#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:05:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180957 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/37/2203708.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203708_Fobs loop_ _publ_author_name 'Li, Dan' 'Shi, Wen-Juan' 'Wu, Tao' 'Ng, Seik Weng' _publ_section_title ; Chloro[pyrimidine-2(1H)-thione-\kS]bis(triphenylphosphine-\kP)copper(I) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m776 _journal_page_last m777 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.564 _cell_angle_gamma 90.000 _cell_length_a 14.4631 _cell_length_b 10.1438 _cell_length_c 24.3932 _exptl_crystal_F_000 1520.00 _reflns_d_resolution_high 0.7696 _cod_data_source_file bt6455Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 445.50 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 377.88 -1.92 1.28 o 2 0 0 38085.73 44669.30 836.26 o 3 0 0 44.02 59.89 7.65 o 4 0 0 4972.13 5481.86 115.16 o 5 0 0 4267.02 4830.70 106.30 o 6 0 0 2325.92 2172.81 59.03 o 7 0 0 45126.45 51432.07 976.84 o 8 0 0 571.74 480.07 28.34 o 9 0 0 71.88 28.49 19.27 o 10 0 0 1857.41 1403.89 125.43 o 11 0 0 647.54 634.31 39.70 o 12 0 0 6043.17 5630.94 143.58 o 13 0 0 447.57 529.57 40.11 o 14 0 0 266.57 280.34 45.26 o 15 0 0 139.16 175.08 39.31 o 16 0 0 28.68 89.22 33.62 o 17 0 0 4.94 -5.17 25.09 o 18 0 0 16.31 41.38 29.22 o 1 1 0 58904.17 60721.30 932.58 o 2 1 0 231.34 277.35 8.84 o 3 1 0 1157.23 1222.19 21.86 o 4 1 0 6523.27 7163.00 100.54 o 5 1 0 5605.65 5698.55 83.28 o 6 1 0 3466.24 3412.03 58.15 o 7 1 0 6008.63 6044.53 91.66 o 8 1 0 18040.58 18598.41 302.66 o 9 1 0 1092.88 971.61 43.47 o 10 1 0 3217.95 2970.40 70.73 o 11 1 0 3979.69 3688.77 83.78 o 12 1 0 2117.70 2237.68 70.13 o 13 1 0 2425.37 2268.36 64.55 o 14 1 0 1579.72 1697.24 56.07 o 15 1 0 10.74 27.74 15.87 o 16 1 0 133.12 143.18 22.87 o 17 1 0 17.69 42.16 19.92 o 18 1 0 264.01 222.21 32.82 o 0 2 0 14815.59 16507.11 313.86 o 1 2 0 19194.65 21885.76 293.18 o 2 2 0 2496.50 2616.10 46.18 o 3 2 0 459.53 438.59 19.11 o 4 2 0 1963.87 1908.45 32.81 o 5 2 0 61.17 84.17 7.56 o 6 2 0 1017.71 961.29 22.55 o 7 2 0 5617.63 5506.12 115.41 o 8 2 0 611.69 671.89 21.05 o 9 2 0 10246.92 10199.11 149.42 o 10 2 0 775.44 710.14 38.34 o 11 2 0 1470.54 1523.31 58.51 o 12 2 0 3992.33 3767.73 87.34 o 13 2 0 2896.60 2939.03 76.11 o 14 2 0 340.72 332.67 38.85 o 15 2 0 1045.88 1077.68 85.82 o 16 2 0 9.12 24.60 22.74 o 17 2 0 545.31 496.27 39.81 o 18 2 0 51.79 85.30 21.59 o 1 3 0 15930.92 17831.15 240.92 o 2 3 0 291.60 342.84 12.73 o 3 3 0 3811.00 4029.81 70.57 o 4 3 0 8472.87 9530.97 156.16 o 5 3 0 2427.74 2213.14 42.26 o 6 3 0 228.07 245.66 11.97 o 7 3 0 2493.57 2305.30 43.06 o 8 3 0 5455.43 5583.75 88.07 o 9 3 0 2687.73 2654.85 87.77 o 10 3 0 135.53 151.89 17.34 o 11 3 0 6336.89 5899.87 351.59 o 12 3 0 1452.97 1337.15 83.90 o 13 3 0 1000.35 980.31 41.65 o 14 3 0 346.18 346.29 33.16 o 15 3 0 238.33 159.27 23.26 o 16 3 0 68.63 90.37 20.40 o 17 3 0 64.25 116.19 21.50 o 18 3 0 108.80 160.34 43.71 o 0 4 0 20888.63 23763.69 452.95 o 1 4 0 270.20 220.58 8.43 o 2 4 0 11534.81 13028.42 180.44 o 3 4 0 3300.56 3742.46 59.04 o 4 4 0 1159.02 1098.34 27.99 o 5 4 0 1098.61 1124.69 30.10 o 6 4 0 4765.06 4800.46 75.65 o 7 4 0 1517.74 1646.45 34.83 o 8 4 0 166.51 185.13 16.14 o 9 4 0 2294.53 2218.21 56.04 o 10 4 0 4038.02 4016.88 86.90 o 11 4 0 38.25 56.32 13.64 o 12 4 0 356.82 368.62 36.86 o 13 4 0 230.25 223.42 23.46 o 14 4 0 149.74 152.24 21.69 o 15 4 0 0.61 -25.01 16.67 o 16 4 0 18.16 5.27 50.69 o 17 4 0 6.13 -8.94 17.97 o 1 5 0 1811.90 2040.17 35.55 o 2 5 0 168.17 169.65 13.66 o 3 5 0 331.26 476.20 15.08 o 4 5 0 449.15 512.40 16.64 o 5 5 0 1525.81 1621.30 80.90 o 6 5 0 630.79 656.26 20.26 o 7 5 0 199.07 203.51 13.28 o 8 5 0 1810.05 1821.27 39.39 o 9 5 0 114.14 121.87 16.81 o 10 5 0 289.26 308.68 70.73 o 11 5 0 269.22 300.03 42.28 o 12 5 0 35.69 27.52 17.98 o 13 5 0 78.85 91.36 23.11 o 14 5 0 431.28 394.66 73.19 o 15 5 0 104.08 94.16 26.41 o 16 5 0 40.19 66.80 25.59 o 17 5 0 82.83 70.86 24.74 o 0 6 0 230.82 253.73 15.04 o 1 6 0 14.39 17.26 4.37 o 2 6 0 949.65 940.54 28.57 o 3 6 0 92.37 110.27 11.97 o 4 6 0 500.87 520.09 23.55 o 5 6 0 945.37 912.56 60.74 o 6 6 0 16.99 8.67 10.57 o 7 6 0 0.25 2.32 9.47 o 8 6 0 10.68 8.88 11.05 o 9 6 0 337.57 340.76 59.09 o 10 6 0 8.88 -6.47 14.44 o 11 6 0 7.80 -7.40 15.54 o 12 6 0 199.19 223.00 31.19 o 13 6 0 76.00 125.84 26.57 o 14 6 0 6.85 14.57 20.66 o 15 6 0 9.19 35.18 20.68 o 16 6 0 46.03 50.57 24.14 o 1 7 0 155.15 154.09 21.18 o 2 7 0 65.98 56.47 18.75 o 3 7 0 53.79 77.99 18.07 o 4 7 0 1900.79 2028.03 61.63 o 5 7 0 261.81 255.93 20.51 o 6 7 0 66.06 78.08 14.20 o 7 7 0 482.41 450.51 33.77 o 8 7 0 3.14 10.96 14.16 o 9 7 0 30.79 32.13 15.98 o 10 7 0 548.67 570.23 42.23 o 11 7 0 13.22 21.06 18.88 o 12 7 0 231.45 202.99 31.54 o 13 7 0 41.24 -3.42 20.21 o 14 7 0 303.13 281.79 38.68 o 15 7 0 94.33 109.55 33.23 o 0 8 0 809.79 803.26 58.71 o 1 8 0 597.90 690.25 61.16 o 2 8 0 4299.49 4054.10 137.58 o 3 8 0 145.68 145.91 28.97 o 4 8 0 492.84 497.48 68.40 o 5 8 0 180.52 245.45 29.32 o 6 8 0 7.41 -0.77 15.65 o 7 8 0 4.56 1.46 14.83 o 8 8 0 141.55 131.13 20.01 o 9 8 0 1009.61 975.06 52.04 o 10 8 0 568.51 564.72 36.17 o 11 8 0 93.09 94.27 24.85 o 12 8 0 130.92 127.30 35.04 o 13 8 0 146.75 174.35 32.22 o 14 8 0 5.91 38.91 36.72 o 1 9 0 1093.86 976.41 87.28 o 2 9 0 35.97 47.56 17.96 o 3 9 0 1761.16 1612.05 71.38 o 4 9 0 16.38 -4.34 15.08 o 5 9 0 2350.70 2093.20 88.19 o 6 9 0 6.44 12.15 16.64 o 7 9 0 313.19 421.99 54.83 o 8 9 0 323.00 347.37 38.40 o 9 9 0 559.69 492.37 45.91 o 10 9 0 337.50 274.03 36.62 o 11 9 0 73.36 68.70 25.05 o 12 9 0 48.06 69.83 55.09 o 13 9 0 1.06 22.67 22.33 o 0 10 0 12.34 5.17 19.65 o 1 10 0 142.88 121.83 24.95 o 2 10 0 464.94 385.72 57.15 o 3 10 0 36.42 58.58 21.21 o 4 10 0 134.85 179.23 29.24 o 5 10 0 18.73 27.66 20.07 o 6 10 0 201.80 177.38 36.85 o 7 10 0 47.47 64.68 23.47 o 8 10 0 78.49 78.82 25.43 o 9 10 0 587.25 495.93 47.68 o 10 10 0 41.89 70.54 25.88 o 11 10 0 256.73 334.78 43.02 o 1 11 0 18.71 4.20 19.44 o 2 11 0 1.25 6.22 17.41 o 3 11 0 38.01 42.12 21.39 o 4 11 0 2.16 -10.74 19.03 o 5 11 0 16.28 -5.53 19.71 o 6 11 0 5.80 14.16 20.47 o 7 11 0 79.16 63.70 25.19 o 8 11 0 611.69 587.04 53.69 o 9 11 0 30.69 39.95 29.74 o 0 12 0 1463.24 1597.73 108.10 o 1 12 0 50.91 31.29 44.22 o 2 12 0 360.11 404.34 44.80 o 3 12 0 6.99 3.92 20.26 o 4 12 0 102.15 77.59 25.89 o 5 12 0 31.60 55.65 25.71 o 6 12 0 163.75 193.48 34.43 o 7 12 0 35.69 61.67 26.79 o -18 1 1 8.85 46.33 20.44 o -17 1 1 40.13 42.37 21.58 o -16 1 1 39.17 35.02 17.62 o -15 1 1 5.56 6.50 20.31 o -14 1 1 16.59 38.82 14.45 o -13 1 1 191.42 190.56 22.02 o -12 1 1 117.68 121.38 18.31 o -11 1 1 88.90 87.19 15.77 o -10 1 1 1915.37 2082.64 54.92 o -9 1 1 1738.42 1727.42 59.28 o -8 1 1 3110.74 3374.60 71.37 o -7 1 1 5290.25 5344.94 99.44 o -6 1 1 6348.86 6706.92 97.89 o -5 1 1 6394.01 6925.13 98.98 o -4 1 1 6073.96 6482.83 91.75 o -3 1 1 16381.54 18534.78 245.46 o -2 1 1 5122.33 5429.13 88.05 o -1 1 1 6261.23 7195.87 112.89 o 0 1 1 3233.99 3660.82 59.36 o 1 1 1 1915.62 1980.15 42.14 o 2 1 1 588.83 590.29 11.94 o 3 1 1 4728.34 5083.98 72.08 o 4 1 1 9519.17 10890.10 148.89 o 5 1 1 8149.57 8390.69 118.29 o 6 1 1 2659.56 2790.98 47.47 o 7 1 1 63.92 64.76 8.12 o 8 1 1 49.98 39.22 8.00 o 9 1 1 2586.25 2448.13 58.64 o 10 1 1 329.04 280.59 21.31 o 11 1 1 1100.29 1022.55 42.06 o 12 1 1 164.62 156.85 19.79 o 13 1 1 291.73 282.27 25.82 o 14 1 1 33.32 32.29 14.92 o 15 1 1 20.52 13.47 27.98 o 16 1 1 3.38 4.54 14.46 o 17 1 1 0.18 42.39 49.91 o 18 1 1 0.77 11.70 19.47 o -18 2 1 68.29 100.18 20.03 o -17 2 1 26.29 3.28 15.49 o -16 2 1 20.50 25.89 26.08 o -15 2 1 718.15 707.99 63.54 o -14 2 1 663.56 666.92 51.01 o -13 2 1 123.57 141.49 20.32 o -12 2 1 297.39 336.05 26.20 o -11 2 1 4.84 7.75 11.18 o -10 2 1 109.87 111.80 15.89 o -9 2 1 0.52 1.29 6.55 o -8 2 1 511.08 415.03 16.66 o -7 2 1 181.74 192.92 15.49 o -6 2 1 1957.75 1869.92 34.67 o -5 2 1 1957.48 2232.68 38.40 o -4 2 1 36.91 13.40 4.69 o -3 2 1 9940.55 10991.45 175.14 o -2 2 1 1040.30 945.50 21.11 o -1 2 1 305.71 384.50 9.62 o 0 2 1 5483.14 6163.11 100.00 o 1 2 1 33595.94 38280.69 589.10 o 2 2 1 11026.64 12469.83 195.29 o 3 2 1 4073.99 4415.61 64.25 o 4 2 1 341.53 322.07 11.59 o 5 2 1 743.34 573.86 16.21 o 6 2 1 1151.06 1226.31 26.67 o 7 2 1 4307.14 4400.84 76.75 o 8 2 1 2233.40 2390.15 45.59 o 9 2 1 506.06 496.01 19.47 o 10 2 1 40.52 54.48 9.93 o 11 2 1 91.62 69.81 14.47 o 12 2 1 18.66 30.86 14.43 o 13 2 1 1050.23 1041.96 42.69 o 14 2 1 87.97 107.60 19.14 o 15 2 1 44.05 54.76 20.47 o 16 2 1 328.55 319.03 29.76 o 17 2 1 35.54 23.07 16.09 o 18 2 1 43.82 86.07 21.08 o -18 3 1 40.82 37.69 20.44 o -17 3 1 116.00 121.40 22.44 o -16 3 1 516.83 546.37 37.86 o -15 3 1 19.91 13.18 17.68 o -14 3 1 1537.95 1478.99 52.53 o -13 3 1 1094.71 988.31 41.43 o -12 3 1 101.95 113.73 18.56 o -11 3 1 42.39 28.98 14.41 o -10 3 1 122.96 108.95 16.12 o -9 3 1 292.97 333.74 24.35 o -8 3 1 1872.31 1829.45 50.77 o -7 3 1 3495.90 3425.30 57.65 o -6 3 1 201.24 219.36 11.22 o -5 3 1 738.88 593.09 23.00 o -4 3 1 405.67 425.91 16.09 o -3 3 1 1990.58 1879.84 53.96 o -2 3 1 49.21 49.69 4.90 o -1 3 1 17176.88 19263.91 259.82 o 0 3 1 895.20 960.78 19.71 o 1 3 1 3620.15 4016.39 70.63 o 2 3 1 294.06 282.64 20.05 o 3 3 1 56.49 70.30 9.95 o 4 3 1 7645.14 8313.61 117.05 o 5 3 1 229.55 231.11 11.03 o 6 3 1 7514.25 7716.94 112.46 o 7 3 1 201.57 214.50 12.35 o 8 3 1 3386.29 3116.43 55.82 o 9 3 1 810.53 824.44 25.04 o 10 3 1 928.89 847.96 80.27 o 11 3 1 1416.99 1267.63 118.10 o 12 3 1 947.66 883.13 39.11 o 13 3 1 409.75 398.66 29.45 o 14 3 1 305.04 311.48 38.50 o 15 3 1 876.88 945.86 69.21 o 16 3 1 122.37 161.57 22.98 o 17 3 1 99.07 138.17 22.52 o 18 3 1 183.16 253.96 53.53 o -17 4 1 3.94 18.02 19.44 o -16 4 1 179.42 197.30 34.02 o -15 4 1 96.56 90.03 24.97 o -14 4 1 46.46 64.12 17.23 o -13 4 1 969.62 1014.33 43.57 o -12 4 1 894.01 864.69 38.08 o -11 4 1 645.29 639.09 32.03 o -10 4 1 486.39 467.50 26.80 o -9 4 1 40.93 42.09 12.76 o -8 4 1 796.88 732.82 22.43 o -7 4 1 1255.80 1239.92 29.00 o -6 4 1 11993.98 11996.58 168.55 o -5 4 1 3433.24 3406.94 66.55 o -4 4 1 3874.33 3782.63 69.96 o -3 4 1 251.39 263.92 10.70 o -2 4 1 25894.12 29138.38 392.08 o -1 4 1 3216.40 3438.23 65.91 o 0 4 1 5365.50 5878.97 85.27 o 1 4 1 19332.45 21849.79 344.85 o 2 4 1 5435.87 6270.41 108.99 o 3 4 1 14971.31 17198.10 236.29 o 4 4 1 5027.00 5372.51 93.86 o 5 4 1 13474.67 14292.59 196.99 o 6 4 1 1273.51 1268.24 30.24 o 7 4 1 7271.19 7284.90 109.90 o 8 4 1 39.06 37.79 8.65 o 9 4 1 74.52 73.63 11.20 o 10 4 1 178.71 164.94 18.11 o 11 4 1 25.56 46.23 13.12 o 12 4 1 56.30 49.72 15.38 o 13 4 1 4.91 2.22 12.47 o 14 4 1 17.36 32.12 19.01 o 15 4 1 38.41 42.94 21.62 o 16 4 1 71.96 100.67 27.58 o 17 4 1 155.49 149.14 31.04 o -17 5 1 40.48 64.29 24.34 o -16 5 1 160.39 246.60 42.80 o -15 5 1 42.52 57.00 23.68 o -14 5 1 132.26 134.08 27.86 o -13 5 1 140.72 162.71 28.20 o -12 5 1 0.92 -22.50 15.00 o -11 5 1 658.25 632.55 43.34 o -10 5 1 5.58 -1.34 13.37 o -9 5 1 129.53 131.36 15.90 o -8 5 1 2088.18 2068.42 42.63 o -7 5 1 6432.37 6232.84 263.49 o -6 5 1 1636.78 1500.02 38.87 o -5 5 1 4857.76 4725.62 112.68 o -4 5 1 617.03 530.37 16.97 o -3 5 1 2760.72 2460.23 43.32 o -2 5 1 12.68 16.68 6.76 o -1 5 1 2790.47 2638.30 43.90 o 0 5 1 3352.82 3680.45 57.75 o 1 5 1 645.26 664.27 29.60 o 2 5 1 5195.04 5637.70 101.87 o 3 5 1 159.97 184.58 13.90 o 4 5 1 24.86 24.20 5.58 o 5 5 1 2080.48 2060.44 45.38 o 6 5 1 5208.12 4876.43 81.11 o 7 5 1 249.60 249.44 18.51 o 8 5 1 1756.76 1648.69 57.86 o 9 5 1 346.46 309.38 29.30 o 10 5 1 92.75 86.23 19.73 o 11 5 1 927.92 965.48 51.28 o 12 5 1 841.93 788.56 49.46 o 13 5 1 297.04 314.13 35.43 o 14 5 1 61.74 13.23 51.34 o 15 5 1 383.68 400.43 43.06 o 16 5 1 63.58 98.08 26.29 o 17 5 1 52.42 43.65 32.97 o -16 6 1 28.55 34.53 22.30 o -15 6 1 1134.95 1149.39 67.17 o -14 6 1 356.00 404.97 69.83 o -13 6 1 443.00 437.09 60.13 o -12 6 1 23.38 18.88 17.92 o -11 6 1 417.62 410.45 37.58 o -10 6 1 168.62 209.75 27.79 o -9 6 1 360.33 309.81 31.11 o -8 6 1 2105.80 1836.44 96.72 o -7 6 1 216.05 220.35 17.58 o -6 6 1 1983.47 1984.51 63.32 o -5 6 1 28.19 38.49 10.07 o -4 6 1 805.10 780.94 33.61 o -3 6 1 81.55 55.40 13.21 o -2 6 1 471.08 337.97 30.35 o -1 6 1 4.17 8.25 6.75 o 0 6 1 89.78 122.44 13.03 o 1 6 1 1713.38 1758.75 41.83 o 2 6 1 1969.38 1879.32 45.04 o 3 6 1 541.19 483.63 21.61 o 4 6 1 33.46 36.54 9.70 o 5 6 1 1324.63 1074.82 71.07 o 6 6 1 244.57 220.09 19.12 o 7 6 1 2790.11 2859.77 64.51 o 8 6 1 514.64 470.77 24.82 o 9 6 1 423.32 411.73 57.28 o 10 6 1 145.14 190.54 26.89 o 11 6 1 724.06 606.68 43.58 o 12 6 1 99.32 109.13 34.14 o 13 6 1 721.39 628.16 48.24 o 14 6 1 1215.57 1112.10 63.91 o 15 6 1 73.08 55.21 52.37 o 16 6 1 476.15 480.44 49.56 o -15 7 1 2.75 -0.90 21.39 o -14 7 1 413.73 371.54 57.28 o -13 7 1 89.82 113.09 36.59 o -12 7 1 2.71 -2.21 17.59 o -11 7 1 1.72 -8.93 15.22 o -10 7 1 156.81 184.97 43.84 o -9 7 1 73.34 96.29 21.64 o -8 7 1 50.02 66.06 17.93 o -7 7 1 3718.16 3600.63 83.51 o -6 7 1 1331.10 1260.50 41.51 o -5 7 1 755.47 698.47 34.73 o -4 7 1 15.00 23.16 9.29 o -3 7 1 647.07 720.88 38.24 o -2 7 1 1293.59 1252.77 50.27 o -1 7 1 597.73 655.07 51.08 o 0 7 1 59.34 43.60 14.44 o 1 7 1 1875.11 1674.50 58.42 o 2 7 1 161.33 150.70 20.63 o 3 7 1 527.47 463.76 32.35 o 4 7 1 902.00 881.17 31.96 o 5 7 1 50.66 63.05 12.88 o 6 7 1 3454.30 3383.97 78.54 o 7 7 1 50.78 45.37 11.45 o 8 7 1 447.82 435.08 28.76 o 9 7 1 9.39 11.98 13.88 o 10 7 1 116.33 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