#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/16/2201638.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201638_Fobs loop_ _publ_author_name 'Gainsford, Graeme J.' 'Chong, S. V.' 'Ingham, B.' 'Tallon, J. L.' _publ_section_title ; Decaammonium dodecatungstate nonahydrate, (NH~4~)~10~[H~2~W~12~O~42~]·9H~2~O: anionic `isomorphism' ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i93 _journal_page_last i94 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 76.159 _cell_angle_beta 80.985 _cell_angle_gamma 88.763 _cell_length_a 11.9451 _cell_length_b 13.2246 _cell_length_c 16.7796 _exptl_crystal_F_000 2852.00 _reflns_d_resolution_high 0.7979 _[local]_cod_data_source_file tk6075Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jt21p in P-1 ACTAB labels (plus transf.)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1030.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h 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6426.85 416.42 o 1 4 0 48561.16 41615.59 3501.43 o 2 4 0 121304.87 117376.84 6655.28 o 3 4 0 27029.74 27176.73 1467.50 o 4 4 0 100203.00 103984.04 2545.81 o 5 4 0 162417.88 170484.86 2703.31 o 6 4 0 14359.12 15317.99 850.63 o 7 4 0 83266.85 96268.47 1528.22 o 8 4 0 16569.89 17428.75 1158.24 o 9 4 0 141.09 -102.58 1250.69 o 10 4 0 9422.24 9940.15 1607.77 o 11 4 0 12008.85 11963.15 1898.68 o 12 4 0 14884.54 14679.35 2292.30 o 13 4 0 1078.91 -808.29 2609.39 o 14 4 0 4017.91 4174.91 2950.25 o -14 5 0 18624.59 17748.26 3694.09 o -13 5 0 44.68 -835.53 2542.59 o -12 5 0 85555.53 81577.01 3469.65 o -11 5 0 214.24 -144.71 1952.32 o -10 5 0 75678.88 79134.39 2812.17 o -9 5 0 99451.05 106603.01 2413.15 o -8 5 0 55.94 390.01 1171.97 o -7 5 0 15744.61 17887.93 1016.29 o -6 5 0 56288.31 56266.93 1356.92 o -5 5 0 49622.57 48459.45 1017.74 o -4 5 0 643.77 881.04 498.91 o -3 5 0 130127.02 127499.91 1121.36 o -2 5 0 19491.03 19523.57 735.31 o -1 5 0 144520.89 128765.45 1092.31 o 0 5 0 85408.78 74751.17 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18108.72 17540.45 835.09 o 4 6 0 9286.75 10522.37 623.92 o 5 6 0 28.49 -310.85 660.10 o 6 6 0 49232.84 49159.67 1505.90 o 7 6 0 273.80 788.89 1194.87 o 8 6 0 32854.66 34908.24 1947.26 o 9 6 0 16162.03 16208.76 1613.07 o 10 6 0 183434.11 193790.75 4431.63 o 11 6 0 35640.49 32219.84 2505.20 o 12 6 0 10532.42 9767.02 2144.93 o 13 6 0 14891.99 12456.58 2577.62 o -13 7 0 4747.13 4769.74 2933.49 o -12 7 0 6542.41 6294.78 2503.91 o -11 7 0 906.23 691.12 2188.24 o -10 7 0 2547.16 2480.30 1933.96 o -9 7 0 9983.02 10498.26 1584.27 o -8 7 0 43506.05 41645.58 1997.10 o -7 7 0 7430.47 8715.62 1230.61 o -6 7 0 14517.35 14496.72 1161.50 o -5 7 0 39385.23 39447.41 1296.66 o -4 7 0 186426.55 181094.48 1722.09 o -3 7 0 118481.33 111841.94 1985.54 o -2 7 0 166833.27 149312.45 1445.25 o -1 7 0 87797.30 75207.73 1197.70 o 0 7 0 38033.71 34136.95 1138.55 o 1 7 0 605.96 528.84 787.12 o 2 7 0 83.60 -59.91 714.11 o 3 7 0 35668.43 28952.06 1564.19 o 4 7 0 13310.80 12627.44 816.09 o 5 7 0 21769.40 16985.62 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