#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/23/2202352.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202352_Fobs loop_ _publ_author_name 'Clegg, William' 'Horsburgh, Lynne' _publ_section_title ; trans-(6-Amino-2-pyridinio)iodobis(triphenylphosphine)palladium(II) iodide ethyl acetate solvate ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m700 _journal_page_last m702 _journal_volume 59 _journal_year 2003 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.0297 _cell_length_b 16.9603 _cell_length_c 17.2897 _exptl_crystal_F_000 2104.00 _reflns_d_resolution_high 0.7378 _[local]_cod_data_source_file bt6322Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' rfwj73 in Cmc2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 749.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, z+1/2' '-x, y, z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 0 -22 7282.25 8365.48 610.28 o 2 0 -22 2093.67 2795.30 305.36 o 4 0 -22 1703.70 2483.54 304.01 o 1 1 -22 2750.10 3074.62 368.49 o 3 1 -22 3121.41 3147.00 234.88 o 5 1 -22 2357.05 2643.35 221.23 o 0 2 -22 6285.45 6563.08 543.04 o 2 2 -22 2622.53 2813.88 283.35 o 4 2 -22 1393.33 1431.80 256.51 o 1 3 -22 1419.29 1517.13 165.30 o 3 3 -22 420.19 391.25 160.19 o 0 4 -22 3443.32 4093.52 460.30 o 2 4 -22 3048.79 3324.77 246.07 o 1 1 -21 1064.09 1134.70 151.93 o 3 1 -21 300.04 389.36 155.56 o 5 1 -21 573.34 745.04 155.23 o 7 1 -21 1271.41 1185.92 134.21 o 9 1 -21 35.33 155.16 160.33 o 0 2 -21 2479.58 3149.66 439.61 o 2 2 -21 5240.01 5614.92 342.00 o 4 2 -21 1129.80 1119.96 155.91 o 6 2 -21 4935.86 5288.13 246.55 o 8 2 -21 2014.81 1686.91 221.48 o 1 3 -21 14741.33 16687.29 518.02 o 3 3 -21 6057.85 7124.91 326.75 o 5 3 -21 11966.06 13068.30 450.24 o 7 3 -21 12509.39 14248.29 473.70 o 0 4 -21 1653.94 1858.15 331.00 o 2 4 -21 909.21 1081.58 135.44 o 4 4 -21 999.30 808.29 126.16 o 6 4 -21 1924.33 2215.31 182.56 o 1 5 -21 756.31 874.41 123.27 o 3 5 -21 234.26 317.36 107.42 o 5 5 -21 893.09 716.43 131.37 o 0 6 -21 1917.18 2229.31 271.55 o 2 6 -21 0.95 114.31 150.36 o 4 6 -21 68.86 61.29 110.34 o 6 6 -21 936.05 1135.22 382.72 o 1 7 -21 1356.03 1423.91 147.97 o 3 7 -21 1405.95 1696.37 336.17 o 5 7 -21 1567.42 2146.32 369.79 o 0 0 -20 5008.81 5513.20 473.22 o 2 0 -20 2370.11 2471.43 223.72 o 4 0 -20 8435.69 9104.11 411.41 o 6 0 -20 2356.38 2346.53 242.09 o 8 0 -20 4404.50 5097.15 227.51 o 1 1 -20 2553.72 2445.33 163.63 o 3 1 -20 585.92 574.11 119.03 o 5 1 -20 2388.41 2411.13 157.61 o 7 1 -20 1556.38 1433.98 127.93 o 9 1 -20 597.91 448.60 150.38 o 0 2 -20 12291.86 13745.29 515.68 o 2 2 -20 4038.60 4270.85 242.63 o 4 2 -20 3431.10 3902.87 225.28 o 6 2 -20 8379.89 9171.27 422.18 o 8 2 -20 5490.95 5691.04 214.30 o 1 3 -20 2915.56 3495.77 266.66 o 3 3 -20 737.79 683.97 133.74 o 5 3 -20 2238.69 2554.67 201.75 o 7 3 -20 2933.91 3285.12 189.14 o 9 3 -20 237.96 108.61 181.01 o 0 4 -20 20740.68 21711.18 1409.33 o 2 4 -20 4706.67 4842.00 226.66 o 4 4 -20 8264.95 8735.98 308.40 o 6 4 -20 9446.54 10153.31 324.11 o 8 4 -20 7603.69 8152.48 291.29 o 10 4 -20 3460.17 3255.68 372.37 o 1 5 -20 256.70 248.14 112.35 o 3 5 -20 291.17 248.67 98.08 o 5 5 -20 1015.60 971.51 133.18 o 7 5 -20 1077.14 1218.58 127.79 o 9 5 -20 1148.74 874.04 222.39 o 0 6 -20 1661.70 2156.24 244.51 o 2 6 -20 4902.80 5831.34 254.45 o 4 6 -20 5652.87 6685.39 275.47 o 6 6 -20 996.08 1054.87 121.75 o 8 6 -20 4043.11 4230.58 460.30 o 1 7 -20 5127.49 5296.66 245.53 o 3 7 -20 1335.82 1321.45 140.15 o 5 7 -20 3333.10 3126.16 195.36 o 7 7 -20 5756.41 5164.10 514.60 o 0 8 -20 222.00 131.62 209.46 o 2 8 -20 431.32 450.99 110.04 o 4 8 -20 77.96 61.05 93.52 o 6 8 -20 125.05 139.64 268.94 o 1 9 -20 10624.24 10629.36 360.34 o 3 9 -20 2276.69 2241.73 180.95 o 5 9 -20 9757.45 9904.10 749.92 o 0 10 -20 359.83 806.81 256.01 o 2 10 -20 3798.80 4499.51 504.26 o 1 1 -19 8538.72 9120.34 275.04 o 3 1 -19 3263.46 3715.29 183.13 o 5 1 -19 6685.96 7474.52 258.67 o 7 1 -19 8149.84 8470.32 207.36 o 9 1 -19 2470.38 2720.25 154.68 o 0 2 -19 1260.57 1249.65 169.94 o 2 2 -19 1770.03 1645.20 133.48 o 4 2 -19 1232.04 1063.23 116.81 o 6 2 -19 1440.77 1183.08 108.76 o 8 2 -19 1382.42 1297.68 115.51 o 10 2 -19 134.97 117.18 92.95 o 1 3 -19 16280.11 18201.96 620.69 o 3 3 -19 5305.70 6184.63 235.14 o 5 3 -19 12041.74 12802.31 317.97 o 7 3 -19 12800.01 13921.73 336.41 o 9 3 -19 4483.04 4902.31 196.28 o 0 4 -19 2513.84 2659.02 263.76 o 2 4 -19 1463.55 1562.80 139.95 o 4 4 -19 650.11 614.52 104.40 o 6 4 -19 3679.06 3855.35 175.87 o 8 4 -19 776.73 963.41 124.10 o 10 4 -19 555.14 442.67 110.36 o 1 5 -19 3386.56 3581.99 196.73 o 3 5 -19 1447.33 1511.87 140.58 o 5 5 -19 2473.89 2524.69 145.79 o 7 5 -19 2540.83 2379.39 157.32 o 9 5 -19 1432.53 1587.00 142.58 o 0 6 -19 7460.78 7718.00 398.25 o 2 6 -19 1962.56 2299.34 167.94 o 4 6 -19 2403.32 2483.29 192.45 o 6 6 -19 4584.66 4811.06 197.08 o 8 6 -19 2996.99 3156.41 182.91 o 10 6 -19 1080.75 1378.30 271.52 o 1 7 -19 3047.98 3427.60 197.79 o 3 7 -19 3581.01 4031.77 207.72 o 5 7 -19 1798.82 1992.68 137.63 o 7 7 -19 3733.10 4007.46 197.08 o 9 7 -19 1262.12 1210.21 243.08 o 0 8 -19 9764.66 9406.42 450.83 o 2 8 -19 1306.70 1260.02 131.64 o 4 8 -19 1246.70 1106.03 126.68 o 6 8 -19 5869.14 5767.57 220.44 o 8 8 -19 2468.65 2185.11 318.07 o 1 9 -19 3037.52 3392.58 203.46 o 3 9 -19 2973.65 3455.14 200.63 o 5 9 -19 3081.70 3348.20 197.02 o 7 9 -19 1955.53 2275.62 336.17 o 0 10 -19 7639.98 8546.94 439.83 o 2 10 -19 1544.92 1750.76 152.52 o 4 10 -19 1529.29 1632.06 146.79 o 1 11 -19 268.18 298.76 94.96 o 3 11 -19 165.98 84.17 89.12 o 5 11 -19 335.42 718.89 307.73 o 0 0 -18 29229.68 31238.01 1233.49 o 2 0 -18 19966.29 22459.17 686.39 o 4 0 -18 19055.83 21211.07 663.27 o 6 0 -18 18279.13 19536.05 554.19 o 8 0 -18 19098.25 20681.46 547.06 o 10 0 -18 6505.15 7377.65 517.19 o 1 1 -18 787.65 1021.56 110.16 o 3 1 -18 746.18 947.29 105.50 o 5 1 -18 767.61 1055.17 122.60 o 7 1 -18 389.56 506.32 75.82 o 9 1 -18 676.08 873.31 87.65 o 11 1 -18 275.92 381.34 163.47 o 0 2 -18 6476.25 8124.45 351.90 o 2 2 -18 369.66 469.14 94.28 o 4 2 -18 179.38 265.32 87.60 o 6 2 -18 3808.13 4394.07 140.25 o 8 2 -18 1341.15 1422.58 110.71 o 10 2 -18 41.94 -49.66 92.66 o 12 2 -18 2616.94 2573.00 362.03 o 1 3 -18 403.64 295.27 90.33 o 3 3 -18 573.67 552.54 97.13 o 5 3 -18 229.27 275.43 72.55 o 7 3 -18 1850.94 1832.78 119.78 o 9 3 -18 19.43 46.22 75.15 o 11 3 -18 139.98 263.95 151.52 o 0 4 -18 2231.45 2842.48 359.44 o 2 4 -18 1279.56 1302.00 126.55 o 4 4 -18 1756.80 1729.15 157.70 o 6 4 -18 3635.38 3781.53 146.30 o 8 4 -18 786.44 736.46 124.44 o 10 4 -18 239.25 252.92 105.08 o 12 4 -18 1095.98 1280.03 362.03 o 1 5 -18 9723.62 10554.76 324.42 o 3 5 -18 5880.59 6725.95 251.62 o 5 5 -18 3885.53 4316.49 177.35 o 7 5 -18 14018.13 14727.87 356.11 o 9 5 -18 2515.60 2842.47 167.92 o 0 6 -18 13019.88 13960.16 549.68 o 2 6 -18 11337.35 12041.04 356.49 o 4 6 -18 7166.48 7442.65 272.96 o 6 6 -18 13188.58 13057.25 349.71 o 8 6 -18 6170.02 6447.24 251.43 o 10 6 -18 6091.98 5643.44 338.04 o 1 7 -18 4623.66 4587.82 214.91 o 3 7 -18 2129.85 2493.96 160.57 o 5 7 -18 2020.30 1921.81 127.68 o 7 7 -18 6292.22 6367.58 245.79 o 9 7 -18 1021.23 1143.24 108.82 o 0 8 -18 214.84 365.68 123.70 o 2 8 -18 443.22 434.62 92.87 o 4 8 -18 173.00 76.38 91.68 o 6 8 -18 288.58 285.22 80.88 o 8 8 -18 170.02 214.77 78.15 o 10 8 -18 288.89 380.88 312.90 o 1 9 -18 1837.69 1830.83 151.77 o 3 9 -18 354.34 332.99 97.74 o 5 9 -18 1536.42 1365.95 116.27 o 7 9 -18 1364.49 1127.83 112.76 o 9 9 -18 99.16 107.60 132.14 o 0 10 -18 4544.56 4789.02 307.80 o 2 10 -18 2470.56 2678.97 169.56 o 4 10 -18 2857.69 2879.61 176.79 o 6 10 -18 2847.03 2722.65 170.32 o 8 10 -18 2082.36 1967.89 343.93 o 1 11 -18 8554.59 8238.98 320.99 o 3 11 -18 2059.39 2111.04 161.79 o 5 11 -18 8591.74 8263.19 304.99 o 0 12 -18 2536.83 3295.78 329.71 o 2 12 -18 754.41 921.99 127.04 o 4 12 -18 764.22 970.18 125.87 o 1 13 -18 4693.84 4632.08 225.22 o 3 13 -18 826.06 838.43 185.02 o 5 13 -18 4989.68 5756.27 566.32 o 1 1 -17 16189.02 16999.00 387.24 o 3 1 -17 11024.79 11822.78 305.73 o 5 1 -17 8778.44 9319.99 214.95 o 7 1 -17 18973.69 19632.53 361.37 o 9 1 -17 5088.83 5399.69 250.76 o 11 1 -17 5011.19 5070.99 457.71 o 13 1 -17 11424.04 11062.60 698.20 o 0 2 -17 12258.99 12923.92 453.43 o 2 2 -17 2109.15 2050.72 128.34 o 4 2 -17 11772.26 12040.09 280.06 o 6 2 -17 2998.80 3343.10 119.10 o 8 2 -17 3166.07 3407.64 124.94 o 10 2 -17 5675.03 5768.48 267.53 o 12 2 -17 1925.93 2053.79 237.69 o 1 3 -17 265.96 203.21 77.74 o 3 3 -17 4768.57 4893.66 186.77 o 5 3 -17 759.29 628.85 64.79 o 7 3 -17 142.54 103.09 65.31 o 9 3 -17 2684.48 2725.99 185.62 o 11 3 -17 496.05 238.62 305.14 o 0 4 -17 8542.58 9314.86 316.41 o 2 4 -17 4815.49 5200.07 197.94 o 4 4 -17 2072.31 2389.47 123.50 o 6 4 -17 8805.78 9358.28 231.96 o 8 4 -17 3037.90 3330.02 152.40 o 10 4 -17 978.97 1064.50 134.53 o 12 4 -17 4458.71 5088.33 355.57 o 1 5 -17 8784.40 9334.94 294.31 o 3 5 -17 627.99 654.30 100.08 o 5 5 -17 8651.99 8762.36 248.25 o 7 5 -17 4502.40 4733.16 179.24 o 9 5 -17 3391.45 3570.72 258.34 o 11 5 -17 2022.45 1975.65 292.21 o 0 6 -17 15668.20 16080.28 589.29 o 2 6 -17 6065.55 6636.86 246.89 o 4 6 -17 4391.67 4536.70 178.94 o 6 6 -17 10809.06 11046.32 291.62 o 8 6 -17 7812.93 7718.66 268.34 o 10 6 -17 1421.56 1396.23 178.75 o 1 7 -17 7742.29 8243.45 279.57 o 3 7 -17 2322.10 2475.93 158.61 o 5 7 -17 8259.76 7907.71 241.65 o 7 7 -17 3230.48 3470.69 176.66 o 9 7 -17 3386.51 3446.62 207.97 o 0 8 -17 7096.78 7035.06 361.16 o 2 8 -17 4313.74 4584.38 205.85 o 4 8 -17 5215.09 4973.67 189.78 o 6 8 -17 3294.96 3219.84 152.50 o 8 8 -17 5973.83 5702.60 232.54 o 10 8 -17 2081.31 2069.50 171.24 o 1 9 -17 3573.32 3650.53 192.49 o 3 9 -17 4201.13 4462.44 208.50 o 5 9 -17 2704.89 2574.70 141.98 o 7 9 -17 2803.18 2820.24 161.58 o 9 9 -17 3189.17 3169.16 160.51 o 11 9 -17 1333.46 1246.42 240.49 o 0 10 -17 9828.85 9915.76 444.23 o 2 10 -17 413.37 473.51 92.31 o 4 10 -17 629.49 568.85 101.48 o 6 10 -17 6232.64 5976.17 210.09 o 8 10 -17 635.64 609.43 96.59 o 10 10 -17 951.45 1073.16 235.32 o 1 11 -17 1589.39 1765.74 143.12 o 3 11 -17 307.96 411.79 97.73 o 5 11 -17 1719.22 1595.01 121.06 o 7 11 -17 694.32 729.42 93.78 o 9 11 -17 611.41 638.72 232.73 o 0 12 -17 17864.43 17557.50 1079.62 o 2 12 -17 3854.47 4028.15 208.12 o 4 12 -17 3723.76 3817.83 285.53 o 6 12 -17 14237.40 12582.04 367.50 o 1 13 -17 287.87 330.98 95.60 o 3 13 -17 1084.11 954.17 128.76 o 5 13 -17 352.92 335.25 104.62 o 0 14 -17 1343.01 1501.15 208.73 o 2 14 -17 1716.80 1792.90 157.87 o 4 14 -17 605.21 686.53 141.93 o 1 15 -17 6495.94 5485.04 320.59 o 0 0 -16 33148.28 34847.96 1311.07 o 2 0 -16 16951.74 16904.41 529.36 o 4 0 -16 9550.05 9530.81 297.72 o 6 0 -16 25086.02 25503.94 672.54 o 8 0 -16 17423.42 17563.62 817.15 o 10 0 -16 4189.76 4359.99 271.53 o 12 0 -16 12417.36 11753.04 667.17 o 1 1 -16 9141.98 9371.92 252.82 o 3 1 -16 21003.21 22378.41 466.29 o 5 1 -16 5036.93 5449.29 153.32 o 7 1 -16 11352.01 12109.99 254.09 o 9 1 -16 7432.35 8001.90 302.66 o 11 1 -16 4308.53 4736.21 292.14 o 13 1 -16 4958.93 5168.25 321.82 o 0 2 -16 6817.08 7359.27 310.85 o 2 2 -16 1061.26 1141.86 101.75 o 4 2 -16 1692.80 2032.50 99.87 o 6 2 -16 3899.45 4247.68 129.18 o 8 2 -16 2690.47 2803.31 177.67 o 10 2 -16 864.13 693.70 139.74 o 12 2 -16 2587.15 2699.52 243.98 o 1 3 -16 1534.14 1820.21 112.45 o 3 3 -16 2951.55 3352.21 132.50 o 5 3 -16 807.46 957.23 70.89 o 7 3 -16 5282.84 5375.31 148.11 o 9 3 -16 958.27 1035.04 129.87 o 11 3 -16 553.43 751.80 150.94 o 13 3 -16 2190.78 2160.47 224.91 o 0 4 -16 5967.88 6004.20 271.27 o 2 4 -16 4956.75 5091.94 166.43 o 4 4 -16 2100.22 2141.81 115.25 o 6 4 -16 5338.10 5336.32 177.21 o 8 4 -16 4046.05 3860.96 205.56 o 10 4 -16 1006.02 1132.26 132.61 o 12 4 -16 2782.84 2708.60 232.20 o 1 5 -16 5399.98 5526.68 211.38 o 3 5 -16 11176.82 11010.28 277.08 o 5 5 -16 2951.92 3179.23 127.42 o 7 5 -16 8997.06 8835.10 220.65 o 9 5 -16 3873.09 3850.35 176.73 o 11 5 -16 2690.36 2822.28 229.47 o 13 5 -16 3532.70 3992.67 424.09 o 0 6 -16 8940.67 9084.44 398.48 o 2 6 -16 4091.15 4039.97 183.55 o 4 6 -16 2022.44 2190.41 124.73 o 6 6 -16 9850.57 9890.84 266.73 o 8 6 -16 1699.52 1624.91 192.38 o 10 6 -16 2742.58 2628.17 175.33 o 12 6 -16 2765.98 3108.28 359.44 o 1 7 -16 17121.80 17430.71 433.94 o 3 7 -16 7629.17 8186.72 236.20 o 5 7 -16 13689.64 13523.22 323.83 o 7 7 -16 13746.24 13740.47 330.10 o 9 7 -16 6320.00 6680.81 283.54 o 11 7 -16 5640.89 5763.75 275.67 o 0 8 -16 235.01 270.12 123.42 o 2 8 -16 2048.69 2204.47 142.04 o 4 8 -16 1194.26 1147.63 99.85 o 6 8 -16 744.15 900.58 91.90 o 8 8 -16 1025.41 1031.51 108.16 o 10 8 -16 675.12 861.30 127.71 o 12 8 -16 143.36 555.97 240.49 o 1 9 -16 8624.94 8433.22 281.86 o 3 9 -16 4350.74 4324.48 201.32 o 5 9 -16 7744.75 7042.94 221.20 o 7 9 -16 5154.38 4860.27 203.44 o 9 9 -16 2648.04 2568.67 189.14 o 11 9 -16 2814.49 2749.44 286.61 o 0 10 -16 510.70 471.38 122.35 o 2 10 -16 4579.69 4238.55 195.07 o 4 10 -16 429.88 361.92 76.30 o 6 10 -16 3272.89 2790.37 140.04 o 8 10 -16 828.77 799.87 104.11 o 10 10 -16 982.68 932.32 128.27 o 1 11 -16 5959.06 6200.23 242.50 o 3 11 -16 2840.63 3254.09 180.14 o 5 11 -16 3624.89 3674.80 165.71 o 7 11 -16 5267.53 5148.79 214.77 o 9 11 -16 1875.19 1863.77 123.43 o 11 11 -16 1225.98 1352.44 289.62 o 0 12 -16 423.45 282.45 120.90 o 2 12 -16 259.01 299.25 87.82 o 4 12 -16 266.36 229.34 84.78 o 6 12 -16 68.70 143.08 74.28 o 8 12 -16 56.65 142.32 77.52 o 1 13 -16 7863.25 7860.31 283.90 o 3 13 -16 2579.48 2444.13 164.21 o 5 13 -16 6092.21 5878.25 256.57 o 7 13 -16 6968.45 6103.42 268.74 o 0 14 -16 11467.37 10399.36 911.54 o 2 14 -16 5978.10 5973.85 261.65 o 4 14 -16 3450.88 3157.30 206.03 o 6 14 -16 8936.90 7527.45 321.86 o 1 15 -16 1761.88 1766.17 155.85 o 3 15 -16 2577.04 2427.07 195.92 o 5 15 -16 1053.49 941.00 173.72 o 0 16 -16 4559.91 4184.03 398.23 o 2 16 -16 1867.77 1600.26 213.35 o 4 16 -16 706.95 465.47 253.42 o 1 1 -15 8788.41 9503.59 249.86 o 3 1 -15 108.34 59.05 45.85 o 5 1 -15 4597.39 4974.29 141.87 o 7 1 -15 9052.24 9140.79 367.87 o 9 1 -15 794.83 674.86 139.56 o 11 1 -15 1067.71 1024.66 161.45 o 13 1 -15 6669.67 6334.99 351.82 o 0 2 -15 39501.82 40770.93 1037.37 o 2 2 -15 25579.05 27248.62 529.38 o 4 2 -15 17126.11 17676.98 312.42 o 6 2 -15 28503.07 29432.72 467.58 o 8 2 -15 14205.92 14532.58 421.49 o 10 2 -15 11585.06 11595.58 374.81 o 12 2 -15 9621.13 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14 10 949.20 883.85 161.63 o 6 14 10 4244.23 4106.98 275.40 o 8 14 10 2826.42 3073.91 318.07 o 10 14 10 166.24 232.89 108.23 o 12 14 10 4756.34 4861.54 418.92 o 1 15 10 11107.50 11138.62 510.95 o 3 15 10 3517.77 3736.65 374.96 o 5 15 10 8583.77 8358.22 426.72 o 7 15 10 7890.27 7887.62 424.09 o 9 15 10 2946.83 2971.51 242.26 o 11 15 10 4238.57 4304.48 292.52 o 0 16 10 8508.48 8562.01 636.14 o 2 16 10 4881.85 4762.10 332.78 o 4 16 10 2783.60 3240.20 280.64 o 6 16 10 9054.29 9448.41 932.23 o 8 16 10 4350.65 4078.74 268.21 o 10 16 10 763.80 612.29 187.48 o 1 17 10 358.17 343.52 143.32 o 3 17 10 233.62 170.17 112.66 o 5 17 10 879.22 720.48 222.39 o 7 17 10 350.36 170.67 183.60 o 9 17 10 159.95 -51.72 149.98 o 0 18 10 17433.26 16826.63 1013.68 o 2 18 10 4682.15 4709.34 344.06 o 4 18 10 4348.48 4308.00 328.75 o 6 18 10 12234.56 11163.45 796.47 o 1 19 10 5674.88 6032.50 405.14 o 3 19 10 3400.46 4078.72 610.28 o 5 19 10 4499.61 5427.86 553.39 o 5 1 11 34422.01 33913.19 853.92 o 7 1 11 26434.37 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11 7552.24 7320.76 491.33 o 13 9 11 5157.60 5619.22 449.95 o 0 10 11 22356.37 22394.13 1065.40 o 2 10 11 11881.07 11969.90 479.96 o 4 10 11 10965.52 10871.21 449.77 o 6 10 11 17096.77 16535.95 841.72 o 8 10 11 11982.07 11873.23 930.93 o 10 10 11 4141.98 4081.62 248.99 o 12 10 11 13470.11 13480.44 731.82 o 14 10 11 5183.75 5122.72 431.85 o 1 11 11 4626.79 4491.85 274.11 o 3 11 11 4003.21 3983.81 261.40 o 5 11 11 3312.41 3201.60 234.92 o 7 11 11 4534.52 4389.45 258.40 o 9 11 11 2308.59 2270.25 197.46 o 11 11 11 1408.98 1163.67 214.63 o 13 11 11 3760.35 3687.53 377.55 o 0 12 11 18677.33 19603.92 1003.34 o 2 12 11 5886.30 6175.50 335.35 o 4 12 11 6154.96 6885.51 358.54 o 6 12 11 11404.22 11709.45 380.24 o 8 12 11 6340.59 6611.98 336.29 o 10 12 11 2629.26 2860.58 229.33 o 12 12 11 6697.14 6984.59 488.74 o 1 13 11 3088.16 3357.77 257.51 o 3 13 11 1887.13 2223.82 204.97 o 5 13 11 3656.63 4055.39 277.02 o 7 13 11 2662.70 2629.56 210.20 o 9 13 11 1927.16 2212.74 206.92 o 11 13 11 1150.71 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7 13 1505.85 1523.11 250.83 o 6 8 13 18532.33 18830.72 837.84 o 8 8 13 12426.73 12479.69 643.90 o 10 8 13 4368.70 4114.21 364.62 o 12 8 13 10217.26 10529.90 618.04 o 14 8 13 7176.45 7349.21 540.46 o 3 9 13 2150.90 2267.86 279.28 o 5 9 13 4938.15 5143.41 424.09 o 7 9 13 1516.10 1542.56 161.75 o 9 9 13 2802.23 3033.29 299.97 o 11 9 13 1698.15 1851.52 279.28 o 13 9 13 991.74 1148.15 224.98 o 0 10 13 11897.56 12531.40 731.82 o 2 10 13 5142.43 5389.07 444.78 o 4 10 13 3453.02 3801.31 382.72 o 6 10 13 7155.13 6930.29 519.77 o 8 10 13 6674.37 6697.69 338.12 o 10 10 13 2540.38 2637.92 214.57 o 12 10 13 4969.26 5050.32 426.68 o 1 11 13 4640.39 4566.82 295.95 o 3 11 13 2993.80 2699.71 323.24 o 5 11 13 4430.84 4111.62 393.06 o 7 11 13 3323.25 3430.36 238.86 o 9 11 13 3557.42 3222.49 250.83 o 11 11 13 1539.72 1841.18 268.94 o 0 12 13 7602.17 7915.52 576.66 o 2 12 13 6374.67 6489.25 356.44 o 4 12 13 3142.33 2779.87 325.83 o 6 12 13 8838.69 8378.41 602.52 o 8 12 13 4878.63 4702.85 288.57 o 10 12 13 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14 14 8824.11 9358.83 475.15 o 4 14 14 5873.77 6247.60 540.46 o 6 14 14 9287.09 9366.23 682.68 o 8 14 14 9549.98 9614.48 703.37 o 10 14 14 1929.47 2368.71 349.10 o 1 15 14 2251.60 2718.09 424.09 o 3 15 14 468.93 697.54 155.42 o 5 15 14 2333.74 2371.30 338.76 o 7 15 14 1200.17 1096.43 248.25 o 9 15 14 888.10 659.41 209.46 o 0 16 14 2972.25 3372.05 408.58 o 2 16 14 1838.02 2091.62 238.86 o 4 16 14 829.54 1052.46 185.69 o 6 16 14 3192.81 2583.34 354.27 o 1 17 14 1049.58 1285.25 200.22 o 3 17 14 1328.92 1466.22 367.20 o 7 1 15 8855.70 8565.70 339.01 o 9 1 15 785.27 755.59 120.31 o 11 1 15 1040.10 991.05 135.16 o 13 1 15 6530.95 6421.46 329.07 o 15 1 15 1438.81 1441.82 188.31 o 6 2 15 29077.98 31201.80 1228.32 o 8 2 15 14704.50 14701.96 490.90 o 10 2 15 10723.02 11086.35 425.13 o 12 2 15 10244.37 9880.72 414.13 o 14 2 15 9076.98 8727.51 576.66 o 7 3 15 7622.98 7085.83 299.46 o 9 3 15 3544.12 3291.37 284.45 o 11 3 15 3327.95 2689.36 299.97 o 13 3 15 5883.31 5182.20 424.09 o 8 4 15 573.01 563.73 149.98 o 10 4 15 5815.98 5683.87 418.92 o 12 4 15 293.87 421.51 175.84 o 14 4 15 432.20 356.86 157.74 o 7 5 15 7875.25 7737.09 475.81 o 9 5 15 1680.56 1683.44 245.66 o 11 5 15 2964.95 2391.98 289.62 o 13 5 15 4972.39 5089.11 431.85 o 8 6 15 862.97 630.97 160.33 o 10 6 15 174.03 230.15 134.47 o 12 6 15 2250.62 2216.14 297.38 o 7 7 15 103.39 67.23 106.02 o 9 7 15 2700.30 2433.36 281.87 o 11 7 15 417.42 336.17 149.98 o 13 7 15 171.56 310.31 217.22 o 8 8 15 19408.55 20247.81 933.52 o 10 8 15 13833.41 13167.54 718.89 o 12 8 15 20234.58 19676.32 956.79 o 9 9 15 687.36 664.58 188.77 o 11 9 15 122.97 -46.55 139.64 o 8 10 15 376.21 387.89 144.81 o 10 10 15 176.47 284.45 181.01 o 9 11 15 1215.01 1230.90 222.39 o 4 12 15 7.83 -33.62 111.19 o 6 12 15 2882.11 2635.06 349.10 o 1 13 15 6951.27 7088.03 581.83 o 3 13 15 1964.10 1877.38 315.48 o 5 13 15 4480.64 4036.63 447.37 o 7 13 15 6182.64 6219.16 543.04 o 0 14 15 10773.67 11352.22 773.19 o 2 14 15 6381.76 6829.43 581.83 o 4 14 15 4611.57 4259.02 465.47 o 6 14 15 10705.43 10721.25 773.19 o 8 14 15 3967.55 3558.24 431.85 o 1 15 15 7116.40 7773.78 454.25 o 3 15 15 2429.16 2593.69 398.23 o 5 15 15 4841.71 4558.99 506.84 o 0 16 15 31.39 162.91 201.70 o 2 16 15 683.16 976.07 223.68 o 8 0 16 17348.10 16919.72 786.12 o 10 0 16 4038.52 4021.12 354.27 o 12 0 16 12305.74 10806.59 633.55 o 14 0 16 10162.67 9997.20 625.79 o 7 1 16 11440.35 11243.61 576.66 o 9 1 16 7226.73 7641.14 337.36 o 11 1 16 4148.37 4531.73 262.16 o 13 1 16 5028.75 5085.83 304.41 o 8 2 16 2856.93 2942.16 199.92 o 10 2 16 764.94 624.00 127.37 o 12 2 16 2712.30 2710.05 331.00 o 14 2 16 2292.85 2063.57 281.87 o 7 3 16 5644.09 4706.39 349.10 o 9 3 16 869.53 1119.71 214.63 o 11 3 16 543.26 594.76 165.50 o 13 3 16 2331.81 2128.22 297.38 o 8 4 16 4203.67 3462.56 318.07 o 10 4 16 1022.92 892.15 196.53 o 12 4 16 3011.96 2578.17 305.14 o 9 5 16 4180.74 3630.64 336.17 o 11 5 16 2583.62 2588.51 310.31 o 13 5 16 3100.75 2808.32 343.93 o 8 6 16 1610.47 1807.56 235.32 o 10 6 16 2612.14 2715.22 315.48 o 12 6 16 2708.31 2539.38 299.97 o 9 7 16 6428.61 6358.80 465.47 o 11 7 16 5782.61 5645.08 465.47 o 8 8 16 1076.39 1065.40 209.46 o 10 8 16 707.14 646.48 196.53 o 9 9 16 2823.76 2940.20 312.90 o 10 10 16 912.92 910.25 206.87 o 9 1 17 5262.83 5217.67 279.32 o 11 1 17 4784.92 4831.93 285.25 o 13 1 17 11735.73 10977.26 656.83 o 8 2 17 3549.28 3754.77 338.76 o 10 2 17 5544.78 5417.52 426.68 o 12 2 17 2200.20 2079.09 287.04 o 9 3 17 2779.52 3069.50 315.48 o 11 3 17 481.08 558.56 181.01 o 13 3 17 326.81 173.26 144.81 o 10 4 17 906.85 881.80 193.94 o 12 4 17 4339.23 4853.79 426.68 o 9 5 17 3136.80 2645.40 297.38 o 11 5 17 2194.36 2329.92 307.73 o 10 6 17 1347.84 1166.25 222.39 o 9 7 17 3375.44 3403.08 331.00 o 11 7 17 2591.00 2314.41 312.90 o 10 8 17 1886.58 1704.13 261.18 o 10 0 18 6565.11 6997.52 483.57 o 12 0 18 14830.29 13997.63 770.61 o 11 1 18 357.67 421.51 181.01 o 10 2 18 75.62 51.72 111.19 o 12 2 18 2459.00 2177.35 299.97 o 11 3 18 122.44 328.41 157.74 o 10 4 18 244.63 343.93 144.81 o 11 5 18 2658.19 2893.65 336.17 o 10 6 18 6160.83 5831.27 449.95 o 11 1 19 4490.95 4383.15 377.55 o