#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203663.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203663_Fobs loop_ _publ_author_name 'Zhu, Bixue' 'Ruang, Wenjuan' 'Zhu, Zhiang' _publ_section_title ; A nickel(II) complex of an unsymmetrical tetradentate Schiff base ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m634 _journal_page_last m636 _journal_volume 60 _journal_year 2004 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.181 _cell_angle_beta 101.862 _cell_angle_gamma 119.151 _cell_length_a 13.8563 _cell_length_b 14.1718 _cell_length_c 15.8629 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.7990 _[local]_cod_data_source_file tk61603sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 031219C in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 475.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 202.63 29.75 4.96 o 2 0 0 1056.65 1095.94 32.23 o 3 0 0 25399.09 26810.94 520.70 o 4 0 0 83.64 86.78 22.32 o 5 0 0 157.23 173.57 24.80 o 6 0 0 1597.04 1720.78 61.99 o 7 0 0 2362.74 2278.67 79.34 o 8 0 0 3157.11 3210.96 101.66 o 9 0 0 3.33 -27.27 29.75 o 10 0 0 282.95 312.42 44.63 o 11 0 0 623.90 706.66 57.03 o 12 0 0 9.15 0.00 34.71 o 13 0 0 29.08 19.84 44.63 o 14 0 0 7.34 -22.32 47.11 o -14 1 0 10.00 0.00 42.15 o -13 1 0 0.13 -39.67 39.67 o -12 1 0 395.34 344.65 52.07 o -11 1 0 165.13 141.33 39.67 o -10 1 0 209.11 171.09 42.15 o -9 1 0 2227.17 2310.90 86.78 o -8 1 0 938.85 835.59 52.07 o -7 1 0 73.00 29.75 29.75 o -6 1 0 487.31 508.30 37.19 o -5 1 0 5348.79 5405.33 126.45 o -4 1 0 988.99 1038.91 39.67 o -3 1 0 344.09 339.69 22.32 o -2 1 0 2223.60 2281.15 52.07 o 1 1 0 6.05 163.65 9.92 o 2 1 0 13509.05 13761.28 272.75 o 3 1 0 8766.67 9699.84 203.32 o 4 1 0 1617.22 1671.19 54.55 o 5 1 0 90.52 121.50 24.80 o 6 1 0 586.67 547.97 39.67 o 7 1 0 1662.94 1576.97 66.95 o 8 1 0 50.51 99.18 37.19 o 9 1 0 174.21 225.64 42.15 o 10 1 0 611.98 580.21 52.07 o 11 1 0 147.88 114.06 39.67 o 12 1 0 44.08 -32.23 42.15 o 13 1 0 14.72 -37.19 39.67 o -15 2 0 115.50 116.54 54.55 o -14 2 0 3.25 -44.63 44.63 o -13 2 0 484.24 500.86 54.55 o -12 2 0 50.23 39.67 37.19 o -11 2 0 21.18 4.96 34.71 o -10 2 0 21.78 -9.92 37.19 o -9 2 0 1452.64 1410.84 64.47 o -8 2 0 16.49 -29.75 29.75 o -7 2 0 1452.69 1497.62 59.51 o -6 2 0 3404.32 3334.94 89.26 o -5 2 0 4745.18 4963.98 116.54 o -4 2 0 3272.62 3691.99 89.26 o -3 2 0 1795.02 1897.24 34.93 o -2 2 0 200.51 173.57 14.88 o -1 2 0 2877.66 2814.24 61.99 o 0 2 0 410.17 490.94 13.06 o 1 2 0 7397.91 7375.04 106.06 o 2 2 0 226186.89 241372.02 6512.44 o 3 2 0 1.47 2.48 17.36 o 4 2 0 2464.06 2491.91 74.39 o 5 2 0 1935.16 1914.18 69.43 o 6 2 0 881.93 771.13 49.59 o 7 2 0 203.82 213.24 34.71 o 8 2 0 233.16 230.59 42.15 o 9 2 0 788.06 857.91 59.51 o 10 2 0 364.12 416.56 52.07 o 11 2 0 34.48 17.36 39.67 o 12 2 0 152.47 104.14 47.11 o 13 2 0 55.75 69.43 52.07 o -15 3 0 47.82 -17.36 44.63 o -14 3 0 329.07 381.84 54.55 o -13 3 0 0.64 -9.92 37.19 o -12 3 0 60.64 74.39 39.67 o -11 3 0 94.51 114.06 44.63 o -10 3 0 1073.11 1081.07 61.99 o -9 3 0 1.99 -7.44 29.75 o -8 3 0 80.73 91.74 27.27 o -7 3 0 4118.07 4430.88 116.54 o -6 3 0 3701.67 3617.33 63.83 o -5 3 0 37.46 47.22 11.90 o -4 3 0 11423.56 12575.20 176.04 o -3 3 0 2423.92 2603.92 44.68 o -2 3 0 3177.96 3233.40 52.07 o -1 3 0 700.02 703.06 18.35 o 0 3 0 28928.67 30917.81 414.51 o 1 3 0 33369.89 34763.90 466.15 o 2 3 0 471.45 523.44 26.03 o 3 3 0 3274.36 3120.75 58.72 o 4 3 0 6256.70 6359.94 151.25 o 5 3 0 1905.38 1795.16 66.95 o 6 3 0 250.29 235.55 37.19 o 7 3 0 574.11 567.81 49.59 o 8 3 0 284.80 280.18 47.11 o 9 3 0 136.04 96.70 42.15 o 10 3 0 4.90 -32.23 32.23 o 11 3 0 148.21 168.61 49.59 o 12 3 0 109.25 84.30 42.15 o -16 4 0 0.81 -52.07 52.07 o -15 4 0 179.26 247.43 44.63 o -14 4 0 322.59 321.61 33.35 o -13 4 0 0.04 -14.30 22.59 o -12 4 0 25.69 -8.59 45.87 o -11 4 0 4020.30 4123.61 86.14 o -10 4 0 24.43 7.76 26.03 o -9 4 0 1209.77 1210.00 38.72 o -8 4 0 23.59 23.80 16.50 o -7 4 0 1515.44 1422.43 40.91 o -6 4 0 1027.98 1125.76 40.91 o -5 4 0 9973.79 10330.52 228.11 o -4 4 0 2642.57 2844.16 50.75 o -3 4 0 10317.96 11444.24 162.11 o -2 4 0 1898.55 1931.86 35.91 o -1 4 0 3308.21 3304.37 59.51 o 0 4 0 279.09 249.05 14.83 o 1 4 0 2692.06 2724.09 50.85 o 2 4 0 4659.20 4535.17 111.58 o 3 4 0 1744.91 1621.17 41.17 o 4 4 0 11192.64 10575.11 235.55 o 5 4 0 500.89 495.90 42.15 o 6 4 0 931.50 984.37 57.03 o 7 4 0 229.92 267.79 42.15 o 8 4 0 203.74 250.43 44.63 o 9 4 0 30.45 57.03 37.19 o 10 4 0 161.32 114.06 42.15 o 11 4 0 174.76 168.61 49.59 o 12 4 0 68.37 9.92 42.15 o -16 5 0 64.24 89.26 54.55 o -15 5 0 89.94 121.50 49.59 o -14 5 0 69.15 15.81 26.60 o -13 5 0 361.12 325.76 30.98 o -12 5 0 1596.36 1595.72 55.79 o -11 5 0 38.53 30.71 42.15 o -10 5 0 286.27 320.86 26.80 o -9 5 0 751.30 771.90 32.12 o -8 5 0 2043.69 2052.84 48.00 o -7 5 0 83.13 74.96 16.59 o -6 5 0 2626.49 2869.73 55.04 o -5 5 0 540.96 544.50 38.43 o -4 5 0 7694.03 7866.51 117.43 o -3 5 0 797.51 766.36 23.62 o -2 5 0 1915.84 2026.56 39.42 o -1 5 0 1723.78 1719.48 36.69 o 0 5 0 254.65 259.40 15.78 o 1 5 0 39.80 39.18 13.06 o 2 5 0 3648.45 3600.25 94.22 o 3 5 0 8812.66 8204.45 281.42 o 4 5 0 19.73 52.07 17.53 o 5 5 0 1036.76 1026.52 57.03 o 6 5 0 836.94 875.27 59.51 o 7 5 0 593.59 617.40 52.07 o 8 5 0 2.59 2.48 39.67 o 9 5 0 283.97 307.46 49.59 o 10 5 0 147.68 158.69 44.63 o 11 5 0 29.80 76.86 44.63 o -16 6 0 22.34 52.07 52.07 o -15 6 0 55.35 -24.80 47.11 o -14 6 0 95.46 114.36 28.51 o -13 6 0 410.77 432.63 48.35 o -12 6 0 529.94 552.79 38.43 o -11 6 0 917.04 947.21 39.31 o -10 6 0 852.89 832.88 35.15 o -9 6 0 4618.95 4519.19 85.43 o -8 6 0 128.19 117.33 20.11 o -7 6 0 2866.27 2857.34 58.56 o -6 6 0 387.27 442.76 22.79 o -5 6 0 2791.91 2972.69 65.71 o -4 6 0 1212.37 1246.32 32.40 o -3 6 0 8266.67 7981.38 120.09 o -2 6 0 5933.83 5989.13 94.68 o -1 6 0 485.57 504.66 21.86 o 0 6 0 3869.35 3716.11 81.82 o 1 6 0 1458.96 1468.57 60.75 o 2 6 0 528.68 451.34 44.63 o 3 6 0 466.18 411.97 43.39 o 4 6 0 1230.98 1362.28 44.68 o 5 6 0 123.74 106.62 32.23 o 6 6 0 824.68 815.76 57.03 o 7 6 0 55.68 22.32 39.67 o 8 6 0 259.39 322.34 49.59 o 10 6 0 4.44 19.84 44.63 o -16 7 0 22.38 -27.27 49.59 o -15 7 0 11.95 -17.36 44.63 o -14 7 0 123.27 83.18 52.07 o -13 7 0 242.68 202.37 40.91 o -12 7 0 551.58 574.43 36.32 o -11 7 0 588.80 561.73 36.69 o -10 7 0 2906.12 3061.49 68.84 o -9 7 0 135.81 126.83 23.56 o -8 7 0 1806.40 1881.66 48.00 o -7 7 0 2027.53 2181.75 50.75 o -6 7 0 1916.18 1990.35 46.44 o -5 7 0 0.25 10.05 16.59 o -4 7 0 1032.78 971.62 28.89 o -3 7 0 3449.49 3569.43 65.73 o -2 7 0 807.81 803.35 42.15 o -1 7 0 117.00 145.92 16.59 o 0 7 0 803.33 773.74 28.89 o 1 7 0 1588.11 1559.10 78.10 o 2 7 0 566.40 550.15 28.89 o 3 7 0 710.65 694.55 34.16 o 4 7 0 477.94 433.61 35.95 o 5 7 0 1450.71 1391.01 74.39 o 6 7 0 0.43 69.43 42.15 o 7 7 0 144.69 158.69 47.11 o 8 7 0 55.55 29.75 47.11 o 9 7 0 16.89 -4.96 42.15 o -16 8 0 14.55 12.40 47.11 o -15 8 0 252.50 292.58 54.55 o -14 8 0 51.15 19.84 37.19 o -13 8 0 39.13 -13.48 27.89 o -12 8 0 11.00 10.72 27.13 o -11 8 0 71.91 69.94 25.02 o -10 8 0 471.42 430.27 30.64 o -9 8 0 5592.32 5764.00 103.27 o -8 8 0 741.01 712.01 44.63 o -7 8 0 1711.58 1842.33 47.34 o -6 8 0 15.52 25.97 16.04 o -5 8 0 3774.35 3656.89 68.38 o -4 8 0 546.76 527.10 25.38 o -3 8 0 667.09 710.77 27.89 o -2 8 0 518.92 533.47 25.38 o -1 8 0 3288.67 3038.48 63.98 o 0 8 0 1499.03 1460.44 42.08 o 1 8 0 16.24 8.86 18.35 o 2 8 0 1014.69 971.97 37.66 o 3 8 0 477.22 459.81 30.64 o 4 8 0 345.16 396.14 31.56 o 5 8 0 38.31 27.27 39.67 o 6 8 0 168.63 220.68 44.63 o 7 8 0 3.11 -42.15 42.15 o 8 8 0 29.23 24.80 47.11 o -16 9 0 60.26 66.95 42.15 o -15 9 0 44.64 59.51 44.63 o -14 9 0 205.30 133.89 44.63 o -13 9 0 204.12 167.26 28.57 o -12 9 0 536.83 453.55 34.16 o -11 9 0 390.21 362.16 31.41 o -10 9 0 1307.41 1207.43 42.93 o -9 9 0 331.44 305.64 28.57 o -8 9 0 4402.69 4580.57 86.78 o -7 9 0 22.93 25.12 19.65 o -6 9 0 3319.55 3357.87 106.62 o -5 9 0 777.68 800.88 44.63 o -4 9 0 237.71 201.53 20.82 o -3 9 0 2.21 -10.94 22.32 o -2 9 0 569.86 485.99 26.12 o -1 9 0 4101.35 3916.17 78.01 o 0 9 0 80.67 59.51 19.29 o 1 9 0 233.79 244.27 24.36 o 2 9 0 387.27 365.32 30.64 o 3 9 0 112.88 115.99 25.38 o 4 9 0 26.29 7.01 25.38 o 5 9 0 317.16 319.86 49.59 o 6 9 0 70.20 54.55 47.11 o 7 9 0 84.29 -47.11 47.11 o -16 10 0 48.68 99.18 47.11 o -15 10 0 171.85 176.05 47.11 o -14 10 0 137.17 188.44 39.67 o -13 10 0 703.91 714.10 57.03 o -12 10 0 56.90 30.99 33.47 o -11 10 0 511.06 458.51 34.16 o -10 10 0 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145.80 150.61 26.12 o -7 13 0 182.32 172.34 47.11 o -6 13 0 939.26 943.15 40.33 o -5 13 0 310.97 331.17 29.65 o -4 13 0 16.45 0.57 22.59 o -3 13 0 54.17 72.17 24.36 o -2 13 0 402.80 419.75 38.43 o -1 13 0 0.39 2.39 35.95 o 0 13 0 62.77 59.24 24.36 o 1 13 0 178.34 190.77 29.75 o 2 13 0 119.21 115.39 43.39 o 3 13 0 36.35 71.70 30.26 o -15 14 0 97.69 131.41 42.15 o -14 14 0 320.56 433.91 49.59 o -13 14 0 32.24 66.95 37.19 o -12 14 0 97.24 57.03 37.19 o -11 14 0 490.87 520.70 47.11 o -10 14 0 123.98 137.70 27.89 o -9 14 0 9.54 37.81 24.36 o -8 14 0 7.79 -19.45 22.59 o -7 14 0 295.94 281.43 29.81 o -6 14 0 59.95 82.25 25.38 o -5 14 0 63.52 122.87 34.71 o -4 14 0 214.62 193.20 28.89 o -3 14 0 520.70 553.59 35.91 o -2 14 0 5.73 5.64 25.38 o -1 14 0 49.57 22.23 25.38 o 0 14 0 11.32 65.94 32.12 o 1 14 0 40.07 93.35 32.12 o -14 15 0 96.20 123.98 39.67 o -13 15 0 25.51 44.63 37.19 o -12 15 0 71.27 114.06 37.19 o -11 15 0 121.72 104.14 37.19 o -10 15 0 395.60 371.93 44.63 o -9 15 0 1.90 -24.09 24.36 o -8 15 0 117.26 144.31 27.13 o -7 15 0 166.30 180.35 28.89 o -6 15 0 94.06 110.02 27.13 o -5 15 0 134.44 144.91 27.89 o -4 15 0 360.50 420.99 34.93 o -3 15 0 11.65 8.00 27.13 o -2 15 0 38.92 93.55 28.89 o -1 15 0 15.47 18.78 34.71 o 0 15 0 13.64 19.31 42.15 o -11 16 0 1.88 59.51 37.19 o -10 16 0 389.61 396.72 49.59 o -9 16 0 63.75 76.86 37.19 o -8 16 0 42.46 54.55 39.67 o -7 16 0 29.28 72.37 27.89 o -6 16 0 14.98 59.73 28.89 o -5 16 0 15.19 59.84 26.12 o -4 16 0 30.02 75.55 70.67 o -3 16 0 87.57 74.47 79.34 o -2 16 0 10.85 0.00 42.15 o -7 17 0 11.14 42.15 42.15 o -6 17 0 63.74 119.02 39.67 o -5 17 0 8.07 109.10 39.67 o 5 -17 1 128.12 203.44 33.31 o 6 -17 1 117.53 119.61 30.64 o 7 -17 1 50.22 54.55 42.15 o 8 -17 1 49.26 54.55 42.15 o 10 -17 1 57.38 57.03 42.15 o 11 -17 1 9.47 64.47 42.15 o 2 -16 1 298.06 309.67 34.16 o 3 -16 1 8.20 61.99 42.15 o 4 -16 1 218.59 218.64 32.40 o 5 -16 1 210.62 218.23 31.56 o 6 -16 1 189.52 252.80 32.40 o 7 -16 1 39.85 136.37 42.15 o 8 -16 1 264.33 292.58 44.63 o 9 -16 1 51.05 49.59 37.19 o 10 -16 1 43.70 -9.92 37.19 o 11 -16 1 441.39 476.07 49.59 o 12 -16 1 264.03 203.32 42.15 o 13 -16 1 316.35 364.49 49.59 o 0 -15 1 14.00 15.82 31.56 o 1 -15 1 72.14 64.62 35.95 o 2 -15 1 1.57 -1.76 27.13 o 3 -15 1 41.97 43.48 24.36 o 4 -15 1 0.24 29.75 26.30 o 5 -15 1 538.78 506.01 35.07 o 6 -15 1 1.34 31.81 25.38 o 7 -15 1 280.89 291.90 30.64 o 8 -15 1 98.19 109.10 37.19 o 9 -15 1 39.49 57.03 34.71 o 10 -15 1 2.14 34.71 32.23 o 11 -15 1 283.41 257.87 42.15 o 12 -15 1 219.75 213.24 42.15 o 13 -15 1 1.11 69.43 39.67 o -2 -14 1 2.54 -7.44 29.75 o -1 -14 1 13.26 77.40 31.56 o 0 -14 1 124.32 142.22 29.75 o 1 -14 1 1.46 -0.55 23.23 o 2 -14 1 89.96 86.46 27.13 o 3 -14 1 238.99 224.85 28.89 o 4 -14 1 772.21 787.54 40.33 o 5 -14 1 12.86 46.49 26.03 o 6 -14 1 1234.50 1305.49 49.00 o 7 -14 1 204.31 218.03 28.05 o 8 -14 1 85.45 116.54 25.38 o 9 -14 1 1.56 14.88 32.23 o 10 -14 1 361.78 364.49 42.15 o 11 -14 1 266.59 297.54 42.15 o 12 -14 1 0.18 52.07 34.71 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