#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/10/2201009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201009_Fobs loop_ _publ_author_name 'Brooks, Neil R.' 'Henderson, Wesley A.' 'Smyrl, William H.' _publ_section_title ; Lithium trifluoromethanesulfonate acetonitrile adduct ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m176 _journal_page_last m177 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.064 _cell_angle_gamma 90.000 _cell_length_a 5.4814 _cell_length_b 14.7900 _cell_length_c 9.4090 _exptl_crystal_F_000 392.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file ac6002Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 02053 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6.09 12.24 0.63 o 2 0 0 9146.45 8543.98 156.60 o 3 0 0 280.01 275.35 4.84 o 4 0 0 4378.58 4469.24 94.88 o 5 0 0 229.69 203.69 4.73 o 6 0 0 511.68 519.48 11.48 o 7 0 0 78.86 82.95 2.46 o 1 1 0 8232.71 7588.40 149.09 o 2 1 0 45.72 31.55 0.59 o 3 1 0 239.13 243.49 3.36 o 4 1 0 165.98 151.49 2.21 o 6 1 0 9.84 11.96 1.01 o 7 1 0 41.06 50.26 1.48 o 0 2 0 1571.14 1433.84 28.46 o 1 2 0 75.05 75.75 1.06 o 2 2 0 1456.48 1668.93 22.20 o 3 2 0 268.50 271.16 3.37 o 4 2 0 17.38 19.13 0.54 o 5 2 0 231.54 229.42 3.71 o 6 2 0 70.01 68.72 1.46 o 7 2 0 1.67 1.04 0.72 o 1 3 0 2066.10 2120.68 25.67 o 2 3 0 534.35 578.33 7.77 o 3 3 0 53.83 66.23 1.04 o 4 3 0 932.38 886.15 11.95 o 5 3 0 34.73 33.26 0.91 o 6 3 0 246.03 246.66 4.05 o 7 3 0 0.09 0.20 0.75 o 0 4 0 1149.00 1215.37 23.99 o 1 4 0 653.67 659.26 8.00 o 2 4 0 827.28 701.76 9.42 o 3 4 0 129.66 151.18 2.16 o 4 4 0 299.78 289.28 4.03 o 5 4 0 1594.50 1617.69 24.48 o 6 4 0 104.94 110.16 2.08 o 1 5 0 92.52 91.27 1.16 o 2 5 0 241.70 229.19 2.84 o 3 5 0 735.49 823.69 11.04 o 4 5 0 341.92 339.85 4.71 o 5 5 0 68.11 75.63 1.32 o 6 5 0 74.78 69.46 1.47 o 0 6 0 14621.41 13557.86 545.66 o 1 6 0 179.15 192.35 2.39 o 2 6 0 744.51 787.80 9.56 o 3 6 0 242.37 239.02 3.31 o 4 6 0 384.96 386.80 5.33 o 5 6 0 11.77 12.37 0.61 o 6 6 0 115.00 112.84 2.10 o 1 7 0 1892.90 1834.51 23.69 o 2 7 0 21.27 23.73 0.50 o 3 7 0 0.29 1.15 0.50 o 4 7 0 231.32 228.02 3.24 o 5 7 0 25.26 22.26 0.69 o 6 7 0 34.25 39.93 1.49 o 0 8 0 1809.00 1870.16 36.85 o 1 8 0 122.97 122.71 1.68 o 2 8 0 1177.77 1260.60 15.17 o 3 8 0 334.85 310.46 4.68 o 4 8 0 0.90 1.07 0.80 o 5 8 0 246.12 238.39 3.77 o 6 8 0 13.11 11.55 0.84 o 1 9 0 569.48 577.38 7.53 o 2 9 0 226.90 214.17 2.89 o 3 9 0 97.96 92.00 1.56 o 4 9 0 118.83 114.29 1.94 o 5 9 0 35.22 32.65 0.94 o 6 9 0 4.00 4.35 0.71 o 0 10 0 136.75 106.23 2.33 o 1 10 0 43.76 43.63 0.82 o 2 10 0 112.88 111.50 1.83 o 3 10 0 25.71 25.25 0.67 o 4 10 0 11.20 9.84 0.55 o 5 10 0 147.06 151.34 2.56 o 6 10 0 7.02 7.13 1.11 o 1 11 0 1100.14 1073.99 15.08 o 2 11 0 74.85 69.93 1.40 o 3 11 0 691.67 685.73 9.76 o 4 11 0 178.92 181.66 2.95 o 5 11 0 129.92 127.52 2.26 o 0 12 0 444.89 439.04 8.84 o 1 12 0 55.22 56.53 1.03 o 2 12 0 356.71 335.20 5.59 o 3 12 0 4.09 3.89 0.49 o 4 12 0 210.34 200.50 3.56 o 5 12 0 265.09 266.51 4.70 o 1 13 0 64.44 62.20 1.12 o 2 13 0 0.24 0.49 0.39 o 3 13 0 346.56 318.62 5.43 o 4 13 0 52.39 54.28 1.38 o 5 13 0 7.28 6.17 0.78 o 0 14 0 6.02 9.21 0.64 o 1 14 0 2.91 3.38 0.38 o 2 14 0 131.04 119.32 2.24 o 3 14 0 69.37 61.09 1.42 o 4 14 0 71.77 64.55 1.54 o 1 15 0 446.71 444.47 7.35 o 2 15 0 60.77 58.37 1.38 o 3 15 0 57.18 57.88 1.42 o 4 15 0 174.96 163.99 3.10 o 0 16 0 1254.72 1257.03 25.03 o 1 16 0 69.26 70.76 1.38 o 2 16 0 287.45 295.19 5.10 o 3 16 0 49.19 49.81 1.38 o 1 17 0 33.32 31.07 1.10 o 2 17 0 29.53 30.45 1.10 o 3 17 0 16.19 19.13 1.36 o 0 18 0 47.01 50.07 1.76 o 1 18 0 12.26 15.54 0.90 o 2 18 0 70.94 73.85 1.83 o 1 19 0 78.26 78.54 2.36 o -7 1 1 32.12 34.38 1.23 o -6 1 1 14.57 14.64 0.73 o -5 1 1 397.71 380.60 5.99 o -4 1 1 214.74 210.84 2.97 o -3 1 1 394.81 384.31 4.72 o -2 1 1 161.49 196.07 3.30 o -1 1 1 251.55 286.68 5.37 o 0 1 1 2416.75 2390.43 29.40 o 1 1 1 125.80 151.91 3.03 o 2 1 1 79.01 102.03 2.14 o 3 1 1 353.36 364.31 4.47 o 4 1 1 104.72 108.18 2.39 o 5 1 1 260.17 254.02 7.75 o 6 1 1 9.47 8.55 1.06 o 7 1 1 38.53 43.46 2.15 o -7 2 1 140.21 145.77 3.71 o -6 2 1 223.79 225.86 3.75 o -5 2 1 397.05 396.88 6.23 o -4 2 1 1089.36 1058.18 14.23 o -3 2 1 1532.80 1562.12 20.78 o -2 2 1 356.39 360.69 4.86 o -1 2 1 8887.70 8470.10 104.56 o 0 2 1 95.83 126.05 1.56 o 1 2 1 8963.63 8559.08 102.95 o 2 2 1 360.13 395.14 5.21 o 3 2 1 2062.88 2111.66 25.53 o 4 2 1 888.18 866.47 12.77 o 5 2 1 243.30 246.88 6.80 o 6 2 1 241.42 238.78 3.95 o 7 2 1 173.12 179.14 3.53 o -7 3 1 38.34 42.34 1.36 o -6 3 1 7.33 7.53 0.59 o -5 3 1 235.61 236.09 3.82 o -4 3 1 239.10 253.76 3.57 o -3 3 1 30.73 23.03 0.61 o -2 3 1 127.14 135.07 2.11 o -1 3 1 289.37 302.04 3.68 o 0 3 1 2081.42 2046.05 24.81 o 1 3 1 542.00 561.13 8.55 o 2 3 1 73.85 76.15 1.92 o 3 3 1 62.44 42.30 0.68 o 4 3 1 136.77 145.81 3.59 o 5 3 1 282.08 275.13 4.42 o 6 3 1 6.62 7.71 0.61 o 7 3 1 65.24 72.59 2.36 o -6 4 1 13.33 12.43 0.74 o -5 4 1 216.69 215.10 3.51 o -4 4 1 24.64 24.50 0.67 o -3 4 1 816.70 842.39 11.27 o -2 4 1 3.57 3.04 0.43 o -1 4 1 5170.35 5445.78 65.51 o 0 4 1 141.26 167.63 2.07 o 1 4 1 6781.26 6980.42 84.12 o 2 4 1 1.86 3.47 0.24 o 3 4 1 938.84 1005.86 12.19 o 4 4 1 45.09 44.89 0.95 o 5 4 1 275.74 276.43 3.92 o 6 4 1 18.42 16.59 0.76 o -6 5 1 40.53 44.23 1.14 o -5 5 1 322.03 317.99 5.06 o -4 5 1 197.02 182.55 2.62 o -3 5 1 3.55 4.69 0.67 o -2 5 1 483.73 461.39 6.74 o -1 5 1 256.53 261.94 3.22 o 0 5 1 4032.17 4014.68 48.40 o 1 5 1 520.87 544.57 7.09 o 2 5 1 863.29 863.97 10.49 o 3 5 1 6.86 10.20 0.38 o 4 5 1 112.51 99.70 2.49 o 5 5 1 343.54 335.90 4.72 o 6 5 1 23.85 25.71 0.99 o -6 6 1 106.49 100.48 1.92 o -5 6 1 88.27 90.11 1.51 o -4 6 1 490.05 477.10 6.50 o -3 6 1 337.34 298.44 5.45 o -2 6 1 105.16 93.13 1.23 o -1 6 1 1550.47 1458.59 17.58 o 0 6 1 936.69 918.47 11.92 o 1 6 1 2055.73 1943.07 23.53 o 2 6 1 113.80 103.32 1.36 o 3 6 1 400.23 352.03 4.85 o 4 6 1 606.52 612.42 8.35 o 5 6 1 44.07 48.08 1.97 o 6 6 1 106.02 102.96 1.99 o -6 7 1 42.40 43.86 1.30 o -5 7 1 180.59 179.07 3.56 o -4 7 1 282.26 277.69 3.88 o -3 7 1 364.82 338.09 4.64 o -2 7 1 585.42 604.29 7.35 o -1 7 1 742.02 788.61 12.69 o 0 7 1 2211.89 2223.11 28.66 o 1 7 1 1526.00 1621.60 19.63 o 2 7 1 778.84 808.96 9.84 o 3 7 1 362.06 336.89 4.64 o 4 7 1 293.10 292.38 4.11 o 5 7 1 301.35 291.70 4.17 o 6 7 1 62.96 65.75 1.61 o -6 8 1 24.63 27.37 1.50 o -5 8 1 53.48 51.35 1.15 o -4 8 1 165.44 165.16 2.62 o -3 8 1 14.00 16.20 0.50 o -2 8 1 18.46 19.29 0.48 o -1 8 1 141.39 153.49 2.08 o 0 8 1 110.36 131.25 1.80 o 1 8 1 109.76 112.85 1.47 o 2 8 1 33.57 35.44 0.59 o 3 8 1 25.63 26.55 0.59 o 4 8 1 103.24 99.64 2.01 o 5 8 1 26.03 27.27 1.41 o 6 8 1 27.30 30.58 1.13 o -6 9 1 32.30 30.77 1.14 o -5 9 1 176.77 174.42 2.84 o -4 9 1 320.52 323.06 4.89 o -3 9 1 73.69 72.49 1.86 o -2 9 1 27.25 26.03 0.59 o -1 9 1 541.32 576.84 7.52 o 0 9 1 1748.41 1697.44 23.63 o 1 9 1 420.05 461.41 6.05 o 2 9 1 53.12 51.65 0.85 o 3 9 1 142.66 138.23 2.22 o 4 9 1 206.84 207.94 3.28 o 5 9 1 274.56 272.66 4.28 o 6 9 1 24.51 23.44 1.05 o -6 10 1 50.93 51.49 2.39 o -5 10 1 53.75 55.49 1.25 o -4 10 1 226.57 215.63 3.39 o -3 10 1 130.77 123.96 2.03 o -2 10 1 1.75 2.67 0.71 o -1 10 1 308.72 286.27 4.12 o 0 10 1 32.13 24.90 0.55 o 1 10 1 151.44 139.38 2.12 o 2 10 1 1.69 1.68 0.50 o 3 10 1 167.05 151.32 2.43 o 4 10 1 180.56 168.51 2.74 o 5 10 1 39.99 37.73 1.01 o 6 10 1 63.85 65.77 2.33 o -5 11 1 48.91 47.12 1.17 o -4 11 1 415.88 418.64 6.32 o -3 11 1 49.17 44.79 1.05 o -2 11 1 141.16 133.63 2.37 o -1 11 1 92.10 93.79 1.53 o 0 11 1 1104.32 1057.53 14.82 o 1 11 1 61.84 64.04 1.12 o 2 11 1 91.72 81.37 1.56 o 3 11 1 23.99 21.89 0.84 o 4 11 1 342.16 332.20 5.06 o 5 11 1 24.38 24.74 1.41 o -5 12 1 10.69 10.81 1.06 o -4 12 1 46.89 45.70 1.12 o -3 12 1 150.55 146.30 2.62 o -2 12 1 40.03 37.21 0.92 o -1 12 1 199.17 179.44 2.72 o 0 12 1 30.68 26.00 0.99 o 1 12 1 100.71 98.22 2.77 o 2 12 1 30.72 27.67 0.82 o 3 12 1 185.72 177.67 3.16 o 4 12 1 41.95 43.70 1.22 o 5 12 1 15.70 16.51 1.01 o -5 13 1 241.11 240.16 4.29 o -4 13 1 41.14 35.09 1.13 o -3 13 1 44.24 45.05 1.15 o -2 13 1 115.46 117.79 2.16 o -1 13 1 112.12 112.11 1.82 o 0 13 1 258.56 275.52 4.05 o 1 13 1 206.16 209.98 3.16 o 2 13 1 182.88 191.21 3.37 o 3 13 1 75.69 76.68 2.07 o 4 13 1 26.23 21.38 0.92 o 5 13 1 297.38 298.86 5.24 o -4 14 1 196.70 200.46 7.24 o -3 14 1 80.79 77.82 1.64 o -2 14 1 71.23 71.11 1.48 o -1 14 1 125.35 133.67 2.46 o 0 14 1 91.41 93.55 1.93 o 1 14 1 175.70 187.79 2.88 o 2 14 1 58.27 59.34 1.33 o 3 14 1 78.93 79.06 1.90 o 4 14 1 332.90 329.02 6.38 o -4 15 1 0.27 -0.04 0.64 o -3 15 1 15.37 12.78 0.76 o -2 15 1 0.23 0.18 0.47 o -1 15 1 332.24 322.60 5.46 o 0 15 1 4.07 4.42 0.44 o 1 15 1 163.13 162.63 3.23 o 2 15 1 0.43 0.74 0.49 o 3 15 1 8.05 6.76 0.66 o 4 15 1 0.14 0.41 0.61 o -3 16 1 42.35 47.40 1.31 o -2 16 1 23.72 22.55 0.90 o -1 16 1 185.83 190.93 3.40 o 0 16 1 5.32 8.17 1.01 o 1 16 1 163.64 168.97 3.08 o 2 16 1 12.68 11.91 0.85 o 3 16 1 53.43 56.18 1.43 o -3 17 1 62.12 61.57 2.67 o -2 17 1 318.50 328.04 5.65 o -1 17 1 8.11 10.53 1.30 o 0 17 1 912.75 912.77 12.96 o 1 17 1 13.13 13.74 0.85 o 2 17 1 297.61 295.08 5.13 o 3 17 1 30.24 31.35 1.83 o -2 18 1 5.78 4.47 0.98 o -1 18 1 574.33 579.85 9.62 o 0 18 1 1.71 5.23 0.67 o 1 18 1 443.49 452.92 7.65 o 2 18 1 11.88 10.34 0.88 o 0 19 1 93.01 96.07 2.58 o -7 0 2 93.66 100.37 3.51 o -6 0 2 166.04 164.04 3.99 o -5 0 2 388.28 382.46 8.51 o -4 0 2 2545.67 2519.64 53.84 o -3 0 2 38.10 35.33 3.51 o -2 0 2 3410.24 3461.75 94.19 o -1 0 2 754.61 812.29 13.95 o 0 0 2 13725.38 10752.06 184.38 o 1 0 2 462.59 486.92 8.37 o 2 0 2 6622.14 6251.74 90.96 o 3 0 2 18.98 18.74 0.57 o 4 0 2 1594.68 1656.08 40.51 o 5 0 2 288.93 280.50 11.67 o 6 0 2 98.58 99.82 4.36 o -7 1 2 17.18 19.40 1.69 o -6 1 2 39.14 36.51 1.22 o -5 1 2 544.41 536.04 8.34 o -4 1 2 73.85 72.22 1.67 o -3 1 2 1717.76 1794.22 34.03 o -2 1 2 262.28 235.33 3.23 o -1 1 2 3925.38 3821.95 51.51 o 0 1 2 365.19 349.43 4.28 o 1 1 2 3103.99 3013.01 36.47 o 2 1 2 160.47 134.64 2.07 o 3 1 2 3331.84 3278.42 60.21 o 4 1 2 66.39 60.44 0.92 o 5 1 2 292.32 303.45 6.16 o 6 1 2 68.51 69.63 1.50 o -6 2 2 1.09 0.58 0.50 o -5 2 2 46.67 49.28 1.07 o -4 2 2 62.01 67.47 1.09 o -3 2 2 608.71 617.75 9.95 o -2 2 2 223.47 235.23 4.32 o -1 2 2 204.79 205.13 2.50 o 0 2 2 296.08 309.33 3.77 o 1 2 2 325.68 321.08 5.58 o 2 2 2 436.76 448.77 8.95 o 3 2 2 354.88 369.45 6.94 o 4 2 2 61.32 68.69 1.15 o 5 2 2 24.05 25.59 1.00 o 6 2 2 1.81 0.82 0.50 o -6 3 2 96.40 91.51 1.73 o -5 3 2 3.75 3.24 0.45 o -4 3 2 449.82 432.85 5.93 o -3 3 2 132.86 126.82 1.81 o -2 3 2 2943.71 3006.03 34.23 o -1 3 2 196.60 198.59 5.36 o 0 3 2 5923.58 5731.99 69.24 o 1 3 2 398.08 404.45 5.49 o 2 3 2 1882.82 1978.61 30.24 o 3 3 2 102.13 103.07 1.45 o 4 3 2 342.66 336.78 4.68 o 5 3 2 3.04 3.44 0.45 o 6 3 2 73.30 72.05 1.50 o -6 4 2 20.44 24.14 0.85 o -5 4 2 493.88 491.71 7.64 o -4 4 2 377.34 375.97 4.65 o -3 4 2 578.17 569.59 8.78 o -2 4 2 154.86 168.03 2.34 o -1 4 2 1035.91 1065.79 15.50 o 0 4 2 2262.92 2204.55 26.66 o 1 4 2 2033.61 2076.65 25.17 o 2 4 2 182.32 202.40 2.54 o 3 4 2 282.09 304.02 6.16 o 4 4 2 197.11 203.53 6.89 o 5 4 2 406.30 395.71 5.49 o 6 4 2 31.85 36.19 1.07 o -6 5 2 52.76 54.97 1.28 o -5 5 2 21.69 22.12 0.74 o -3 5 2 373.73 352.91 5.42 o -2 5 2 199.71 211.91 2.73 o -1 5 2 477.29 480.74 5.86 o 0 5 2 9544.05 9751.20 133.75 o 1 5 2 386.66 389.25 4.76 o 2 5 2 175.62 172.47 2.18 o 3 5 2 185.33 182.89 3.58 o 4 5 2 786.51 764.11 10.39 o 5 5 2 24.61 27.14 0.75 o 6 5 2 85.70 86.09 1.75 o -6 6 2 49.20 43.09 1.34 o -5 6 2 23.33 25.28 0.72 o -4 6 2 172.14 165.94 2.42 o -3 6 2 76.51 75.71 1.19 o -2 6 2 326.99 326.82 5.33 o -1 6 2 615.65 636.25 7.93 o 0 6 2 125.26 146.23 1.84 o 1 6 2 931.39 964.17 13.98 o 2 6 2 647.54 653.48 8.01 o 3 6 2 61.97 60.83 1.18 o 4 6 2 99.21 95.26 2.14 o 5 6 2 12.81 13.89 0.60 o 6 6 2 25.23 23.22 1.16 o -5 7 2 433.49 415.64 6.28 o -4 7 2 153.26 154.17 2.25 o -3 7 2 423.88 401.89 8.97 o -2 7 2 124.99 125.32 1.61 o -1 7 2 316.24 303.67 3.74 o 0 7 2 0.42 6.22 0.49 o 1 7 2 298.81 301.87 3.74 o 2 7 2 171.03 164.56 2.11 o 3 7 2 804.05 786.46 10.63 o 4 7 2 183.42 178.97 2.62 o 5 7 2 270.11 254.32 4.42 o 6 7 2 160.75 164.62 3.26 o -6 8 2 9.97 8.18 0.98 o -5 8 2 204.53 205.89 3.28 o -4 8 2 419.66 416.94 6.25 o -3 8 2 52.57 60.21 1.55 o -2 8 2 231.63 225.21 3.10 o -1 8 2 61.79 63.67 0.87 o 0 8 2 594.13 519.45 6.34 o 1 8 2 42.78 44.88 0.66 o 2 8 2 403.03 379.58 4.71 o 3 8 2 106.13 115.84 1.76 o 4 8 2 224.84 229.99 6.61 o 5 8 2 199.29 204.17 3.26 o 6 8 2 5.34 5.11 0.81 o -6 9 2 34.44 36.41 1.48 o -5 9 2 127.49 129.21 2.61 o -4 9 2 74.94 76.34 1.39 o -3 9 2 196.31 191.50 9.00 o -2 9 2 2.77 3.77 0.47 o -1 9 2 194.31 195.96 2.67 o 0 9 2 436.15 434.18 6.48 o 1 9 2 102.73 104.21 1.70 o 2 9 2 5.25 5.72 0.30 o 3 9 2 373.81 359.14 6.66 o 4 9 2 115.93 113.63 1.94 o 5 9 2 73.79 73.48 1.47 o 6 9 2 32.74 31.65 1.06 o -5 10 2 6.05 5.82 0.58 o -4 10 2 5.84 7.96 0.51 o -3 10 2 54.12 53.53 1.11 o -2 10 2 131.66 135.83 2.16 o -1 10 2 447.67 422.83 6.06 o 0 10 2 280.48 273.63 3.97 o 1 10 2 553.74 539.22 7.66 o 2 10 2 152.11 159.57 2.24 o 3 10 2 29.81 27.85 0.74 o 4 10 2 8.39 10.47 0.81 o 5 10 2 12.40 12.15 0.73 o -5 11 2 119.10 115.89 2.48 o -4 11 2 168.14 160.40 6.04 o -3 11 2 491.11 476.53 7.84 o -2 11 2 100.42 104.46 1.92 o -1 11 2 1003.62 1032.16 14.52 o 0 11 2 2596.95 2685.82 37.37 o 1 11 2 1081.37 1101.31 15.47 o 2 11 2 206.47 212.12 3.16 o 3 11 2 350.63 356.08 5.97 o 4 11 2 338.80 332.07 5.65 o 5 11 2 79.24 76.07 1.53 o -5 12 2 109.17 113.68 2.90 o -4 12 2 197.05 189.75 3.37 o -3 12 2 41.77 42.98 1.07 o -2 12 2 351.68 338.03 5.64 o -1 12 2 324.56 343.68 4.97 o 0 12 2 1124.60 1104.95 15.50 o 1 12 2 602.89 617.76 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79.02 74.81 2.86 o 3 9 9 103.34 107.44 2.05 o -3 10 9 35.11 33.08 1.58 o -2 10 9 100.86 108.61 3.66 o -1 10 9 1.68 2.60 0.80 o 0 10 9 120.89 131.44 2.77 o 1 10 9 0.92 0.84 0.80 o 2 10 9 159.41 173.87 4.12 o 3 10 9 52.58 57.07 2.67 o -2 11 9 25.99 21.93 1.97 o -1 11 9 38.21 43.58 2.39 o 0 11 9 0.28 0.82 0.84 o 1 11 9 31.47 37.04 1.59 o 2 11 9 17.72 18.16 1.05 o -1 12 9 11.33 12.79 1.55 o 0 12 9 0.09 -0.73 0.84 o 1 12 9 6.04 7.25 1.04 o -3 0 10 117.53 105.57 4.36 o -2 0 10 68.61 69.36 2.74 o -1 0 10 653.50 656.76 14.78 o 0 0 10 21.37 18.45 0.99 o 1 0 10 522.61 524.44 22.07 o 2 0 10 38.43 37.86 1.83 o 3 0 10 233.64 235.61 8.93 o 4 0 10 68.52 73.52 3.23 o -3 1 10 56.06 58.91 1.99 o -2 1 10 107.79 108.17 2.02 o -1 1 10 0.72 0.74 0.42 o 0 1 10 74.20 68.13 1.41 o 1 1 10 0.87 1.75 0.63 o 2 1 10 133.13 137.12 2.50 o 3 1 10 27.59 26.99 2.52 o 4 1 10 28.57 29.40 1.49 o -4 2 10 10.62 10.12 1.55 o -3 2 10 2.07 2.94 0.74 o -2 2 10 92.50 87.33 1.71 o -1 2 10 13.26 11.03 0.65 o 0 2 10 201.70 199.28 3.41 o 1 2 10 18.17 17.27 1.03 o 2 2 10 131.48 132.40 2.43 o 3 2 10 2.47 2.21 0.59 o 4 2 10 6.87 7.96 0.99 o -3 3 10 113.38 113.42 2.56 o -2 3 10 19.85 23.26 0.94 o -1 3 10 327.19 317.90 5.54 o 0 3 10 6.92 6.55 0.54 o 1 3 10 477.35 484.35 12.15 o 2 3 10 13.28 12.35 0.72 o 3 3 10 55.03 52.02 2.88 o -3 4 10 17.72 17.10 0.94 o -2 4 10 153.53 146.42 3.09 o -1 4 10 158.84 157.80 2.79 o 0 4 10 234.16 230.48 3.91 o 1 4 10 225.79 224.51 5.86 o 2 4 10 145.73 140.32 2.58 o 3 4 10 36.19 40.11 1.19 o -3 5 10 45.44 48.14 1.46 o -2 5 10 132.95 130.79 2.82 o -1 5 10 107.69 109.01 3.57 o 0 5 10 191.90 202.34 4.89 o 1 5 10 171.92 184.86 5.38 o 2 5 10 195.85 198.41 3.88 o 3 5 10 25.92 24.65 1.54 o -3 6 10 5.33 5.39 0.75 o -2 6 10 3.31 4.18 0.64 o -1 6 10 66.54 63.78 1.99 o 0 6 10 0.52 0.08 0.47 o 1 6 10 35.37 34.49 1.02 o 2 6 10 3.08 3.02 0.61 o 3 6 10 10.93 11.22 0.78 o -3 7 10 83.76 84.40 2.58 o -2 7 10 145.54 144.51 3.13 o -1 7 10 26.35 26.99 0.91 o 0 7 10 201.43 204.66 3.55 o 1 7 10 30.23 28.44 0.96 o 2 7 10 160.42 171.18 3.10 o 3 7 10 44.01 40.81 2.10 o -2 8 10 28.47 31.62 1.44 o -1 8 10 144.21 143.44 6.68 o 0 8 10 0.15 0.38 0.54 o 1 8 10 97.77 98.43 2.16 o 2 8 10 17.14 17.90 0.93 o -2 9 10 112.57 118.37 3.28 o -1 9 10 12.30 15.75 1.24 o 0 9 10 46.80 48.00 1.41 o 1 9 10 7.44 8.66 0.80 o 2 9 10 111.41 120.76 2.66 o -1 10 10 5.57 5.19 0.94 o 0 10 10 1.09 2.49 0.94 o 1 10 10 10.84 8.08 1.04 o 0 11 10 229.24 242.22 7.73 o -2 1 11 42.34 44.85 1.19 o -1 1 11 11.64 11.75 0.74 o 0 1 11 36.26 35.92 1.02 o 1 1 11 23.10 25.17 0.95 o 2 1 11 36.88 38.45 1.14 o 3 1 11 8.54 11.39 1.41 o -2 2 11 166.15 157.51 3.59 o -1 2 11 63.25 65.05 1.50 o 0 2 11 206.50 207.16 3.58 o 1 2 11 87.95 88.51 1.81 o 2 2 11 257.69 269.79 6.25 o -2 3 11 38.36 43.42 1.38 o -1 3 11 99.46 100.62 2.06 o 0 3 11 37.37 38.13 1.09 o 1 3 11 131.37 137.46 3.61 o 2 3 11 24.65 26.01 1.28 o -2 4 11 0.47 0.80 0.64 o -1 4 11 0.10 0.30 0.52 o 0 4 11 6.68 6.90 0.63 o 1 4 11 0.11 0.35 0.56 o 2 4 11 0.38 0.88 0.61 o -2 5 11 20.92 20.96 1.05 o -1 5 11 28.70 27.13 0.96 o 0 5 11 2.01 1.78 0.58 o 1 5 11 43.65 42.92 1.52 o 2 5 11 12.36 11.71 0.80 o -2 6 11 112.65 105.47 3.02 o -1 6 11 8.01 8.08 0.66 o 0 6 11 175.18 168.58 3.05 o 1 6 11 16.02 16.78 0.89 o 2 6 11 148.00 149.69 3.35 o -1 7 11 115.92 110.36 2.59 o 0 7 11 5.49 7.61 0.70 o 1 7 11 121.56 121.26 2.38 o 0 8 11 36.97 38.06 1.69 o -1 0 12 219.68 225.91 7.31 o 0 0 12 11.35 12.51 1.55 o -1 1 12 4.35 3.22 0.94 o 0 1 12 46.01 44.64 1.41 o -1 2 12 6.62 7.40 0.99 o 0 2 12 5.83 5.36 0.94 o 0 3 12 1.13 0.70 0.89 o