#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/23/2202377.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2202377_Fobs
loop_
_publ_author_name
'Zhang, Yiqun'
'Khoo, Lian Ee'
'Tou, Teck Yong'
'Ng, Seik Weng'
_publ_section_title
;
 Bis[3-(4-methylcoumarinyl-7-oxy)-\m-methoxy-1,1,3,3-tetramethyldistannoxane]
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m894
_journal_page_last               m896
_journal_volume                  59
_journal_year                    2003
_space_group_IT_number           2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                104.874
_cell_angle_beta                 93.419
_cell_angle_gamma                115.266
_cell_length_a                   8.8105
_cell_length_b                   9.7173
_cell_length_c                   12.7245
_exptl_crystal_F_000             504.00
_reflns_d_resolution_high        0.8410
_[local]_cod_data_source_file    bt6347Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            256.27
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
1 0 0 15056.85 14216.12 130.46 o
2 0 0 93.07 211.96 77.81 o
3 0 0 26.95 0.00 83.54 o
4 0 0 1755.65 1884.69 121.73 o
5 0 0 8705.25 8380.86 212.43 o
6 0 0 6441.72 6088.96 172.81 o
7 0 0 1334.49 1292.74 85.45 o
8 0 0 22.80 -73.75 49.17 o
9 0 0 0.75 -73.52 52.99 o
-9 1 0 1091.83 1157.17 67.31 o
-8 1 0 293.85 296.45 58.24 o
-7 1 0 350.12 297.41 75.90 o
-6 1 0 489.66 490.27 93.09 o
-5 1 0 850.47 758.55 115.53 o
-4 1 0 7697.65 7639.49 217.68 o
-3 1 0 5627.47 5302.72 183.79 o
-2 1 0 2.30 18.62 65.88 o
-1 1 0 382.30 432.31 88.32 o
0 1 0 6962.58 7327.32 201.21 o
1 1 0 5764.47 5618.51 110.53 o
2 1 0 7715.38 7436.60 209.57 o
3 1 0 1462.72 1365.78 117.91 o
4 1 0 2136.85 2199.76 135.10 o
5 1 0 2713.32 2578.32 131.28 o
6 1 0 84.76 27.21 72.56 o
7 1 0 188.05 244.90 56.33 o
8 1 0 521.93 437.76 60.63 o
-10 2 0 705.39 777.65 66.83 o
-9 2 0 513.17 393.84 58.24 o
-8 2 0 64.68 71.13 59.67 o
-7 2 0 2.95 47.26 68.74 o
-6 2 0 1406.72 1327.11 117.44 o
-5 2 0 6866.83 6353.91 196.20 o
-4 2 0 9144.87 8699.75 232.01 o
-3 2 0 236.16 211.48 97.39 o
-2 2 0 37.45 -78.29 81.15 o
-1 2 0 2001.07 2027.63 89.75 o
0 2 0 12185.28 12689.13 191.72 o
1 2 0 17745.29 18080.79 256.83 o
2 2 0 5989.64 5519.93 189.52 o
3 2 0 3283.75 3371.72 156.10 o
4 2 0 1.72 -9.07 80.20 o
5 2 0 74.18 0.00 79.72 o
6 2 0 1808.21 1775.37 91.18 o
7 2 0 2477.74 2477.12 81.15 o
8 2 0 426.01 432.03 57.76 o
-10 3 0 23.95 -3.82 53.47 o
-9 3 0 875.85 831.59 60.63 o
-8 3 0 2686.25 2729.65 102.16 o
-7 3 0 1281.24 1163.85 103.59 o
-6 3 0 72.19 59.67 95.95 o
-5 3 0 2.85 74.95 91.18 o
-4 3 0 1431.59 1431.66 116.48 o
-3 3 0 8809.30 8393.27 224.85 o
-2 3 0 14591.70 13821.54 277.36 o
-1 3 0 2984.94 3016.15 134.62 o
0 3 0 836.35 1095.42 156.10 o
1 3 0 68.69 28.88 78.05 o
2 3 0 6475.66 6719.10 209.09 o
3 3 0 5498.28 5471.71 185.70 o
4 3 0 3934.26 3662.93 144.65 o
5 3 0 18.89 28.17 67.31 o
6 3 0 132.24 158.49 54.42 o
7 3 0 22.50 25.78 49.65 o
-10 4 0 85.52 86.41 53.47 o
-9 4 0 805.84 866.44 63.01 o
-8 4 0 264.61 232.48 67.79 o
-7 4 0 118.87 199.07 79.24 o
-6 4 0 1600.90 1453.14 117.91 o
-5 4 0 156.86 267.33 89.27 o
-4 4 0 3245.12 3215.62 159.44 o
-3 4 0 5826.85 5928.09 195.73 o
-2 4 0 1816.90 1872.76 125.07 o
-1 4 0 2110.88 2173.68 193.10 o
0 4 0 2444.57 2666.19 117.27 o
1 4 0 85.19 0.00 70.04 o
2 4 0 7678.52 7929.26 221.03 o
3 4 0 4294.52 4431.98 149.42 o
4 4 0 13.40 107.41 62.06 o
5 4 0 355.97 452.55 59.19 o
6 4 0 28.03 28.17 50.12 o
-10 5 0 2.06 75.43 49.17 o
-9 5 0 46.24 -1.91 51.08 o
-8 5 0 1630.29 1609.24 90.70 o
-7 5 0 4221.44 4242.46 138.92 o
-6 5 0 4426.65 4290.20 153.72 o
-5 5 0 427.31 327.00 95.48 o
-4 5 0 83.00 93.57 83.54 o
-3 5 0 5840.92 5680.33 197.16 o
-2 5 0 12234.01 11949.74 268.76 o
-1 5 0 15440.82 15412.10 319.13 o
0 5 0 4600.95 4562.62 143.78 o
1 5 0 3.74 -118.99 79.33 o
2 5 0 85.39 303.61 84.97 o
3 5 0 1857.81 1943.41 102.16 o
4 5 0 4376.26 4331.73 119.82 o
5 5 0 2355.13 2296.19 82.11 o
6 5 0 130.26 43.44 54.90 o
-10 6 0 424.31 548.51 60.15 o
-9 6 0 6.32 9.55 49.17 o
-8 6 0 652.48 574.29 72.08 o
-7 6 0 156.00 157.53 76.86 o
-6 6 0 590.97 608.66 98.34 o
-5 6 0 2934.52 2529.63 132.23 o
-4 6 0 1166.55 1447.41 112.66 o
-3 6 0 1434.54 1332.36 120.78 o
-2 6 0 1709.90 1487.51 129.85 o
-1 6 0 3.54 5.76 63.39 o
0 6 0 1067.27 1096.38 85.56 o
1 6 0 1164.60 1275.78 84.71 o
2 6 0 0.50 -6.68 71.61 o
3 6 0 702.53 774.79 71.61 o
4 6 0 829.12 856.89 63.49 o
5 6 0 2.97 24.82 52.03 o
-10 7 0 222.04 247.28 55.38 o
-9 7 0 17.74 32.46 50.60 o
-8 7 0 0.13 94.52 51.08 o
-7 7 0 1149.76 1013.47 86.41 o
-6 7 0 3475.41 3503.00 131.28 o
-5 7 0 3159.07 2769.27 132.71 o
-4 7 0 405.81 453.51 95.95 o
-3 7 0 9.58 163.26 82.11 o
-2 7 0 809.32 710.82 104.55 o
-1 7 0 3158.59 3232.77 100.42 o
0 7 0 4569.75 4818.99 113.92 o
1 7 0 1621.37 1352.57 77.60 o
2 7 0 51.21 -20.53 63.01 o
3 7 0 5.87 -40.58 53.94 o
4 7 0 198.05 224.37 58.72 o
-9 8 0 382.77 380.95 59.67 o
-8 8 0 308.05 410.55 54.90 o
-7 8 0 32.20 67.79 58.24 o
-6 8 0 73.88 127.46 65.88 o
-5 8 0 441.60 371.88 80.20 o
-4 8 0 2720.47 2884.32 115.05 o
-3 8 0 1641.16 1556.73 106.93 o
-2 8 0 58.33 46.31 72.08 o
-1 8 0 62.42 88.83 49.59 o
0 8 0 41.16 42.58 77.81 o
1 8 0 1140.11 971.38 68.98 o
2 8 0 1449.64 1451.71 84.50 o
3 8 0 239.86 274.02 62.54 o
-9 9 0 11.50 -34.85 56.33 o
-8 9 0 38.23 135.10 52.51 o
-7 9 0 70.70 63.49 52.03 o
-6 9 0 179.08 131.28 57.29 o
-5 9 0 1550.44 1681.33 79.24 o
-4 9 0 1488.06 1501.36 82.59 o
-3 9 0 114.67 135.10 61.10 o
-2 9 0 346.97 306.00 64.45 o
-1 9 0 5.56 43.85 38.48 o
0 9 0 554.47 676.38 48.91 o
1 9 0 1319.53 1329.79 67.07 o
-8 10 0 1413.10 1356.71 82.59 o
-7 10 0 710.95 752.83 64.45 o
-6 10 0 3.99 -10.50 52.51 o
-5 10 0 4.78 33.42 49.65 o
-4 10 0 744.07 702.22 66.83 o
-3 10 0 2190.53 2308.60 84.02 o
-2 10 0 1351.21 1419.72 77.81 o
-1 10 0 243.05 271.85 45.90 o
-6 11 0 363.33 339.89 63.97 o
-5 11 0 1.96 39.62 52.03 o
-4 11 0 354.46 332.26 63.01 o
3 -11 1 1403.27 1227.82 77.81 o
4 -11 1 1734.58 1613.54 81.63 o
5 -11 1 387.89 353.26 61.10 o
6 -11 1 5.42 5.73 52.51 o
0 -10 1 366.50 449.38 101.44 o
1 -10 1 29.86 9.35 40.67 o
2 -10 1 292.72 331.78 58.72 o
3 -10 1 859.35 872.65 67.31 o
4 -10 1 34.17 65.88 52.03 o
5 -10 1 360.68 263.04 58.72 o
6 -10 1 182.34 192.86 53.94 o
7 -10 1 16.23 75.90 53.47 o
8 -10 1 457.95 510.32 62.06 o
-1 -9 1 2331.14 2209.36 192.62 o
0 -9 1 1357.73 1423.22 55.52 o
1 -9 1 0.80 -12.40 88.79 o
2 -9 1 82.24 73.99 58.72 o
3 -9 1 450.42 453.51 67.31 o
4 -9 1 2352.98 2280.44 94.04 o
5 -9 1 2474.33 2513.40 94.04 o
6 -9 1 637.95 561.87 66.36 o
7 -9 1 21.04 127.94 48.22 o
8 -9 1 12.34 63.97 48.69 o
9 -9 1 353.51 461.15 59.19 o
-3 -8 1 71.99 6.21 59.67 o
-2 -8 1 75.61 65.40 57.76 o
-1 -8 1 14.61 -11.68 57.52 o
0 -8 1 883.14 1007.13 75.43 o
1 -8 1 4878.38 5126.74 101.27 o
2 -8 1 432.67 419.14 80.20 o
3 -8 1 18.78 164.70 68.74 o
4 -8 1 224.19 181.88 76.86 o
5 -8 1 72.01 -50.12 73.04 o
6 -8 1 1292.19 1212.06 84.97 o
7 -8 1 1407.29 1477.01 81.63 o
8 -8 1 276.14 320.32 55.38 o
9 -8 1 204.05 168.51 56.33 o
-4 -7 1 27.32 71.61 51.56 o
-3 -7 1 233.41 197.16 55.38 o
-2 -7 1 63.71 68.27 61.58 o
-1 -7 1 644.47 692.35 119.82 o
0 -7 1 1998.12 1967.04 85.72 o
1 -7 1 5016.88 5094.12 114.26 o
2 -7 1 469.48 532.28 91.66 o
3 -7 1 140.28 15.75 91.66 o
4 -7 1 10.38 127.94 81.15 o
5 -7 1 2551.95 2421.74 123.16 o
6 -7 1 3832.10 3771.77 132.71 o
7 -7 1 1376.73 1388.22 89.75 o
8 -7 1 24.60 14.80 54.42 o
9 -7 1 75.03 93.57 52.03 o
10 -7 1 146.26 165.65 55.85 o
-5 -6 1 298.95 359.47 53.94 o
-4 -6 1 2113.51 2058.93 76.86 o
-3 -6 1 3425.40 3542.63 114.57 o
-2 -6 1 1687.80 1668.44 105.98 o
-1 -6 1 19.90 -59.19 97.15 o
0 -6 1 356.78 418.15 72.23 o
1 -6 1 4898.11 4969.01 122.58 o
2 -6 1 9309.25 9089.29 221.98 o
3 -6 1 6539.49 6097.56 191.91 o
4 -6 1 1990.69 2274.71 124.12 o
5 -6 1 141.65 273.54 93.57 o
6 -6 1 78.23 31.98 87.84 o
7 -6 1 1791.60 1830.27 104.55 o
8 -6 1 2762.20 2846.61 101.68 o
9 -6 1 548.13 546.60 57.76 o
10 -6 1 0.63 88.79 49.65 o
-6 -5 1 82.93 173.29 50.60 o
-5 -5 1 605.10 622.50 56.81 o
-4 -5 1 1085.17 1140.93 75.90 o
-3 -5 1 401.03 440.14 73.52 o
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-1 -5 1 3371.94 3696.23 129.61 o
0 -5 1 349.10 450.20 121.49 o
1 -5 1 6421.19 6410.75 342.04 o
2 -5 1 3182.78 3043.77 159.44 o
3 -5 1 259.81 174.24 90.22 o
4 -5 1 378.88 392.41 99.29 o
5 -5 1 4.08 239.64 84.02 o
6 -5 1 2044.11 1928.61 120.78 o
7 -5 1 1843.95 1769.16 105.98 o
8 -5 1 976.71 1000.59 78.29 o
9 -5 1 21.09 -30.55 50.60 o
10 -5 1 124.33 186.65 54.42 o
-7 -4 1 737.26 615.82 64.92 o
-6 -4 1 72.97 66.36 46.78 o
-5 -4 1 177.11 144.17 59.67 o
-4 -4 1 444.56 402.43 74.47 o
-3 -4 1 5796.19 5605.38 172.81 o
-2 -4 1 8390.28 8152.67 216.73 o
-1 -4 1 5480.38 5435.94 165.17 o
0 -4 1 20.19 -26.27 85.21 o
1 -4 1 65.83 26.86 57.09 o
2 -4 1 3363.22 3166.45 149.90 o
3 -4 1 19159.60 18648.31 323.66 o
4 -4 1 9876.79 9255.89 236.78 o
5 -4 1 968.37 927.55 116.00 o
6 -4 1 3.55 -136.05 90.70 o
7 -4 1 312.85 153.24 85.93 o
8 -4 1 1033.86 1044.50 81.63 o
9 -4 1 1496.65 1567.23 71.13 o
10 -4 1 407.33 300.75 62.54 o
-7 -3 1 352.63 384.77 56.81 o
-6 -3 1 2056.87 1993.06 83.54 o
-5 -3 1 1019.04 1007.27 88.32 o
-4 -3 1 347.54 334.64 89.27 o
-3 -3 1 1325.11 1556.73 111.23 o
-2 -3 1 417.92 422.96 95.48 o
-1 -3 1 2491.44 2286.53 131.76 o
0 -3 1 9025.31 8910.50 163.86 o
1 -3 1 1764.06 1941.12 95.95 o
2 -3 1 539.85 710.34 101.68 o
3 -3 1 217.67 116.96 96.91 o
4 -3 1 109.16 135.10 89.75 o
5 -3 1 4397.11 4317.41 176.63 o
6 -3 1 1875.27 1941.02 123.64 o
7 -3 1 0.13 148.94 72.08 o
8 -3 1 570.85 692.20 69.70 o
9 -3 1 309.01 444.92 52.99 o
10 -3 1 231.47 230.57 58.24 o
-8 -2 1 356.64 340.37 57.76 o
-7 -2 1 1903.73 1789.21 76.86 o
-6 -2 1 1348.99 1341.91 86.41 o
-5 -2 1 3.93 0.00 71.13 o
-4 -2 1 568.62 460.67 96.91 o
-3 -2 1 280.36 374.26 95.00 o
-2 -2 1 11166.19 11232.72 251.10 o
-1 -2 1 22136.99 20637.04 310.30 o
0 -2 1 5599.88 5287.55 182.60 o
1 -2 1 735.40 710.08 56.03 o
2 -2 1 3068.61 3216.10 136.53 o
3 -2 1 7.38 -73.52 93.09 o
4 -2 1 11891.65 11209.80 258.74 o
5 -2 1 10637.53 10037.84 242.99 o
6 -2 1 1755.54 1579.17 124.12 o
7 -2 1 18.04 76.86 72.08 o
8 -2 1 0.03 123.64 53.94 o
9 -2 1 172.24 235.35 51.56 o
-8 -1 1 11.12 20.53 47.26 o
-7 -1 1 62.35 81.15 55.85 o
-6 -1 1 1054.22 1071.24 92.13 o
-5 -1 1 8522.25 8124.98 207.18 o
-4 -1 1 9357.29 9149.91 232.96 o
-3 -1 1 1605.34 1619.27 116.00 o
-2 -1 1 72.11 -120.78 88.79 o
-1 -1 1 9.44 112.85 40.84 o
0 -1 1 10435.51 11131.98 127.42 o
1 -1 1 41539.92 40143.77 231.90 o
2 -1 1 14435.08 14597.76 252.53 o
3 -1 1 148.35 -10.02 96.91 o
4 -1 1 348.24 273.06 98.34 o
5 -1 1 1464.65 1407.31 122.21 o
6 -1 1 4653.97 4456.33 158.01 o
7 -1 1 2665.42 2627.49 113.14 o
8 -1 1 170.09 196.68 56.81 o
9 -1 1 1.96 -48.22 50.60 o
-9 0 1 248.62 268.76 54.90 o
-8 0 1 5.85 -78.77 52.51 o
-7 0 1 20.70 -5.25 63.01 o
-6 0 1 2681.08 2443.22 131.28 o
-5 0 1 4629.16 4397.61 166.61 o
-4 0 1 15.54 151.33 75.43 o
-3 0 1 1905.63 1650.30 126.03 o
-2 0 1 237.80 282.61 81.63 o
-1 0 1 9299.64 9449.10 116.27 o
1 0 1 11311.23 11210.79 136.37 o
2 0 1 97.02 196.20 86.41 o
3 0 1 1670.45 1501.36 126.51 o
4 0 1 322.55 361.38 100.25 o
5 0 1 4318.11 3832.87 161.35 o
6 0 1 2863.44 2944.47 125.55 o
7 0 1 362.46 315.07 67.79 o
8 0 1 34.27 -6.21 48.69 o
9 0 1 13.83 -80.68 56.33 o
-9 1 1 2790.72 2749.70 87.36 o
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-6 1 1 12.54 -3.82 89.27 o
-5 1 1 3502.33 3290.57 148.94 o
-4 1 1 16841.64 16813.27 309.34 o
-3 1 1 11536.54 11003.10 255.87 o
-2 1 1 1146.75 1213.97 98.34 o
-1 1 1 783.28 858.84 53.96 o
0 1 1 5289.02 5207.11 163.74 o
1 1 1 6995.81 7228.98 140.88 o
2 1 1 14006.91 13354.19 276.88 o
3 1 1 9310.82 8747.01 234.39 o
4 1 1 21.28 -43.92 82.11 o
5 1 1 0.61 -119.58 79.72 o
6 1 1 242.51 241.08 68.27 o
7 1 1 1275.18 1191.06 72.08 o
8 1 1 1655.44 1612.11 79.24 o
-10 2 1 218.46 146.08 59.67 o
-9 2 1 25.65 28.64 50.60 o
-8 2 1 1023.46 1056.92 76.38 o
-7 2 1 2308.32 2400.26 116.00 o
-6 2 1 443.76 389.06 96.43 o
-5 2 1 5003.74 4779.99 180.45 o
-4 2 1 3205.06 3038.51 158.01 o
-3 2 1 504.45 503.63 112.18 o
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-1 2 1 9996.71 10111.03 163.71 o
0 2 1 833.38 935.86 93.26 o
1 2 1 4442.65 5178.37 144.28 o
2 2 1 1305.54 1415.90 115.05 o
3 2 1 25.18 -51.56 81.15 o
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6 2 1 175.55 173.29 60.63 o
7 2 1 437.83 523.21 56.33 o
8 2 1 109.25 195.73 55.38 o
-10 3 1 7.53 24.82 52.99 o
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-5 3 1 461.04 520.34 103.11 o
-4 3 1 1908.31 1885.65 126.03 o
-3 3 1 10897.71 10502.33 257.78 o
-2 3 1 24749.39 24259.42 372.36 o
-1 3 1 2032.14 1941.11 102.56 o
0 3 1 1364.91 1492.22 105.79 o
1 3 1 88.12 118.13 83.06 o
2 3 1 2096.99 1939.59 134.62 o
3 3 1 8811.42 8391.36 221.50 o
4 3 1 5552.29 5506.56 162.79 o
5 3 1 214.16 312.68 69.22 o
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0 4 1 15467.73 15141.76 245.39 o
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2 4 1 848.43 907.50 116.00 o
3 4 1 114.74 27.21 88.79 o
4 4 1 886.96 914.18 84.50 o
5 4 1 1820.43 1793.99 83.06 o
6 4 1 1021.89 938.53 64.92 o
-10 5 1 259.30 185.70 58.72 o
-9 5 1 94.76 45.83 53.94 o
-8 5 1 444.15 382.38 67.79 o
-7 5 1 2651.93 2725.35 121.73 o
-6 5 1 1812.01 1656.03 118.87 o
-5 5 1 38.86 99.29 96.43 o
-4 5 1 62.55 10.02 93.09 o
-3 5 1 1431.63 1458.39 121.73 o
-2 5 1 6461.30 6765.89 209.57 o
-1 5 1 8603.36 8825.00 172.83 o
0 5 1 1359.96 1367.50 125.31 o
1 5 1 10.54 103.24 70.72 o
2 5 1 83.62 -3.82 86.88 o
3 5 1 593.83 504.59 83.06 o
4 5 1 2096.32 2151.54 90.22 o
5 5 1 1239.44 1239.27 73.04 o
-10 6 1 1238.20 1293.22 74.47 o
-9 6 1 291.77 355.17 54.90 o
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