#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/16/2201640.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2201640_Fobs
loop_
_publ_author_name
'Gainsford, Graeme J.'
'Robinson, Natalie'
'Tallon, J. L.'
_publ_section_title
;
 (NH~4~)~2~(NH~3~(CH~2~)~6~NH~3~)~4~[H~2~W~12~O~42~]·8H~2~O: a
 novel ammonium 1,6-hexanediammonium dodecatungstate
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m521
_journal_page_last               m523
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                85.993
_cell_angle_beta                 84.851
_cell_angle_gamma                87.695
_cell_length_a                   10.9870
_cell_length_b                   10.9800
_cell_length_c                   14.6810
_exptl_crystal_F_000             1600.00
_reflns_d_resolution_high        0.9203
_[local]_cod_data_source_file    tk6077Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title
' woxp1 in P-1  FINAL DATASET  (a>b)  DAUTER  Half moleculesDiamh2+'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            658.83
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 893.63 1005.57 40.34 o
3 0 0 655.42 734.45 21.36 o
4 0 0 47663.46 52811.59 1539.50 o
5 0 0 1731.55 1942.91 54.58 o
6 0 0 51075.88 55231.48 1678.91 o
7 0 0 30914.53 32258.85 1029.30 o
8 0 0 3688.68 3950.49 169.67 o
9 0 0 34137.25 33330.86 2134.53 o
10 0 0 24108.03 23476.30 1671.20 o
11 0 0 550.07 571.30 46.27 o
-11 1 0 761.76 734.45 59.33 o
-10 1 0 64.54 161.37 14.83 o
-9 1 0 78426.41 78709.56 5052.16 o
-8 1 0 97408.40 102569.70 4432.21 o
-7 1 0 3.42 30.26 7.12 o
-6 1 0 18201.78 19368.60 608.09 o
-5 1 0 36816.93 42441.48 1185.32 o
-4 1 0 67.62 176.79 8.31 o
-2 1 0 4914.33 4273.22 143.57 o
-1 1 0 83338.69 89434.43 3510.89 o
1 1 0 6881.86 7008.72 295.44 o
2 1 0 6239.24 6115.28 173.82 o
3 1 0 83963.39 86745.80 2448.96 o
4 1 0 62060.91 61864.07 2064.53 o
5 1 0 8183.33 8795.60 250.35 o
6 1 0 37122.68 39125.19 1228.04 o
7 1 0 67463.77 68168.59 2116.73 o
8 1 0 37265.12 38452.44 1656.96 o
9 1 0 23128.05 22894.91 1467.12 o
10 1 0 5508.12 5326.84 383.24 o
11 1 0 8312.75 7596.04 593.26 o
-11 2 0 2596.44 2746.18 304.34 o
-10 2 0 52113.25 51189.63 4025.24 o
-9 2 0 245080.64 255973.06 23540.37 o
-8 2 0 151328.75 158644.78 10225.35 o
-7 2 0 2978.20 3094.42 109.75 o
-5 2 0 31164.06 35342.59 1153.29 o
-4 2 0 4900.28 5436.00 155.43 o
-3 2 0 25822.78 27619.60 822.85 o
-2 2 0 62403.82 64165.31 1852.74 o
-1 2 0 62015.55 63769.61 1786.29 o
0 2 0 96761.66 99711.39 5664.99 o
1 2 0 65234.97 55146.64 3173.92 o
2 2 0 6096.80 7084.65 205.27 o
3 2 0 23647.19 26593.86 747.50 o
4 2 0 731.40 678.68 19.58 o
5 2 0 3128.64 3487.15 101.45 o
6 2 0 8734.27 9406.06 402.23 o
7 2 0 8956.29 9050.11 281.80 o
8 2 0 4200.31 4483.23 298.41 o
9 2 0 548.20 433.08 29.66 o
11 2 0 19380.46 17758.50 1383.47 o
-10 3 0 10706.86 10183.23 799.11 o
-7 3 0 2105.46 2432.35 105.01 o
-6 3 0 6975.50 7272.12 223.66 o
-5 3 0 25872.59 28762.80 891.07 o
-4 3 0 15058.67 16331.73 462.74 o
-3 3 0 2296.45 2415.74 70.60 o
-2 3 0 45662.10 43062.03 1207.87 o
-1 3 0 187684.58 195238.55 7633.42 o
0 3 0 57427.57 54707.04 1786.29 o
2 3 0 1000.50 1708.58 51.61 o
3 3 0 55400.02 53295.09 1733.49 o
4 3 0 44272.62 44375.50 1280.24 o
5 3 0 2264.77 2146.99 68.22 o
6 3 0 8334.40 7967.42 244.42 o
7 3 0 639.42 710.72 23.73 o
8 3 0 6773.27 6561.40 436.04 o
9 3 0 3879.33 3636.66 241.45 o
10 3 0 771.51 774.79 62.29 o
11 3 0 10612.21 9573.96 821.07 o
-10 4 0 35765.16 33727.75 2632.87 o
-9 4 0 54148.15 52447.93 3722.68 o
-8 4 0 27889.92 29512.08 1898.42 o
-7 4 0 32.77 52.21 9.49 o
-6 4 0 30.50 140.01 8.90 o
-5 4 0 3535.31 3923.20 119.84 o
-4 4 0 786.09 749.28 24.32 o
-3 4 0 907.46 1234.56 50.43 o
-2 4 0 6734.66 7003.38 206.45 o
-1 4 0 16902.77 16172.14 453.84 o
0 4 0 492.28 340.53 10.09 o
3 4 0 112059.38 115802.85 4583.49 o
4 4 0 2941.87 3214.85 100.26 o
5 4 0 88508.75 82964.38 2606.17 o
6 4 0 56518.38 52594.45 1634.42 o
7 4 0 15323.58 14814.18 637.75 o
8 4 0 21579.83 20230.01 1301.01 o
9 4 0 7587.74 7355.77 525.03 o
10 4 0 6916.24 6195.96 490.03 o
11 4 0 5936.42 5071.15 443.76 o
-9 5 0 39411.53 39266.98 3071.88 o
-8 5 0 2669.67 2885.00 185.69 o
-7 5 0 18750.08 18270.48 1179.39 o
-6 5 0 23541.51 23638.26 1014.47 o
-5 5 0 80513.56 82047.80 2554.56 o
-4 5 0 400.98 507.23 17.80 o
-3 5 0 28465.99 28314.89 867.34 o
-2 5 0 4321.19 4206.18 121.02 o
-1 5 0 19091.26 19458.18 542.24 o
0 5 0 4761.27 3767.17 112.13 o
4 5 0 107701.30 103562.20 3227.90 o
5 5 0 216879.05 200772.44 7111.35 o
6 5 0 23212.59 20736.65 686.99 o
7 5 0 168.59 277.64 19.58 o
8 5 0 5133.60 4819.61 313.24 o
9 5 0 40309.02 36550.46 2615.07 o
10 5 0 5906.06 5336.33 420.62 o
-9 6 0 1144.73 1153.29 130.52 o
-8 6 0 51389.32 52502.50 5363.62 o
-7 6 0 4985.69 4957.83 317.98 o
-6 6 0 27995.21 28583.63 1844.43 o
-5 6 0 1043.97 983.62 45.09 o
-4 6 0 134428.09 131302.83 3974.22 o
-3 6 0 75497.31 71629.05 2199.20 o
-2 6 0 176.01 223.66 8.90 o
-1 6 0 7749.58 7463.75 240.86 o
0 6 0 793.34 686.99 24.32 o
5 6 0 3074.27 2956.19 100.85 o
6 6 0 56.09 59.33 7.71 o
7 6 0 15493.83 13610.46 936.16 o
8 6 0 46468.03 42930.33 3159.08 o
9 6 0 41857.87 36012.38 2886.78 o
10 6 0 9596.16 7718.84 701.82 o
-8 7 0 5077.66 5121.57 567.75 o
-7 7 0 3202.13 2793.05 283.58 o
-6 7 0 1554.92 1795.78 167.30 o
-5 7 0 33854.69 31310.24 2027.75 o
-4 7 0 183813.25 170192.50 10874.37 o
-3 7 0 55574.25 52904.13 1636.20 o
-2 7 0 757.30 726.14 35.00 o
-1 7 0 4644.41 4662.39 153.06 o
0 7 0 15685.42 16017.30 504.27 o
7 7 0 3699.94 3150.78 236.71 o
8 7 0 11.90 82.46 17.80 o
9 7 0 3365.44 3198.24 250.35 o
-8 8 0 3877.40 3773.70 457.40 o
-7 8 0 4870.78 4266.10 475.20 o
-6 8 0 453.43 560.03 61.11 o
-5 8 0 287.17 413.50 40.34 o
-4 8 0 5234.14 4773.93 306.71 o
-3 8 0 90.16 222.47 16.02 o
-2 8 0 5267.05 5572.45 371.97 o
-1 8 0 41624.47 37757.73 1869.94 o
0 8 0 30730.48 27961.31 1251.77 o
-7 9 0 150.47 128.74 23.14 o
-6 9 0 8460.41 7202.71 806.23 o
-5 9 0 90014.95 78675.15 8796.20 o
-4 9 0 128118.59 110445.75 11079.64 o
-3 9 0 20216.30 17983.35 1165.75 o
-2 9 0 4734.79 4320.68 285.36 o
-1 9 0 1800.19 1423.81 109.75 o
-6 10 0 1790.86 1287.96 215.35 o
-5 10 0 72620.40 61521.77 7617.99 o
-4 10 0 39568.37 35449.97 3900.65 o
-3 10 0 41.79 100.85 14.83 o
-2 10 0 2856.14 2644.73 217.13 o
-1 10 0 125215.71 109199.33 7760.37 o
-2 11 0 6746.42 5705.93 449.69 o
1 -10 1 144976.83 117401.08 8413.55 o
2 -10 1 34940.74 32290.89 2513.03 o
3 -10 1 413.52 464.52 38.56 o
4 -10 1 216.47 199.33 29.07 o
5 -10 1 23.50 72.97 18.39 o
6 -10 1 495.69 617.58 102.04 o
1 -9 1 103.57 230.78 17.80 o
2 -9 1 97.72 149.50 13.64 o
3 -9 1 5594.54 4929.95 319.17 o
4 -9 1 3863.30 3756.49 377.90 o
5 -9 1 956.24 900.56 101.45 o
6 -9 1 2278.81 1733.49 200.52 o
7 -9 1 117.45 108.57 21.95 o
0 -8 1 142546.36 112024.41 4923.43 o
1 -8 1 109071.80 112870.38 10249.08 o
2 -8 1 193.48 353.58 24.92 o
3 -8 1 4606.40 4162.28 274.08 o
4 -8 1 5358.98 4856.98 319.17 o
5 -8 1 10518.49 9640.40 621.73 o
6 -8 1 800.37 1009.13 73.56 o
7 -8 1 129.95 218.91 29.66 o
8 -8 1 16766.67 15931.87 1913.25 o
-9 -7 1 3443.65 2936.02 259.85 o
-8 -7 1 14686.12 12754.99 1017.43 o
-7 -7 1 4205.97 3186.97 253.32 o
-6 -7 1 3653.60 3227.31 293.07 o
0 -7 1 118067.86 111908.72 3429.02 o
1 -7 1 11593.53 11318.13 373.75 o
2 -7 1 36035.85 33693.34 1045.32 o
3 -7 1 358.08 573.08 20.76 o
4 -7 1 77381.13 72143.41 4639.26 o
5 -7 1 16371.15 15346.33 987.18 o
6 -7 1 11753.79 11437.96 735.04 o
7 -7 1 16505.05 16201.80 1154.47 o
8 -7 1 2741.20 2868.39 226.03 o
-10 -6 1 1029.21 555.29 55.77 o
-9 -6 1 98425.80 90733.06 7294.67 o
-8 -6 1 101264.91 94016.14 6949.39 o
-7 -6 1 2118.65 1888.33 127.55 o
-6 -6 1 13740.58 12802.45 832.93 o
-4 -6 1 23611.62 21337.61 686.99 o
-1 -6 1 15927.42 16627.17 587.92 o
0 -6 1 3982.21 3852.01 119.84 o
1 -6 1 37927.79 35851.02 1101.68 o
2 -6 1 74731.35 71236.91 2173.69 o
3 -6 1 2186.25 2248.44 69.41 o
4 -6 1 8932.90 9165.20 284.17 o
5 -6 1 39649.67 39574.29 1719.85 o
6 -6 1 99973.35 94895.93 6188.84 o
7 -6 1 45550.46 44286.51 2864.24 o
8 -6 1 14.97 69.41 11.27 o
9 -6 1 4733.70 4226.94 331.04 o
-10 -5 1 2974.00 2355.22 195.18 o
-9 -5 1 69483.26 64944.85 5117.42 o
-8 -5 1 3132.13 2885.59 188.06 o
-7 -5 1 62045.02 60514.42 3880.48 o
-6 -5 1 27866.79 27015.07 869.71 o
-5 -5 1 10939.65 11432.62 363.67 o
-4 -5 1 18140.47 17620.28 581.98 o
-3 -5 1 20862.83 20921.74 668.01 o
-2 -5 1 19637.15 17127.28 972.35 o
-1 -5 1 985.62 1069.05 32.04 o
0 -5 1 4363.83 4749.01 135.86 o
1 -5 1 70.90 125.77 5.93 o
2 -5 1 68.58 180.35 8.90 o
3 -5 1 1539.50 1631.45 51.02 o
4 -5 1 9966.24 9226.31 292.47 o
5 -5 1 82508.13 84174.03 2569.98 o
6 -5 1 52187.61 54024.20 2339.80 o
7 -5 1 21809.21 22525.90 1460.59 o
8 -5 1 11760.14 11970.71 772.42 o
9 -5 1 2016.32 2178.43 171.45 o
-11 -4 1 2069.00 1798.16 155.43 o
-10 -4 1 3637.28 3226.12 258.07 o
-9 -4 1 3779.98 3565.46 254.51 o
-8 -4 1 29757.13 28137.51 1847.40 o
-7 -4 1 61655.79 59560.46 2647.11 o
-6 -4 1 6089.82 5798.48 183.32 o
-5 -4 1 851.77 953.36 30.85 o
-4 -4 1 34569.68 34775.44 1070.83 o
-3 -4 1 107778.66 107346.59 3025.01 o
-2 -4 1 84806.37 85193.23 3395.20 o
-1 -4 1 15710.16 12891.44 366.04 o
0 -4 1 142.37 183.32 6.53 o
1 -4 1 31835.00 31051.58 863.78 o
2 -4 1 28503.42 29473.52 825.81 o
3 -4 1 1079.41 1566.19 45.09 o
4 -4 1 226.64 425.36 14.83 o
5 -4 1 38975.63 43220.43 1325.33 o
6 -4 1 55998.36 59616.23 1848.58 o
7 -4 1 765.37 859.03 56.95 o
8 -4 1 41837.45 43191.36 2788.89 o
9 -4 1 11284.09 11348.97 809.20 o
10 -4 1 576.10 583.17 47.46 o
-11 -3 1 4106.82 3843.70 331.63 o
-10 -3 1 5272.20 5103.78 399.26 o
-9 -3 1 3761.80 3916.08 253.32 o
-8 -3 1 531.51 659.11 43.31 o
-7 -3 1 20244.05 20148.73 626.48 o
-6 -3 1 6467.22 6299.78 196.96 o
-5 -3 1 16515.94 16559.54 510.79 o
-4 -3 1 63355.28 62519.62 1773.24 o
-3 -3 1 38508.01 36923.61 1099.90 o
-2 -3 1 49315.36 48944.16 1602.98 o
-1 -3 1 44314.26 43645.20 1217.36 o
0 -3 1 2614.88 2763.98 78.90 o
1 -3 1 13190.80 13167.30 372.56 o
2 -3 1 28.91 134.08 5.34 o
3 -3 1 5968.20 6370.97 180.94 o
4 -3 1 60948.22 63471.80 1777.39 o
5 -3 1 412923.31 416729.84 17787.57 o
6 -3 1 188816.59 196158.09 6079.09 o
7 -3 1 6.03 129.33 10.09 o
8 -3 1 2681.61 2959.75 191.03 o
10 -3 1 16770.62 16564.88 1295.08 o
-11 -2 1 33188.33 31336.34 2476.84 o
-10 -2 1 33284.70 32576.84 2337.43 o
-9 -2 1 3557.31 3662.76 238.49 o
-8 -2 1 60652.67 62566.48 4095.24 o
-7 -2 1 67685.00 68712.02 2103.09 o
-6 -2 1 8082.24 7850.55 246.79 o
-5 -2 1 422.89 485.88 15.42 o
-4 -2 1 68627.91 67507.12 1966.64 o
-3 -2 1 182479.75 174433.08 6852.69 o
-2 -2 1 7914.96 7903.35 233.15 o
-1 -2 1 57912.56 58958.30 2295.90 o
0 -2 1 20293.03 20823.86 813.35 o
1 -2 1 67.71 781.91 31.44 o
2 -2 1 34276.28 34653.82 971.16 o
3 -2 1 51186.11 58318.78 1713.32 o
4 -2 1 33985.78 35031.13 976.50 o
5 -2 1 180081.31 192606.86 6198.92 o
7 -2 1 2993.23 3331.13 118.06 o
8 -2 1 53676.54 54412.79 3522.75 o
9 -2 1 157968.31 158737.33 10137.55 o
10 -2 1 38430.85 38227.59 2717.11 o
11 -2 1 11807.89 10169.58 1124.22 o
-11 -1 1 8231.68 8171.50 641.31 o
-10 -1 1 39749.64 39350.63 2804.32 o
-9 -1 1 10313.36 10139.92 650.21 o
-8 -1 1 19341.79 20361.12 1304.57 o
-7 -1 1 1730.20 1844.43 57.55 o
-6 -1 1 13399.52 14445.17 465.71 o
-5 -1 1 23530.59 24025.66 691.74 o
-4 -1 1 307959.56 310512.81 12905.68 o
-2 -1 1 4990.10 3577.33 103.82 o
-1 -1 1 2274.12 3178.66 132.30 o
0 -1 1 59631.02 65339.95 2553.96 o
1 -1 1 54560.92 47167.95 1854.52 o
2 -1 1 30509.64 30411.46 984.80 o
4 -1 1 4439.35 4312.97 141.19 o
5 -1 1 3833.77 4000.91 115.68 o
6 -1 1 21238.27 22203.77 676.90 o
7 -1 1 2471.60 2947.29 91.36 o
8 -1 1 16327.66 17351.53 762.93 o
9 -1 1 19738.82 19887.11 1279.06 o
10 -1 1 951.54 988.96 71.78 o
11 -1 1 5755.46 5288.87 415.87 o
-11 0 1 17071.38 15940.18 1241.68 o
-10 0 1 11848.45 12153.43 870.90 o
-9 0 1 15128.80 15616.85 1001.41 o
-7 0 1 13637.82 14512.81 447.31 o
-6 0 1 40024.41 44446.69 1375.76 o
-5 0 1 7570.23 7912.25 326.29 o
-4 0 1 58120.76 55470.56 1786.89 o
-3 0 1 4813.00 4980.38 145.35 o
-2 0 1 7245.54 6620.73 188.66 o
-1 0 1 23733.97 22416.75 873.27 o
1 0 1 72726.11 63227.96 2483.37 o
2 0 1 4389.86 4417.38 180.35 o
3 0 1 128715.55 138191.11 4460.69 o
4 0 1 65023.80 70341.69 1964.86 o
5 0 1 48012.61 52010.10 1492.04 o
6 0 1 16482.37 18325.06 565.37 o
7 0 1 5702.01 6334.78 195.18 o
8 0 1 34473.70 35721.68 1566.79 o
9 0 1 39930.83 41141.66 2638.80 o
10 0 1 5827.90 6277.23 629.44 o
11 0 1 442.05 605.12 48.65 o
-11 1 1 15030.84 13993.71 1090.40 o
-10 1 1 2228.34 2123.26 153.65 o
-9 1 1 151.79 214.17 16.02 o
-8 1 1 5377.16 5645.42 365.45 o
-7 1 1 3155.84 3606.99 111.53 o
-6 1 1 20678.01 22162.83 674.53 o
-5 1 1 29512.78 30387.72 867.93 o
-4 1 1 62785.27 66567.40 2167.16 o
-2 1 1 27746.31 29068.92 1209.65 o
-1 1 1 14775.60 11155.57 450.87 o
0 1 1 632.39 593.85 26.70 o
1 1 1 3191.77 3256.38 129.33 o
2 1 1 485.66 482.32 20.17 o
3 1 1 8910.86 8863.23 253.32 o
4 1 1 17782.93 18330.40 523.84 o
5 1 1 64.20 160.77 8.31 o
6 1 1 1858.67 2101.90 67.04 o
7 1 1 11220.19 10700.55 327.48 o
8 1 1 90894.74 91679.89 3919.64 o
9 1 1 16524.62 16719.71 1080.32 o
10 1 1 30808.37 29354.27 2089.45 o
11 1 1 25713.25 23747.42 1861.64 o
-10 2 1 1661.05 1637.98 128.74 o
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-8 2 1 10551.21 11180.49 720.21 o
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-5 2 1 108036.83 115646.23 3719.71 o
-4 2 1 114067.31 122160.76 3477.07 o
-3 2 1 2177.34 2062.16 61.70 o
-2 2 1 1533.74 1683.07 48.05 o
-1 2 1 50303.45 48162.84 1356.77 o
1 2 1 15441.00 12202.67 344.68 o
2 2 1 21664.05 21345.33 625.29 o
3 2 1 411.94 450.28 13.64 o
4 2 1 9948.06 10138.73 285.95 o
5 2 1 454.62 519.10 16.02 o
6 2 1 16218.86 16147.82 495.37 o
7 2 1 3079.02 3588.60 110.35 o
8 2 1 15013.66 14805.28 949.80 o
9 2 1 30037.53 29214.86 1877.06 o
10 2 1 120758.95 111523.10 8057.59 o
11 2 1 21196.20 19865.15 1556.70 o
-10 3 1 269.72 399.85 34.41 o
-8 3 1 7545.01 7915.81 511.98 o
-7 3 1 301.98 481.13 23.14 o
-6 3 1 6319.66 6477.75 198.74 o
-5 3 1 44148.49 47332.28 1446.36 o
-4 3 1 843.44 930.82 27.88 o
-3 3 1 65487.26 69779.28 1971.39 o
-2 3 1 2841.06 3211.29 91.95 o
-1 3 1 84231.58 86132.37 2816.78 o
0 3 1 53133.54 49779.46 1988.59 o
3 3 1 100.39 138.82 5.34 o
4 3 1 24147.25 22714.56 648.43 o
5 3 1 192.71 236.12 8.90 o
6 3 1 13042.52 12951.36 401.63 o
7 3 1 183.52 205.86 8.90 o
8 3 1 4164.92 4076.26 261.03 o
9 3 1 13248.56 13058.14 844.20 o
10 3 1 18037.63 16468.18 1290.92 o
11 3 1 366.68 290.10 25.51 o
-10 4 1 2055.43 2288.19 179.16 o
-9 4 1 47619.36 49311.38 3496.65 o
-8 4 1 7251.35 6775.57 433.08 o
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