#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2200907.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2200907_Fobs loop_ _publ_author_name 'Barnes, John C.' 'Brimacombe, John S.' 'Connolly, Lisa M. C.' 'Dix, Alexander P.' _publ_section_title ; Methyl (2'R,3'R)-6-deoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-2-O-toluene-p-sulfonyl-\a-L-mannopyranoside ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o224 _journal_page_last o226 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.7709 _cell_length_b 14.0181 _cell_length_c 18.1744 _exptl_crystal_F_000 952.00 _reflns_d_resolution_high 0.7507 _[local]_cod_data_source_file dn6017Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Lisa's First Compound' _shelx_refln_list_code 4 _shelx_f_calc_maximum 198.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 380.66 442.39 12.74 o 2 1 0 11000.47 10096.04 151.88 o 3 1 0 152.47 155.45 4.59 o 4 1 0 988.74 968.37 19.37 o 5 1 0 3239.21 3229.77 82.06 o 6 1 0 3.83 9.17 6.63 o 1 2 0 7553.06 7337.71 108.56 o 2 2 0 473.50 424.04 11.72 o 3 2 0 558.92 571.85 10.19 o 4 2 0 2089.27 2195.15 38.73 o 5 2 0 179.56 183.48 6.63 o 6 2 0 73.97 56.57 8.15 o 7 2 0 285.24 273.69 14.27 o 1 3 0 108.90 127.42 7.14 o 2 3 0 977.78 1017.30 18.86 o 3 3 0 297.69 354.73 10.70 o 4 3 0 25.80 37.21 4.59 o 5 3 0 5.26 -4.08 5.10 o 6 3 0 568.08 522.92 23.44 o 7 3 0 264.41 244.64 18.86 o 8 3 0 240.91 228.33 31.09 o 0 4 0 4523.56 4588.04 124.36 o 1 4 0 1880.70 1862.84 36.19 o 2 4 0 3015.06 2927.54 49.95 o 3 4 0 44.09 61.16 7.14 o 4 4 0 738.86 688.05 19.37 o 5 4 0 1529.41 1472.94 31.60 o 6 4 0 10.22 12.74 7.14 o 7 4 0 820.51 764.50 58.61 o 8 4 0 908.76 936.26 51.48 o 1 5 0 404.74 446.47 20.39 o 2 5 0 23.42 17.84 12.23 o 3 5 0 1791.78 1954.07 53.01 o 4 5 0 1407.79 1518.31 37.72 o 5 5 0 1753.46 1661.52 36.19 o 6 5 0 970.88 1052.98 33.13 o 7 5 0 5145.44 5175.69 133.53 o 8 5 0 260.07 293.06 36.19 o 0 6 0 722.70 724.24 53.52 o 1 6 0 3056.87 2873.01 69.82 o 2 6 0 1140.23 1480.59 50.97 o 3 6 0 2072.85 2125.83 59.63 o 4 6 0 1446.57 1540.22 48.42 o 5 6 0 157.37 146.28 20.39 o 6 6 0 2088.00 2124.30 51.99 o 7 6 0 621.25 601.92 32.11 o 8 6 0 175.28 202.34 32.62 o 1 7 0 5.29 -8.15 13.25 o 2 7 0 842.72 877.14 32.11 o 3 7 0 7.48 17.33 15.29 o 4 7 0 1322.98 1273.66 42.81 o 5 7 0 542.41 484.70 27.01 o 6 7 0 1.53 2.55 17.84 o 7 7 0 22.97 14.27 12.23 o 8 7 0 652.40 650.85 48.93 o 0 8 0 4.78 -0.51 22.94 o 1 8 0 919.89 1075.40 41.28 o 2 8 0 1281.83 1368.46 51.99 o 3 8 0 396.15 378.17 29.56 o 4 8 0 15.50 54.53 16.82 o 5 8 0 721.82 708.44 31.60 o 6 8 0 160.12 160.55 21.41 o 7 8 0 628.85 639.64 37.72 o 8 8 0 57.97 74.92 33.64 o 9 8 0 44.65 52.50 70.33 o 1 9 0 0.07 35.17 22.43 o 2 9 0 803.98 813.94 39.75 o 3 9 0 20.34 1.53 18.35 o 4 9 0 0.15 14.27 24.97 o 5 9 0 969.30 1083.56 42.81 o 6 9 0 106.54 85.62 24.46 o 7 9 0 735.43 842.48 49.44 o 8 9 0 64.97 54.53 46.38 o 9 9 0 944.62 1014.24 90.21 o 0 10 0 1297.25 1279.78 75.94 o 1 10 0 1727.53 1733.39 60.65 o 2 10 0 2494.50 2528.47 77.47 o 3 10 0 128.00 126.40 26.50 o 4 10 0 825.25 774.19 41.28 o 5 10 0 309.91 287.96 25.99 o 6 10 0 843.24 832.80 47.40 o 7 10 0 30.59 69.82 24.46 o 8 10 0 17.85 10.70 59.63 o 9 10 0 41.44 -12.74 42.81 o 1 11 0 722.51 686.52 44.85 o 2 11 0 155.30 131.49 24.46 o 3 11 0 61.05 55.04 23.95 o 4 11 0 113.16 130.48 26.50 o 5 11 0 2.93 -1.53 22.43 o 6 11 0 12.65 40.77 28.54 o 7 11 0 160.10 212.53 35.68 o 8 11 0 46.26 34.15 46.38 o 9 11 0 1.16 12.23 47.91 o 0 12 0 1861.12 1976.50 104.48 o 1 12 0 29.85 1.02 26.50 o 2 12 0 375.99 274.71 33.13 o 3 12 0 81.98 33.64 27.01 o 4 12 0 17.24 -17.84 26.50 o 5 12 0 83.36 204.38 34.66 o 6 12 0 12.96 33.13 33.64 o 7 12 0 75.78 124.87 30.07 o 8 12 0 68.98 7.14 47.40 o 1 13 0 386.73 303.25 35.17 o 2 13 0 87.51 66.77 33.13 o 3 13 0 23.49 13.25 26.50 o 4 13 0 0.09 3.57 39.75 o 5 13 0 3.85 2.55 33.13 o 6 13 0 89.13 93.27 32.62 o 7 13 0 52.16 66.26 36.19 o 8 13 0 162.41 371.04 98.37 o 0 14 0 1453.21 1470.91 111.62 o 1 14 0 19.81 33.64 41.28 o 2 14 0 670.32 724.75 59.63 o 3 14 0 23.59 108.05 50.46 o 4 14 0 69.37 65.75 51.48 o 5 14 0 98.43 125.38 44.34 o 6 14 0 48.05 45.36 33.64 o 7 14 0 16.00 -3.06 38.73 o 1 15 0 127.99 135.57 48.42 o 2 15 0 1.16 42.81 41.79 o 3 15 0 126.24 60.65 36.70 o 4 15 0 119.39 173.80 46.38 o 5 15 0 11.07 -16.82 37.72 o 6 15 0 63.92 27.52 39.75 o 0 16 0 0.80 162.07 94.80 o 1 16 0 398.95 472.97 56.57 o 2 16 0 243.96 151.88 41.28 o 3 16 0 249.98 206.93 60.65 o 4 16 0 0.08 -11.21 40.26 o 5 16 0 31.56 -24.97 57.08 o 6 16 0 178.26 322.62 57.59 o 1 17 0 276.91 286.43 48.93 o 2 17 0 107.45 48.93 42.81 o 3 17 0 1.44 -1.02 38.73 o 4 17 0 444.23 445.96 62.18 o 0 18 0 25.35 19.37 74.92 o 1 18 0 195.74 319.56 66.77 o 2 18 0 58.77 91.74 55.04 o 3 18 0 154.90 152.39 53.52 o 2 0 1 471.24 435.77 9.68 o 3 0 1 8647.93 8209.75 188.07 o 4 0 1 73.88 62.18 5.61 o 5 0 1 1593.86 1720.64 44.85 o 6 0 1 31.04 22.94 6.12 o -7 1 1 56.38 58.10 7.14 o -6 1 1 67.01 83.59 18.35 o -5 1 1 704.45 679.90 16.82 o -4 1 1 951.42 991.82 20.39 o -3 1 1 2544.22 2489.23 44.34 o -2 1 1 1711.53 1796.07 29.56 o -1 1 1 7560.47 7139.45 97.86 o 1 1 1 7462.01 7074.72 109.07 o 2 1 1 1679.78 1795.57 30.58 o 3 1 1 2543.75 2506.04 46.38 o 4 1 1 928.78 1014.24 30.07 o 5 1 1 694.89 720.16 16.31 o 6 1 1 66.36 50.97 9.68 o 7 1 1 53.13 48.93 10.70 o -8 2 1 163.23 132.51 20.39 o -7 2 1 442.80 406.21 18.86 o -6 2 1 39.38 41.28 4.59 o -5 2 1 459.28 413.34 11.72 o -4 2 1 559.57 611.09 12.74 o -3 2 1 653.73 671.23 13.76 o -2 2 1 1702.16 1656.43 28.03 o -1 2 1 4743.24 4538.10 67.28 o 0 2 1 10990.08 10529.26 166.66 o 1 2 1 4748.10 4504.97 69.32 o 2 2 1 1689.64 1658.46 26.50 o 3 2 1 675.89 700.29 14.78 o 4 2 1 574.74 661.04 13.25 o 5 2 1 482.75 484.19 17.84 o 6 2 1 37.53 37.21 4.59 o 7 2 1 458.84 452.59 17.84 o 8 2 1 165.24 134.55 20.90 o -8 3 1 107.49 70.33 12.74 o -7 3 1 1078.24 991.31 40.77 o -6 3 1 725.79 763.99 22.43 o -5 3 1 926.92 916.39 19.37 o -4 3 1 544.52 535.66 12.74 o -3 3 1 2440.69 2501.97 41.28 o -2 3 1 820.94 826.17 16.82 o -1 3 1 8927.01 8771.92 130.48 o 0 3 1 5336.17 5388.73 79.51 o 1 3 1 8884.24 8701.58 124.36 o 2 3 1 844.98 847.58 17.33 o 3 3 1 2451.87 2485.66 42.81 o 4 3 1 544.76 530.57 13.76 o 5 3 1 919.82 891.92 19.88 o 6 3 1 718.08 764.50 22.43 o 7 3 1 1060.53 1061.13 38.23 o 8 3 1 107.11 90.72 16.31 o -8 4 1 132.58 118.75 24.97 o -7 4 1 1506.42 1506.07 46.89 o -6 4 1 1254.00 1245.12 29.56 o -5 4 1 503.45 475.01 14.78 o -4 4 1 1942.42 1937.25 39.24 o -3 4 1 1931.80 2022.37 37.21 o -2 4 1 1008.58 1003.54 21.41 o -1 4 1 1687.39 1724.21 32.11 o 0 4 1 450.18 416.40 14.27 o 1 4 1 1724.83 1738.99 32.11 o 2 4 1 991.42 1032.59 23.95 o 3 4 1 1952.33 2046.83 37.72 o 4 4 1 1948.26 2000.96 40.26 o 5 4 1 490.03 507.63 16.31 o 6 4 1 1243.71 1232.89 29.56 o 7 4 1 1490.23 1444.40 50.46 o 8 4 1 132.39 205.40 27.52 o -8 5 1 20.30 -9.17 18.86 o -7 5 1 8.46 13.76 5.61 o -6 5 1 239.03 257.38 16.31 o -5 5 1 754.78 724.75 20.39 o -4 5 1 58.87 47.40 11.21 o -3 5 1 2177.22 2265.48 52.50 o -2 5 1 1540.46 1519.83 39.24 o -1 5 1 94.44 101.93 14.27 o 0 5 1 3944.90 3976.95 108.56 o 1 5 1 98.81 108.56 12.23 o 2 5 1 1537.95 1517.80 41.28 o 3 5 1 2138.23 2164.06 48.42 o 4 5 1 63.01 34.15 9.68 o 5 5 1 757.97 779.79 26.50 o 6 5 1 251.65 251.78 13.25 o 7 5 1 8.57 10.19 5.10 o 8 5 1 23.62 31.09 35.17 o -8 6 1 119.80 123.85 30.58 o -7 6 1 573.32 569.30 25.99 o -6 6 1 440.65 455.64 22.94 o -5 6 1 2201.83 2233.88 64.22 o -4 6 1 666.56 567.26 25.99 o -3 6 1 187.46 166.15 15.80 o -2 6 1 3798.07 3778.18 93.78 o -1 6 1 1287.27 1261.94 42.30 o 0 6 1 1735.00 1750.71 73.90 o 1 6 1 1301.37 1308.83 44.34 o 2 6 1 3782.25 3817.93 111.62 o 3 6 1 196.40 177.36 15.80 o 4 6 1 659.91 701.31 29.05 o 5 6 1 2205.09 2288.93 62.18 o 6 6 1 444.91 414.36 19.88 o 7 6 1 561.12 578.98 25.99 o 8 6 1 124.52 121.30 26.50 o -8 7 1 81.74 139.14 51.99 o -7 7 1 522.32 564.20 31.60 o -6 7 1 21.11 25.48 16.82 o -5 7 1 2068.16 2057.54 62.69 o -4 7 1 1383.05 1499.96 49.95 o -3 7 1 389.12 487.24 27.01 o -2 7 1 1010.58 1020.87 41.28 o -1 7 1 1878.81 2009.12 58.10 o 0 7 1 1466.25 1579.98 49.44 o 1 7 1 1880.82 2061.61 58.10 o 2 7 1 975.04 979.58 37.21 o 3 7 1 378.53 425.57 25.99 o 4 7 1 1354.63 1487.72 43.83 o 5 7 1 2079.62 2073.33 74.92 o 6 7 1 20.00 36.70 14.78 o 7 7 1 526.08 496.93 28.54 o 8 7 1 80.87 74.41 29.05 o -9 8 1 428.54 536.68 88.68 o -8 8 1 313.84 339.95 50.97 o -7 8 1 319.58 399.58 38.23 o -6 8 1 389.84 378.17 26.50 o -5 8 1 814.30 810.88 34.66 o -4 8 1 587.29 639.64 31.60 o -3 8 1 510.39 589.18 31.09 o -2 8 1 1182.12 1231.36 51.48 o -1 8 1 378.58 445.96 31.60 o 0 8 1 328.48 425.57 28.03 o 1 8 1 376.42 430.16 30.07 o 2 8 1 1204.87 1310.36 49.44 o 3 8 1 513.01 573.89 30.07 o 4 8 1 584.89 535.66 27.52 o 5 8 1 801.54 720.67 35.17 o 6 8 1 381.54 340.46 23.95 o 7 8 1 324.50 333.83 28.03 o 8 8 1 311.16 444.43 46.89 o -9 9 1 61.34 -25.99 50.46 o -8 9 1 400.65 428.63 54.53 o -7 9 1 232.93 268.09 32.62 o -6 9 1 86.36 62.18 21.41 o -5 9 1 847.46 777.76 44.85 o -4 9 1 41.93 45.36 17.84 o -3 9 1 596.15 687.54 41.79 o -2 9 1 61.00 115.19 21.41 o -1 9 1 11.39 23.44 17.84 o 0 9 1 0.36 42.81 31.09 o 1 9 1 10.10 15.29 19.37 o 2 9 1 60.57 66.77 19.37 o 3 9 1 616.75 732.39 40.26 o 4 9 1 44.24 58.61 20.90 o 5 9 1 863.51 843.50 37.21 o 6 9 1 80.02 66.77 20.90 o 7 9 1 231.55 212.53 27.01 o 8 9 1 402.19 404.17 55.55 o 9 9 1 61.50 46.89 50.97 o -9 10 1 151.50 167.17 107.54 o -8 10 1 157.75 187.56 44.85 o -7 10 1 139.66 189.09 35.17 o -6 10 1 256.01 317.52 30.58 o -5 10 1 45.38 34.66 24.97 o -4 10 1 113.01 79.00 24.97 o -3 10 1 728.03 608.04 37.21 o -2 10 1 427.87 339.44 31.60 o -1 10 1 1558.29 1447.46 59.12 o 0 10 1 657.93 717.10 49.95 o 1 10 1 1556.79 1486.20 67.79 o 2 10 1 420.01 385.31 31.60 o 3 10 1 734.83 743.10 41.79 o 4 10 1 112.97 107.03 21.92 o 5 10 1 44.03 12.74 19.88 o 6 10 1 253.57 237.51 27.52 o 7 10 1 140.60 152.39 29.05 o 8 10 1 155.18 172.27 56.06 o 9 10 1 148.61 38.23 61.67 o -9 11 1 36.34 79.00 64.22 o -8 11 1 54.96 133.53 76.45 o -7 11 1 89.61 113.66 35.68 o -6 11 1 11.42 10.19 28.54 o -5 11 1 252.45 209.98 32.62 o -4 11 1 224.57 156.98 28.54 o -3 11 1 185.97 143.73 30.58 o -2 11 1 1142.66 1023.93 44.85 o -1 11 1 675.18 720.16 45.36 o 0 11 1 143.49 139.65 36.19 o 1 11 1 693.73 710.48 42.81 o 2 11 1 1135.80 1056.54 47.91 o 3 11 1 193.48 198.77 33.64 o 4 11 1 218.22 272.16 37.21 o 5 11 1 261.00 158.00 25.48 o 6 11 1 12.83 47.91 29.56 o 7 11 1 91.03 68.30 30.07 o 8 11 1 57.94 20.90 76.45 o 9 11 1 35.75 -15.29 45.36 o -8 12 1 65.22 42.30 53.52 o -7 12 1 81.29 88.17 36.19 o -6 12 1 105.01 78.49 33.64 o -5 12 1 23.95 -15.29 25.48 o -4 12 1 8.25 -7.65 26.50 o -3 12 1 360.56 365.94 44.85 o -2 12 1 578.07 631.99 43.32 o -1 12 1 370.60 453.61 37.72 o 0 12 1 173.24 223.24 35.68 o 1 12 1 374.98 361.36 33.13 o 2 12 1 564.48 517.31 38.73 o 3 12 1 365.34 359.32 36.19 o 4 12 1 8.24 -21.92 25.48 o 5 12 1 27.47 114.17 31.60 o 6 12 1 105.31 177.36 35.17 o 7 12 1 84.19 18.86 39.24 o 8 12 1 64.39 7.65 54.02 o -8 13 1 14.98 -55.55 63.71 o -7 13 1 227.78 294.08 46.89 o -6 13 1 13.21 -2.04 32.62 o -5 13 1 94.64 69.82 36.70 o -4 13 1 45.60 61.16 34.66 o -3 13 1 194.22 89.70 32.62 o -2 13 1 1566.15 1642.66 85.11 o -1 13 1 96.78 121.30 32.62 o 0 13 1 1084.10 1046.35 55.55 o 1 13 1 101.87 117.22 31.60 o 2 13 1 1570.64 1460.71 74.41 o 3 13 1 194.37 180.42 37.72 o 4 13 1 44.04 20.90 32.62 o 5 13 1 89.41 169.72 41.79 o 6 13 1 12.52 41.79 32.62 o 7 13 1 221.35 118.75 41.79 o 8 13 1 14.01 -52.50 52.50 o -7 14 1 16.31 0.51 39.75 o -6 14 1 13.04 5.10 35.17 o -5 14 1 9.67 36.70 36.70 o -4 14 1 69.26 64.22 39.75 o -3 14 1 207.93 338.93 55.55 o -2 14 1 125.63 59.12 34.66 o -1 14 1 130.44 86.13 31.60 o 0 14 1 672.33 804.77 58.10 o 1 14 1 137.18 203.87 35.68 o 2 14 1 121.47 91.74 35.17 o 3 14 1 203.21 215.59 58.10 o 4 14 1 64.70 23.44 35.17 o 5 14 1 10.31 -48.42 48.42 o 6 14 1 10.42 -17.33 35.68 o 7 14 1 16.99 62.69 39.24 o -6 15 1 97.38 116.20 41.79 o -5 15 1 119.37 111.62 42.81 o -4 15 1 83.83 64.22 41.79 o -3 15 1 280.49 386.84 51.99 o -2 15 1 58.07 137.10 43.83 o -1 15 1 170.68 177.87 49.44 o 0 15 1 22.56 -6.12 36.19 o 1 15 1 163.58 136.59 38.73 o 2 15 1 58.35 26.50 37.72 o 3 15 1 284.42 222.73 45.87 o 4 15 1 82.30 171.76 49.95 o 5 15 1 122.36 160.55 44.34 o 6 15 1 95.60 92.25 41.28 o -6 16 1 57.74 -40.26 61.67 o -5 16 1 163.54 264.52 62.18 o -4 16 1 160.40 163.60 43.83 o -3 16 1 39.71 67.28 46.38 o -2 16 1 36.06 27.01 37.72 o -1 16 1 159.83 33.64 39.75 o 0 16 1 497.43 354.73 67.79 o 1 16 1 156.76 83.08 41.79 o 2 16 1 37.39 4.59 39.75 o 3 16 1 38.15 -38.23 38.23 o 4 16 1 164.81 162.07 44.85 o 5 16 1 168.78 159.53 59.63 o 6 16 1 60.16 90.72 55.55 o -4 17 1 0.05 -18.35 63.20 o -3 17 1 24.41 31.60 47.91 o -2 17 1 116.85 144.75 52.50 o -1 17 1 8.93 9.68 41.79 o 0 17 1 66.95 173.29 46.89 o 1 17 1 8.43 17.33 44.85 o 2 17 1 120.05 168.70 57.08 o 3 17 1 23.97 -21.41 47.91 o 4 17 1 0.11 -17.33 55.04 o -3 18 1 127.64 282.36 65.24 o -2 18 1 12.55 12.23 50.46 o -1 18 1 25.11 -6.63 50.46 o 0 18 1 68.84 57.59 51.99 o 1 18 1 24.08 33.64 52.50 o 2 18 1 12.00 -50.97 50.97 o 3 18 1 124.35 14.78 61.16 o 1 0 2 138.29 143.73 4.59 o 2 0 2 2502.04 2446.92 41.79 o 3 0 2 2819.67 2886.26 49.95 o 4 0 2 1127.77 1149.30 31.60 o 5 0 2 28.03 23.95 11.21 o 6 0 2 235.16 216.10 12.23 o 7 0 2 636.11 606.00 23.44 o -8 1 2 278.24 259.93 26.50 o -7 1 2 49.04 38.73 5.10 o -6 1 2 65.45 65.75 8.15 o -5 1 2 683.05 733.92 17.84 o -4 1 2 1552.00 1603.42 33.13 o -3 1 2 2224.84 2202.28 36.70 o -2 1 2 3101.80 3120.71 50.97 o -1 1 2 8207.76 7755.64 115.19 o 1 1 2 8171.39 7859.10 116.20 o 2 1 2 3029.71 2934.17 46.89 o 3 1 2 2231.20 2200.24 36.70 o 4 1 2 1523.23 1583.03 29.56 o 5 1 2 678.81 745.14 19.37 o 6 1 2 65.59 91.23 8.66 o 7 1 2 46.61 46.89 8.15 o 8 1 2 283.05 249.23 24.97 o -8 2 2 686.91 679.90 62.18 o -7 2 2 1269.42 1269.59 47.91 o -6 2 2 1152.95 1111.08 28.03 o -5 2 2 231.08 233.94 10.19 o -4 2 2 1796.93 1690.06 30.58 o -3 2 2 1481.88 1460.20 25.99 o -2 2 2 1906.76 1864.88 29.56 o -1 2 2 12907.97 12741.74 179.91 o 0 2 2 39249.19 35677.88 512.22 o 1 2 2 12922.10 12814.11 187.56 o 2 2 2 1896.34 1879.66 36.19 o 3 2 2 1467.54 1481.61 25.48 o 4 2 2 1798.75 1817.99 32.11 o 5 2 2 228.13 230.37 11.21 o 6 2 2 1159.15 1157.46 25.48 o 7 2 2 1261.74 1252.77 43.32 o 8 2 2 715.23 735.96 61.16 o -8 3 2 500.47 543.82 60.14 o -7 3 2 1881.29 1986.69 63.20 o -6 3 2 46.09 34.66 7.14 o -5 3 2 34.70 41.79 4.59 o -4 3 2 191.47 204.89 9.17 o -3 3 2 3880.55 3937.20 65.24 o -2 3 2 2138.31 2141.12 36.19 o -1 3 2 14709.66 14142.81 203.87 o 0 3 2 172.22 201.32 11.21 o 1 3 2 14713.16 14036.29 200.30 o 2 3 2 2160.63 2223.18 35.17 o 3 3 2 3860.51 3982.05 63.20 o 4 3 2 184.10 211.51 8.66 o 5 3 2 32.37 43.83 4.59 o 6 3 2 47.69 45.36 7.14 o 7 3 2 1886.16 1954.58 67.28 o 8 3 2 501.48 392.96 42.81 o -8 4 2 155.43 190.62 29.05 o -7 4 2 1155.17 1125.86 41.28 o -6 4 2 431.01 380.72 13.25 o -5 4 2 3230.60 3246.08 64.73 o -4 4 2 399.00 425.06 13.25 o -3 4 2 9000.82 9437.55 162.07 o -2 4 2 2270.95 2418.89 44.34 o -1 4 2 2039.48 2090.15 39.24 o 0 4 2 1598.69 1519.83 28.54 o 1 4 2 2018.87 2044.79 34.66 o 2 4 2 2294.80 2387.80 42.81 o 3 4 2 8931.58 9402.38 147.29 o 4 4 2 394.10 418.44 14.27 o 5 4 2 3187.55 3174.22 62.18 o 6 4 2 437.47 405.19 14.27 o 7 4 2 1117.89 1033.61 39.24 o 8 4 2 154.79 141.69 31.09 o -8 5 2 38.49 13.76 22.94 o -7 5 2 157.71 163.09 19.88 o -6 5 2 2430.53 2394.43 65.75 o -5 5 2 342.17 321.09 17.33 o -4 5 2 127.56 97.86 13.76 o -3 5 2 2386.37 2627.35 61.67 o -2 5 2 67.25 104.99 13.25 o -1 5 2 4294.34 4298.04 96.33 o 0 5 2 12.34 3.57 11.21 o 1 5 2 4280.49 4179.80 89.70 o 2 5 2 61.88 118.24 12.74 o 3 5 2 2391.97 2701.25 60.14 o 4 5 2 122.01 127.42 13.25 o 5 5 2 347.04 318.03 15.29 o 6 5 2 2415.59 2412.27 64.73 o 7 5 2 160.13 189.60 24.46 o 8 5 2 37.75 57.59 21.92 o -9 6 2 212.56 224.25 55.55 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