#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/36/2203652.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203652_Fobs loop_ _publ_author_name Vasu 'Nirmala, K. A.' 'Chopra, Deepak' 'Mohan, S.' 'Saravanan, J.' _publ_section_title ; Methyl 2-amino-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o758 _journal_page_last o759 _journal_volume 60 _journal_year 2004 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 121.018 _cell_angle_gamma 90.000 _cell_length_a 16.9153 _cell_length_b 14.0033 _cell_length_c 10.1423 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file ob6362Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' jsu in C 1 2/c 1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 557.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 831.58 1148.01 34.10 o 4 0 0 310731.63 378882.34 4186.65 o 6 0 0 2344.39 2339.15 46.10 o 8 0 0 47657.27 53559.07 379.85 o 10 0 0 921.65 905.16 46.83 o 12 0 0 7129.46 6918.39 212.17 o 14 0 0 208.77 229.24 37.51 o 16 0 0 1042.54 894.16 90.93 o 1 1 0 4086.24 5414.44 35.85 o 3 1 0 760.62 855.42 17.34 o 5 1 0 9199.81 11292.43 93.00 o 7 1 0 169.54 211.59 13.36 o 9 1 0 3029.70 3232.85 47.36 o 11 1 0 0.50 16.72 14.61 o 13 1 0 643.72 722.94 42.98 o 15 1 0 1.97 35.39 34.24 o 17 1 0 102.27 134.90 62.52 o 0 2 0 15638.00 20082.03 142.05 o 2 2 0 7.44 8.52 6.30 o 4 2 0 11650.48 14409.90 94.04 o 6 2 0 31.83 56.98 9.59 o 8 2 0 4044.15 4560.04 57.80 o 10 2 0 3.03 20.38 13.32 o 12 2 0 1286.33 1317.04 67.52 o 14 2 0 0.00 62.51 29.91 o 16 2 0 305.81 346.75 37.04 o 1 3 0 4012.09 4599.90 35.57 o 3 3 0 2260.44 2704.88 32.36 o 5 3 0 2078.57 2313.67 31.73 o 7 3 0 639.65 675.09 21.10 o 9 3 0 900.92 967.28 28.03 o 11 3 0 68.53 68.33 21.07 o 13 3 0 316.30 271.59 32.81 o 15 3 0 0.27 30.64 24.73 o 0 4 0 479.77 474.53 19.88 o 2 4 0 0.63 0.00 7.02 o 4 4 0 355.33 307.79 14.59 o 6 4 0 2.11 11.93 9.88 o 8 4 0 225.27 262.56 15.88 o 10 4 0 18.26 44.78 16.51 o 12 4 0 111.01 81.91 25.46 o 14 4 0 11.63 7.43 23.86 o 16 4 0 18.99 69.10 30.15 o 1 5 0 57.87 115.49 10.34 o 3 5 0 265.61 286.76 18.45 o 5 5 0 215.94 211.06 14.49 o 7 5 0 195.29 182.02 15.93 o 9 5 0 120.32 82.25 16.89 o 11 5 0 33.66 61.54 18.41 o 13 5 0 14.50 20.08 44.38 o 15 5 0 4.57 47.08 28.27 o 0 6 0 111.04 233.59 37.82 o 2 6 0 48.18 51.68 9.35 o 4 6 0 3.22 9.09 11.32 o 6 6 0 42.36 36.53 11.19 o 8 6 0 19.02 39.51 15.57 o 10 6 0 4.45 58.73 18.94 o 12 6 0 20.78 26.16 23.26 o 14 6 0 0.04 0.00 27.03 o 16 6 0 3.95 10.64 24.60 o 1 7 0 4683.16 5385.18 71.54 o 3 7 0 2618.71 2792.34 36.55 o 5 7 0 2976.68 2954.46 60.92 o 7 7 0 834.43 723.00 31.70 o 9 7 0 895.39 808.28 36.44 o 11 7 0 155.58 128.73 22.50 o 13 7 0 159.94 121.48 47.28 o 15 7 0 21.73 12.11 28.83 o 0 8 0 5747.98 6419.14 117.19 o 2 8 0 14.72 28.22 12.99 o 4 8 0 4486.14 4917.04 65.01 o 6 8 0 59.16 78.02 15.40 o 8 8 0 1703.98 1678.53 49.94 o 10 8 0 27.00 52.97 20.19 o 12 8 0 420.03 411.12 32.95 o 14 8 0 1.80 0.00 32.32 o 1 9 0 24.94 37.26 14.78 o 3 9 0 14.47 34.67 14.26 o 5 9 0 6.97 0.00 12.89 o 7 9 0 200.20 228.85 38.83 o 9 9 0 44.42 17.86 19.29 o 11 9 0 175.14 172.78 25.70 o 13 9 0 36.75 102.14 29.50 o 0 10 0 2910.32 2601.46 65.74 o 2 10 0 36.71 61.89 19.45 o 4 10 0 1771.90 1481.64 40.22 o 6 10 0 81.79 75.91 20.05 o 8 10 0 580.21 503.29 32.95 o 10 10 0 31.44 26.61 19.82 o 12 10 0 101.41 96.47 29.50 o 1 11 0 1221.72 1265.47 38.33 o 3 11 0 1007.87 976.85 34.92 o 5 11 0 593.59 663.90 40.08 o 7 11 0 320.00 314.88 42.23 o 9 11 0 197.09 261.60 33.94 o 11 11 0 67.85 123.75 31.72 o 0 12 0 422.88 364.68 43.66 o 2 12 0 44.29 70.32 19.12 o 4 12 0 335.09 363.35 26.82 o 6 12 0 162.59 166.71 41.97 o 8 12 0 126.26 108.21 29.21 o 10 12 0 103.58 115.42 31.90 o 1 13 0 4.57 24.86 26.16 o 3 13 0 0.96 24.68 20.22 o 5 13 0 22.15 21.40 24.88 o 7 13 0 5.29 0.00 45.70 o 9 13 0 32.03 33.37 28.53 o 0 14 0 16.74 68.20 45.47 o 2 14 0 0.42 23.08 29.11 o 4 14 0 17.09 19.18 22.54 o 6 14 0 6.02 32.65 32.70 o 8 14 0 12.78 33.74 28.88 o 1 15 0 0.01 23.64 33.41 o 3 15 0 9.44 63.72 29.11 o 5 15 0 1.19 53.04 45.47 o 7 15 0 24.53 83.21 47.36 o 0 16 0 25.55 94.72 49.25 o 2 16 0 0.17 13.51 41.68 o 4 16 0 15.75 68.20 49.25 o -17 1 1 52.33 36.08 30.72 o -15 1 1 662.08 525.46 39.25 o -13 1 1 223.39 205.78 22.51 o -11 1 1 2504.33 2326.52 53.45 o -9 1 1 1219.76 1168.27 27.71 o -7 1 1 8682.94 9581.59 67.81 o -5 1 1 5304.09 4938.00 39.62 o -3 1 1 24088.08 28640.16 139.63 o -1 1 1 6096.65 5174.89 33.99 o 1 1 1 20190.75 24447.43 131.31 o 3 1 1 2194.38 1821.50 20.83 o 5 1 1 4658.86 5401.21 46.11 o 7 1 1 300.45 246.32 12.21 o 9 1 1 999.07 1081.93 36.13 o 11 1 1 24.02 19.62 20.04 o 13 1 1 191.78 122.56 26.92 o 15 1 1 6.74 0.00 31.52 o -16 2 1 164.82 199.31 31.90 o -14 2 1 81.99 70.76 24.36 o -12 2 1 569.89 580.89 30.45 o -10 2 1 613.52 486.72 27.83 o -8 2 1 953.40 908.38 27.75 o -6 2 1 2160.67 1824.24 34.68 o -4 2 1 14.98 34.07 7.53 o -2 2 1 1626.45 1410.71 17.17 o 0 2 1 3742.74 3744.87 28.69 o 2 2 1 1108.30 1197.30 18.36 o 4 2 1 967.47 887.58 16.99 o 6 2 1 605.30 565.65 19.69 o 8 2 1 122.65 111.51 20.29 o 10 2 1 164.13 140.41 18.80 o 12 2 1 19.10 5.99 20.87 o 14 2 1 41.82 27.13 23.26 o 16 2 1 10.96 0.00 32.15 o -17 3 1 40.99 119.51 31.74 o -15 3 1 1.27 30.85 24.73 o -13 3 1 137.62 130.26 26.25 o -11 3 1 103.34 104.69 16.15 o -9 3 1 380.53 326.84 17.10 o -7 3 1 1313.11 1274.37 27.43 o -5 3 1 642.58 509.32 13.47 o -3 3 1 12752.30 15171.64 87.22 o -1 3 1 570.37 573.80 14.36 o 1 3 1 16360.83 18898.95 102.46 o 3 3 1 131.59 129.90 8.77 o 5 3 1 2151.20 2078.46 26.56 o 7 3 1 38.52 24.84 12.25 o 9 3 1 235.04 226.09 17.26 o 11 3 1 0.01 0.00 17.66 o 13 3 1 11.20 59.51 23.08 o 15 3 1 6.26 51.71 45.86 o -16 4 1 4.40 17.72 28.87 o -14 4 1 0.64 39.60 25.41 o -12 4 1 1.74 0.00 19.44 o -10 4 1 2.58 30.83 14.98 o -8 4 1 57.37 42.20 9.65 o -6 4 1 2.05 0.00 5.61 o -4 4 1 690.78 760.59 16.51 o -2 4 1 915.09 1076.04 19.37 o 0 4 1 3006.99 3823.17 35.82 o 2 4 1 1324.66 1197.04 23.91 o 4 4 1 938.06 850.30 21.91 o 6 4 1 303.19 270.24 11.63 o 8 4 1 68.95 85.88 16.51 o 10 4 1 46.79 33.09 16.89 o 12 4 1 9.45 19.07 21.66 o 14 4 1 2.99 55.41 24.51 o -17 5 1 17.73 11.06 27.65 o -15 5 1 144.82 183.89 44.17 o -13 5 1 205.08 176.69 28.44 o -11 5 1 615.25 648.87 31.70 o -9 5 1 1135.44 1077.76 42.70 o -7 5 1 2225.55 2221.15 30.61 o -5 5 1 3518.98 3546.79 38.18 o -3 5 1 3882.99 3998.21 40.79 o -1 5 1 4025.11 4006.14 40.56 o 1 5 1 2846.75 3063.17 33.67 o 3 5 1 1530.11 1444.16 28.89 o 5 5 1 2255.02 2393.13 62.00 o 7 5 1 229.79 214.94 20.19 o 9 5 1 741.39 756.88 34.32 o 11 5 1 5.73 37.05 23.86 o 13 5 1 135.56 237.55 31.72 o 15 5 1 1.89 35.28 52.41 o -16 6 1 66.53 55.17 31.14 o -14 6 1 0.07 49.00 23.86 o -12 6 1 264.80 259.89 25.43 o -10 6 1 5.61 30.42 15.57 o -8 6 1 957.15 977.10 34.94 o -6 6 1 32.39 43.30 12.24 o -4 6 1 3841.02 4276.59 45.29 o -2 6 1 303.86 286.28 15.22 o 0 6 1 8456.87 9678.33 73.38 o 2 6 1 196.37 179.87 14.73 o 4 6 1 3871.32 4025.31 53.07 o 6 6 1 26.38 42.15 12.93 o 8 6 1 1039.21 973.76 37.60 o 10 6 1 11.38 0.00 19.12 o 12 6 1 205.21 148.10 39.37 o 14 6 1 6.02 0.00 42.87 o -15 7 1 1.90 0.00 33.77 o -13 7 1 16.79 44.73 23.26 o -11 7 1 2.09 19.32 21.33 o -9 7 1 175.14 191.86 21.13 o -7 7 1 169.64 165.21 15.98 o -5 7 1 869.75 895.59 28.03 o -3 7 1 1500.43 1452.77 28.05 o -1 7 1 1816.58 1908.72 32.44 o 1 7 1 2252.17 2232.05 33.28 o 3 7 1 721.40 680.82 24.14 o 5 7 1 558.65 602.30 23.91 o 7 7 1 35.58 44.59 17.47 o 9 7 1 13.83 25.40 18.41 o 11 7 1 0.16 0.00 18.97 o 13 7 1 20.56 0.00 23.86 o -14 8 1 33.39 48.94 25.52 o -12 8 1 197.16 213.29 26.32 o -10 8 1 40.48 51.99 18.75 o -8 8 1 1020.97 975.42 38.26 o -6 8 1 96.95 143.57 16.46 o -4 8 1 2554.72 2508.62 37.73 o -2 8 1 544.28 684.07 22.24 o 0 8 1 2405.27 2547.78 38.88 o 2 8 1 1132.38 1205.81 25.94 o 4 8 1 1289.43 1243.04 33.53 o 6 8 1 585.41 638.31 31.87 o 8 8 1 419.16 381.32 29.95 o 10 8 1 195.76 206.15 25.91 o 12 8 1 100.46 110.52 28.93 o 14 8 1 38.55 46.41 66.30 o -15 9 1 7.58 21.03 33.44 o -13 9 1 59.99 97.43 24.11 o -11 9 1 89.09 114.88 22.61 o -9 9 1 237.47 278.07 26.77 o -7 9 1 520.31 535.74 30.66 o -5 9 1 484.74 477.07 24.70 o -3 9 1 1582.29 1519.72 53.66 o -1 9 1 784.99 688.97 23.58 o 1 9 1 1807.00 1777.77 34.17 o 3 9 1 807.62 714.51 28.41 o 5 9 1 961.51 1014.08 33.95 o 7 9 1 402.34 316.06 27.51 o 9 9 1 326.28 280.16 28.46 o 11 9 1 133.26 161.50 35.16 o 13 9 1 74.25 44.68 77.67 o -14 10 1 256.50 202.55 34.86 o -12 10 1 74.40 54.13 24.01 o -10 10 1 656.63 594.68 37.78 o -8 10 1 388.77 382.90 33.36 o -6 10 1 1117.68 1022.98 34.69 o -4 10 1 1096.39 1084.69 34.93 o -2 10 1 1043.81 958.40 28.32 o 0 10 1 1255.84 1299.12 31.70 o 2 10 1 326.32 325.50 22.73 o 4 10 1 484.22 487.69 38.16 o 6 10 1 50.04 28.29 25.52 o 8 10 1 77.69 61.38 25.91 o 10 10 1 13.91 0.00 25.91 o 12 10 1 5.55 0.00 73.88 o -13 11 1 3.82 24.46 22.41 o -11 11 1 37.09 70.29 24.06 o -9 11 1 36.18 67.98 21.30 o -7 11 1 109.48 107.16 22.66 o -5 11 1 242.68 234.48 23.40 o -3 11 1 119.22 127.49 20.48 o -1 11 1 657.79 616.00 48.01 o 1 11 1 90.25 150.12 20.70 o 3 11 1 572.78 528.72 33.50 o 5 11 1 92.90 96.11 27.40 o 7 11 1 269.90 217.85 33.22 o 9 11 1 64.15 45.27 28.53 o 11 11 1 90.34 75.51 59.90 o -12 12 1 3.24 50.95 28.80 o -10 12 1 526.16 439.94 33.84 o -8 12 1 54.74 57.78 22.95 o -6 12 1 1245.27 1017.75 45.17 o -4 12 1 151.63 173.30 22.30 o -2 12 1 1788.32 1566.05 59.68 o 0 12 1 240.19 220.77 33.71 o 2 12 1 1265.25 1026.44 43.73 o 4 12 1 313.58 334.56 30.53 o 6 12 1 449.58 364.31 39.81 o 8 12 1 183.33 234.86 34.91 o 10 12 1 106.46 130.97 38.79 o -11 13 1 0.01 24.90 30.87 o -9 13 1 276.59 256.90 36.67 o -7 13 1 85.80 118.36 32.77 o -5 13 1 856.82 773.76 38.66 o -3 13 1 662.16 654.94 43.75 o -1 13 1 1376.14 1179.38 60.98 o 1 13 1 1383.73 1394.12 61.03 o 3 13 1 1033.75 856.16 43.64 o 5 13 1 1078.58 960.11 55.59 o 7 13 1 372.83 388.49 42.60 o 9 13 1 424.52 378.72 66.05 o -10 14 1 1.21 74.90 34.52 o -8 14 1 59.40 95.02 32.77 o -6 14 1 42.54 62.34 29.11 o -4 14 1 78.15 96.61 34.83 o -2 14 1 104.71 140.87 29.50 o 0 14 1 65.97 87.72 28.77 o 2 14 1 32.70 133.95 29.66 o 4 14 1 62.55 86.08 29.11 o 6 14 1 3.05 3.10 28.26 o 8 14 1 49.59 32.65 30.43 o -7 15 1 100.69 50.77 37.89 o -5 15 1 383.61 397.83 71.99 o -3 15 1 128.23 100.40 34.83 o -1 15 1 353.33 377.51 46.83 o 1 15 1 99.46 172.68 37.22 o 3 15 1 171.66 136.40 42.70 o 5 15 1 68.91 71.17 57.35 o -4 16 1 368.81 458.45 75.78 o -2 16 1 65.56 97.83 37.22 o 0 16 1 507.27 522.25 71.99 o 2 16 1 47.51 46.22 33.41 o -18 0 2 5.43 53.04 41.68 o -16 0 2 8.32 18.55 25.35 o -14 0 2 2.49 47.99 23.67 o -12 0 2 336.30 324.18 34.52 o -10 0 2 48.16 43.91 13.39 o -8 0 2 2842.98 2520.94 46.78 o -6 0 2 1247.95 1572.63 33.93 o -4 0 2 12260.17 12213.65 105.50 o -2 0 2 13083.91 16453.51 126.37 o 0 0 2 18120.01 19438.41 146.98 o 2 0 2 9886.76 11098.69 127.41 o 4 0 2 7463.87 7336.92 83.96 o 6 0 2 2578.74 2625.12 51.28 o 8 0 2 1598.57 1608.14 66.30 o 10 0 2 502.06 396.94 58.73 o 12 0 2 110.28 98.51 41.68 o 14 0 2 63.60 64.41 41.68 o -17 1 2 0.26 18.12 22.54 o -15 1 2 99.37 101.38 25.29 o -13 1 2 17.53 23.39 15.26 o -11 1 2 390.59 397.24 19.69 o -9 1 2 117.35 99.66 10.38 o -7 1 2 1246.15 1209.56 22.45 o -5 1 2 238.24 213.60 10.86 o -3 1 2 265.32 211.23 10.93 o -1 1 2 734.53 591.26 13.24 o 1 1 2 170.60 152.57 10.50 o 3 1 2 495.74 401.39 14.06 o 5 1 2 6.87 18.89 9.57 o 7 1 2 114.78 159.76 12.44 o 9 1 2 3.47 9.54 15.86 o 11 1 2 7.96 0.00 21.07 o 13 1 2 9.58 10.10 28.04 o 15 1 2 0.51 42.50 68.20 o -18 2 2 12.82 0.00 28.17 o -16 2 2 1.60 0.00 20.87 o -14 2 2 37.26 20.21 25.60 o -12 2 2 149.79 136.25 18.09 o -10 2 2 25.80 18.37 10.16 o -8 2 2 1782.91 1581.63 35.61 o -6 2 2 39.70 92.45 9.72 o -4 2 2 7316.15 6705.22 50.78 o -2 2 2 167.61 145.72 10.78 o 0 2 2 6133.61 5409.90 41.53 o 2 2 2 35.67 61.80 8.84 o 4 2 2 2432.06 2202.07 30.47 o 6 2 2 52.88 88.70 10.41 o 8 2 2 432.17 467.39 22.17 o 10 2 2 72.02 68.42 37.56 o 12 2 2 52.72 64.24 29.51 o 14 2 2 33.84 52.29 40.01 o -17 3 2 25.29 73.42 30.70 o -15 3 2 5.63 0.00 27.87 o -13 3 2 291.14 258.00 27.98 o -11 3 2 4.40 32.33 11.57 o -9 3 2 1925.43 1555.65 30.22 o -7 3 2 70.64 82.58 10.17 o -5 3 2 4872.33 4123.41 40.32 o -3 3 2 4612.84 4720.65 40.70 o -1 3 2 4743.79 4097.90 44.02 o 1 3 2 9114.52 9159.86 62.95 o 3 3 2 3113.21 2708.80 32.67 o 5 3 2 2576.02 2290.19 32.20 o 7 3 2 785.02 726.92 25.70 o 9 3 2 496.69 457.43 32.67 o 11 3 2 127.91 148.47 26.73 o 13 3 2 50.06 85.05 26.92 o -18 4 2 23.56 31.90 28.27 o -16 4 2 9.20 22.36 23.86 o -14 4 2 158.21 128.03 35.01 o -12 4 2 126.01 116.28 19.11 o -10 4 2 776.54 776.98 25.68 o -8 4 2 891.98 753.44 19.78 o -6 4 2 3723.18 3626.43 40.69 o -4 4 2 3309.82 2845.47 33.32 o -2 4 2 8639.97 9704.27 67.12 o 0 4 2 3241.73 2630.04 29.28 o 2 4 2 2330.67 2629.99 31.99 o 4 4 2 1281.92 922.62 21.20 o 6 4 2 66.24 97.88 11.39 o 8 4 2 235.68 224.64 22.97 o 10 4 2 1.33 5.55 23.63 o 12 4 2 10.41 21.97 21.58 o 14 4 2 0.64 69.05 27.76 o -17 5 2 0.26 29.05 26.25 o -15 5 2 99.06 55.97 30.57 o -13 5 2 11.79 0.24 20.87 o -11 5 2 310.58 329.38 26.80 o -9 5 2 281.17 258.58 16.07 o -7 5 2 1366.44 1509.59 27.80 o -5 5 2 1680.11 1426.37 25.68 o -3 5 2 4712.40 5402.07 50.01 o -1 5 2 2662.41 2136.40 33.61 o 1 5 2 6347.21 7258.44 58.52 o 3 5 2 585.11 435.97 15.38 o 5 5 2 2848.34 2824.27 45.28 o 7 5 2 1.15 9.83 15.08 o 9 5 2 644.97 598.32 28.76 o 11 5 2 19.12 87.19 22.45 o 13 5 2 99.77 120.46 27.88 o -16 6 2 0.06 8.12 26.73 o -14 6 2 21.29 12.15 22.30 o -12 6 2 0.41 0.00 16.02 o -10 6 2 5.74 22.16 16.51 o -8 6 2 137.20 130.89 11.88 o -6 6 2 67.11 184.16 12.89 o -4 6 2 1204.55 1207.21 25.11 o -2 6 2 1720.18 2426.65 35.10 o 0 6 2 1845.01 1870.28 28.94 o 2 6 2 2671.07 2914.79 66.08 o 4 6 2 440.85 412.58 20.16 o 6 6 2 1259.91 1336.55 44.30 o 8 6 2 2.68 11.30 18.09 o 10 6 2 400.62 410.20 30.50 o 12 6 2 15.49 36.90 38.17 o 14 6 2 77.90 79.57 40.19 o -17 7 2 0.09 33.14 28.27 o -15 7 2 82.39 83.35 26.25 o -13 7 2 6.05 18.12 18.41 o -11 7 2 545.83 511.46 31.21 o -9 7 2 2.97 0.00 14.18 o -7 7 2 1924.08 1983.48 40.15 o -5 7 2 22.60 56.87 11.18 o -3 7 2 5066.47 5952.10 59.67 o -1 7 2 104.83 180.67 13.38 o 1 7 2 5411.15 5727.67 57.46 o 3 7 2 19.43 49.01 12.28 o 5 7 2 1993.35 2003.63 45.95 o 7 7 2 0.28 0.00 17.88 o 9 7 2 555.12 529.44 33.35 o 11 7 2 1.46 36.37 37.89 o 13 7 2 118.16 58.27 38.23 o -16 8 2 84.07 110.54 29.84 o -14 8 2 158.62 164.11 29.84 o -12 8 2 387.55 364.45 30.22 o -10 8 2 599.55 622.48 33.52 o -8 8 2 1022.36 917.62 31.18 o -6 8 2 1284.07 1430.88 47.23 o -4 8 2 1008.44 903.84 24.94 o -2 8 2 882.71 996.19 26.39 o 0 8 2 333.87 337.00 16.63 o 2 8 2 702.20 942.49 28.92 o 4 8 2 130.75 125.88 17.01 o 6 8 2 597.94 690.55 33.70 o 8 8 2 27.66 20.10 28.85 o 10 8 2 288.84 269.56 42.10 o 12 8 2 1.20 26.52 37.51 o -15 9 2 22.94 47.85 27.35 o -13 9 2 7.76 9.19 20.31 o -11 9 2 15.00 14.97 18.80 o -9 9 2 0.12 7.62 18.09 o -7 9 2 29.27 51.33 15.51 o -5 9 2 31.77 20.69 14.25 o -3 9 2 253.46 340.46 19.65 o -1 9 2 151.71 132.09 13.87 o 1 9 2 229.89 287.33 19.82 o 3 9 2 93.96 104.47 20.53 o 5 9 2 7.04 0.00 22.87 o 7 9 2 22.33 57.47 30.51 o 9 9 2 11.29 14.89 27.03 o 11 9 2 4.17 0.00 37.51 o -14 10 2 8.48 22.39 36.64 o -12 10 2 586.21 574.70 36.90 o -10 10 2 1.12 22.21 19.49 o -8 10 2 1979.49 1767.22 53.40 o -6 10 2 40.70 110.00 18.06 o -4 10 2 4340.25 4056.33 76.56 o -2 10 2 351.63 426.59 24.85 o 0 10 2 5103.62 4999.14 96.05 o 2 10 2 430.19 556.02 33.02 o 4 10 2 2916.61 2755.99 65.37 o 6 10 2 167.20 255.78 34.09 o 8 10 2 1024.81 1029.12 61.28 o 10 10 2 29.20 86.55 30.20 o -13 11 2 124.38 142.79 25.03 o -11 11 2 346.42 345.26 30.66 o -9 11 2 310.86 361.79 29.95 o -7 11 2 711.52 680.54 36.58 o -5 11 2 520.38 536.33 31.93 o -3 11 2 684.35 755.54 35.42 o -1 11 2 484.00 544.16 33.11 o 1 11 2 337.70 411.43 31.43 o 3 11 2 209.60 219.11 27.34 o 5 11 2 144.96 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