#------------------------------------------------------------------------------ #$Date: 2016-04-02 23:58:04 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180932 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/12/2201279.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201279_Fobs loop_ _publ_author_name 'Kooijman, Huub' 'Spek, Anthony L.' 'Zondervan, Charon' 'Feringa, Ben L.' _publ_section_title ; Dichloro{2,2'-thiobis[(4S)-4-isopropyl-1,3-oxazolinylphenyl]}zinc(II) ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m429 _journal_page_last m431 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _exptl_crystal_F_000 1128.00 _cod_data_source_file bt6167Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S1176A MOKA 60KV100MA LNT MON 041094' _shelx_refln_list_code 4 _shelx_f_calc_maximum 238.47 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 31176.98 29450.91 1382.94 o 4 0 0 41794.23 43788.43 654.14 o 6 0 0 241.87 256.46 11.69 o 8 0 0 251.04 245.83 14.85 o 10 0 0 340.43 367.49 33.53 o 12 0 0 35.63 34.77 17.44 o 1 1 0 10416.58 10666.52 162.75 o 2 1 0 306.32 356.99 23.25 o 3 1 0 12044.63 12804.41 181.98 o 4 1 0 4756.40 4451.77 66.17 o 5 1 0 346.35 375.47 11.18 o 6 1 0 277.41 287.04 11.38 o 7 1 0 10.79 23.90 10.42 o 8 1 0 455.01 453.87 17.04 o 9 1 0 229.15 214.97 14.85 o 10 1 0 708.06 708.47 21.81 o 11 1 0 0.35 12.81 13.58 o 12 1 0 44.33 35.46 17.31 o 0 2 0 20041.28 19623.07 102.72 o 1 2 0 2567.54 2757.72 12.32 o 2 2 0 4297.36 4429.36 65.28 o 3 2 0 9166.87 10066.21 108.20 o 4 2 0 4939.51 5234.86 120.72 o 5 2 0 344.81 297.07 10.42 o 6 2 0 1611.41 1548.63 20.84 o 7 2 0 1738.21 1679.93 30.40 o 8 2 0 393.38 409.10 16.75 o 9 2 0 2088.70 2123.84 44.71 o 10 2 0 194.65 209.11 15.48 o 11 2 0 161.33 169.21 21.46 o 12 2 0 0.32 3.32 15.40 o 1 3 0 10080.69 10420.09 98.62 o 2 3 0 2576.74 2958.29 53.21 o 3 3 0 26651.51 26265.27 290.63 o 4 3 0 234.31 220.81 8.52 o 5 3 0 444.85 418.20 11.69 o 6 3 0 712.74 702.58 15.48 o 7 3 0 3250.42 3190.84 31.62 o 8 3 0 1804.41 1643.31 29.06 o 9 3 0 410.01 346.05 17.04 o 10 3 0 218.39 242.90 17.07 o 11 3 0 158.31 206.13 17.38 o 12 3 0 94.03 132.22 17.71 o 0 4 0 35229.54 34772.96 366.19 o 1 4 0 12179.35 12965.40 148.44 o 2 4 0 16273.66 16428.98 154.22 o 3 4 0 514.22 570.48 21.91 o 4 4 0 16013.84 16898.44 264.69 o 5 4 0 2318.77 2391.41 84.95 o 6 4 0 5746.80 5895.97 113.57 o 7 4 0 271.35 282.51 15.20 o 8 4 0 543.22 545.77 18.01 o 9 4 0 4.37 33.37 12.95 o 10 4 0 152.08 161.06 19.23 o 11 4 0 0.50 16.37 13.58 o 12 4 0 5.02 18.33 15.18 o 1 5 0 1977.15 2091.43 22.80 o 2 5 0 2414.76 2598.97 23.25 o 3 5 0 669.81 689.41 15.65 o 4 5 0 27720.84 28236.77 805.71 o 5 5 0 2825.95 2846.50 40.69 o 6 5 0 476.99 496.15 14.85 o 7 5 0 1648.23 1589.57 24.64 o 8 5 0 1672.30 1737.02 27.17 o 9 5 0 95.16 64.50 13.91 o 10 5 0 21.02 9.84 13.91 o 11 5 0 2.34 28.55 13.87 o 12 5 0 119.02 119.71 25.49 o 0 6 0 17486.11 17754.13 91.21 o 1 6 0 7326.99 7726.03 73.33 o 2 6 0 134.45 182.59 7.89 o 3 6 0 2820.55 2910.24 50.08 o 4 6 0 3209.10 3312.19 72.43 o 5 6 0 2182.93 2189.51 32.19 o 6 6 0 1580.83 1590.95 22.74 o 7 6 0 148.09 184.30 26.38 o 8 6 0 50.90 56.29 13.23 o 9 6 0 202.47 206.61 31.30 o 10 6 0 43.59 47.76 15.65 o 11 6 0 20.36 24.30 22.36 o 1 7 0 14938.36 15711.08 134.14 o 2 7 0 5784.69 6427.32 33.19 o 3 7 0 6885.65 6819.74 175.72 o 4 7 0 829.45 931.05 16.44 o 5 7 0 2189.58 2225.33 25.27 o 6 7 0 1910.91 1922.45 31.75 o 7 7 0 429.08 467.01 16.40 o 8 7 0 578.06 604.38 33.53 o 9 7 0 39.68 46.05 13.91 o 10 7 0 13.95 13.25 14.22 o 11 7 0 193.25 195.39 27.72 o 0 8 0 15403.63 15784.81 139.95 o 1 8 0 671.12 601.50 12.32 o 2 8 0 2865.11 2752.52 24.00 o 3 8 0 5413.82 5696.30 112.67 o 4 8 0 6533.42 6592.68 40.15 o 5 8 0 15.28 23.04 11.18 o 6 8 0 4.42 16.89 11.58 o 7 8 0 105.06 98.33 12.60 o 8 8 0 29.98 34.09 25.93 o 9 8 0 512.30 539.93 29.51 o 10 8 0 660.55 649.21 33.98 o 11 8 0 193.10 188.70 18.30 o 1 9 0 4.77 25.49 8.22 o 2 9 0 452.38 465.00 12.65 o 3 9 0 114.49 126.04 11.05 o 4 9 0 795.59 768.55 17.38 o 5 9 0 3247.80 3259.29 32.23 o 6 9 0 1394.80 1432.29 24.29 o 7 9 0 112.56 117.49 12.95 o 8 9 0 1220.06 1255.72 26.56 o 9 9 0 118.32 129.42 16.99 o 10 9 0 922.88 1049.66 41.14 o 11 9 0 42.73 31.75 21.01 o 0 10 0 20685.62 21454.74 265.14 o 1 10 0 10.00 21.32 22.36 o 2 10 0 462.61 460.90 13.87 o 3 10 0 214.87 202.77 21.01 o 4 10 0 3412.64 3339.70 58.13 o 5 10 0 38.31 33.70 11.96 o 6 10 0 919.05 930.99 21.18 o 7 10 0 560.89 601.61 19.57 o 8 10 0 0.85 12.97 13.28 o 9 10 0 916.78 1030.18 25.93 o 10 10 0 356.34 369.43 21.47 o 1 11 0 9662.91 9791.95 133.24 o 2 11 0 288.29 281.12 23.25 o 3 11 0 5540.90 5471.49 142.18 o 4 11 0 693.54 627.43 18.33 o 5 11 0 581.34 602.70 17.31 o 6 11 0 5.13 1.84 11.69 o 7 11 0 29.82 28.14 28.62 o 8 11 0 59.90 71.52 17.44 o 9 11 0 5.24 0.00 15.48 o 10 11 0 47.94 68.77 16.10 o 0 12 0 795.92 816.03 68.41 o 1 12 0 854.61 831.17 56.34 o 2 12 0 5702.54 5640.25 160.52 o 3 12 0 3.73 38.63 11.05 o 4 12 0 152.21 140.25 13.50 o 5 12 0 701.41 685.36 20.57 o 6 12 0 62.83 82.36 12.95 o 7 12 0 123.50 147.42 15.14 o 8 12 0 73.46 83.04 15.18 o 9 12 0 444.33 422.33 32.64 o 10 12 0 79.68 99.54 20.12 o 1 13 0 1440.20 1310.19 23.37 o 2 13 0 460.03 448.99 24.59 o 3 13 0 0.69 12.74 12.07 o 4 13 0 2488.76 2521.80 51.87 o 5 13 0 14.88 45.47 14.31 o 6 13 0 1730.51 1811.46 57.23 o 7 13 0 309.33 313.42 18.34 o 8 13 0 495.98 528.17 27.72 o 9 13 0 12.73 15.31 15.77 o 0 14 0 428.61 406.34 16.40 o 1 14 0 0.00 0.00 11.69 o 2 14 0 33.81 29.01 12.32 o 3 14 0 327.82 317.21 26.83 o 4 14 0 531.73 557.85 22.36 o 5 14 0 155.17 138.11 15.48 o 6 14 0 225.00 247.78 17.38 o 7 14 0 403.72 411.27 24.59 o 8 14 0 118.32 176.93 17.38 o 1 15 0 991.21 1031.43 29.06 o 2 15 0 24.39 23.75 12.32 o 3 15 0 748.43 715.01 21.47 o 4 15 0 602.91 612.86 20.54 o 5 15 0 2005.32 2071.07 40.24 o 6 15 0 14.30 0.00 14.54 o 7 15 0 36.26 38.02 15.77 o 8 15 0 25.82 20.57 20.57 o 0 16 0 13.26 8.24 12.95 o 1 16 0 269.02 237.87 16.11 o 2 16 0 604.59 595.58 20.54 o 3 16 0 163.23 120.52 15.77 o 4 16 0 325.26 339.24 23.70 o 5 16 0 493.71 482.35 20.54 o 6 16 0 459.45 444.52 26.83 o 7 16 0 146.35 133.80 18.01 o 1 17 0 337.40 331.32 19.23 o 2 17 0 991.79 1060.45 28.62 o 3 17 0 128.09 107.34 15.81 o 4 17 0 313.38 320.81 37.11 o 5 17 0 23.97 30.48 15.02 o 6 17 0 1149.87 1258.94 54.10 o 0 18 0 2142.32 2157.34 111.33 o 1 18 0 115.53 120.80 21.91 o 2 18 0 1421.12 1501.50 135.48 o 3 18 0 346.80 364.27 19.91 o 4 18 0 417.24 453.09 21.18 o 5 18 0 62.32 44.19 16.04 o 1 19 0 676.60 673.64 68.41 o 2 19 0 11.64 22.32 22.80 o 3 19 0 299.47 312.30 19.28 o 4 19 0 23.21 0.00 16.40 o 0 20 0 24.25 44.41 15.66 o 1 20 0 135.35 141.58 17.67 o 1 0 1 1190.91 1190.24 46.05 o 2 0 1 4067.18 4161.49 48.29 o 3 0 1 5483.98 5935.85 136.82 o 4 0 1 120.73 143.51 11.18 o 5 0 1 7342.50 7282.03 192.26 o 6 0 1 83.08 48.09 10.28 o 7 0 1 58.23 76.38 13.86 o 8 0 1 1227.77 1171.38 33.09 o 9 0 1 2531.25 2478.44 66.17 o 10 0 1 73.93 86.17 14.22 o 11 0 1 888.81 841.04 25.29 o 12 0 1 244.81 236.29 34.43 o -12 1 1 129.36 147.55 26.83 o -11 1 1 59.33 13.41 21.46 o -10 1 1 298.30 338.92 25.04 o -9 1 1 718.48 752.06 30.40 o -8 1 1 2011.08 2017.40 41.14 o -7 1 1 743.39 798.56 25.04 o -6 1 1 2112.87 2232.92 33.98 o -5 1 1 5170.42 5506.73 46.50 o -4 1 1 273.61 267.38 12.52 o -3 1 1 7315.27 7692.25 41.14 o -2 1 1 3793.19 3870.27 24.14 o -1 1 1 35403.94 35406.52 203.89 o 0 1 1 1983.59 2031.29 7.60 o 1 1 1 35220.38 31882.32 194.05 o 2 1 1 3880.24 3805.88 24.14 o 3 1 1 7304.32 7264.80 39.35 o 4 1 1 174.89 152.91 10.73 o 5 1 1 5101.02 5307.31 44.71 o 6 1 1 2189.58 2206.09 33.09 o 7 1 1 786.03 837.01 25.04 o 8 1 1 1981.08 1985.21 38.45 o 9 1 1 703.34 707.34 28.62 o 10 1 1 378.57 395.25 25.04 o 11 1 1 69.58 49.18 22.36 o 12 1 1 118.56 120.72 25.04 o -12 2 1 47.73 46.50 22.36 o -11 2 1 41.27 50.97 19.67 o -10 2 1 332.51 411.35 26.83 o -9 2 1 132.73 146.66 20.57 o -8 2 1 1071.40 1010.49 31.30 o -7 2 1 183.41 209.25 17.88 o -6 2 1 225.13 219.98 16.99 o -5 2 1 606.75 603.61 17.88 o -4 2 1 8704.24 8952.23 51.87 o -3 2 1 2574.41 2790.92 25.93 o -2 2 1 11346.93 11985.49 44.71 o -1 2 1 2432.76 2469.89 16.99 o 0 2 1 11291.30 11236.71 363.51 o 1 2 1 2824.65 2766.78 17.88 o 2 2 1 11103.47 11233.44 42.92 o 3 2 1 2338.06 2410.87 24.14 o 4 2 1 8585.55 8419.26 50.08 o 5 2 1 502.08 480.21 16.10 o 6 2 1 244.39 252.18 16.10 o 7 2 1 186.05 212.83 17.88 o 8 2 1 1043.00 986.35 29.51 o 9 2 1 114.04 159.17 18.78 o 10 2 1 359.16 432.81 25.93 o 11 2 1 46.28 55.44 20.57 o 12 2 1 23.50 18.78 24.14 o -12 3 1 287.78 318.35 27.72 o -11 3 1 6.31 0.00 20.57 o -10 3 1 85.38 84.95 20.57 o -9 3 1 253.40 290.63 23.25 o -8 3 1 2883.85 2921.48 47.39 o -7 3 1 336.51 354.12 20.57 o -6 3 1 3697.07 3658.33 42.92 o -5 3 1 3464.67 3625.25 39.35 o -4 3 1 2139.57 2065.69 27.72 o -3 3 1 824.26 739.54 16.10 o -2 3 1 18488.70 18846.99 221.77 o -1 3 1 8838.15 9368.95 37.56 o 0 3 1 867.07 888.01 10.73 o 1 3 1 9480.79 9812.49 37.56 o 2 3 1 17995.47 17375.07 209.25 o 3 3 1 932.12 846.84 16.10 o 4 3 1 2044.46 1855.55 25.04 o 5 3 1 3588.83 3621.67 38.45 o 6 3 1 3432.94 3293.48 41.14 o 7 3 1 282.87 306.72 19.67 o 8 3 1 2960.18 2912.54 45.61 o 9 3 1 220.65 196.73 22.36 o 10 3 1 60.34 23.25 21.46 o 11 3 1 5.96 16.10 19.67 o 12 3 1 284.79 328.19 28.62 o -12 4 1 48.07 11.63 24.14 o -11 4 1 107.98 89.42 23.25 o -10 4 1 329.99 329.08 25.04 o -9 4 1 3978.87 4010.66 59.02 o -8 4 1 107.90 98.37 18.78 o -7 4 1 19.39 69.75 16.10 o -6 4 1 1545.54 1589.96 31.30 o -5 4 1 9108.92 9366.26 62.60 o -4 4 1 1119.43 1063.25 21.46 o -3 4 1 714.52 763.68 16.99 o -2 4 1 6633.59 7212.94 40.24 o -1 4 1 3034.40 3070.82 25.04 o 0 4 1 251.90 264.31 11.63 o 1 4 1 3227.80 3275.60 25.04 o 2 4 1 6320.86 6634.36 38.45 o 3 4 1 981.66 1018.54 18.78 o 4 4 1 1215.09 1129.42 21.46 o 5 4 1 9379.47 9242.86 60.81 o 6 4 1 1459.58 1512.16 29.51 o 7 4 1 24.63 16.99 15.20 o 8 4 1 137.05 167.22 18.78 o 9 4 1 4045.09 3941.81 58.13 o 10 4 1 297.76 320.14 24.14 o 11 4 1 120.29 132.35 22.36 o 12 4 1 57.59 0.00 25.04 o -12 5 1 37.25 55.44 22.36 o -11 5 1 43.05 81.38 20.57 o -10 5 1 311.94 281.69 25.04 o -9 5 1 225.90 236.97 22.36 o -8 5 1 596.70 613.45 26.83 o -7 5 1 3038.86 2990.34 45.61 o -6 5 1 777.99 785.14 25.04 o -5 5 1 5615.54 5968.15 51.87 o -4 5 1 3578.19 3544.77 37.56 o -3 5 1 3753.88 3937.34 35.77 o -2 5 1 362.70 383.63 13.41 o -1 5 1 1335.10 1319.90 18.78 o 0 5 1 45.57 53.07 5.98 o 1 5 1 988.88 947.89 16.10 o 2 5 1 452.94 500.77 13.41 o 3 5 1 3849.46 3887.26 34.88 o 4 5 1 3716.36 3680.69 37.56 o 5 5 1 5596.94 5764.27 50.97 o 6 5 1 918.73 930.01 25.04 o 7 5 1 3147.87 3074.40 44.71 o 8 5 1 528.05 540.12 25.04 o 9 5 1 222.69 217.30 22.36 o 10 5 1 368.23 347.86 25.04 o 11 5 1 52.04 34.88 22.36 o 12 5 1 46.67 63.49 25.04 o -11 6 1 7.42 4.47 21.46 o -10 6 1 127.27 114.46 22.36 o -9 6 1 1400.43 1462.98 39.35 o -8 6 1 599.81 597.35 26.83 o -7 6 1 444.35 418.50 24.14 o -6 6 1 1336.72 1367.29 31.30 o -5 6 1 4350.82 4352.26 47.39 o -4 6 1 8475.67 8640.14 59.91 o -3 6 1 856.30 966.67 21.46 o -2 6 1 6529.83 6990.27 46.50 o -1 6 1 907.68 947.00 17.88 o 0 6 1 7677.40 7832.27 126.53 o 1 6 1 798.53 889.77 16.99 o 2 6 1 7066.53 7499.99 47.39 o 3 6 1 1013.31 1117.80 21.46 o 4 6 1 8332.87 8333.42 57.23 o 5 6 1 4338.12 4286.98 45.61 o 6 6 1 1522.71 1483.54 32.19 o 7 6 1 533.53 517.76 23.25 o 8 6 1 599.83 602.72 25.93 o 9 6 1 1362.20 1339.57 37.56 o 10 6 1 126.91 143.08 23.25 o 11 6 1 1.55 0.00 20.57 o -11 7 1 43.95 72.43 23.25 o -10 7 1 183.58 245.02 23.25 o -9 7 1 897.92 877.25 33.09 o -8 7 1 932.17 968.46 31.30 o -7 7 1 190.88 226.24 19.67 o -6 7 1 4975.39 4878.97 56.34 o -5 7 1 1383.03 1427.21 30.40 o -4 7 1 1252.22 1186.66 25.93 o -3 7 1 257.58 285.26 15.20 o -2 7 1 3341.64 3500.05 35.77 o -1 7 1 1317.55 1418.26 23.25 o 0 7 1 7.78 9.39 9.39 o 1 7 1 1152.54 1231.37 20.57 o 2 7 1 3400.50 3716.46 35.77 o 3 7 1 181.48 211.93 13.41 o 4 7 1 1387.83 1372.66 26.83 o 5 7 1 1449.87 1434.36 29.51 o 6 7 1 5238.57 5103.42 54.55 o 7 7 1 154.91 132.35 18.78 o 8 7 1 886.86 879.04 30.40 o 9 7 1 966.17 924.64 33.09 o 10 7 1 159.41 161.86 25.04 o 11 7 1 62.87 113.57 24.14 o -11 8 1 618.20 631.33 34.88 o -10 8 1 713.94 750.27 33.98 o -9 8 1 572.09 636.70 30.40 o -8 8 1 600.92 625.07 27.72 o -7 8 1 748.62 855.79 28.62 o -6 8 1 572.05 520.45 25.93 o -5 8 1 1041.38 1010.49 26.83 o -4 8 1 1801.13 1766.12 32.19 o -3 8 1 573.70 633.12 20.57 o -2 8 1 1907.26 1843.03 28.62 o -1 8 1 550.13 510.61 16.99 o 0 8 1 13967.70 14366.06 254.41 o 1 8 1 546.34 473.95 16.10 o 2 8 1 2005.89 1982.53 29.51 o 3 8 1 704.42 789.61 20.57 o 4 8 1 1780.23 1643.61 30.40 o 5 8 1 1104.51 1087.40 27.72 o 6 8 1 497.28 489.15 23.25 o 7 8 1 834.35 900.50 29.51 o 8 8 1 558.69 594.67 27.72 o 9 8 1 676.14 706.45 30.40 o 10 8 1 671.00 680.52 34.88 o 11 8 1 530.38 572.31 32.19 o -11 9 1 9.38 12.52 23.25 o -10 9 1 61.91 26.83 22.36 o -9 9 1 214.82 245.92 25.93 o -8 9 1 84.85 79.59 20.57 o -7 9 1 372.19 362.17 22.36 o -6 9 1 444.40 456.96 24.14 o -5 9 1 844.33 864.73 27.72 o -4 9 1 490.72 510.61 22.36 o -3 9 1 2309.11 2254.38 34.88 o -2 9 1 616.02 554.43 19.67 o -1 9 1 7013.95 6781.91 53.65 o 0 9 1 442.33 398.08 11.96 o 1 9 1 6778.09 6825.73 52.76 o 2 9 1 713.48 715.39 20.57 o 3 9 1 2232.17 2305.35 34.88 o 4 9 1 598.08 606.29 22.36 o 5 9 1 1023.02 1033.74 28.62 o 6 9 1 486.19 452.49 23.25 o 7 9 1 348.73 329.08 22.36 o 8 9 1 81.61 77.80 20.57 o 9 9 1 208.67 297.78 23.25 o 10 9 1 57.56 48.29 23.25 o 11 9 1 21.94 43.82 23.25 o -10 10 1 57.42 50.97 23.25 o -9 10 1 1019.43 916.60 36.66 o -8 10 1 566.43 533.86 28.62 o -7 10 1 32.16 0.00 17.88 o -6 10 1 609.42 691.25 26.83 o -5 10 1 791.46 734.17 27.72 o -4 10 1 2342.05 2319.66 40.24 o -3 10 1 588.10 569.63 23.25 o -2 10 1 5749.77 5792.88 54.55 o -1 10 1 1085.55 1055.20 25.93 o 0 10 1 5272.83 5043.18 136.37 o 1 10 1 1123.09 1175.92 25.93 o 2 10 1 6033.98 6257.89 55.44 o 3 10 1 721.06 709.13 24.14 o 4 10 1 2222.50 2294.62 37.56 o 5 10 1 618.92 656.37 25.04 o 6 10 1 729.96 816.44 27.72 o 7 10 1 29.00 33.98 16.99 o 8 10 1 564.31 566.05 28.62 o 9 10 1 1061.37 1165.19 38.45 o 10 10 1 43.98 63.49 21.46 o -10 11 1 345.95 397.94 29.51 o -9 11 1 211.80 164.54 26.83 o -8 11 1 2232.37 2334.86 49.18 o -7 11 1 163.90 143.97 23.25 o -6 11 1 778.37 814.65 29.51 o -5 11 1 279.95 282.58 22.36 o -4 11 1 911.94 855.79 29.51 o -3 11 1 166.54 135.92 18.78 o -2 11 1 274.46 280.79 19.67 o -1 11 1 213.41 167.22 19.67 o 0 11 1 4652.25 4614.81 87.64 o 1 11 1 234.35 251.28 16.99 o 2 11 1 328.49 342.49 19.67 o 3 11 1 166.39 99.26 17.88 o 4 11 1 978.22 978.30 28.62 o 5 11 1 268.08 275.43 20.57 o 6 11 1 876.02 937.16 30.40 o 7 11 1 151.46 156.49 21.46 o 8 11 1 1979.59 1957.49 47.39 o 9 11 1 200.73 206.57 25.93 o 10 11 1 410.08 433.71 30.40 o -10 12 1 314.14 370.22 30.40 o -9 12 1 421.72 406.88 29.51 o -8 12 1 245.00 199.42 25.93 o -7 12 1 854.75 864.73 33.98 o -6 12 1 284.19 296.89 23.25 o -5 12 1 1177.06 1186.66 33.98 o -4 12 1 2167.86 2211.45 42.03 o -3 12 1 8.56 25.93 16.99 o -2 12 1 1200.03 1181.29 32.19 o -1 12 1 280.42 272.74 20.57 o 0 12 1 2373.54 2278.03 61.26 o 1 12 1 220.25 247.70 17.88 o 2 12 1 1327.29 1392.33 31.30 o 3 12 1 0.55 0.00 15.20 o 4 12 1 2110.53 2150.65 40.24 o 5 12 1 1093.64 1126.74 33.09 o 6 12 1 218.19 177.06 21.46 o 7 12 1 766.17 830.75 32.19 o 8 12 1 278.77 304.04 25.93 o 9 12 1 449.49 451.59 30.40 o 10 12 1 302.22 261.12 29.51 o -9 13 1 27.25 34.88 23.25 o -8 13 1 4.70 8.05 19.67 o -7 13 1 559.68 621.50 30.40 o -6 13 1 165.42 174.38 23.25 o -5 13 1 1260.48 1211.69 36.66 o -4 13 1 923.87 875.46 30.40 o -3 13 1 405.18 408.67 23.25 o -2 13 1 71.66 82.27 17.88 o -1 13 1 774.82 715.39 27.72 o 0 13 1 806.63 769.64 54.10 o 1 13 1 888.83 901.39 26.83 o 2 13 1 39.02 61.70 14.31 o 3 13 1 670.13 678.73 25.93 o 4 13 1 924.78 916.60 30.40 o 5 13 1 1462.78 1442.41 38.45 o 6 13 1 179.23 173.48 22.36 o 7 13 1 523.32 642.96 31.30 o 8 13 1 6.27 15.20 19.67 o 9 13 1 26.66 28.62 23.25 o -8 14 1 68.55 52.76 22.36 o -7 14 1 159.72 181.53 25.04 o -6 14 1 140.70 154.70 23.25 o -5 14 1 2365.21 2366.16 49.18 o -4 14 1 1151.40 1060.57 33.98 o -3 14 1 257.99 277.21 22.36 o -2 14 1 1584.33 1496.96 36.66 o -1 14 1 1537.68 1446.88 35.77 o 0 14 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18.78 o -6 4 2 898.57 902.29 25.04 o -5 4 2 618.22 601.82 20.57 o -4 4 2 2555.49 2390.30 30.40 o -3 4 2 753.00 716.29 16.99 o -2 4 2 3237.14 3287.22 28.62 o -1 4 2 414.51 445.33 12.52 o 0 4 2 7205.54 7099.86 114.02 o 1 4 2 644.02 671.57 13.41 o 2 4 2 2613.68 2651.42 25.93 o 3 4 2 667.26 599.14 15.20 o 4 4 2 2585.67 2300.88 29.51 o 5 4 2 492.23 457.85 17.88 o 6 4 2 763.76 752.06 24.14 o 7 4 2 194.26 185.11 17.88 o 8 4 2 202.26 200.31 20.57 o 9 4 2 808.48 818.23 31.30 o 10 4 2 16.83 42.03 17.88 o 11 4 2 122.48 125.19 22.36 o 12 4 2 1.71 0.00 23.25 o -11 5 2 23.41 69.75 20.57 o -10 5 2 134.97 126.09 22.36 o -9 5 2 169.48 152.02 20.57 o -8 5 2 2050.11 2081.79 42.03 o -7 5 2 1419.42 1420.05 33.98 o -6 5 2 2680.82 2834.74 41.14 o -5 5 2 4777.63 4743.94 47.39 o -4 5 2 3197.60 3280.07 36.66 o -3 5 2 3417.81 3530.46 34.88 o -2 5 2 2941.56 3031.47 29.51 o -1 5 2 7436.95 7486.57 42.92 o 0 5 2 737.27 765.28 23.25 o 1 5 2 8006.40 8219.85 43.82 o 2 5 2 2723.49 2720.28 27.72 o 3 5 2 3566.21 3621.67 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20.57 o -8 7 2 522.03 474.84 25.04 o -7 7 2 417.05 400.62 23.25 o -6 7 2 62.54 54.55 16.99 o -5 7 2 595.97 659.05 23.25 o -4 7 2 1435.23 1396.80 27.72 o -3 7 2 2027.40 1888.63 29.51 o -2 7 2 871.27 963.10 20.57 o -1 7 2 4638.49 4612.49 40.24 o 0 7 2 3564.70 3206.94 38.90 o 1 7 2 5002.25 5068.55 41.14 o 2 7 2 669.76 727.91 17.88 o 3 7 2 2198.79 2132.76 30.40 o 4 7 2 1532.16 1491.59 27.72 o 5 7 2 685.89 718.97 23.25 o 6 7 2 31.43 26.83 15.20 o 7 7 2 500.51 498.99 23.25 o 8 7 2 443.67 440.86 24.14 o 9 7 2 102.87 116.25 21.46 o 10 7 2 399.08 413.14 28.62 o 11 7 2 70.99 93.90 23.25 o -11 8 2 145.59 126.98 24.14 o -10 8 2 137.59 136.82 23.25 o -9 8 2 877.88 889.77 33.98 o -8 8 2 617.65 630.44 28.62 o -7 8 2 30.54 30.40 18.78 o -6 8 2 601.22 566.05 25.04 o -5 8 2 2555.07 2559.31 40.24 o -4 8 2 2546.28 2635.32 37.56 o -3 8 2 299.66 318.35 16.10 o -2 8 2 4543.15 4568.67 43.82 o -1 8 2 381.34 287.05 15.20 o 0 8 2 12046.37 12486.37 181.08 o 1 8 2 456.56 425.66 16.10 o 2 8 2 3915.77 3946.28 40.24 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285.26 21.46 o -1 13 2 199.18 110.89 20.57 o 0 13 2 2729.55 2710.96 37.11 o 1 13 2 167.01 134.14 17.88 o 2 13 2 388.10 387.21 21.46 o 3 13 2 1501.13 1450.46 34.88 o 4 13 2 4182.52 4204.71 57.23 o 5 13 2 1302.65 1351.20 36.66 o 6 13 2 1022.44 1001.55 33.98 o 7 13 2 226.48 246.81 23.25 o 8 13 2 263.92 248.60 26.83 o 9 13 2 332.50 255.75 28.62 o -8 14 2 267.64 267.38 27.72 o -7 14 2 570.85 572.31 31.30 o -6 14 2 263.94 290.63 25.93 o -5 14 2 278.54 285.26 24.14 o -4 14 2 508.68 532.97 28.62 o -3 14 2 916.18 894.24 31.30 o -2 14 2 199.08 194.94 20.57 o -1 14 2 484.99 480.21 25.04 o 0 14 2 314.75 354.40 15.77 o 1 14 2 580.89 619.71 25.93 o 2 14 2 146.66 126.09 19.67 o 3 14 2 843.36 821.81 29.51 o 4 14 2 635.69 718.97 29.51 o 5 14 2 199.71 217.30 23.25 o 6 14 2 238.58 301.36 24.14 o 7 14 2 512.19 494.51 30.40 o 8 14 2 280.01 240.55 28.62 o -8 15 2 268.99 341.60 27.72 o -7 15 2 128.98 118.04 25.04 o -6 15 2 253.17 236.97 25.04 o -5 15 2 389.74 417.61 26.83 o -4 15 2 502.02 472.16 28.62 o -3 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