#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180932 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/12/2201273.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201273_Fobs loop_ _publ_author_name 'Ravikumar, Bagavath Singh' 'Sridhar, Balasubramanian' 'Rajaram, Ramaswamy Karunanandam' _publ_section_title ; DL-Valinium dihydrogen phosphate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o879 _journal_page_last o881 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.730 _cell_angle_gamma 90.000 _cell_length_a 9.2010 _cell_length_b 10.0035 _cell_length_c 11.1950 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8419 _cod_data_source_file bt6161Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' DL-VALINE PHOSPHATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 150.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x-1/2, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8350.58 8208.35 28.20 o 4 0 0 969.30 953.13 9.62 o 6 0 0 660.28 650.16 7.88 o 8 0 0 70.44 77.11 4.31 o 10 0 0 168.40 179.95 7.06 o 1 1 0 167.45 188.29 2.21 o 2 1 0 3773.58 3684.59 19.31 o 3 1 0 1856.87 1982.64 17.09 o 4 1 0 95.72 100.61 2.86 o 5 1 0 4.32 4.27 3.52 o 6 1 0 0.02 -3.86 4.09 o 7 1 0 29.58 27.10 3.20 o 8 1 0 203.28 195.25 6.05 o 9 1 0 6.32 7.47 5.21 o 0 2 0 8405.36 8574.44 26.48 o 1 2 0 159.78 167.58 2.60 o 2 2 0 8339.93 8469.90 32.55 o 3 2 0 4.18 17.47 1.75 o 4 2 0 195.23 183.29 3.75 o 5 2 0 64.12 71.85 2.92 o 6 2 0 320.33 304.91 5.68 o 7 2 0 17.96 8.85 5.49 o 8 2 0 107.14 116.84 4.93 o 9 2 0 6.42 8.36 3.52 o 1 3 0 305.85 281.40 3.55 o 2 3 0 161.68 146.08 2.95 o 3 3 0 21.11 15.17 1.89 o 4 3 0 2030.01 2171.63 19.50 o 5 3 0 1.84 -0.78 3.58 o 6 3 0 141.92 137.62 4.52 o 7 3 0 35.49 32.54 3.24 o 8 3 0 153.40 170.24 5.67 o 9 3 0 39.40 41.98 3.93 o 0 4 0 4142.64 4738.34 27.30 o 1 4 0 2179.72 2375.22 19.67 o 2 4 0 35.53 29.58 2.04 o 3 4 0 5.78 2.57 1.73 o 4 4 0 949.01 974.93 9.87 o 5 4 0 143.53 152.99 4.24 o 6 4 0 0.63 1.60 4.08 o 7 4 0 7.34 8.57 2.71 o 8 4 0 188.76 207.36 6.49 o 9 4 0 0.07 -5.75 5.75 o 1 5 0 359.26 333.60 4.79 o 2 5 0 9.61 5.72 1.85 o 3 5 0 2509.24 2553.43 22.23 o 4 5 0 88.24 90.31 3.38 o 5 5 0 650.81 654.74 8.81 o 6 5 0 117.04 112.98 4.52 o 7 5 0 196.67 174.69 5.80 o 8 5 0 175.78 169.57 6.46 o 9 5 0 21.09 24.72 4.01 o 0 6 0 446.93 509.78 6.32 o 1 6 0 1.12 -3.49 3.98 o 2 6 0 72.61 71.36 3.18 o 3 6 0 3.43 7.69 2.16 o 4 6 0 218.11 237.33 5.56 o 5 6 0 68.31 66.05 3.76 o 6 6 0 51.85 47.60 3.80 o 7 6 0 120.85 123.87 5.24 o 8 6 0 0.13 -1.53 4.75 o 1 7 0 565.15 550.64 7.37 o 2 7 0 2.29 -2.63 4.33 o 3 7 0 1124.30 1197.45 11.92 o 4 7 0 371.01 360.37 7.14 o 5 7 0 1209.66 1178.36 13.09 o 6 7 0 0.33 -4.99 5.21 o 7 7 0 134.10 138.62 6.09 o 8 7 0 0.00 2.19 5.93 o 0 8 0 601.53 602.79 8.75 o 1 8 0 747.62 738.82 9.61 o 2 8 0 1.40 -0.67 4.83 o 3 8 0 9.99 11.69 3.11 o 4 8 0 24.08 23.15 3.27 o 5 8 0 0.00 8.49 4.58 o 6 8 0 0.25 -2.76 4.49 o 7 8 0 113.85 113.65 5.83 o 1 9 0 935.78 927.11 11.60 o 2 9 0 114.13 102.66 5.02 o 3 9 0 182.48 168.07 5.68 o 4 9 0 3.21 5.68 4.68 o 5 9 0 256.37 273.58 7.96 o 6 9 0 0.43 -2.52 4.83 o 0 10 0 18.06 18.82 3.30 o 1 10 0 0.20 -4.36 5.47 o 2 10 0 1.54 0.45 5.15 o 3 10 0 27.06 25.94 3.92 o 4 10 0 88.20 93.52 5.42 o 5 10 0 40.55 46.45 4.33 o 1 11 0 472.89 483.85 10.69 o 2 11 0 0.03 -6.56 6.56 o 3 11 0 211.17 189.25 7.40 o -10 0 1 0.82 9.27 4.89 o -8 0 1 41.88 39.47 3.35 o -6 0 1 154.44 134.74 3.79 o -4 0 1 2840.41 3113.41 23.51 o -2 0 1 17263.31 17459.82 147.65 o 0 0 1 5461.60 5206.87 32.19 o 2 0 1 3104.15 2957.69 18.30 o 4 0 1 4970.26 5225.68 33.33 o 6 0 1 1054.18 1084.49 10.86 o 8 0 1 697.80 710.02 10.91 o -10 1 1 32.74 38.66 4.28 o -9 1 1 6.93 8.03 4.23 o -8 1 1 384.70 378.13 7.81 o -7 1 1 63.78 64.41 3.83 o -6 1 1 502.38 490.89 6.72 o -5 1 1 548.10 572.56 6.36 o -4 1 1 255.83 289.89 4.20 o -3 1 1 1069.71 1200.08 11.13 o -2 1 1 1062.05 1034.64 9.96 o -1 1 1 337.98 349.85 3.60 o 0 1 1 64.08 82.65 1.93 o 1 1 1 262.09 249.50 2.81 o 2 1 1 3081.51 3186.15 19.53 o 3 1 1 246.87 243.71 3.76 o 4 1 1 1218.80 1209.54 12.59 o 5 1 1 48.51 45.96 2.57 o 6 1 1 2003.27 1934.93 19.52 o 7 1 1 126.77 139.67 5.17 o 8 1 1 335.92 337.17 7.71 o 9 1 1 1.38 0.00 4.68 o -10 2 1 26.79 31.59 3.98 o -9 2 1 19.01 16.54 3.59 o -8 2 1 92.80 87.91 4.27 o -7 2 1 473.95 458.37 7.80 o -6 2 1 0.25 4.05 3.33 o -5 2 1 4.98 7.73 1.86 o -4 2 1 408.34 401.70 5.07 o -3 2 1 1.11 -1.56 2.90 o -2 2 1 361.33 365.04 3.80 o -1 2 1 3996.68 3691.89 18.35 o 0 2 1 1042.95 1068.92 6.93 o 1 2 1 20.38 36.07 1.91 o 2 2 1 5.18 -0.13 3.01 o 3 2 1 732.14 842.20 8.19 o 4 2 1 943.15 906.68 8.90 o 5 2 1 53.38 50.08 2.69 o 6 2 1 623.60 619.11 8.53 o 7 2 1 727.42 713.15 10.19 o 8 2 1 187.39 189.20 6.21 o 9 2 1 24.83 21.11 3.89 o -9 3 1 3.82 5.27 4.94 o -8 3 1 0.14 4.12 3.59 o -7 3 1 1.57 6.34 4.14 o -6 3 1 617.26 653.65 8.00 o -5 3 1 153.55 150.38 3.85 o -4 3 1 2686.77 2827.54 24.92 o -3 3 1 1353.41 1581.15 14.54 o -2 3 1 1516.21 1441.57 12.48 o -1 3 1 1339.45 1351.21 13.09 o 0 3 1 7392.91 7378.28 21.62 o 1 3 1 465.15 431.19 4.45 o 2 3 1 2213.11 2179.39 19.01 o 3 3 1 14.69 19.91 1.98 o 4 3 1 1323.22 1400.30 14.60 o 5 3 1 0.03 1.92 3.45 o 6 3 1 0.14 -2.24 4.56 o 7 3 1 45.40 40.81 3.61 o 8 3 1 30.49 24.90 3.74 o 9 3 1 0.00 -5.78 5.94 o -9 4 1 25.41 26.01 4.18 o -8 4 1 6.00 0.87 5.02 o -7 4 1 87.60 89.80 4.14 o -6 4 1 0.64 1.53 3.90 o -5 4 1 518.93 504.09 6.85 o -4 4 1 1095.08 1116.19 10.97 o -3 4 1 312.41 403.51 5.23 o -2 4 1 993.25 1087.21 10.86 o -1 4 1 766.12 826.14 8.38 o 0 4 1 2190.01 2526.24 14.37 o 1 4 1 395.76 410.82 4.85 o 2 4 1 244.30 247.52 4.17 o 3 4 1 241.11 275.38 4.72 o 4 4 1 236.70 250.15 4.86 o 5 4 1 306.89 302.68 6.15 o 6 4 1 228.18 216.70 5.59 o 7 4 1 119.30 111.57 5.05 o 8 4 1 7.19 5.69 5.08 o 9 4 1 166.51 185.29 7.24 o -9 5 1 3.70 1.06 5.52 o -8 5 1 23.85 27.25 3.29 o -7 5 1 6.64 1.19 4.75 o -6 5 1 7.75 6.69 2.44 o -5 5 1 72.02 84.60 3.74 o -4 5 1 102.50 100.91 3.51 o -3 5 1 1236.64 1311.12 12.81 o -2 5 1 1753.13 1680.83 16.85 o -1 5 1 262.35 314.31 4.66 o 0 5 1 1366.55 1379.65 9.31 o 1 5 1 1057.53 1047.78 10.67 o 2 5 1 540.85 530.71 6.34 o 3 5 1 238.19 246.69 4.83 o 4 5 1 119.85 123.93 4.07 o 5 5 1 248.90 227.17 5.64 o 6 5 1 318.98 266.44 6.48 o 7 5 1 75.74 71.79 4.37 o 8 5 1 6.69 4.50 5.14 o -8 6 1 14.51 9.33 5.27 o -7 6 1 73.35 68.27 4.34 o -6 6 1 3.42 6.97 4.23 o -5 6 1 396.13 391.52 7.24 o -4 6 1 219.28 213.50 5.32 o -3 6 1 911.42 946.11 9.81 o -2 6 1 1465.47 1469.31 14.06 o -1 6 1 420.25 376.87 5.63 o 0 6 1 58.07 53.66 2.02 o 1 6 1 1241.84 1220.14 12.78 o 2 6 1 189.75 190.69 4.49 o 3 6 1 1039.51 1111.98 10.47 o 4 6 1 210.58 210.80 5.52 o 5 6 1 15.79 14.11 3.01 o 6 6 1 35.43 34.20 3.26 o 7 6 1 10.02 15.90 3.45 o 8 6 1 32.44 43.50 4.49 o -8 7 1 1.36 -4.77 5.41 o -7 7 1 182.77 181.52 6.44 o -6 7 1 372.73 352.93 7.68 o -5 7 1 714.94 693.95 10.06 o -4 7 1 368.82 372.47 7.14 o -3 7 1 275.05 265.29 5.95 o -2 7 1 137.08 131.36 4.12 o -1 7 1 253.24 244.97 5.24 o 0 7 1 6.08 6.57 3.17 o 1 7 1 9.48 11.49 2.54 o 2 7 1 7.14 7.78 2.67 o 3 7 1 963.53 941.81 10.83 o 4 7 1 56.10 54.09 3.52 o 5 7 1 57.00 55.56 3.80 o 6 7 1 0.08 1.16 2.45 o 7 7 1 147.82 143.56 6.21 o -7 8 1 173.18 177.69 6.71 o -6 8 1 7.94 2.68 5.80 o -5 8 1 54.20 58.06 3.89 o -4 8 1 681.37 663.13 9.81 o -3 8 1 2375.14 2372.29 23.76 o -2 8 1 78.12 79.67 4.20 o -1 8 1 822.46 826.78 10.20 o 0 8 1 65.44 76.97 2.96 o 1 8 1 806.56 800.19 10.12 o 2 8 1 579.70 590.12 9.13 o 3 8 1 1462.54 1504.19 14.56 o 4 8 1 66.30 66.12 4.11 o 5 8 1 43.43 42.70 4.01 o 6 8 1 0.47 7.14 4.59 o 7 8 1 70.87 88.10 5.25 o -6 9 1 5.93 16.51 3.26 o -5 9 1 27.88 25.75 3.87 o -4 9 1 75.48 76.50 4.40 o -3 9 1 28.58 26.43 3.48 o -2 9 1 98.60 95.69 4.64 o -1 9 1 146.45 148.98 5.43 o 0 9 1 133.34 109.70 5.53 o 1 9 1 275.02 234.89 6.45 o 2 9 1 6.19 9.46 3.20 o 3 9 1 250.43 246.50 6.87 o 4 9 1 50.74 44.01 4.08 o 5 9 1 95.26 101.88 5.68 o 6 9 1 27.46 28.41 4.08 o -5 10 1 88.20 82.21 5.36 o -4 10 1 6.28 -1.45 6.22 o -3 10 1 130.55 142.44 6.13 o -2 10 1 0.04 6.21 4.89 o -1 10 1 374.40 370.30 8.42 o 0 10 1 13.44 8.37 2.95 o 1 10 1 189.54 187.63 6.30 o 2 10 1 34.28 41.61 4.12 o 3 10 1 212.68 218.07 7.28 o 4 10 1 7.20 11.17 3.57 o 5 10 1 310.39 294.39 9.18 o -4 11 1 2.17 1.10 6.70 o -3 11 1 2.96 8.80 3.61 o -2 11 1 76.86 70.58 5.24 o -1 11 1 55.42 63.65 4.89 o 0 11 1 0.69 6.44 4.04 o 1 11 1 191.61 182.55 7.02 o 2 11 1 1.73 3.61 5.38 o 3 11 1 44.36 48.01 5.03 o -10 0 2 17.69 25.21 3.93 o -8 0 2 72.08 70.81 4.08 o -6 0 2 647.87 672.50 7.56 o -4 0 2 1490.63 1459.96 13.79 o -2 0 2 2033.25 1782.24 13.00 o 0 0 2 10017.32 9458.96 60.92 o 2 0 2 571.93 631.19 6.29 o 4 0 2 141.32 169.41 3.93 o 6 0 2 0.03 -4.47 4.47 o 8 0 2 101.04 107.18 5.34 o -10 1 2 290.50 292.11 8.43 o -9 1 2 8.91 13.66 2.98 o -8 1 2 1108.77 1120.45 12.63 o -7 1 2 193.21 187.24 5.26 o -6 1 2 616.82 583.03 7.06 o -5 1 2 171.84 166.81 3.69 o -4 1 2 322.06 298.28 4.18 o -3 1 2 356.21 383.28 4.13 o -2 1 2 170.29 182.19 2.79 o -1 1 2 134.11 103.20 2.09 o 0 1 2 3360.04 3299.92 18.33 o 1 1 2 2421.41 2450.79 16.39 o 2 1 2 407.98 349.65 4.16 o 3 1 2 487.68 512.47 5.61 o 4 1 2 1149.96 1149.53 11.92 o 5 1 2 421.18 415.01 6.23 o 6 1 2 1804.65 1690.26 16.14 o 7 1 2 5.35 6.32 2.29 o 8 1 2 156.86 166.49 6.18 o 9 1 2 16.65 6.29 6.29 o -10 2 2 1.21 -1.01 4.77 o -9 2 2 426.37 426.11 8.98 o -8 2 2 4.51 8.20 2.98 o -7 2 2 465.05 464.28 7.74 o -6 2 2 24.11 16.84 2.13 o -5 2 2 634.59 665.97 6.99 o -4 2 2 60.01 67.17 2.57 o -3 2 2 28.44 22.38 1.83 o -2 2 2 585.29 550.39 5.56 o -1 2 2 35.21 20.93 1.78 o 0 2 2 2234.75 2246.87 11.33 o 1 2 2 105.76 163.54 2.86 o 2 2 2 929.24 931.71 9.67 o 3 2 2 378.31 453.53 5.50 o 4 2 2 27.95 25.78 2.35 o 5 2 2 537.73 513.34 7.15 o 6 2 2 0.13 -4.30 4.64 o 7 2 2 547.49 532.32 9.17 o 8 2 2 34.46 39.07 4.15 o 9 2 2 3.53 5.99 4.96 o -10 3 2 25.92 23.58 3.98 o -9 3 2 3.38 7.44 2.89 o -8 3 2 0.96 4.01 4.01 o -7 3 2 81.01 75.34 3.95 o -6 3 2 510.94 497.33 7.07 o -5 3 2 455.40 457.23 6.20 o -4 3 2 82.19 76.88 2.80 o -3 3 2 108.09 136.07 3.13 o -2 3 2 373.45 314.37 4.00 o -1 3 2 1795.88 1862.52 16.05 o 0 3 2 1291.69 1178.38 7.90 o 1 3 2 1347.02 1354.17 12.70 o 2 3 2 4345.54 4345.19 28.61 o 3 3 2 174.72 168.77 3.76 o 4 3 2 2853.74 3014.16 29.02 o 5 3 2 34.09 23.98 2.82 o 6 3 2 46.09 53.40 3.35 o 7 3 2 15.89 18.16 2.76 o 8 3 2 187.80 195.05 6.93 o -9 4 2 127.26 120.05 5.87 o -8 4 2 121.60 130.33 5.08 o -7 4 2 502.05 514.42 8.57 o -6 4 2 199.01 180.49 4.92 o -5 4 2 1.15 4.18 3.55 o -4 4 2 133.55 131.52 3.49 o -3 4 2 117.57 133.11 3.30 o -2 4 2 53.36 58.37 2.44 o -1 4 2 104.31 117.08 2.95 o 0 4 2 21.89 13.05 1.27 o 1 4 2 565.35 683.14 6.71 o 2 4 2 3549.89 3777.10 28.77 o 3 4 2 370.07 375.23 5.63 o 4 4 2 274.16 262.30 5.23 o 5 4 2 495.12 487.82 7.86 o 6 4 2 104.39 103.20 4.31 o 7 4 2 140.22 136.88 5.42 o 8 4 2 77.70 89.60 5.25 o -9 5 2 22.60 32.21 3.84 o -8 5 2 29.24 22.98 3.08 o -7 5 2 327.43 316.86 7.23 o -6 5 2 135.71 127.45 4.62 o -5 5 2 67.99 71.92 3.30 o -4 5 2 79.34 97.00 3.24 o -3 5 2 450.81 459.64 6.12 o -2 5 2 20.98 25.00 2.22 o -1 5 2 24.53 18.74 2.04 o 0 5 2 13.70 30.78 4.36 o 1 5 2 1080.96 1097.71 11.37 o 2 5 2 1465.62 1484.71 15.32 o 3 5 2 491.35 511.15 7.00 o 4 5 2 57.33 72.32 3.62 o 5 5 2 1.49 1.04 4.14 o 6 5 2 0.01 3.52 4.11 o 7 5 2 0.11 1.39 4.64 o 8 5 2 73.87 78.77 5.28 o -9 6 2 57.21 61.10 5.02 o -8 6 2 0.08 -2.89 4.55 o -7 6 2 19.78 24.56 2.85 o -6 6 2 2.65 0.72 4.17 o -5 6 2 757.84 719.80 9.55 o -4 6 2 644.69 660.24 8.09 o -3 6 2 260.83 241.02 4.98 o -2 6 2 182.56 181.23 4.27 o -1 6 2 393.15 354.66 5.60 o 0 6 2 164.86 163.10 2.88 o 1 6 2 1292.07 1252.29 12.38 o 2 6 2 12.76 14.60 2.27 o 3 6 2 1210.55 1241.80 12.63 o 4 6 2 384.45 378.30 7.29 o 5 6 2 433.76 449.28 8.27 o 6 6 2 33.56 28.11 3.46 o 7 6 2 38.11 45.44 4.05 o -8 7 2 14.01 21.16 3.40 o -7 7 2 0.13 -5.38 5.38 o -6 7 2 227.55 195.91 5.95 o -5 7 2 20.89 20.57 3.04 o -4 7 2 26.39 17.36 3.26 o -3 7 2 25.76 24.40 3.01 o -2 7 2 40.28 48.85 3.10 o -1 7 2 145.53 157.06 4.42 o 0 7 2 127.12 132.30 5.89 o 1 7 2 48.55 40.43 3.51 o 2 7 2 188.04 182.18 5.49 o 3 7 2 364.12 347.44 7.18 o 4 7 2 313.06 295.25 6.87 o 5 7 2 111.03 118.19 5.00 o 6 7 2 66.36 77.92 4.80 o 7 7 2 0.09 -5.06 5.06 o -7 8 2 13.67 10.93 3.71 o -6 8 2 15.59 4.84 5.58 o -5 8 2 637.66 626.47 10.05 o -4 8 2 251.24 257.84 6.36 o -3 8 2 1365.19 1347.11 13.49 o -2 8 2 277.74 259.52 6.36 o -1 8 2 747.67 741.57 9.84 o 0 8 2 2.58 3.61 3.53 o 1 8 2 2651.52 2653.37 27.56 o 2 8 2 55.05 53.97 3.86 o 3 8 2 567.63 581.36 9.36 o 4 8 2 2.48 3.79 4.89 o 5 8 2 260.85 279.94 7.90 o 6 8 2 0.30 -4.97 5.37 o -7 9 2 0.01 8.00 4.43 o -6 9 2 2.18 9.26 4.96 o -5 9 2 22.41 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61.33 4.90 o -8 5 10 63.03 74.09 4.96 o -7 5 10 228.98 228.52 7.40 o -6 5 10 109.30 90.40 5.58 o -5 5 10 161.70 160.86 5.65 o -4 5 10 119.62 109.77 4.77 o -3 5 10 580.29 585.35 10.15 o -2 5 10 4.18 2.68 5.12 o -1 5 10 168.25 178.75 6.65 o 0 5 10 23.66 23.88 2.84 o 1 5 10 27.91 29.42 3.98 o -7 6 10 43.19 43.58 4.68 o -6 6 10 5.71 0.48 5.74 o -5 6 10 121.19 126.66 5.84 o -4 6 10 62.86 68.34 4.56 o -3 6 10 66.53 60.81 4.96 o -2 6 10 81.25 75.85 5.02 o -1 6 10 5.62 4.89 5.94 o 0 6 10 223.44 230.37 5.93 o -6 7 10 1.26 1.56 5.19 o -5 7 10 69.10 73.50 5.50 o -4 7 10 0.75 3.55 4.33 o -3 7 10 11.10 18.53 3.61 o -2 7 10 11.08 9.79 6.46 o -1 7 10 226.57 235.33 7.96 o -8 0 11 4.33 6.47 5.21 o -6 0 11 21.07 28.74 3.27 o -4 0 11 166.76 155.32 5.34 o -2 0 11 95.22 85.43 4.58 o 0 0 11 18.69 23.09 2.90 o -9 1 11 4.43 4.15 3.37 o -8 1 11 132.97 142.03 6.41 o -7 1 11 8.40 7.53 5.60 o -6 1 11 0.11 0.85 4.86 o -5 1 11 57.17 53.28 3.86 o -4 1 11 69.47 75.24 4.24 o -3 1 11 162.93 167.61 5.53 o -2 1 11 116.76 114.62 4.93 o -1 1 11 22.22 27.99 3.54 o 0 1 11 139.95 150.92 5.47 o 1 1 11 4.59 6.43 3.05 o -9 2 11 24.38 22.79 4.25 o -8 2 11 58.41 64.73 4.83 o -7 2 11 50.26 47.91 4.45 o -6 2 11 3.22 8.77 4.72 o -5 2 11 0.92 -3.83 4.21 o -4 2 11 3.88 6.91 4.05 o -3 2 11 53.68 59.36 3.90 o -2 2 11 22.75 11.72 5.97 o -1 2 11 122.69 125.40 5.33 o 0 2 11 9.69 8.52 3.03 o 1 2 11 34.67 37.56 4.34 o -8 3 11 56.37 61.20 5.15 o -7 3 11 37.89 45.44 3.95 o -6 3 11 148.29 138.39 6.00 o -5 3 11 47.01 47.86 3.76 o -4 3 11 193.92 181.59 6.18 o -3 3 11 33.72 26.16 3.51 o -2 3 11 124.62 122.99 5.22 o -1 3 11 0.27 0.94 4.99 o 0 3 11 217.57 230.75 5.40 o 1 3 11 113.31 105.87 5.83 o -8 4 11 61.19 65.93 5.30 o -7 4 11 3.27 -0.51 5.74 o -6 4 11 15.94 20.50 3.42 o -5 4 11 48.72 47.85 4.24 o -4 4 11 78.04 88.81 5.09 o -3 4 11 18.56 21.33 3.51 o -2 4 11 12.86 8.45 3.43 o -1 4 11 59.65 59.06 4.53 o 0 4 11 15.23 15.80 2.64 o -7 5 11 0.05 -0.51 5.19 o -6 5 11 96.05 93.14 5.47 o -5 5 11 14.37 14.23 3.48 o -4 5 11 1.23 7.28 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