#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2203713.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203713_Fobs loop_ _publ_author_name 'Gao, Shan' 'Zhang, Zhu-Yan' 'Huo, Li-Hua' 'Zhao, Jing-Gui' 'Zain, Sharifuddin M.' 'Ng, Seik Weng' _publ_section_title ; (4-Oxo-1,4-dihydropyridin-1-yl)acetic acid ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1006 _journal_page_last o1008 _journal_volume 60 _journal_year 2004 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.7413 _cell_length_b 9.5950 _cell_length_c 15.0688 _exptl_crystal_F_000 320.00 _reflns_d_resolution_high 0.7705 _[local]_cod_data_source_file bt6460Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gao29 in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 65.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 348.30 358.06 8.41 o 4 0 0 68.52 47.53 3.19 o 6 0 0 9.65 -0.17 0.62 o 1 1 0 1.92 0.68 0.07 o 2 1 0 54.07 56.55 5.00 o 3 1 0 73.15 82.45 2.23 o 4 1 0 1.13 2.20 0.36 o 5 1 0 5.20 4.76 1.02 o 6 1 0 17.26 0.95 0.62 o 0 2 0 891.68 871.12 17.59 o 1 2 0 123.20 100.74 1.73 o 2 2 0 23.18 26.26 0.50 o 3 2 0 0.33 0.19 0.38 o 4 2 0 0.66 0.82 0.19 o 5 2 0 2.93 3.45 0.50 o 6 2 0 24.46 25.45 3.67 o 1 3 0 1102.71 1100.95 11.12 o 2 3 0 101.27 82.48 1.15 o 3 3 0 67.67 82.65 1.73 o 4 3 0 6.60 7.83 0.25 o 5 3 0 52.09 52.44 2.84 o 0 4 0 3499.33 3719.83 31.20 o 1 4 0 55.61 52.81 0.85 o 2 4 0 12.94 15.00 0.32 o 3 4 0 5.71 8.07 0.99 o 4 4 0 5.72 5.14 0.29 o 5 4 0 2.19 1.52 0.93 o 1 5 0 76.16 82.02 2.68 o 2 5 0 209.05 192.63 0.99 o 3 5 0 31.06 26.38 1.05 o 4 5 0 28.78 27.05 1.08 o 5 5 0 1.86 2.34 0.80 o 0 6 0 157.31 157.94 3.99 o 1 6 0 35.10 37.14 1.34 o 2 6 0 121.90 116.71 2.90 o 3 6 0 35.75 36.51 0.90 o 4 6 0 30.68 34.15 0.95 o 5 6 0 0.02 0.08 0.88 o 1 7 0 13.75 14.17 0.71 o 2 7 0 0.04 0.44 0.21 o 3 7 0 46.05 51.25 1.03 o 4 7 0 30.71 39.60 1.38 o 5 7 0 0.51 2.30 1.32 o 0 8 0 6.25 5.95 0.39 o 1 8 0 0.64 1.21 0.26 o 2 8 0 20.73 22.58 1.20 o 3 8 0 8.18 9.98 0.42 o 4 8 0 4.26 4.90 1.05 o 1 9 0 11.54 11.93 0.44 o 2 9 0 33.48 29.44 1.32 o 3 9 0 18.45 17.57 0.54 o 4 9 0 0.22 -0.11 1.25 o 0 10 0 170.17 156.07 6.38 o 1 10 0 4.82 5.59 0.35 o 2 10 0 1.35 1.60 0.33 o 3 10 0 0.06 0.94 0.60 o 1 11 0 14.05 11.38 0.70 o 2 11 0 9.00 8.82 0.60 o 0 12 0 0.20 0.18 0.68 o 1 12 0 5.14 5.64 0.46 o 1 0 1 87.53 70.43 0.82 o 2 0 1 145.01 138.59 2.89 o 3 0 1 212.65 191.35 4.43 o 4 0 1 12.44 11.98 0.52 o 5 0 1 0.05 0.44 0.27 o 6 0 1 0.01 0.44 0.36 o 1 1 1 4104.99 4331.15 18.81 o 2 1 1 81.06 82.06 1.40 o 3 1 1 239.11 270.60 4.20 o 4 1 1 1.07 0.56 0.15 o 5 1 1 19.30 20.15 0.77 o 6 1 1 1.28 0.35 0.39 o 0 2 1 1730.73 1672.19 17.77 o 1 2 1 397.68 391.11 4.91 o 2 2 1 265.33 271.68 2.58 o 3 2 1 108.20 111.89 1.64 o 4 2 1 35.79 34.40 0.57 o 5 2 1 20.80 23.24 0.87 o 6 2 1 7.40 -0.51 0.51 o 0 3 1 850.12 776.62 9.15 o 1 3 1 600.25 608.65 8.14 o 2 3 1 192.94 176.26 1.42 o 3 3 1 210.93 235.64 5.20 o 4 3 1 61.47 64.38 1.07 o 5 3 1 6.66 5.51 0.33 o 0 4 1 96.99 95.01 2.36 o 1 4 1 42.53 41.38 0.86 o 2 4 1 300.31 296.59 4.48 o 3 4 1 73.57 65.77 1.44 o 4 4 1 19.25 18.76 0.50 o 5 4 1 10.62 10.64 0.90 o 0 5 1 7.17 7.13 0.23 o 1 5 1 438.15 463.15 5.24 o 2 5 1 8.04 9.27 0.17 o 3 5 1 77.97 79.07 1.66 o 4 5 1 10.29 10.57 0.55 o 5 5 1 6.05 8.29 0.88 o 0 6 1 32.89 44.63 1.08 o 1 6 1 10.71 12.53 0.20 o 2 6 1 24.91 24.21 0.31 o 3 6 1 55.63 61.80 1.34 o 4 6 1 21.57 22.62 1.08 o 5 6 1 6.56 8.59 1.06 o 0 7 1 0.06 0.14 0.23 o 1 7 1 17.23 20.38 0.41 o 2 7 1 4.31 4.83 0.20 o 3 7 1 266.96 298.85 4.41 o 4 7 1 13.46 15.23 0.91 o 5 7 1 8.38 11.10 0.86 o 0 8 1 89.43 76.02 1.44 o 1 8 1 6.30 6.97 0.21 o 2 8 1 115.49 114.09 1.35 o 3 8 1 80.93 76.88 1.68 o 4 8 1 3.32 3.73 0.75 o 0 9 1 0.13 0.24 0.29 o 1 9 1 37.80 36.75 0.77 o 2 9 1 26.81 26.14 0.67 o 3 9 1 1.36 1.62 0.41 o 4 9 1 0.22 -0.06 0.72 o 0 10 1 60.07 59.65 2.01 o 1 10 1 1.44 1.16 0.23 o 2 10 1 12.79 10.48 0.38 o 3 10 1 20.52 18.49 1.02 o 0 11 1 5.54 7.51 0.47 o 1 11 1 0.26 0.68 0.27 o 2 11 1 2.67 2.50 0.28 o 0 12 1 4.47 6.88 0.54 o 1 12 1 5.14 4.55 0.37 o 1 0 2 24.95 18.67 0.41 o 2 0 2 67.05 66.47 1.58 o 3 0 2 20.71 22.01 0.44 o 4 0 2 14.91 17.14 0.31 o 5 0 2 22.51 27.00 0.52 o 6 0 2 0.72 0.73 0.40 o 0 1 2 438.28 380.06 4.45 o 1 1 2 4197.41 4347.70 26.60 o 2 1 2 140.50 151.67 1.01 o 3 1 2 78.10 85.41 0.98 o 4 1 2 0.73 0.52 0.16 o 5 1 2 43.69 55.53 2.14 o 6 1 2 13.22 -0.02 0.51 o 0 2 2 4351.91 4458.71 25.37 o 1 2 2 93.72 96.80 1.53 o 2 2 2 1120.93 1185.08 21.24 o 3 2 2 6.99 9.56 0.38 o 4 2 2 11.77 14.55 0.56 o 5 2 2 5.35 6.19 0.64 o 6 2 2 1.76 1.75 0.66 o 0 3 2 256.07 202.71 2.96 o 1 3 2 81.65 85.87 2.08 o 2 3 2 27.81 25.97 0.74 o 3 3 2 1.39 2.44 0.12 o 4 3 2 9.01 8.20 0.21 o 5 3 2 14.11 14.34 0.43 o 0 4 2 169.75 181.56 2.18 o 1 4 2 292.51 263.67 2.27 o 2 4 2 4.24 6.53 0.25 o 3 4 2 30.22 27.57 0.57 o 4 4 2 40.31 45.63 1.92 o 5 4 2 12.60 10.86 0.51 o 0 5 2 138.10 152.60 4.41 o 1 5 2 28.66 33.10 0.40 o 2 5 2 152.16 130.92 1.73 o 3 5 2 133.93 125.92 2.55 o 4 5 2 1.10 1.07 0.37 o 5 5 2 4.22 6.14 0.78 o 0 6 2 125.64 118.79 2.16 o 1 6 2 3.17 2.52 0.13 o 2 6 2 145.10 132.94 1.59 o 3 6 2 30.76 35.01 0.66 o 4 6 2 76.70 83.06 3.23 o 5 6 2 6.27 7.41 0.67 o 0 7 2 47.24 41.67 0.45 o 1 7 2 16.89 15.84 0.31 o 2 7 2 80.19 77.32 1.19 o 3 7 2 26.59 23.14 0.69 o 4 7 2 7.08 6.94 0.58 o 5 7 2 4.71 7.68 0.75 o 0 8 2 33.39 37.57 0.91 o 1 8 2 33.58 31.39 0.58 o 2 8 2 151.71 161.09 2.78 o 3 8 2 4.77 5.45 0.59 o 4 8 2 5.56 6.89 0.58 o 0 9 2 6.39 4.39 0.39 o 1 9 2 106.94 99.76 1.59 o 2 9 2 14.53 15.13 0.66 o 3 9 2 0.94 1.04 0.37 o 4 9 2 2.59 3.70 0.76 o 0 10 2 1.56 1.73 0.37 o 1 10 2 10.21 11.78 0.37 o 2 10 2 4.89 5.60 0.30 o 3 10 2 1.60 2.13 0.50 o 0 11 2 3.03 2.98 0.49 o 1 11 2 34.90 33.19 0.78 o 2 11 2 5.82 5.32 0.37 o 0 12 2 0.36 -0.11 0.56 o 1 12 2 7.42 7.22 0.37 o 1 0 3 114.49 137.60 2.14 o 2 0 3 67.57 83.75 1.08 o 3 0 3 9.99 12.19 0.80 o 4 0 3 20.24 22.91 0.62 o 5 0 3 28.91 36.00 2.02 o 6 0 3 3.16 2.91 0.90 o 0 1 3 309.72 277.63 1.81 o 1 1 3 3503.80 3635.55 44.53 o 2 1 3 233.08 257.10 3.48 o 3 1 3 88.91 97.37 2.26 o 4 1 3 66.49 68.31 2.56 o 5 1 3 10.45 10.72 0.39 o 6 1 3 4.06 3.40 1.31 o 0 2 3 801.00 816.26 57.73 o 1 2 3 273.58 309.79 8.31 o 2 2 3 103.81 103.65 1.64 o 3 2 3 89.82 100.69 1.99 o 4 2 3 73.52 94.61 1.49 o 5 2 3 1.79 1.73 0.25 o 6 2 3 1.90 1.77 0.40 o 0 3 3 33.66 39.07 0.51 o 1 3 3 8.46 7.44 0.28 o 2 3 3 312.90 327.48 3.87 o 3 3 3 107.88 118.75 1.81 o 4 3 3 5.07 6.66 0.32 o 5 3 3 20.47 22.07 0.64 o 0 4 3 141.92 131.24 1.38 o 1 4 3 469.99 458.08 8.40 o 2 4 3 190.62 197.43 1.65 o 3 4 3 9.19 9.49 0.41 o 4 4 3 13.92 14.86 0.44 o 5 4 3 1.64 2.14 0.36 o 0 5 3 265.49 245.72 7.70 o 1 5 3 82.60 81.11 1.33 o 2 5 3 244.14 240.20 3.25 o 3 5 3 96.70 94.99 1.33 o 4 5 3 52.53 56.84 0.89 o 5 5 3 6.98 6.43 0.48 o 0 6 3 1.35 1.69 0.22 o 1 6 3 26.64 23.07 0.29 o 2 6 3 184.85 169.69 2.51 o 3 6 3 127.51 122.23 1.78 o 4 6 3 25.67 33.88 1.09 o 5 6 3 8.04 9.10 0.83 o 0 7 3 23.36 23.52 0.84 o 1 7 3 164.91 160.60 2.22 o 2 7 3 155.59 144.63 1.89 o 3 7 3 32.17 33.98 0.47 o 4 7 3 12.04 16.48 0.49 o 5 7 3 1.42 1.31 1.18 o 0 8 3 0.03 0.40 0.34 o 1 8 3 14.57 16.00 0.34 o 2 8 3 3.75 4.99 0.26 o 3 8 3 10.38 9.48 0.52 o 4 8 3 8.69 9.12 0.54 o 0 9 3 4.60 4.81 0.36 o 1 9 3 15.29 15.64 0.58 o 2 9 3 13.40 14.72 0.56 o 3 9 3 12.66 14.60 0.42 o 4 9 3 13.56 14.97 0.80 o 0 10 3 4.24 7.79 0.42 o 1 10 3 5.54 4.76 0.32 o 2 10 3 6.93 5.53 0.46 o 3 10 3 6.62 7.19 0.54 o 0 11 3 6.13 4.45 0.41 o 1 11 3 1.26 1.26 0.31 o 2 11 3 16.39 15.36 0.73 o 0 12 3 18.61 21.64 0.81 o 1 12 3 0.45 1.15 0.41 o 0 0 4 847.59 735.45 27.56 o 1 0 4 2916.08 3011.26 74.65 o 2 0 4 740.56 814.32 12.15 o 3 0 4 24.16 25.02 0.54 o 4 0 4 106.86 69.49 2.81 o 5 0 4 3.55 3.17 1.09 o 6 0 4 1.13 1.24 0.43 o 0 1 4 1483.66 1568.81 35.39 o 1 1 4 55.92 59.94 1.11 o 2 1 4 179.38 172.30 1.52 o 3 1 4 1.88 2.82 0.44 o 4 1 4 4.34 3.45 0.41 o 5 1 4 14.30 17.55 0.73 o 6 1 4 0.02 1.09 0.40 o 0 2 4 40.18 44.63 0.52 o 1 2 4 1149.23 1232.34 22.24 o 2 2 4 232.21 231.21 2.41 o 3 2 4 36.04 36.66 0.30 o 4 2 4 72.15 80.86 2.39 o 5 2 4 14.94 12.35 0.61 o 0 3 4 292.61 281.83 7.26 o 1 3 4 1432.34 1570.91 33.72 o 2 3 4 236.27 269.02 3.61 o 3 3 4 0.78 1.66 0.20 o 4 3 4 19.30 23.95 0.50 o 5 3 4 2.66 2.10 0.34 o 0 4 4 174.81 151.90 2.13 o 1 4 4 286.89 254.70 4.55 o 2 4 4 221.22 217.06 2.74 o 3 4 4 29.65 32.28 0.46 o 4 4 4 54.40 57.18 1.32 o 5 4 4 6.62 7.23 0.40 o 0 5 4 138.42 129.43 2.79 o 1 5 4 16.04 14.07 0.35 o 2 5 4 109.24 97.26 1.69 o 3 5 4 9.87 7.74 0.27 o 4 5 4 0.08 0.25 0.33 o 5 5 4 2.85 3.02 0.59 o 0 6 4 293.86 302.66 4.54 o 1 6 4 199.29 183.91 1.96 o 2 6 4 38.51 34.12 0.78 o 3 6 4 17.09 16.77 0.40 o 4 6 4 65.29 68.37 1.61 o 5 6 4 1.14 1.10 0.63 o 0 7 4 3.17 2.66 0.25 o 1 7 4 167.01 156.64 1.36 o 2 7 4 127.44 122.73 2.89 o 3 7 4 0.66 0.84 0.34 o 4 7 4 6.99 6.67 0.52 o 0 8 4 5.52 6.89 0.44 o 1 8 4 17.87 17.30 0.47 o 2 8 4 35.53 36.24 0.86 o 3 8 4 27.01 27.22 0.88 o 4 8 4 26.91 28.52 0.92 o 0 9 4 0.25 0.93 0.31 o 1 9 4 37.84 39.61 1.18 o 2 9 4 4.41 5.34 0.36 o 3 9 4 6.60 6.03 0.40 o 4 9 4 10.21 11.96 0.82 o 0 10 4 4.17 4.60 0.40 o 1 10 4 6.08 5.89 0.35 o 2 10 4 16.42 13.04 0.76 o 3 10 4 3.49 1.84 0.45 o 0 11 4 0.00 0.35 0.43 o 1 11 4 6.90 7.10 0.39 o 2 11 4 16.07 19.28 1.17 o 0 12 4 1.65 2.11 0.60 o 1 12 4 7.55 10.36 0.49 o 1 0 5 2142.20 2435.35 54.09 o 2 0 5 1144.40 1252.27 14.21 o 3 0 5 0.11 0.40 0.27 o 4 0 5 0.29 0.23 0.30 o 5 0 5 8.79 11.77 0.69 o 0 1 5 5.47 4.20 0.18 o 1 1 5 1722.22 1809.92 25.03 o 2 1 5 354.28 373.36 4.24 o 3 1 5 93.53 95.46 1.39 o 4 1 5 51.28 61.63 1.66 o 5 1 5 24.34 29.01 1.57 o 0 2 5 51.57 52.19 0.82 o 1 2 5 226.84 245.46 4.77 o 2 2 5 356.69 352.60 4.80 o 3 2 5 45.71 46.02 0.69 o 4 2 5 48.54 54.27 1.71 o 5 2 5 9.75 9.58 0.54 o 0 3 5 33.16 37.45 2.06 o 1 3 5 6.89 7.94 0.22 o 2 3 5 157.87 174.24 2.94 o 3 3 5 60.49 57.72 1.11 o 4 3 5 1.71 1.28 0.28 o 5 3 5 2.35 2.12 0.42 o 0 4 5 143.09 129.69 2.87 o 1 4 5 586.03 557.66 7.25 o 2 4 5 75.59 77.30 1.44 o 3 4 5 53.68 58.20 1.44 o 4 4 5 23.79 29.99 0.63 o 5 4 5 2.63 3.65 0.64 o 0 5 5 328.31 319.58 3.06 o 1 5 5 145.08 135.85 3.70 o 2 5 5 47.19 46.36 0.78 o 3 5 5 39.17 37.24 1.02 o 4 5 5 22.44 18.76 0.56 o 5 5 5 12.23 11.61 1.09 o 0 6 5 79.97 69.49 0.98 o 1 6 5 446.84 452.90 9.20 o 2 6 5 16.06 15.95 0.38 o 3 6 5 26.12 26.30 0.62 o 4 6 5 5.14 5.22 0.46 o 5 6 5 5.59 5.04 0.50 o 0 7 5 6.58 5.06 0.57 o 1 7 5 13.79 14.91 0.28 o 2 7 5 153.44 153.04 1.56 o 3 7 5 25.51 22.36 0.65 o 4 7 5 9.31 9.59 0.43 o 0 8 5 10.17 10.77 0.36 o 1 8 5 36.75 34.04 0.78 o 2 8 5 13.73 14.66 0.33 o 3 8 5 6.79 7.00 0.39 o 4 8 5 3.50 3.91 0.44 o 0 9 5 15.99 17.24 1.07 o 1 9 5 19.80 19.00 0.45 o 2 9 5 0.06 0.08 0.30 o 3 9 5 1.73 1.49 0.36 o 0 10 5 2.18 2.82 0.38 o 1 10 5 19.85 19.55 0.75 o 2 10 5 12.48 11.73 0.70 o 3 10 5 5.60 3.54 0.51 o 0 11 5 0.45 0.80 0.44 o 1 11 5 1.95 2.30 0.40 o 2 11 5 5.28 6.18 0.50 o 0 12 5 3.87 3.44 0.57 o 0 0 6 1949.16 2119.80 92.78 o 1 0 6 244.95 246.51 1.80 o 2 0 6 22.67 16.57 1.03 o 3 0 6 18.55 19.99 0.49 o 4 0 6 188.92 209.10 5.25 o 5 0 6 33.95 38.45 1.79 o 0 1 6 24.46 23.76 1.88 o 1 1 6 1.92 1.04 0.14 o 2 1 6 647.53 674.67 9.40 o 3 1 6 160.12 191.39 3.65 o 4 1 6 75.81 93.21 2.93 o 5 1 6 1.37 1.08 0.38 o 0 2 6 46.65 46.22 0.60 o 1 2 6 99.76 107.98 1.70 o 2 2 6 375.54 407.38 5.43 o 3 2 6 25.86 27.17 0.30 o 4 2 6 24.96 26.14 1.07 o 5 2 6 3.36 4.01 0.86 o 0 3 6 705.29 680.11 15.91 o 1 3 6 195.83 195.97 2.99 o 2 3 6 112.39 104.28 2.36 o 3 3 6 82.75 84.32 0.82 o 4 3 6 28.19 33.70 1.26 o 5 3 6 20.15 18.21 1.68 o 0 4 6 40.23 30.67 0.35 o 1 4 6 17.50 17.68 0.38 o 2 4 6 58.64 60.14 1.82 o 3 4 6 25.21 21.09 0.45 o 4 4 6 31.70 31.75 0.73 o 5 4 6 2.41 2.52 0.45 o 0 5 6 25.33 18.94 0.42 o 1 5 6 113.75 116.97 2.64 o 2 5 6 37.94 44.98 0.76 o 3 5 6 47.83 51.38 1.25 o 4 5 6 14.90 17.28 0.38 o 5 5 6 3.01 3.73 0.44 o 0 6 6 100.24 103.51 0.84 o 1 6 6 99.83 96.64 1.99 o 2 6 6 0.54 0.43 0.17 o 3 6 6 18.25 16.65 0.74 o 4 6 6 0.84 1.64 0.45 o 5 6 6 6.51 7.51 0.74 o 0 7 6 4.54 3.85 0.39 o 1 7 6 6.63 6.02 0.29 o 2 7 6 28.88 30.48 0.65 o 3 7 6 16.48 16.48 0.51 o 4 7 6 0.39 0.86 0.39 o 0 8 6 22.95 20.81 0.79 o 1 8 6 129.81 122.32 1.93 o 2 8 6 74.42 67.04 1.85 o 3 8 6 1.47 1.23 0.34 o 4 8 6 1.55 1.21 0.43 o 0 9 6 4.26 3.48 0.55 o 1 9 6 8.43 9.49 0.32 o 2 9 6 29.31 28.45 0.87 o 3 9 6 16.80 16.64 0.67 o 0 10 6 1.31 2.25 0.47 o 1 10 6 30.90 33.20 0.94 o 2 10 6 0.20 0.32 0.43 o 3 10 6 0.19 1.25 0.42 o 0 11 6 5.20 5.79 0.59 o 1 11 6 2.13 1.52 0.40 o 2 11 6 7.23 7.54 0.54 o 1 0 7 3.39 2.56 0.19 o 2 0 7 3.69 3.04 0.20 o 3 0 7 20.36 20.17 0.47 o 4 0 7 187.05 236.86 4.52 o 5 0 7 13.51 16.51 1.24 o 0 1 7 1.68 1.15 0.73 o 1 1 7 384.38 407.82 6.58 o 2 1 7 230.60 242.63 4.83 o 3 1 7 13.91 14.46 0.46 o 4 1 7 40.56 47.80 1.71 o 5 1 7 1.65 0.95 0.49 o 0 2 7 564.54 560.88 10.43 o 1 2 7 326.52 329.34 5.68 o 2 2 7 155.31 152.53 2.44 o 3 2 7 0.10 0.99 0.21 o 4 2 7 15.99 20.17 1.08 o 5 2 7 6.96 9.34 0.55 o 0 3 7 715.05 757.94 19.48 o 1 3 7 232.38 235.20 4.76 o 2 3 7 88.89 89.26 1.72 o 3 3 7 20.66 26.55 0.91 o 4 3 7 2.94 2.83 0.31 o 5 3 7 0.46 0.94 0.44 o 0 4 7 46.25 42.77 0.96 o 1 4 7 4.23 6.21 0.18 o 2 4 7 19.19 13.37 1.33 o 3 4 7 46.54 46.92 1.46 o 4 4 7 26.04 26.75 0.73 o 5 4 7 0.62 1.13 0.42 o 0 5 7 19.07 16.34 0.39 o 1 5 7 17.61 17.98 0.52 o 2 5 7 28.59 28.09 0.93 o 3 5 7 46.20 45.64 1.20 o 4 5 7 0.57 0.94 0.35 o 5 5 7 18.45 20.05 1.19 o 0 6 7 5.17 3.84 0.25 o 1 6 7 127.69 119.20 2.27 o 2 6 7 1.27 0.83 0.23 o 3 6 7 0.41 1.43 0.36 o 4 6 7 0.33 0.45 0.39 o 0 7 7 643.75 610.43 5.90 o 1 7 7 116.09 105.05 1.45 o 2 7 7 9.74 11.34 0.41 o 3 7 7 11.98 14.20 0.56 o 4 7 7 0.08 0.41 0.42 o 0 8 7 89.30 85.81 2.70 o 1 8 7 35.28 36.35 0.67 o 2 8 7 30.39 29.38 0.83 o 3 8 7 0.24 0.44 0.39 o 4 8 7 5.75 6.69 0.64 o 0 9 7 3.66 3.84 0.47 o 1 9 7 14.59 13.78 0.31 o 2 9 7 4.74 4.12 0.50 o 3 9 7 0.65 0.85 0.37 o 0 10 7 1.67 2.43 0.46 o 1 10 7 3.72 5.11 0.36 o 2 10 7 6.29 7.39 0.44 o 0 11 7 67.36 69.72 3.35 o 1 11 7 2.26 2.42 0.44 o 0 0 8 5.16 9.55 1.43 o 1 0 8 3.20 2.14 0.45 o 2 0 8 1.20 2.00 0.20 o 3 0 8 726.46 811.75 9.35 o 4 0 8 6.37 7.56 0.42 o 5 0 8 14.42 11.63 1.42 o 0 1 8 6.88 8.97 0.29 o 1 1 8 341.76 342.99 6.26 o 2 1 8 8.43 10.30 0.56 o 3 1 8 310.02 303.76 5.36 o 4 1 8 9.41 6.89 0.74 o 5 1 8 8.68 7.04 1.47 o 0 2 8 401.63 368.67 3.28 o 1 2 8 17.01 15.31 0.45 o 2 2 8 84.84 82.45 1.94 o 3 2 8 78.03 86.40 2.01 o 4 2 8 11.82 13.42 0.43 o 5 2 8 1.96 0.84 0.51 o 0 3 8 156.10 147.05 2.70 o 1 3 8 24.49 26.38 0.83 o 2 3 8 14.23 16.17 0.96 o 3 3 8 58.49 51.32 1.20 o 4 3 8 20.76 24.37 0.69 o 5 3 8 0.30 0.77 0.44 o 0 4 8 60.81 61.21 6.13 o 1 4 8 114.94 122.21 2.21 o 2 4 8 42.06 35.14 2.18 o 3 4 8 110.11 107.27 1.21 o 4 4 8 0.50 0.89 0.34 o 5 4 8 3.74 3.91 0.62 o 0 5 8 70.45 59.88 2.24 o 1 5 8 60.32 54.06 0.93 o 2 5 8 99.55 105.15 2.19 o 3 5 8 8.38 9.19 0.35 o 4 5 8 4.45 5.37 0.37 o 5 5 8 5.92 6.30 0.69 o 0 6 8 7.77 6.73 0.31 o 1 6 8 20.31 17.37 0.68 o 2 6 8 20.47 15.63 1.39 o 3 6 8 3.96 4.15 0.47 o 4 6 8 1.38 0.81 0.39 o 0 7 8 52.91 56.85 1.05 o 1 7 8 113.84 113.07 2.27 o 2 7 8 3.27 2.11 0.45 o 3 7 8 4.52 5.32 0.38 o 4 7 8 3.72 2.83 0.44 o 0 8 8 14.95 13.20 0.39 o 1 8 8 82.38 85.18 1.77 o 2 8 8 6.12 7.37 0.35 o 3 8 8 12.50 13.25 0.83 o 0 9 8 1.55 0.95 0.38 o 1 9 8 1.03 1.11 0.28 o 2 9 8 0.05 0.52 0.39 o 3 9 8 11.09 10.18 0.51 o 0 10 8 1.40 1.27 0.47 o 1 10 8 5.22 4.77 0.46 o 2 10 8 2.94 3.38 0.44 o 0 11 8 0.05 0.45 0.57 o 1 11 8 4.92 4.37 0.51 o 1 0 9 7.43 9.10 0.37 o 2 0 9 65.01 69.16 2.02 o 3 0 9 4.84 7.76 0.29 o 4 0 9 0.59 0.42 0.25 o 5 0 9 0.48 1.63 2.41 o 0 1 9 102.79 102.00 1.45 o 1 1 9 21.98 18.97 0.27 o 2 1 9 259.58 270.19 4.16 o 3 1 9 35.53 33.96 1.17 o 4 1 9 10.28 11.00 0.73 o 5 1 9 0.42 0.09 0.81 o 0 2 9 334.07 370.86 4.46 o 1 2 9 126.56 131.68 2.66 o 2 2 9 63.15 61.48 1.81 o 3 2 9 99.55 101.39 2.54 o 4 2 9 17.64 19.80 0.76 o 5 2 9 0.92 0.46 0.47 o 0 3 9 449.15 445.76 12.58 o 1 3 9 133.17 141.32 2.50 o 2 3 9 95.38 89.10 3.29 o 3 3 9 77.20 74.01 1.29 o 4 3 9 2.76 3.68 0.35 o 5 3 9 0.77 1.41 0.43 o 0 4 9 91.51 86.52 2.64 o 1 4 9 68.73 68.93 1.43 o 2 4 9 13.93 13.38 1.02 o 3 4 9 14.59 14.83 0.66 o 4 4 9 19.06 18.03 0.50 o 5 4 9 1.10 1.59 0.52 o 0 5 9 1.82 2.28 0.34 o 1 5 9 19.59 18.00 0.29 o 2 5 9 55.49 49.90 1.59 o 3 5 9 4.68 5.90 0.43 o 4 5 9 2.62 1.68 0.43 o 0 6 9 296.56 280.62 5.55 o 1 6 9 25.04 23.51 0.88 o 2 6 9 141.67 136.01 2.14 o 3 6 9 36.79 31.95 0.85 o 4 6 9 0.87 0.32 0.39 o 0 7 9 246.28 241.81 3.29 o 1 7 9 14.56 14.05 0.58 o 2 7 9 14.18 11.38 0.97 o 3 7 9 4.40 5.68 0.56 o 4 7 9 0.69 0.70 0.46 o 0 8 9 63.14 57.00 1.37 o 1 8 9 7.60 6.79 0.38 o 2 8 9 2.83 2.10 0.40 o 3 8 9 7.37 7.87 0.70 o 0 9 9 50.76 48.15 4.37 o 1 9 9 2.33 1.96 0.37 o 2 9 9 0.00 -0.03 0.38 o 3 9 9 16.20 19.22 0.76 o 0 10 9 3.46 4.21 0.49 o 1 10 9 2.77 3.12 0.37 o 2 10 9 0.14 0.52 0.48 o 0 11 9 13.58 17.27 0.86 o 0 0 10 53.67 58.52 2.64 o 1 0 10 77.65 73.85 0.69 o 2 0 10 164.67 161.72 2.47 o 3 0 10 0.17 0.08 0.25 o 4 0 10 2.61 1.73 0.78 o 5 0 10 3.22 1.77 1.40 o 0 1 10 336.90 324.21 8.56 o 1 1 10 35.63 32.15 0.68 o 2 1 10 30.56 30.56 0.38 o 3 1 10 143.96 153.30 3.08 o 4 1 10 19.02 20.55 1.49 o 5 1 10 10.73 15.06 0.87 o 0 2 10 0.76 1.00 0.41 o 1 2 10 110.34 111.76 2.58 o 2 2 10 5.03 3.85 0.20 o 3 2 10 61.90 62.29 2.00 o 4 2 10 25.79 24.22 0.73 o 5 2 10 12.24 16.80 0.86 o 0 3 10 135.49 115.87 2.49 o 1 3 10 41.04 38.29 0.84 o 2 3 10 12.76 10.57 0.63 o 3 3 10 18.11 17.64 0.99 o 4 3 10 2.71 2.60 0.34 o 5 3 10 1.74 1.80 0.49 o 0 4 10 42.14 48.49 2.20 o 1 4 10 64.89 69.04 1.36 o 2 4 10 41.62 38.23 0.95 o 3 4 10 2.89 3.83 0.35 o 4 4 10 4.42 4.74 0.41 o 0 5 10 86.56 89.63 2.05 o 1 5 10 22.70 21.33 0.72 o 2 5 10 39.64 33.57 1.28 o 3 5 10 38.25 37.47 1.45 o 4 5 10 1.97 1.88 0.49 o 0 6 10 143.07 153.93 1.23 o 1 6 10 207.60 221.94 4.77 o 2 6 10 17.59 16.22 0.70 o 3 6 10 8.36 7.77 0.58 o 4 6 10 0.17 0.62 0.41 o 0 7 10 38.55 40.23 1.38 o 1 7 10 33.16 29.54 0.88 o 2 7 10 3.49 2.67 0.35 o 3 7 10 4.33 3.51 0.49 o 4 7 10 2.55 1.73 0.47 o 0 8 10 50.68 52.16 1.74 o 1 8 10 17.75 15.77 0.77 o 2 8 10 3.54 3.53 0.45 o 3 8 10 0.97 1.28 0.45 o 0 9 10 0.31 1.36 0.39 o 1 9 10 0.57 0.68 0.25 o 2 9 10 1.69 1.96 0.42 o 0 10 10 0.61 0.80 0.41 o 1 10 10 5.98 7.38 0.43 o 1 0 11 1.13 1.54 0.32 o 2 0 11 236.32 228.42 3.18 o 3 0 11 8.45 8.70 0.55 o 4 0 11 0.22 0.12 0.36 o 5 0 11 0.62 1.21 1.37 o 0 1 11 141.06 130.01 2.66 o 1 1 11 7.34 7.32 0.42 o 2 1 11 8.80 8.65 0.58 o 3 1 11 23.05 25.51 0.54 o 4 1 11 46.16 54.45 2.31 o 5 1 11 6.88 8.42 1.53 o 0 2 11 96.99 104.77 1.51 o 1 2 11 142.72 150.67 3.52 o 2 2 11 43.27 39.95 0.72 o 3 2 11 0.47 0.36 0.19 o 4 2 11 9.61 9.06 0.37 o 0 3 11 23.35 24.27 0.49 o 1 3 11 49.18 49.59 1.41 o 2 3 11 12.05 14.53 0.56 o 3 3 11 6.96 7.70 0.34 o 4 3 11 0.75 1.17 0.35 o 0 4 11 96.44 109.29 1.98 o 1 4 11 12.77 12.77 0.34 o 2 4 11 43.48 37.73 0.74 o 3 4 11 31.08 30.56 1.15 o 4 4 11 0.93 1.51 0.39 o 0 5 11 133.50 131.61 4.07 o 1 5 11 160.88 161.95 2.26 o 2 5 11 18.79 21.91 1.08 o 3 5 11 3.31 4.21 0.39 o 4 5 11 10.00 10.72 0.92 o 0 6 11 7.61 8.39 1.13 o 1 6 11 17.27 18.36 0.89 o 2 6 11 3.19 2.13 0.29 o 3 6 11 1.00 1.15 0.44 o 4 6 11 1.12 1.38 0.56 o 0 7 11 9.35 8.32 0.75 o 1 7 11 40.16 40.11 0.93 o 2 7 11 41.98 42.45 1.50 o 3 7 11 5.15 6.44 0.49 o 0 8 11 32.78 32.18 2.03 o 1 8 11 19.15 15.41 0.81 o 2 8 11 0.53 1.10 0.55 o 3 8 11 1.63 1.55 0.48 o 0 9 11 40.61 44.16 0.83 o 1 9 11 0.44 0.71 0.28 o 2 9 11 3.76 4.12 0.58 o 0 10 11 2.79 2.09 0.49 o 1 10 11 6.03 6.53 0.49 o 0 0 12 1.34 2.11 0.65 o 1 0 12 10.76 9.54 0.59 o 2 0 12 175.02 183.13 5.21 o 3 0 12 16.39 22.79 1.83 o 4 0 12 30.01 28.33 2.52 o 0 1 12 127.50 113.61 1.61 o 1 1 12 14.26 12.17 0.60 o 2 1 12 13.21 14.11 0.56 o 3 1 12 5.31 4.10 0.51 o 4 1 12 4.92 4.90 0.74 o 0 2 12 12.45 10.68 0.39 o 1 2 12 63.86 66.06 2.11 o 2 2 12 6.45 6.70 0.39 o 3 2 12 23.55 21.27 0.57 o 4 2 12 23.93 23.81 0.76 o 0 3 12 128.34 130.28 3.97 o 1 3 12 27.11 26.77 0.96 o 2 3 12 40.94 40.75 1.00 o 3 3 12 4.97 3.93 0.59 o 4 3 12 2.33 2.65 0.73 o 0 4 12 44.41 49.67 2.21 o 1 4 12 12.05 11.60 0.78 o 2 4 12 56.98 48.71 2.00 o 3 4 12 1.45 0.68 0.42 o 4 4 12 2.79 2.97 0.63 o 0 5 12 0.84 1.36 0.49 o 1 5 12 44.99 43.07 1.19 o 2 5 12 4.32 5.41 0.48 o 3 5 12 5.47 4.89 0.43 o 4 5 12 3.82 4.26 0.47 o 0 6 12 0.40 0.43 0.43 o 1 6 12 6.60 6.65 0.66 o 2 6 12 7.10 6.98 0.53 o 3 6 12 1.13 1.11 0.47 o 0 7 12 1.89 1.87 0.54 o 1 7 12 74.69 82.58 1.14 o 2 7 12 19.93 21.27 0.61 o 3 7 12 4.91 6.26 0.61 o 0 8 12 16.23 17.69 1.23 o 1 8 12 42.45 47.18 0.97 o 2 8 12 6.33 8.78 0.94 o 0 9 12 8.70 8.09 0.74 o 1 9 12 6.33 6.56 0.45 o 1 0 13 87.35 84.65 0.74 o 2 0 13 156.10 161.10 4.50 o 3 0 13 1.06 1.34 0.34 o 4 0 13 4.55 7.25 1.04 o 0 1 13 9.42 12.32 0.60 o 1 1 13 77.07 75.50 1.31 o 2 1 13 60.61 58.62 1.49 o 3 1 13 1.34 1.55 0.29 o 4 1 13 20.86 18.49 1.95 o 0 2 13 7.69 7.54 0.57 o 1 2 13 21.57 23.34 0.67 o 2 2 13 21.52 20.84 0.82 o 3 2 13 1.18 0.73 0.24 o 4 2 13 24.26 25.63 0.63 o 0 3 13 2.23 1.74 0.47 o 1 3 13 66.54 67.64 1.02 o 2 3 13 11.21 12.75 0.42 o 3 3 13 24.15 22.16 0.56 o 4 3 13 24.42 25.07 1.95 o 0 4 13 26.13 27.01 1.67 o 1 4 13 13.74 12.88 0.73 o 2 4 13 27.73 30.24 1.89 o 3 4 13 2.68 2.76 0.48 o 4 4 13 1.51 2.04 0.53 o 0 5 13 19.81 18.42 2.14 o 1 5 13 3.58 3.97 0.51 o 2 5 13 18.29 18.24 0.58 o 3 5 13 3.70 3.71 0.49 o 0 6 13 7.94 7.20 0.65 o 1 6 13 4.24 3.62 0.40 o 2 6 13 32.71 29.87 1.05 o 3 6 13 0.17 0.72 0.50 o 0 7 13 0.66 0.57 0.40 o 1 7 13 19.20 18.66 1.34 o 2 7 13 8.70 9.46 0.84 o 3 7 13 0.60 0.30 0.50 o 0 8 13 3.01 2.49 0.41 o 1 8 13 18.76 15.90 1.51 o 2 8 13 20.59 22.64 1.07 o 0 9 13 0.00 0.77 0.48 o 1 9 13 0.96 1.57 0.43 o 0 0 14 119.20 102.95 17.10 o 1 0 14 158.23 155.38 1.50 o 2 0 14 3.44 3.35 0.48 o 3 0 14 8.52 7.44 0.94 o 4 0 14 1.68 1.22 1.02 o 0 1 14 124.92 116.66 7.12 o 1 1 14 171.76 177.43 3.91 o 2 1 14 0.76 1.09 0.34 o 3 1 14 0.17 0.83 0.26 o 4 1 14 3.88 2.62 0.40 o 0 2 14 26.05 27.13 1.54 o 1 2 14 10.23 8.95 0.53 o 2 2 14 3.38 4.22 0.71 o 3 2 14 5.14 4.57 0.56 o 4 2 14 9.76 8.80 1.09 o 0 3 14 0.65 0.91 0.61 o 1 3 14 38.26 35.70 1.57 o 2 3 14 4.87 4.76 0.37 o 3 3 14 1.08 1.96 0.44 o 4 3 14 0.71 0.48 0.50 o 0 4 14 85.37 81.74 1.99 o 1 4 14 17.62 17.77 0.55 o 2 4 14 4.26 4.50 0.43 o 3 4 14 1.24 0.92 0.56 o 0 5 14 6.79 6.07 1.19 o 1 5 14 55.70 54.49 2.61 o 2 5 14 0.36 1.15 0.33 o 3 5 14 1.63 2.18 0.47 o 0 6 14 2.18 1.82 0.47 o 1 6 14 5.43 5.65 0.45 o 2 6 14 18.16 19.59 1.01 o 3 6 14 0.50 0.73 0.52 o 0 7 14 1.57 1.58 0.43 o 1 7 14 3.20 2.87 0.43 o 2 7 14 2.36 2.07 0.57 o 0 8 14 0.41 0.29 0.50 o 1 8 14 2.16 1.10 0.39 o 1 0 15 62.39 67.71 1.05 o 2 0 15 25.32 23.41 0.92 o 3 0 15 0.87 1.18 0.56 o 0 1 15 0.34 0.15 0.46 o 1 1 15 49.67 52.39 1.15 o 2 1 15 22.20 23.35 0.77 o 3 1 15 4.08 3.92 0.42 o 0 2 15 3.09 3.60 0.47 o 1 2 15 7.53 6.53 0.52 o 2 2 15 17.43 18.56 0.96 o 3 2 15 4.94 5.50 0.71 o 0 3 15 5.82 5.60 0.84 o 1 3 15 9.24 8.80 0.84 o 2 3 15 6.21 6.98 0.64 o 3 3 15 12.38 13.23 0.64 o 0 4 15 13.73 10.72 1.87 o 1 4 15 3.03 2.11 0.61 o 2 4 15 0.78 0.46 0.42 o 3 4 15 11.27 12.63 1.70 o 0 5 15 0.41 1.57 0.68 o 1 5 15 0.82 0.86 0.47 o 2 5 15 30.62 30.69 1.48 o 3 5 15 4.84 5.09 0.82 o 0 6 15 0.08 1.25 0.60 o 1 6 15 2.00 1.26 0.39 o 2 6 15 42.45 43.21 1.91 o 0 7 15 0.89 1.52 0.46 o 1 7 15 2.95 3.19 0.40 o 0 0 16 132.51 124.75 16.47 o 1 0 16 1.28 1.97 0.54 o 2 0 16 3.38 4.44 0.61 o 3 0 16 0.02 0.07 0.44 o 0 1 16 36.23 32.36 1.44 o 1 1 16 15.27 16.09 0.84 o 2 1 16 18.66 19.21 1.12 o 3 1 16 3.80 3.77 0.53 o 0 2 16 24.34 24.67 0.86 o 1 2 16 20.55 17.55 1.40 o 2 2 16 4.30 3.07 0.73 o 3 2 16 3.30 4.19 0.75 o 0 3 16 2.37 1.81 0.92 o 1 3 16 9.78 8.58 0.94 o 2 3 16 6.42 6.42 0.84 o 3 3 16 6.93 5.49 1.29 o 0 4 16 33.40 39.87 1.03 o 1 4 16 4.32 3.36 0.56 o 2 4 16 17.53 17.30 1.57 o 0 5 16 0.52 0.05 0.72 o 1 5 16 4.64 3.82 0.51 o 2 5 16 7.76 6.86 0.66 o 0 6 16 0.30 0.14 0.55 o 1 6 16 7.34 7.34 0.90 o 0 7 16 0.00 1.07 0.56 o 1 0 17 16.11 19.42 1.99 o 2 0 17 0.18 0.25 0.73 o 3 0 17 0.03 0.08 0.46 o 0 1 17 53.31 57.26 5.23 o 1 1 17 6.83 6.06 0.64 o 2 1 17 0.32 0.42 0.37 o 0 2 17 20.27 20.06 2.10 o 1 2 17 1.55 1.97 0.40 o 2 2 17 2.88 2.48 0.72 o 0 3 17 0.33 0.33 0.64 o 1 3 17 7.27 7.17 0.59 o 2 3 17 0.74 0.87 0.61 o 0 4 17 2.93 2.24 1.63 o 1 4 17 4.59 3.85 1.04 o 2 4 17 3.07 2.07 1.09 o 0 5 17 4.10 2.02 3.12 o 1 5 17 9.80 8.59 0.81 o 0 6 17 11.38 9.55 0.70 o 0 0 18 5.94 5.67 1.97 o 1 0 18 15.49 14.55 1.30 o 2 0 18 0.01 0.01 0.70 o 0 1 18 75.68 87.91 2.61 o 1 1 18 4.62 3.17 0.58 o 2 1 18 0.79 -0.16 0.43 o 0 2 18 55.98 62.66 1.23 o 1 2 18 5.79 3.86 1.06 o 2 2 18 4.92 3.48 0.98 o 0 3 18 3.68 1.85 1.48 o 1 3 18 2.16 1.23 0.91 o 0 4 18 1.39 1.79 1.47 o 1 4 18 15.04 17.34 1.24 o 1 0 19 49.37 55.96 1.31 o 0 1 19 16.27 15.26 2.63 o 1 1 19 5.64 3.81 1.03 o 0 2 19 0.42 0.24 0.64 o