.45 891.09 35.41 o 1 1 1 25938.39 28382.27 1053.39 o 2 1 1 12537.88 10724.59 1397.48 o 3 1 1 2066.56 1784.63 140.10 o 4 1 1 794.87 741.63 112.41 o 5 1 1 1051.78 1082.38 148.59 o 6 1 1 432.18 410.08 117.78 o 7 1 1 575.65 513.41 147.04 o 8 1 1 171.22 150.15 124.84 o 9 1 1 158.89 159.41 100.88 o 10 1 1 123.79 135.42 122.10 o -10 2 1 123.05 126.53 128.90 o -9 2 1 93.74 98.27 110.08 o -8 2 1 690.69 706.10 97.88 o -7 2 1 360.70 405.14 71.55 o -6 2 1 157.43 159.30 49.57 o -5 2 1 485.91 505.42 69.30 o -4 2 1 4990.75 4929.24 346.71 o -3 2 1 3269.18 3148.53 151.61 o -2 2 1 5297.38 5071.36 199.03 o -1 2 1 15189.92 15923.75 355.72 o 0 2 1 6158.37 6408.40 310.19 o 1 2 1 15188.85 16391.61 696.68 o 2 2 1 5298.18 4574.36 363.75 o 3 2 1 3271.72 2986.20 180.15 o 4 2 1 4993.40 4449.53 240.39 o 5 2 1 486.21 412.28 103.69 o 6 2 1 157.68 167.84 79.82 o 7 2 1 360.20 348.60 115.26 o 8 2 1 690.40 703.55 163.08 o 9 2 1 93.27 130.25 120.79 o 10 2 1 122.84 112.78 116.79 o -10 3 1 18.68 3.77 84.26 o -9 3 1 157.18 100.79 106.79 o -8 3 1 1855.54 1963.71 157.49 o -7 3 1 2446.55 2471.29 161.31 o -6 3 1 290.19 276.96 67.03 o -5 3 1 1011.45 980.73 92.42 o -4 3 1 5903.44 7078.56 380.06 o -3 3 1 246.29 194.27 45.33 o -2 3 1 5389.75 5782.56 197.02 o -1 3 1 6526.27 6751.93 197.62 o 0 3 1 1848.52 1811.07 110.82 o 1 3 1 6523.84 6522.07 408.61 o 2 3 1 5395.80 5220.86 160.32 o 3 3 1 246.29 207.11 65.14 o 4 3 1 5903.03 5391.97 268.73 o 5 3 1 1011.99 958.53 140.90 o 6 3 1 291.06 273.30 112.77 o 7 3 1 2444.53 2627.70 273.65 o 8 3 1 1855.94 1886.13 260.00 o 9 3 1 157.49 189.58 109.17 o 10 3 1 18.67 17.50 76.30 o -10 4 1 137.83 170.60 113.72 o -9 4 1 144.55 136.18 120.30 o -8 4 1 573.01 570.48 96.40 o -7 4 1 341.35 358.20 76.60 o -6 4 1 26.94 52.67 59.53 o -5 4 1 1289.68 1270.12 117.50 o -4 4 1 919.20 959.94 91.02 o -3 4 1 2133.98 2194.02 118.56 o -2 4 1 3817.01 4075.20 497.24 o -1 4 1 4946.07 5321.28 354.48 o 0 4 1 88.33 57.43 20.97 o 1 4 1 4943.03 5018.20 356.63 o 2 4 1 3814.21 3720.63 126.61 o 3 4 1 2135.75 2033.88 126.07 o 4 4 1 918.67 895.88 127.07 o 5 4 1 1289.74 1232.03 160.04 o 6 4 1 27.04 0.00 89.36 o 7 4 1 341.94 446.37 136.29 o 8 4 1 573.68 521.55 160.46 o 9 4 1 144.83 141.11 111.44 o 10 4 1 138.01 179.30 130.69 o -10 5 1 65.55 66.62 105.96 o -9 5 1 196.37 177.21 96.39 o -8 5 1 15.20 20.90 51.53 o -7 5 1 18.22 0.08 44.42 o -6 5 1 65.21 75.18 63.72 o -5 5 1 0.22 11.03 43.26 o -4 5 1 1028.63 1061.53 106.39 o -3 5 1 1154.59 1211.99 98.62 o -2 5 1 419.49 438.72 50.17 o -1 5 1 325.83 306.93 21.29 o 0 5 1 53.78 72.18 23.15 o 1 5 1 326.28 301.85 36.88 o 2 5 1 419.46 391.29 58.17 o 3 5 1 1153.64 1117.81 119.14 o 4 5 1 1027.39 989.46 130.79 o 5 5 1 0.18 0.00 48.83 o 6 5 1 65.52 46.70 64.92 o 7 5 1 18.30 44.43 69.22 o 8 5 1 15.25 64.94 121.03 o 9 5 1 195.77 170.87 120.14 o -10 6 1 193.73 254.88 238.23 o -9 6 1 62.75 33.41 66.19 o -8 6 1 27.79 45.49 56.60 o -7 6 1 65.62 79.42 66.61 o -6 6 1 62.13 86.22 66.95 o -5 6 1 216.00 177.44 54.56 o -4 6 1 313.37 299.37 64.55 o -3 6 1 300.05 309.63 53.16 o -2 6 1 162.26 174.10 37.89 o -1 6 1 1414.62 1388.29 88.68 o 0 6 1 142.75 116.51 24.28 o 1 6 1 1411.84 1435.59 76.84 o 2 6 1 162.68 164.45 40.92 o 3 6 1 298.95 275.24 58.18 o 4 6 1 313.18 278.25 78.11 o 5 6 1 216.25 199.82 83.43 o 6 6 1 61.79 74.12 85.23 o 7 6 1 65.49 109.04 105.40 o 8 6 1 27.93 97.17 157.67 o 10 6 1 193.71 210.19 148.36 o -9 7 1 0.58 0.00 58.39 o -8 7 1 60.15 65.32 70.06 o -7 7 1 59.07 58.52 64.60 o -6 7 1 227.75 277.54 85.90 o -5 7 1 132.27 144.62 61.38 o -4 7 1 11.42 7.79 32.80 o -3 7 1 171.56 175.90 46.14 o -2 7 1 1033.30 1014.68 52.08 o -1 7 1 580.72 569.21 61.90 o 0 7 1 2026.48 2072.40 184.19 o 1 7 1 580.51 619.59 140.01 o 2 7 1 1033.21 946.63 75.97 o 3 7 1 171.66 164.03 61.14 o 4 7 1 11.53 0.00 70.31 o 5 7 1 132.13 166.87 88.33 o 6 7 1 228.40 230.22 90.45 o 7 7 1 59.13 87.89 130.69 o 8 7 1 60.07 62.99 114.19 o 9 7 1 0.58 0.00 92.77 o -7 8 1 187.51 198.15 101.30 o -6 8 1 53.78 58.04 52.01 o -5 8 1 88.19 72.27 51.84 o -4 8 1 113.87 121.96 43.21 o -3 8 1 1072.74 1175.53 109.03 o -2 8 1 1341.18 1296.37 147.09 o -1 8 1 102.13 110.20 79.60 o 0 8 1 1001.85 1131.28 199.03 o 1 8 1 101.97 101.61 111.04 o 2 8 1 1339.47 1260.83 205.91 o 3 8 1 1070.83 1035.39 163.30 o 4 8 1 114.04 121.58 98.74 o 5 8 1 88.49 60.77 58.86 o 6 8 1 54.09 75.19 104.96 o 7 8 1 187.66 216.78 147.77 o -8 9 1 5.98 32.23 85.94 o -7 9 1 55.25 73.75 77.16 o -6 9 1 21.04 0.00 72.84 o -5 9 1 44.16 73.17 90.74 o -4 9 1 72.22 66.98 96.30 o -3 9 1 626.42 671.95 122.35 o -2 9 1 733.76 775.12 132.71 o -1 9 1 138.31 179.03 135.31 o 0 9 1 568.21 638.62 187.87 o 1 9 1 138.96 130.23 104.15 o 2 9 1 733.82 779.22 185.51 o 3 9 1 625.58 626.93 314.87 o -6 10 1 115.78 120.03 107.18 o -5 10 1 32.96 58.54 97.85 o -4 10 1 172.39 197.26 215.44 o -3 10 1 1.96 13.83 55.79 o -2 10 1 67.61 73.50 78.67 o -1 10 1 260.87 288.81 146.36 o 0 10 1 117.24 115.72 111.81 o 1 10 1 260.69 295.05 142.33 o 2 10 1 67.70 82.02 145.42 o -4 11 1 178.65 195.21 137.40 o -3 11 1 59.43 46.33 64.28 o -2 11 1 0.07 4.39 104.49 o -1 11 1 10.02 4.17 67.14 o 0 11 1 169.67 125.57 106.08 o 1 11 1 10.06 37.50 74.63 o 2 11 1 0.07 0.00 80.96 o 1 0 2 1264.63 1112.04 57.57 o 2 0 2 23.41 43.25 18.91 o 3 0 2 1892.48 1749.57 112.51 o 4 0 2 388.38 361.75 94.10 o 5 0 2 2660.73 2469.34 223.62 o 6 0 2 2303.99 2288.22 221.74 o 7 0 2 566.15 519.66 78.13 o 8 0 2 83.16 36.33 87.16 o 9 0 2 33.92 21.86 83.95 o 10 0 2 36.08 0.00 106.44 o -10 1 2 158.49 141.33 122.21 o -9 1 2 46.20 74.70 142.14 o -8 1 2 40.40 62.14 65.41 o -7 1 2 166.53 149.34 56.64 o -6 1 2 2855.05 2835.96 157.98 o -5 1 2 2870.69 2874.18 148.00 o -4 1 2 706.14 687.25 70.76 o -3 1 2 17342.47 19464.42 566.61 o -2 1 2 4192.98 3665.45 627.54 o -1 1 2 16201.28 17451.68 410.34 o 0 1 2 1291.15 1355.10 83.34 o 1 1 2 16201.32 17476.68 674.78 o 2 1 2 4190.57 4474.34 235.14 o 3 1 2 17355.23 16358.50 1558.81 o 4 1 2 706.50 720.58 113.69 o 5 1 2 2868.78 2884.99 229.52 o 6 1 2 2854.02 2895.14 261.63 o 7 1 2 166.32 170.51 93.99 o 8 1 2 40.49 55.56 89.97 o 9 1 2 46.19 95.45 112.28 o 10 1 2 158.43 110.22 115.87 o -10 2 2 104.23 55.03 97.87 o -9 2 2 148.79 145.41 103.20 o -8 2 2 468.27 538.96 88.24 o -7 2 2 2541.44 2503.18 148.98 o -6 2 2 124.43 129.62 53.18 o -5 2 2 1015.34 1023.04 92.39 o -4 2 2 900.01 938.12 79.12 o -3 2 2 2867.76 2876.51 147.63 o -2 2 2 361.18 322.46 44.16 o -1 2 2 3835.75 3988.00 99.45 o 0 2 2 943.24 917.96 24.02 o 1 2 2 3833.19 3636.90 123.16 o 2 2 2 360.93 331.98 52.38 o 3 2 2 2868.42 2628.14 164.72 o 4 2 2 900.11 891.39 122.59 o 5 2 2 1015.23 955.91 144.74 o 6 2 2 124.54 88.87 69.09 o 7 2 2 2544.08 2311.72 265.13 o 8 2 2 468.15 522.71 152.09 o 9 2 2 148.70 126.24 112.88 o 10 2 2 104.56 66.27 87.12 o -10 3 2 264.26 360.34 231.32 o -9 3 2 55.85 58.60 90.15 o -8 3 2 41.52 31.11 62.69 o -7 3 2 202.64 193.86 57.68 o -6 3 2 443.13 460.30 74.60 o -5 3 2 1092.63 1080.57 100.39 o -4 3 2 394.19 397.47 66.09 o -3 3 2 293.71 279.15 50.83 o -2 3 2 1595.44 1465.15 80.89 o -1 3 2 22748.93 25370.23 603.16 o 0 3 2 38.63 77.03 23.30 o 1 3 2 22730.52 23756.33 1043.77 o 2 3 2 1598.99 1581.72 95.36 o 3 3 2 293.69 250.60 52.16 o 4 3 2 393.68 405.45 96.34 o 5 3 2 1092.35 1114.16 156.62 o 6 3 2 442.29 491.09 118.89 o 7 3 2 202.32 178.93 88.25 o 8 3 2 41.61 64.08 86.28 o 9 3 2 56.04 53.36 89.06 o 10 3 2 263.54 263.90 153.56 o -10 4 2 229.65 263.18 139.35 o -9 4 2 114.92 143.28 88.77 o -8 4 2 1644.36 1862.67 163.12 o -7 4 2 301.66 271.69 71.05 o -6 4 2 1902.28 2023.74 147.08 o -5 4 2 560.30 567.70 83.14 o -4 4 2 1436.62 1507.01 109.00 o -3 4 2 1764.79 1700.33 103.94 o -2 4 2 6175.80 7194.48 350.72 o -1 4 2 314.58 310.25 27.27 o 0 4 2 190.77 162.05 34.22 o 1 4 2 313.26 299.51 31.99 o 2 4 2 6175.41 6127.89 258.52 o 3 4 2 1764.10 1798.04 116.59 o 4 4 2 1436.07 1432.87 158.67 o 5 4 2 560.50 507.75 116.75 o 6 4 2 1902.72 1914.74 219.82 o 7 4 2 301.72 273.89 109.52 o 8 4 2 1644.10 1654.97 244.11 o 9 4 2 114.91 129.27 121.87 o 10 4 2 229.93 272.90 126.08 o -10 5 2 2.06 56.75 94.85 o -9 5 2 136.61 104.74 81.32 o -8 5 2 114.15 96.71 66.04 o -7 5 2 108.64 109.74 63.60 o -6 5 2 1448.08 1456.06 135.12 o -5 5 2 21.92 27.39 42.34 o -4 5 2 1390.91 1432.40 116.40 o -3 5 2 1848.86 1793.80 112.76 o -2 5 2 8861.99 9989.25 480.75 o -1 5 2 1569.67 1585.35 60.98 o 0 5 2 2.81 5.30 25.80 o 1 5 2 1570.89 1526.67 79.73 o 2 5 2 8857.15 8825.00 380.73 o 3 5 2 1849.30 1795.57 125.85 o 4 5 2 1390.70 1293.04 142.77 o 5 5 2 22.02 17.19 57.83 o 6 5 2 1448.56 1442.19 198.21 o 7 5 2 108.24 96.64 95.02 o 8 5 2 114.15 135.39 114.23 o 9 5 2 136.74 85.93 112.55 o 10 5 2 2.05 0.00 88.33 o -10 6 2 59.56 35.33 84.22 o -9 6 2 18.09 13.18 81.31 o -8 6 2 80.92 125.16 75.51 o -7 6 2 260.15 301.67 88.07 o -6 6 2 200.55 229.52 73.56 o -5 6 2 558.31 639.81 95.52 o -4 6 2 2155.01 2136.60 145.14 o -3 6 2 1117.79 1137.79 85.88 o -2 6 2 161.30 165.59 34.91 o -1 6 2 2860.88 2989.49 124.83 o 0 6 2 148.23 192.86 43.69 o 1 6 2 2860.63 2884.50 145.23 o 2 6 2 161.44 153.17 38.99 o 3 6 2 1118.73 1091.41 104.77 o 4 6 2 2155.11 1953.80 177.93 o 5 6 2 558.15 599.92 138.99 o 6 6 2 200.41 239.29 102.19 o 7 6 2 259.40 342.55 130.19 o 8 6 2 80.62 57.91 94.29 o 9 6 2 18.21 26.33 83.02 o 10 6 2 59.83 119.14 172.92 o -9 7 2 55.14 48.16 74.94 o -8 7 2 33.01 20.23 50.11 o -7 7 2 166.15 182.97 73.17 o -6 7 2 79.62 120.60 64.36 o -5 7 2 115.89 117.97 50.17 o -4 7 2 424.82 435.11 66.83 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31 373.23 446.28 300.37 o 1 6 31 117.40 167.96 196.10 o 0 0 32 1.16 13.18 112.79 o 1 0 32 162.56 169.18 138.45 o 2 0 32 0.25 0.00 84.67 o 3 0 32 5.71 43.83 79.55 o -3 1 32 20.64 64.45 120.06 o -2 1 32 83.28 101.96 115.38 o -1 1 32 212.83 298.46 149.93 o 0 1 32 22.81 34.73 89.18 o 1 1 32 212.26 246.85 157.03 o 2 1 32 83.23 83.34 106.09 o 3 1 32 20.52 39.06 100.10 o 4 1 32 1.81 0.00 96.19 o -3 2 32 20.32 0.00 106.44 o -2 2 32 21.18 40.41 87.54 o 0 2 32 88.36 132.02 129.77 o 1 2 32 10.38 43.98 86.81 o 2 2 32 21.17 15.08 83.79 o 3 2 32 20.44 24.41 94.24 o 4 2 32 0.85 19.04 95.21 o -4 3 32 49.65 110.84 160.50 o -3 3 32 91.80 38.08 109.86 o -1 3 32 52.89 60.54 130.37 o 0 3 32 73.37 112.24 122.32 o 1 3 32 53.25 120.77 128.38 o -4 4 32 51.95 31.74 94.24 o -3 4 32 112.12 200.68 164.35 o -1 4 32 69.66 100.09 157.57 o 0 4 32 73.35 10.74 111.32 o 1 4 32 69.87 102.54 159.16 o 2 4 32 6.03 0.00 101.56 o 3 4 32 112.08 144.04 165.03 o 4 4 32 51.85 53.71 106.44 o -1 5 32 33.74 0.00 94.24 o 1 5 32 33.67 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