#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2201691.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2201691_Fobs loop_ _publ_author_name 'Qi, Jian Ying' 'Chen, Jian' 'Yang, Qi Yun' 'Zhou, Zhong Yuan' 'Chan, Albert S. C.' _publ_section_title ; N,N'-Bis[2-(2-pyridyl)methyl]pyridine-2,6-dicarboxamide hemihydrate ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1232 _journal_page_last o1233 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 126.310 _cell_angle_gamma 90.000 _cell_length_a 17.7841 _cell_length_b 17.6115 _cell_length_c 14.2169 _exptl_crystal_F_000 1500.00 _reflns_d_resolution_high 0.7682 _[local]_cod_data_source_file ww6046Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' QJY56 in C2/c C19H17N5O2.1/2(H2O)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 483.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 10956.97 8623.53 106.38 o 6 0 0 1133.03 1197.17 48.91 o 8 0 0 5803.06 6041.64 297.47 o 10 0 0 110.40 117.30 29.09 o 12 0 0 151.29 123.09 35.98 o 14 0 0 276.78 241.55 54.40 o 16 0 0 1.10 14.04 43.87 o 18 0 0 8.11 -22.81 52.65 o 3 1 0 5.10 12.28 8.11 o 5 1 0 28.78 8.92 8.38 o 7 1 0 10434.40 10624.83 256.09 o 9 1 0 349.02 378.24 28.59 o 11 1 0 25.59 12.99 16.22 o 13 1 0 163.05 178.32 26.29 o 15 1 0 324.15 259.75 32.86 o 17 1 0 0.16 -14.04 34.75 o 0 2 0 27950.11 25419.84 309.63 o 2 2 0 998.14 1810.05 52.28 o 4 2 0 697.14 775.27 29.03 o 6 2 0 143.69 112.09 15.89 o 8 2 0 1988.27 2055.41 70.42 o 10 2 0 1.91 -7.73 12.72 o 12 2 0 21.13 -1.47 17.42 o 14 2 0 16.59 19.09 20.68 o 16 2 0 54.23 46.47 33.44 o 18 2 0 0.81 3.51 50.89 o 1 3 0 2998.80 2891.31 79.03 o 3 3 0 8331.24 6807.43 152.66 o 5 3 0 5111.79 4726.37 75.53 o 7 3 0 62.03 91.66 15.29 o 9 3 0 75.09 65.61 17.07 o 11 3 0 26.86 19.59 16.66 o 13 3 0 45.41 41.50 20.05 o 15 3 0 60.40 39.50 23.68 o 17 3 0 0.26 -14.95 33.23 o 0 4 0 1377.15 1027.19 19.52 o 2 4 0 30823.13 27636.75 475.98 o 4 4 0 4576.00 3942.58 68.89 o 6 4 0 3582.54 3878.20 101.28 o 8 4 0 693.81 617.61 37.82 o 10 4 0 351.56 392.01 31.02 o 12 4 0 651.25 631.14 43.06 o 14 4 0 5.61 -11.96 19.86 o 16 4 0 3.49 13.34 36.98 o 18 4 0 0.05 -33.34 49.14 o 1 5 0 6786.15 6515.07 60.92 o 3 5 0 16398.94 16111.07 265.05 o 5 5 0 0.23 3.47 13.49 o 7 5 0 63.63 97.53 22.11 o 9 5 0 208.04 262.61 34.96 o 11 5 0 417.05 484.29 37.97 o 13 5 0 6.54 -12.43 20.04 o 15 5 0 7.28 -8.65 21.95 o 17 5 0 4.30 7.02 57.91 o 0 6 0 4154.24 3742.12 117.60 o 2 6 0 3362.77 3265.74 56.58 o 4 6 0 1599.32 1640.38 80.13 o 6 6 0 1448.65 1555.82 56.40 o 8 6 0 26.56 27.39 19.52 o 10 6 0 898.12 956.61 72.01 o 12 6 0 153.29 125.87 27.40 o 14 6 0 2.30 -9.04 21.49 o 16 6 0 44.30 3.51 47.38 o 1 7 0 1404.18 1405.22 35.40 o 3 7 0 495.41 423.24 40.47 o 5 7 0 0.23 -2.95 15.99 o 7 7 0 193.00 185.24 31.03 o 9 7 0 39.32 50.49 26.05 o 11 7 0 1624.10 1826.20 77.78 o 13 7 0 116.38 118.57 31.38 o 15 7 0 3.87 14.68 31.05 o 17 7 0 0.10 3.51 56.16 o 0 8 0 1286.64 1443.96 58.83 o 2 8 0 23.70 60.26 15.53 o 4 8 0 16546.48 16593.07 181.25 o 6 8 0 23.66 80.43 23.26 o 8 8 0 37.41 17.29 22.86 o 10 8 0 45.62 45.11 28.96 o 12 8 0 81.45 64.02 24.92 o 14 8 0 18.12 10.99 25.39 o 16 8 0 0.43 -17.55 56.16 o 1 9 0 2596.60 2150.58 49.58 o 3 9 0 190.95 213.66 27.95 o 5 9 0 2753.59 2518.43 77.62 o 7 9 0 33.40 39.40 23.63 o 9 9 0 197.34 258.00 58.74 o 11 9 0 285.21 389.45 52.54 o 13 9 0 21.42 18.18 25.88 o 15 9 0 7.69 17.88 45.46 o 17 9 0 0.03 -29.83 66.69 o 0 10 0 657.71 688.26 40.24 o 2 10 0 664.90 541.70 35.08 o 4 10 0 2.54 -12.99 17.48 o 6 10 0 361.40 482.18 67.32 o 8 10 0 215.98 171.09 37.77 o 10 10 0 335.86 429.75 53.24 o 12 10 0 1.09 -6.51 32.86 o 14 10 0 4.09 -10.19 36.45 o 16 10 0 11.39 -12.28 66.69 o 1 11 0 1066.66 1107.12 40.32 o 3 11 0 173.08 161.67 25.83 o 5 11 0 34.85 19.58 22.67 o 7 11 0 11.50 25.68 25.96 o 9 11 0 49.90 70.20 41.78 o 11 11 0 5.07 4.35 32.97 o 13 11 0 12.28 10.32 39.79 o 15 11 0 10.09 32.47 57.08 o 0 12 0 72.36 110.70 30.64 o 2 12 0 4.58 -2.63 13.04 o 4 12 0 65.49 32.38 22.78 o 6 12 0 400.28 374.52 46.59 o 8 12 0 1289.18 1382.78 74.80 o 10 12 0 115.84 155.41 42.27 o 12 12 0 8.61 -1.51 36.69 o 14 12 0 21.73 55.22 52.97 o 1 13 0 2.72 3.57 16.01 o 3 13 0 114.80 77.07 23.69 o 5 13 0 353.37 421.80 48.85 o 7 13 0 387.18 496.15 55.09 o 9 13 0 51.01 33.89 36.69 o 11 13 0 130.23 110.96 44.64 o 13 13 0 138.79 199.32 69.32 o 15 13 0 4.00 24.06 62.01 o 0 14 0 680.36 725.84 81.25 o 2 14 0 1764.98 1656.89 57.49 o 4 14 0 8.13 -8.01 23.92 o 6 14 0 93.76 126.25 37.56 o 8 14 0 376.24 413.68 56.86 o 10 14 0 63.37 65.14 45.03 o 12 14 0 30.84 43.73 61.42 o 14 14 0 9.82 21.94 58.32 o 1 15 0 1868.98 1795.81 62.39 o 3 15 0 287.86 294.43 35.42 o 5 15 0 30.72 -2.58 28.77 o 7 15 0 170.65 86.13 41.89 o 9 15 0 199.17 245.76 52.73 o 11 15 0 9.78 -13.29 50.70 o 13 15 0 43.58 44.78 66.87 o 0 16 0 1403.14 1427.88 277.29 o 2 16 0 593.12 644.89 47.98 o 4 16 0 284.75 299.37 42.86 o 6 16 0 58.02 24.68 34.90 o 8 16 0 39.34 27.32 40.34 o 10 16 0 191.06 214.15 73.04 o 12 16 0 69.22 127.07 68.20 o 1 17 0 363.89 329.14 39.44 o 3 17 0 0.72 -4.75 28.43 o 5 17 0 7.34 -11.86 28.95 o 7 17 0 0.00 13.06 40.75 o 9 17 0 9.20 -5.09 40.76 o 11 17 0 7.23 -10.58 60.18 o 0 18 0 13.45 -17.67 35.92 o 2 18 0 81.41 88.80 31.22 o 4 18 0 4.07 3.80 31.51 o 6 18 0 12.03 28.42 31.60 o 8 18 0 36.00 -3.43 44.46 o 10 18 0 0.03 7.82 66.15 o 1 19 0 31.04 21.33 31.62 o 3 19 0 2.08 -10.21 33.60 o 5 19 0 19.81 32.08 38.04 o 7 19 0 5.58 -11.45 40.78 o 9 19 0 8.65 45.73 61.52 o 0 20 0 16.69 48.21 50.96 o 2 20 0 34.97 25.09 43.05 o 4 20 0 71.73 103.79 45.11 o 6 20 0 5.82 -27.85 40.47 o 8 20 0 0.15 4.21 63.55 o 1 21 0 9.24 -7.05 36.56 o 3 21 0 4.50 44.89 49.23 o 5 21 0 14.77 -13.34 44.90 o 7 21 0 6.35 -24.97 59.41 o 0 22 0 0.44 -38.12 86.87 o 2 22 0 65.16 47.28 52.52 o 4 22 0 22.73 19.31 54.61 o -17 1 1 32.17 26.69 23.44 o -15 1 1 56.09 51.34 21.85 o -13 1 1 88.74 58.46 20.27 o -11 1 1 32.55 24.74 15.05 o -9 1 1 0.59 -8.91 10.19 o -7 1 1 3728.47 3845.81 74.66 o -5 1 1 1098.74 1111.79 29.13 o 1 1 1 3468.47 2298.09 25.53 o 3 1 1 79686.82 83118.25 805.24 o 5 1 1 1448.05 1370.02 35.68 o 7 1 1 1087.46 1063.66 35.86 o 9 1 1 274.47 268.66 27.61 o 11 1 1 1.52 -7.14 15.76 o 13 1 1 0.05 -6.53 18.33 o 15 1 1 39.42 15.98 35.35 o 17 1 1 0.74 2.60 33.44 o -18 2 1 10.62 -15.79 47.38 o -16 2 1 61.14 63.96 24.64 o -14 2 1 2.51 -17.54 17.54 o -12 2 1 8.53 -4.75 15.35 o -10 2 1 309.99 354.71 28.37 o -8 2 1 618.22 619.11 27.98 o -6 2 1 306.95 297.22 20.14 o -4 2 1 7780.78 9432.57 134.53 o 2 2 1 3688.40 2903.06 47.18 o 4 2 1 863.29 964.38 34.53 o 6 2 1 4088.26 4111.31 130.45 o 8 2 1 533.00 538.32 28.82 o 10 2 1 213.31 219.38 25.83 o 12 2 1 32.93 18.58 18.85 o 14 2 1 53.85 43.35 33.44 o 16 2 1 20.56 8.48 35.70 o -19 3 1 22.39 -26.32 45.63 o -17 3 1 0.60 1.38 26.43 o -15 3 1 3.37 4.09 20.37 o -13 3 1 145.02 156.08 24.58 o -11 3 1 414.28 441.38 42.30 o -9 3 1 140.03 102.45 25.49 o -7 3 1 4846.26 5399.05 105.66 o -5 3 1 287.89 399.32 22.57 o -3 3 1 43143.04 40318.60 218.86 o -1 3 1 23984.42 18299.23 136.02 o 1 3 1 48423.99 44828.66 443.44 o 3 3 1 2808.09 3107.84 57.92 o 5 3 1 986.23 1009.84 39.49 o 7 3 1 2067.70 1843.02 50.32 o 9 3 1 19.27 25.40 15.68 o 11 3 1 44.30 18.46 17.73 o 13 3 1 82.02 68.46 22.29 o 15 3 1 5.83 11.70 33.44 o 17 3 1 1.56 7.76 35.22 o -18 4 1 0.49 -1.75 49.14 o -16 4 1 139.16 158.96 30.90 o -14 4 1 160.08 98.40 22.80 o -12 4 1 144.00 149.99 24.77 o -10 4 1 537.11 524.15 30.58 o -8 4 1 1983.06 1920.44 59.37 o -6 4 1 14.93 33.13 14.42 o -4 4 1 1542.73 1785.80 43.51 o -2 4 1 1896.26 2270.57 33.66 o 0 4 1 8.08 25.04 7.35 o 2 4 1 11402.37 10315.32 221.40 o 4 4 1 77.85 33.47 13.49 o 6 4 1 514.47 500.29 33.06 o 8 4 1 174.18 166.57 21.54 o 10 4 1 124.49 87.48 21.27 o 12 4 1 60.24 50.47 20.15 o 14 4 1 0.80 -15.97 29.93 o 16 4 1 26.21 24.46 38.72 o -17 5 1 44.85 9.74 41.56 o -15 5 1 13.83 9.00 20.40 o -13 5 1 8.09 6.10 21.16 o -11 5 1 44.40 35.98 17.39 o -9 5 1 508.80 616.36 40.43 o -7 5 1 1751.08 1680.12 54.77 o -5 5 1 21.45 4.64 12.64 o -3 5 1 11145.24 11478.47 112.96 o -1 5 1 372.10 418.37 14.78 o 1 5 1 21658.96 18015.69 291.59 o 3 5 1 6180.10 6841.60 219.82 o 5 5 1 763.24 912.14 40.43 o 7 5 1 128.36 133.95 25.29 o 9 5 1 225.72 237.82 26.28 o 11 5 1 5.09 -4.58 18.34 o 13 5 1 38.67 25.87 21.33 o 15 5 1 48.02 46.93 40.20 o 17 5 1 4.50 -15.79 49.14 o -18 6 1 2.29 -14.04 59.67 o -16 6 1 0.16 -16.87 24.16 o -14 6 1 398.11 448.27 45.34 o -12 6 1 1665.39 1471.23 121.59 o -10 6 1 0.18 5.51 20.37 o -8 6 1 44.71 36.65 20.92 o -6 6 1 752.39 890.75 48.63 o -4 6 1 1386.66 1505.60 46.26 o -2 6 1 612.32 825.00 21.37 o 0 6 1 417.46 524.43 20.32 o 2 6 1 7594.69 8187.56 93.19 o 4 6 1 1730.62 1667.32 53.32 o 6 6 1 1560.06 1754.70 79.36 o 8 6 1 1674.79 1741.27 68.59 o 10 6 1 247.31 207.95 27.36 o 12 6 1 77.05 55.41 22.95 o 14 6 1 89.58 113.38 45.18 o 16 6 1 17.07 14.86 39.48 o -17 7 1 3.19 -27.12 38.28 o -15 7 1 0.09 -0.98 29.30 o -13 7 1 820.51 784.65 74.73 o -11 7 1 668.11 861.77 59.99 o -9 7 1 23.18 22.78 22.53 o -7 7 1 413.43 449.66 40.13 o -5 7 1 16706.17 16941.31 211.92 o -3 7 1 536.40 475.77 21.60 o -1 7 1 3250.51 3478.30 41.88 o 1 7 1 12726.21 11841.67 122.41 o 3 7 1 1496.80 1490.51 51.33 o 5 7 1 2319.55 2561.19 73.26 o 7 7 1 2356.75 2418.84 76.31 o 9 7 1 1222.21 1296.75 64.13 o 11 7 1 694.12 760.66 46.69 o 13 7 1 34.40 14.57 22.15 o 15 7 1 18.78 -10.88 36.98 o -18 8 1 43.12 49.14 61.42 o -16 8 1 0.32 -4.07 31.13 o -14 8 1 372.95 407.72 43.08 o -12 8 1 1410.99 1645.87 85.28 o -10 8 1 109.03 128.89 33.06 o -8 8 1 10.46 3.31 20.12 o -6 8 1 82.67 61.46 21.23 o -4 8 1 4689.19 5313.93 69.60 o -2 8 1 667.34 703.85 21.15 o 0 8 1 73.39 111.66 14.57 o 2 8 1 7323.97 7441.24 165.62 o 4 8 1 8697.66 9138.69 138.41 o 6 8 1 2021.24 2039.32 75.25 o 8 8 1 297.61 332.31 63.02 o 10 8 1 1126.83 1120.28 64.10 o 12 8 1 60.86 60.46 28.59 o 14 8 1 8.55 -14.31 39.56 o 16 8 1 5.75 -19.30 56.16 o -17 9 1 4.38 -27.88 48.88 o -15 9 1 45.17 11.89 33.30 o -13 9 1 160.36 210.13 58.43 o -11 9 1 1560.62 1758.46 84.38 o -9 9 1 92.56 63.91 28.63 o -7 9 1 196.20 169.25 31.74 o -5 9 1 5399.37 5558.49 109.42 o -3 9 1 378.11 391.82 22.39 o -1 9 1 1899.91 1876.57 35.39 o 1 9 1 1354.68 1194.28 49.39 o 3 9 1 2.27 5.23 16.74 o 5 9 1 576.26 663.05 47.74 o 7 9 1 621.01 627.63 52.70 o 9 9 1 264.90 347.53 46.94 o 11 9 1 184.60 216.40 44.54 o 13 9 1 75.42 84.28 38.37 o 15 9 1 1.58 10.53 63.18 o -16 10 1 28.98 35.60 37.03 o -14 10 1 2.14 5.79 30.66 o -12 10 1 28.00 36.91 33.34 o -10 10 1 9.03 9.44 29.82 o -8 10 1 0.75 2.53 22.86 o -6 10 1 366.00 358.25 39.60 o -4 10 1 1.74 1.55 12.03 o -2 10 1 91.48 65.73 12.26 o 0 10 1 322.15 353.98 30.67 o 2 10 1 504.21 533.28 35.46 o 4 10 1 146.98 195.92 31.38 o 6 10 1 103.63 82.79 28.93 o 8 10 1 0.21 3.18 27.51 o 10 10 1 51.31 44.92 34.78 o 12 10 1 2.76 -15.00 35.52 o 14 10 1 31.37 13.97 48.21 o -17 11 1 63.94 146.23 65.46 o -15 11 1 14.88 35.61 43.20 o -13 11 1 10.31 -12.31 41.56 o -11 11 1 214.38 312.48 55.45 o -9 11 1 494.90 584.30 58.70 o -7 11 1 133.26 191.33 36.36 o -5 11 1 475.51 518.71 46.68 o -3 11 1 172.00 173.73 16.85 o -1 11 1 66.71 58.07 14.87 o 1 11 1 22.12 17.31 15.96 o 3 11 1 200.57 215.95 33.09 o 5 11 1 559.84 615.82 53.32 o 7 11 1 295.25 325.63 46.52 o 9 11 1 11.94 -2.80 28.02 o 11 11 1 30.60 44.89 39.19 o 13 11 1 18.15 22.54 37.83 o 15 11 1 19.63 15.79 82.48 o -16 12 1 10.90 9.57 44.51 o -14 12 1 13.56 -15.21 57.91 o -12 12 1 2.41 -22.12 44.67 o -10 12 1 26.36 37.92 34.60 o -8 12 1 34.75 84.37 35.34 o -6 12 1 0.52 -21.51 21.51 o -4 12 1 751.85 760.90 51.55 o -2 12 1 349.85 320.38 26.13 o 0 12 1 1.51 -10.00 15.17 o 2 12 1 38.33 24.67 18.48 o 4 12 1 0.01 -11.73 20.37 o 6 12 1 41.67 26.00 29.98 o 8 12 1 6.41 12.70 32.07 o 10 12 1 23.75 11.61 35.83 o 12 12 1 34.99 26.36 39.74 o 14 12 1 0.01 -28.08 73.71 o -15 13 1 2.07 9.65 58.32 o -13 13 1 43.81 46.83 54.43 o -11 13 1 50.21 89.26 43.88 o -9 13 1 78.66 83.92 38.10 o -7 13 1 64.80 127.58 37.46 o -5 13 1 861.73 816.81 55.03 o -3 13 1 249.82 287.57 29.57 o -1 13 1 444.97 498.15 37.12 o 1 13 1 322.29 348.22 29.75 o 3 13 1 2.38 -3.63 19.89 o 5 13 1 125.30 61.93 29.94 o 7 13 1 5.37 -14.93 29.35 o 9 13 1 2.66 -2.54 34.60 o 11 13 1 291.45 486.50 66.10 o 13 13 1 20.73 -5.38 54.96 o -14 14 1 16.89 -32.99 54.56 o -12 14 1 37.40 26.41 51.94 o -10 14 1 0.16 -8.94 36.58 o -8 14 1 613.35 735.00 69.24 o -6 14 1 2.53 16.40 29.92 o -4 14 1 3.59 9.90 23.00 o -2 14 1 1149.87 1083.46 46.68 o 0 14 1 1140.66 882.57 43.27 o 2 14 1 1.29 -14.62 18.57 o 4 14 1 114.73 143.35 36.68 o 6 14 1 307.85 264.80 47.14 o 8 14 1 1.52 -0.33 35.05 o 10 14 1 120.29 148.58 54.74 o 12 14 1 103.85 107.72 60.24 o -13 15 1 9.78 -20.38 58.86 o -11 15 1 97.99 129.03 61.13 o -9 15 1 59.55 43.10 37.77 o -7 15 1 597.70 718.34 69.02 o -5 15 1 315.45 257.92 39.75 o -3 15 1 33.88 13.06 21.39 o -1 15 1 722.44 823.07 52.05 o 1 15 1 25.65 -10.91 20.83 o 3 15 1 1.00 -10.32 26.30 o 5 15 1 71.80 41.50 32.01 o 7 15 1 614.65 563.13 65.05 o 9 15 1 0.09 -7.59 38.68 o 11 15 1 4.35 29.34 45.15 o 13 15 1 19.85 13.52 62.96 o -14 16 1 1.13 -38.61 96.52 o -12 16 1 3.14 46.38 63.18 o -10 16 1 93.93 104.75 56.72 o -8 16 1 161.00 164.00 45.74 o -6 16 1 109.16 96.68 34.17 o -4 16 1 7.32 -24.90 24.90 o -2 16 1 11.32 -3.16 24.26 o 0 16 1 333.60 342.57 38.49 o 2 16 1 193.34 207.75 32.54 o 4 16 1 128.16 158.49 41.15 o 6 16 1 214.52 248.48 50.07 o 8 16 1 49.92 4.33 39.92 o 10 16 1 25.72 -4.21 45.97 o 12 16 1 2.76 -42.05 58.95 o -13 17 1 25.58 22.35 67.42 o -11 17 1 34.67 29.99 61.34 o -9 17 1 182.00 221.52 69.19 o -7 17 1 29.08 30.09 29.33 o -5 17 1 40.83 8.38 28.44 o -3 17 1 6.17 -7.08 27.38 o -1 17 1 214.98 185.31 36.01 o 1 17 1 214.81 211.88 32.99 o 3 17 1 6.44 -18.37 29.18 o 5 17 1 3.86 17.65 36.78 o 7 17 1 13.13 63.66 43.90 o 9 17 1 2.86 -5.15 46.47 o 11 17 1 5.82 19.82 62.96 o -12 18 1 0.10 -47.50 75.42 o 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