#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/23/2202357.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2202357_Fobs loop_ _publ_author_name 'Ejsmont, Krzysztof' 'Zaleski, Jacek' 'Sporzy\'nski, Andrzej' 'Lewandowski, Micha\/l' _publ_section_title ; 5-Formyl-2-furanboronic acid at 100K ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1324 _journal_page_last o1326 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.310 _cell_angle_gamma 90.000 _cell_length_a 3.7550 _cell_length_b 7.7580 _cell_length_c 20.6940 _exptl_crystal_F_000 288.00 _reflns_d_resolution_high 0.8260 _[local]_cod_data_source_file bt6327Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 105.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1.47 0.46 0.68 o 4 0 0 19.19 17.78 3.38 o 1 1 0 853.17 821.32 31.93 o 2 1 0 168.15 148.32 6.90 o 3 1 0 4.89 6.94 2.26 o 4 1 0 1.13 1.52 1.64 o 1 2 0 397.64 405.89 4.41 o 2 2 0 21.37 17.88 2.12 o 3 2 0 120.03 161.11 5.57 o 4 2 0 6.75 3.09 2.69 o 1 3 0 167.22 132.48 12.20 o 2 3 0 59.59 54.65 4.06 o 3 3 0 3.84 3.78 1.86 o 4 3 0 0.00 1.79 2.65 o 0 4 0 49.95 54.71 3.28 o 1 4 0 28.64 24.78 3.35 o 2 4 0 108.26 125.01 7.90 o 3 4 0 25.52 26.26 3.36 o 4 4 0 0.08 2.74 2.84 o 1 5 0 100.42 96.98 6.46 o 2 5 0 37.00 30.64 3.54 o 3 5 0 0.20 2.49 1.94 o 0 6 0 43.51 44.68 7.23 o 1 6 0 173.25 177.27 5.20 o 2 6 0 9.31 9.90 3.89 o 3 6 0 0.55 0.85 1.59 o 1 7 0 133.06 135.78 5.30 o 2 7 0 12.17 8.58 3.62 o 3 7 0 1.70 1.69 1.76 o 0 8 0 12.56 14.80 3.72 o 1 8 0 2.54 2.90 1.91 o 2 8 0 8.05 5.74 2.43 o 1 9 0 1.76 1.09 2.28 o -3 0 1 0.31 0.73 1.07 o -1 0 1 2510.73 2259.53 203.49 o 1 0 1 4347.52 3913.78 185.53 o 3 0 1 0.14 0.66 1.16 o -4 1 1 0.16 0.59 1.26 o -3 1 1 8.35 6.53 1.73 o -2 1 1 73.20 75.50 3.23 o -1 1 1 1539.90 1331.49 14.22 o 1 1 1 43.33 39.21 1.37 o 2 1 1 7.21 7.78 1.24 o 3 1 1 0.29 1.36 1.00 o 4 1 1 11.98 8.01 3.58 o -4 2 1 0.12 1.16 1.99 o -3 2 1 37.91 36.40 2.94 o -2 2 1 97.62 95.24 2.82 o -1 2 1 377.66 296.59 19.72 o 0 2 1 96.47 83.93 2.66 o 1 2 1 208.16 183.57 3.82 o 2 2 1 0.33 0.74 0.86 o 3 2 1 33.80 38.78 3.14 o 4 2 1 0.30 1.12 1.74 o -4 3 1 12.32 9.82 4.47 o -3 3 1 0.07 1.08 1.08 o -2 3 1 36.93 32.32 2.95 o -1 3 1 337.02 356.74 10.56 o 0 3 1 5.67 5.87 1.39 o 1 3 1 672.64 599.99 35.74 o 2 3 1 171.58 167.42 4.40 o 3 3 1 0.40 0.91 0.99 o 4 3 1 19.36 15.11 3.76 o -4 4 1 0.14 1.96 2.29 o -3 4 1 3.36 3.46 2.57 o -2 4 1 7.52 5.86 3.08 o -1 4 1 48.25 47.35 2.90 o 0 4 1 323.37 328.40 17.05 o 1 4 1 271.80 262.41 5.12 o 2 4 1 357.61 345.24 26.74 o 3 4 1 32.29 36.69 4.17 o 4 4 1 1.06 3.72 3.25 o -3 5 1 84.40 98.00 6.87 o -2 5 1 18.82 17.61 3.07 o -1 5 1 212.43 228.18 10.47 o 0 5 1 306.72 295.26 12.80 o 1 5 1 60.70 57.29 2.80 o 2 5 1 0.00 0.62 1.36 o 3 5 1 0.02 0.40 1.06 o -3 6 1 5.47 5.44 2.35 o -2 6 1 246.58 272.96 6.11 o -1 6 1 3.27 3.75 1.92 o 0 6 1 222.08 223.92 5.98 o 1 6 1 8.41 11.00 3.70 o 2 6 1 93.52 95.72 4.88 o 3 6 1 26.41 22.48 4.88 o -3 7 1 9.14 7.78 3.57 o -2 7 1 20.50 17.85 3.39 o -1 7 1 9.62 9.07 2.28 o 0 7 1 385.09 368.05 6.20 o 1 7 1 0.99 4.08 1.99 o 2 7 1 6.30 6.51 2.52 o 3 7 1 1.04 1.55 2.12 o -2 8 1 4.83 5.15 2.39 o -1 8 1 16.89 14.91 2.77 o 0 8 1 2.61 4.01 1.81 o 1 8 1 18.54 16.88 2.90 o 2 8 1 11.12 12.10 3.83 o -1 9 1 0.04 0.32 1.73 o 0 9 1 2.92 2.33 1.84 o 1 9 1 33.52 37.23 3.97 o -4 0 2 11.62 5.09 2.67 o -2 0 2 780.98 841.35 13.29 o 2 0 2 26.79 20.50 2.23 o 4 0 2 6.33 4.76 2.80 o -4 1 2 11.97 12.51 3.31 o -3 1 2 6.75 7.09 1.59 o -2 1 2 687.29 697.67 17.23 o -1 1 2 11054.61 11601.16 766.12 o 0 1 2 902.25 801.79 3.86 o 1 1 2 20.81 22.65 1.27 o 2 1 2 115.79 109.36 5.08 o 3 1 2 5.29 6.48 1.74 o 4 1 2 1.35 0.51 2.19 o -4 2 2 0.05 0.68 1.96 o -3 2 2 3.85 5.16 1.75 o -2 2 2 166.33 158.87 6.94 o -1 2 2 26.78 26.65 0.92 o 0 2 2 2495.16 2558.26 125.48 o 1 2 2 159.01 126.19 4.54 o 2 2 2 8.94 6.62 1.64 o 3 2 2 12.88 11.87 2.43 o 4 2 2 0.08 1.02 1.60 o -4 3 2 8.78 6.70 2.43 o -3 3 2 0.26 0.86 1.11 o -2 3 2 70.99 65.83 2.89 o -1 3 2 184.19 182.93 6.70 o 0 3 2 54.89 49.58 2.80 o 1 3 2 28.89 27.62 3.69 o 2 3 2 382.33 375.18 10.31 o 3 3 2 12.16 10.11 2.10 o 4 3 2 0.12 0.98 1.71 o -4 4 2 0.09 1.11 1.95 o -3 4 2 6.30 3.53 1.94 o -2 4 2 40.73 39.42 3.20 o -1 4 2 4.77 2.97 0.92 o 0 4 2 79.39 74.75 5.62 o 1 4 2 817.75 741.91 51.24 o 2 4 2 6.56 13.11 2.50 o 3 4 2 2.73 1.20 2.00 o 4 4 2 22.97 21.03 4.99 o -3 5 2 25.53 23.36 4.32 o -2 5 2 1.64 4.54 2.51 o -1 5 2 2.50 2.45 2.11 o 0 5 2 126.22 121.34 3.75 o 1 5 2 11.95 12.91 1.57 o 2 5 2 2.49 1.34 1.53 o 3 5 2 1.49 2.81 2.36 o -3 6 2 1.30 1.81 1.75 o -2 6 2 9.44 7.51 3.65 o -1 6 2 523.32 619.57 9.70 o 0 6 2 10.79 12.17 2.54 o 1 6 2 154.30 143.19 5.03 o 2 6 2 34.32 36.39 4.93 o 3 6 2 19.99 20.60 3.83 o -3 7 2 0.15 1.57 2.59 o -2 7 2 4.21 4.48 3.10 o -1 7 2 16.61 14.58 2.72 o 0 7 2 9.88 10.21 2.07 o 1 7 2 112.96 118.20 6.50 o 2 7 2 1.03 1.57 1.97 o 3 7 2 2.65 3.11 2.79 o -2 8 2 7.00 3.68 2.52 o -1 8 2 29.71 33.36 4.50 o 0 8 2 19.24 20.70 3.16 o 1 8 2 42.92 44.59 3.68 o 2 8 2 7.93 4.53 2.71 o -1 9 2 0.07 1.68 1.64 o 0 9 2 7.43 5.77 2.20 o 1 9 2 3.35 2.72 1.82 o -3 0 3 25.46 24.20 2.71 o -1 0 3 6163.93 6358.51 96.17 o 1 0 3 350.67 309.17 28.31 o 3 0 3 176.67 205.62 6.59 o -4 1 3 8.55 13.96 4.14 o -3 1 3 27.91 28.38 1.92 o -2 1 3 607.08 618.17 14.85 o -1 1 3 3726.96 3482.75 160.62 o 0 1 3 1673.86 1752.02 43.51 o 1 1 3 1.72 3.01 0.85 o 2 1 3 9.03 9.53 1.82 o 3 1 3 13.87 11.23 2.51 o 4 1 3 1.07 1.14 1.78 o -4 2 3 4.28 2.18 2.02 o -3 2 3 73.99 83.19 3.60 o -2 2 3 12.80 19.25 3.80 o -1 2 3 566.74 442.76 29.21 o 0 2 3 70.05 71.33 4.58 o 1 2 3 4.34 3.09 1.05 o 2 2 3 71.74 82.22 4.81 o 3 2 3 112.13 124.83 5.68 o 4 2 3 4.93 2.35 2.33 o -4 3 3 0.35 1.80 1.81 o -3 3 3 10.10 5.60 3.07 o -2 3 3 66.64 66.75 3.22 o -1 3 3 129.50 137.20 4.08 o 0 3 3 2184.00 2281.77 102.32 o 1 3 3 1049.51 1006.90 86.24 o 2 3 3 54.31 63.91 2.91 o 3 3 3 0.06 1.11 1.20 o 4 3 3 19.50 27.36 5.43 o -4 4 3 0.56 0.97 1.76 o -3 4 3 11.80 11.83 3.67 o -2 4 3 99.16 116.05 3.99 o -1 4 3 111.72 112.35 3.79 o 0 4 3 118.49 112.94 6.13 o 1 4 3 344.33 335.03 23.77 o 2 4 3 1.97 2.17 1.07 o 3 4 3 48.61 47.26 4.19 o 4 4 3 10.14 8.76 3.59 o -3 5 3 63.49 72.68 5.04 o -2 5 3 73.85 80.62 4.26 o -1 5 3 124.00 138.37 7.38 o 0 5 3 0.19 1.25 1.11 o 1 5 3 139.65 118.88 11.44 o 2 5 3 52.44 48.36 3.79 o 3 5 3 0.53 1.59 2.31 o -3 6 3 0.72 1.41 2.01 o -2 6 3 1.42 2.76 2.38 o -1 6 3 133.84 128.58 4.89 o 0 6 3 269.85 255.10 4.56 o 1 6 3 2.28 2.16 1.21 o 2 6 3 4.06 2.13 1.48 o 3 6 3 7.59 7.21 2.71 o -2 7 3 34.28 36.52 4.68 o -1 7 3 9.41 10.84 2.72 o 0 7 3 18.02 14.96 2.39 o 1 7 3 59.80 65.25 5.16 o 2 7 3 24.40 23.05 3.77 o -2 8 3 12.42 9.26 3.62 o -1 8 3 71.87 70.37 4.39 o 0 8 3 14.03 15.77 3.08 o 1 8 3 2.84 4.04 2.01 o 2 8 3 0.10 1.07 2.07 o -1 9 3 0.66 1.29 1.73 o 0 9 3 22.69 26.23 3.98 o 1 9 3 0.14 0.74 1.46 o -4 0 4 0.36 0.79 1.66 o -2 0 4 42.06 33.56 2.04 o 0 0 4 145.17 149.71 8.62 o 2 0 4 321.05 247.30 3.36 o 4 0 4 0.06 1.90 2.01 o -4 1 4 11.61 8.13 2.76 o -3 1 4 5.90 6.15 1.31 o -2 1 4 24.62 28.31 2.61 o -1 1 4 420.69 391.36 36.57 o 0 1 4 424.90 464.71 9.96 o 1 1 4 19.82 18.77 1.35 o 2 1 4 114.14 106.72 2.70 o 3 1 4 3.92 2.61 2.50 o 4 1 4 9.80 5.90 2.41 o -4 2 4 0.95 1.09 1.43 o -3 2 4 103.99 103.86 3.45 o -2 2 4 689.66 745.75 23.67 o -1 2 4 712.11 683.16 13.70 o 0 2 4 271.35 304.77 3.98 o 1 2 4 172.04 145.39 8.71 o 2 2 4 129.59 127.53 4.06 o 3 2 4 28.94 36.54 3.89 o 4 2 4 15.13 12.47 2.84 o -4 3 4 2.23 1.86 1.80 o -3 3 4 1.75 1.21 1.14 o -2 3 4 1.88 2.03 0.77 o -1 3 4 468.80 461.04 27.00 o 0 3 4 110.75 128.09 2.22 o 1 3 4 419.02 371.96 36.17 o 2 3 4 14.97 11.77 1.81 o 3 3 4 16.71 11.87 1.95 o 4 3 4 12.40 14.16 4.59 o -4 4 4 0.13 1.05 2.23 o -3 4 4 2.72 2.00 1.43 o -2 4 4 2.09 2.51 1.44 o -1 4 4 149.54 180.02 4.93 o 0 4 4 668.35 736.63 6.56 o 1 4 4 24.39 22.75 1.64 o 2 4 4 127.66 130.25 6.16 o 3 4 4 0.16 2.40 2.02 o 4 4 4 0.09 0.91 1.78 o -3 5 4 14.95 15.66 4.50 o -2 5 4 291.10 387.88 10.24 o -1 5 4 66.43 67.50 4.86 o 0 5 4 362.60 387.49 20.38 o 1 5 4 17.78 15.15 2.03 o 2 5 4 18.08 15.86 2.94 o 3 5 4 46.18 45.68 4.30 o -3 6 4 41.06 39.45 5.49 o -2 6 4 2.30 2.38 2.24 o -1 6 4 32.66 26.78 3.68 o 0 6 4 48.09 37.66 2.91 o 1 6 4 73.78 72.60 3.95 o 2 6 4 1.82 2.82 1.79 o 3 6 4 0.79 1.94 1.92 o -2 7 4 27.70 29.23 6.48 o -1 7 4 49.74 50.11 4.05 o 0 7 4 105.09 96.42 3.71 o 1 7 4 72.05 84.85 4.50 o 2 7 4 40.66 38.01 4.28 o -2 8 4 0.78 2.06 1.70 o -1 8 4 18.02 14.59 2.89 o 0 8 4 70.50 78.15 4.25 o 1 8 4 0.16 1.29 1.39 o 2 8 4 1.02 2.41 2.79 o -1 9 4 3.50 2.18 1.92 o 0 9 4 0.57 1.43 1.69 o 1 9 4 19.71 26.63 5.85 o -3 0 5 34.99 36.34 3.04 o -1 0 5 94.92 89.56 1.98 o 1 0 5 872.24 769.71 107.71 o 3 0 5 35.14 29.88 4.34 o -4 1 5 0.27 1.66 2.10 o -3 1 5 152.85 165.22 6.69 o -2 1 5 1629.92 1647.31 74.79 o -1 1 5 64.69 62.24 2.10 o 0 1 5 188.60 204.01 11.12 o 1 1 5 746.24 701.66 45.76 o 2 1 5 639.50 636.94 42.16 o 3 1 5 2.13 1.88 1.58 o 4 1 5 1.02 2.59 1.78 o -4 2 5 0.52 1.53 1.92 o -3 2 5 60.09 69.83 4.08 o -2 2 5 996.73 1046.46 52.27 o -1 2 5 0.92 1.09 0.65 o 0 2 5 882.11 959.88 14.46 o 1 2 5 185.04 162.97 6.82 o 2 2 5 105.85 101.17 3.18 o 3 2 5 16.21 15.47 3.35 o 4 2 5 0.97 1.41 1.87 o -4 3 5 7.19 8.02 3.76 o -3 3 5 24.57 24.13 3.13 o -2 3 5 11.42 8.99 1.59 o -1 3 5 118.01 119.69 2.99 o 0 3 5 30.60 36.19 1.43 o 1 3 5 102.34 95.02 3.55 o 2 3 5 110.97 109.93 4.37 o 3 3 5 9.76 9.25 2.15 o 4 3 5 9.33 6.49 3.65 o -4 4 5 13.64 13.34 4.17 o -3 4 5 8.99 9.92 2.46 o -2 4 5 43.89 52.65 4.91 o -1 4 5 54.45 51.10 6.20 o 0 4 5 8.28 7.34 1.10 o 1 4 5 82.53 81.50 5.61 o 2 4 5 11.23 7.73 2.19 o 3 4 5 51.61 56.07 5.82 o -3 5 5 0.74 1.28 1.88 o -2 5 5 137.82 174.69 7.07 o -1 5 5 516.46 523.42 33.64 o 0 5 5 158.52 170.72 5.04 o 1 5 5 51.77 45.60 2.40 o 2 5 5 67.18 75.41 5.44 o 3 5 5 25.35 28.21 3.87 o -3 6 5 0.84 1.27 2.37 o -2 6 5 14.71 15.33 4.01 o -1 6 5 0.33 0.26 1.11 o 0 6 5 34.54 33.59 2.75 o 1 6 5 24.02 19.33 2.31 o 2 6 5 31.38 30.91 3.37 o 3 6 5 17.77 15.35 3.50 o -2 7 5 1.05 0.85 1.78 o -1 7 5 114.80 119.65 4.76 o 0 7 5 4.09 4.55 1.78 o 1 7 5 0.00 1.23 1.19 o 2 7 5 5.97 5.77 3.12 o -2 8 5 3.34 4.17 3.29 o -1 8 5 45.40 47.94 4.80 o 0 8 5 1.47 0.97 1.31 o 1 8 5 2.59 0.77 1.97 o 2 8 5 3.93 1.59 2.32 o 0 9 5 23.82 22.56 3.42 o -4 0 6 3.64 3.70 1.73 o -2 0 6 178.12 182.68 10.81 o 0 0 6 21.02 22.33 1.72 o 2 0 6 1.39 1.13 0.73 o 4 0 6 68.00 82.15 8.87 o -4 1 6 0.02 0.59 1.17 o -3 1 6 4.04 3.58 1.17 o -2 1 6 30.44 30.77 1.59 o -1 1 6 308.36 292.02 6.05 o 0 1 6 34.24 30.17 1.72 o 1 1 6 1205.39 1357.08 17.31 o 2 1 6 13.04 15.19 1.76 o 3 1 6 25.68 22.93 3.36 o 4 1 6 6.78 4.18 3.28 o -4 2 6 10.04 7.73 2.28 o -3 2 6 0.11 1.17 1.11 o -2 2 6 2.99 1.36 1.30 o -1 2 6 807.68 819.94 18.69 o 0 2 6 1824.93 1881.61 62.18 o 1 2 6 299.46 293.16 18.99 o 2 2 6 195.42 205.38 4.14 o 3 2 6 19.36 17.68 2.99 o 4 2 6 14.79 13.55 3.29 o -4 3 6 5.82 4.08 3.11 o -3 3 6 39.39 46.48 3.53 o -2 3 6 30.49 26.41 3.21 o -1 3 6 468.04 474.14 24.05 o 0 3 6 239.57 266.31 2.94 o 1 3 6 536.20 535.55 22.11 o 2 3 6 10.23 8.08 1.97 o 3 3 6 5.52 6.77 2.71 o 4 3 6 0.78 1.30 2.59 o -3 4 6 102.46 111.36 7.19 o -2 4 6 180.58 188.13 6.72 o -1 4 6 11.57 9.90 1.57 o 0 4 6 105.44 113.63 4.51 o 1 4 6 3.89 3.91 1.27 o 2 4 6 34.51 42.67 3.74 o 3 4 6 113.54 137.01 8.46 o -3 5 6 0.36 0.41 1.55 o -2 5 6 27.05 27.46 4.44 o -1 5 6 6.05 10.09 2.35 o 0 5 6 72.44 74.02 2.90 o 1 5 6 91.02 83.45 3.83 o 2 5 6 3.08 1.97 1.34 o 3 5 6 5.33 4.43 2.52 o -3 6 6 4.80 4.31 2.66 o -2 6 6 26.61 21.46 4.25 o -1 6 6 11.07 8.75 2.04 o 0 6 6 19.91 16.84 2.91 o 1 6 6 14.80 11.41 2.13 o 2 6 6 69.46 71.28 4.66 o 3 6 6 6.15 5.07 2.51 o -2 7 6 0.16 0.38 1.68 o -1 7 6 25.53 24.23 3.58 o 0 7 6 29.46 27.26 3.34 o 1 7 6 10.70 10.26 3.19 o 2 7 6 5.26 3.78 2.08 o -2 8 6 52.51 58.98 6.56 o -1 8 6 0.24 1.23 1.52 o 0 8 6 89.30 100.11 4.43 o 1 8 6 27.95 28.00 4.41 o 2 8 6 9.52 7.01 3.48 o 0 9 6 27.64 32.80 3.96 o -3 0 7 173.44 188.88 7.11 o -1 0 7 2.55 1.92 0.94 o 1 0 7 102.08 120.97 25.26 o 3 0 7 20.15 24.41 10.92 o -4 1 7 2.16 1.30 1.68 o -3 1 7 17.28 16.24 1.79 o -2 1 7 8.96 7.22 1.32 o -1 1 7 183.99 173.03 3.02 o 0 1 7 1286.37 1353.34 10.13 o 1 1 7 25.76 25.77 1.83 o 2 1 7 0.69 0.57 0.60 o 3 1 7 70.57 85.39 6.00 o 4 1 7 12.14 9.68 2.83 o -4 2 7 44.84 37.21 4.04 o -3 2 7 122.80 141.85 7.95 o -2 2 7 62.86 57.99 2.69 o -1 2 7 4.09 3.55 1.27 o 0 2 7 348.55 340.98 6.16 o 1 2 7 159.41 156.63 4.38 o 2 2 7 254.94 281.92 12.22 o 3 2 7 19.57 18.33 3.15 o 4 2 7 7.58 6.02 2.53 o -4 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0.27 0.74 1.68 o -2 0 8 143.06 141.68 4.91 o 0 0 8 80.71 86.41 3.66 o 2 0 8 402.29 425.71 89.26 o 4 0 8 0.02 0.63 2.07 o -4 1 8 2.99 1.67 2.09 o -3 1 8 0.10 0.45 1.15 o -2 1 8 74.51 80.14 3.06 o -1 1 8 734.10 736.38 58.57 o 0 1 8 69.96 89.24 2.85 o 1 1 8 607.35 696.52 11.11 o 2 1 8 4.32 4.47 1.26 o 3 1 8 10.47 6.24 2.70 o 4 1 8 10.99 11.02 3.21 o -4 2 8 2.27 2.56 2.68 o -3 2 8 188.15 218.48 15.64 o -2 2 8 55.33 52.21 4.06 o -1 2 8 152.33 146.64 9.37 o 1 2 8 170.73 167.55 7.43 o 2 2 8 117.58 114.35 7.14 o 3 2 8 0.23 1.32 1.84 o 4 2 8 4.13 1.69 2.39 o -4 3 8 29.68 27.57 4.08 o -3 3 8 0.61 1.22 1.50 o -2 3 8 50.70 46.94 2.87 o -1 3 8 151.88 161.80 4.36 o 0 3 8 38.88 39.95 1.78 o 1 3 8 459.33 493.06 17.33 o 2 3 8 82.39 82.64 4.20 o 3 3 8 80.36 85.13 5.87 o 4 3 8 3.58 1.86 2.00 o -3 4 8 6.64 3.13 2.30 o -2 4 8 0.47 1.54 1.38 o -1 4 8 253.59 239.95 17.26 o 0 4 8 89.09 106.32 6.48 o 1 4 8 7.21 5.17 1.34 o 2 4 8 9.28 7.38 1.98 o 3 4 8 2.10 2.48 1.71 o -3 5 8 10.33 6.33 2.55 o -2 5 8 49.79 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