#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:05:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180957 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/37/2203714.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2203714_Fobs loop_ _publ_author_name 'Wu, Hai-Qiang' 'An, Lin-Kun' 'Huang, Zhi-Shu' 'Gu, Lian-Quan' 'Zain, Sharifuddin M.' 'Ng, Seik Weng' _publ_section_title ; Ethyl 3-methyl-5-nitro-1H-imidazole-2-carboxylate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o994 _journal_page_last o995 _journal_volume 60 _journal_year 2004 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.9397 _cell_length_b 6.7676 _cell_length_c 15.0278 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.7794 _cod_data_source_file bt6461Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Pnma' _shelx_refln_list_code 4 _shelx_f_calc_maximum 76.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 244.82 169.30 2.29 o 4 0 0 615.03 543.25 7.17 o 6 0 0 343.27 362.06 4.93 o 8 0 0 645.51 586.39 5.40 o 2 1 0 4353.12 4148.74 34.97 o 4 1 0 313.81 383.46 2.29 o 6 1 0 504.31 519.74 3.79 o 8 1 0 545.16 507.25 3.26 o 10 1 0 1.74 2.29 0.28 o 2 2 0 6.92 7.86 0.12 o 4 2 0 265.12 255.29 1.68 o 6 2 0 188.25 184.39 1.29 o 8 2 0 480.98 437.57 3.31 o 10 2 0 66.96 67.06 1.39 o 2 3 0 296.06 314.61 1.80 o 4 3 0 4.04 8.26 0.16 o 6 3 0 227.98 238.51 1.89 o 8 3 0 215.70 229.21 3.32 o 10 3 0 1.26 0.24 0.31 o 0 4 0 5398.59 5639.01 49.67 o 2 4 0 69.40 63.64 0.46 o 4 4 0 23.93 21.46 0.27 o 6 4 0 19.06 20.34 0.35 o 8 4 0 208.10 221.57 2.40 o 10 4 0 23.84 24.22 0.63 o 2 5 0 1.28 1.79 0.35 o 4 5 0 3.11 1.73 0.29 o 6 5 0 49.49 47.03 0.96 o 8 5 0 45.96 49.04 0.94 o 0 6 0 594.28 593.21 5.46 o 2 6 0 12.00 13.74 0.31 o 4 6 0 0.33 0.18 0.22 o 6 6 0 1.21 0.95 0.29 o 8 6 0 49.93 54.30 1.66 o 2 7 0 0.03 0.15 0.18 o 4 7 0 0.78 0.41 0.44 o 6 7 0 13.30 13.00 0.48 o 0 8 0 95.62 90.44 1.83 o 2 8 0 0.03 0.26 0.44 o 4 8 0 1.30 1.11 0.32 o 2 0 1 502.47 467.03 3.46 o 3 0 1 489.32 494.15 4.42 o 4 0 1 286.52 277.49 2.87 o 5 0 1 4.65 10.28 0.19 o 6 0 1 0.28 -0.09 0.09 o 7 0 1 349.93 339.91 2.65 o 8 0 1 8.60 6.89 0.48 o 9 0 1 27.32 21.20 0.45 o 11 0 1 7.60 6.75 0.54 o 0 1 1 7.11 8.48 0.14 o 1 1 1 90.69 93.02 0.56 o 2 1 1 3317.49 3060.86 16.21 o 3 1 1 510.56 550.52 2.62 o 4 1 1 3.68 4.52 0.08 o 5 1 1 741.00 800.01 8.99 o 6 1 1 13.23 13.17 0.14 o 7 1 1 4.47 6.78 0.13 o 8 1 1 27.20 25.66 0.28 o 9 1 1 11.89 13.32 0.24 o 10 1 1 0.14 0.49 0.23 o 11 1 1 5.19 6.93 0.41 o 1 2 1 3744.73 3764.67 21.02 o 2 2 1 1.09 1.38 0.07 o 3 2 1 176.93 171.78 0.76 o 4 2 1 87.14 78.80 0.42 o 5 2 1 14.66 17.03 0.16 o 6 2 1 4.28 3.58 0.14 o 7 2 1 233.05 218.35 1.25 o 8 2 1 10.13 8.61 0.19 o 9 2 1 21.91 18.65 0.29 o 10 2 1 2.85 4.12 0.25 o 11 2 1 6.39 6.85 0.44 o 0 3 1 1037.82 1017.40 7.24 o 1 3 1 53.90 51.13 0.28 o 2 3 1 194.45 192.74 0.81 o 3 3 1 11.95 9.69 0.10 o 4 3 1 3.99 3.34 0.08 o 5 3 1 328.02 342.93 1.71 o 6 3 1 7.82 8.37 0.14 o 7 3 1 0.43 0.44 0.13 o 8 3 1 8.97 8.39 0.23 o 9 3 1 9.67 9.28 0.28 o 10 3 1 0.06 -0.10 0.22 o 1 4 1 972.39 1008.94 4.20 o 2 4 1 65.41 54.53 0.29 o 3 4 1 11.39 10.49 0.12 o 4 4 1 0.46 0.29 0.07 o 5 4 1 39.40 37.14 0.30 o 6 4 1 19.13 20.35 0.28 o 7 4 1 85.36 84.19 0.69 o 8 4 1 8.19 8.30 0.28 o 9 4 1 11.48 10.20 0.30 o 10 4 1 0.24 -0.01 0.23 o 0 5 1 374.41 359.49 2.39 o 1 5 1 12.52 10.23 0.14 o 2 5 1 0.01 -0.04 0.07 o 3 5 1 6.54 6.35 0.12 o 4 5 1 15.07 15.45 0.22 o 5 5 1 91.26 90.63 0.71 o 6 5 1 1.88 2.32 0.20 o 7 5 1 0.18 0.15 0.20 o 8 5 1 2.25 1.69 0.24 o 9 5 1 4.63 4.31 0.29 o 1 6 1 179.95 171.86 1.07 o 2 6 1 7.57 7.48 0.18 o 3 6 1 0.42 0.13 0.11 o 4 6 1 0.91 0.68 0.17 o 5 6 1 19.91 20.94 0.37 o 6 6 1 9.02 9.84 0.29 o 7 6 1 26.48 28.20 0.47 o 8 6 1 3.00 4.03 0.30 o 0 7 1 60.54 60.99 0.94 o 1 7 1 3.45 3.63 0.23 o 2 7 1 0.56 0.11 0.15 o 3 7 1 2.50 1.79 0.20 o 4 7 1 7.14 7.29 0.27 o 5 7 1 17.49 16.00 0.34 o 6 7 1 0.25 -0.20 0.20 o 1 8 1 31.25 27.19 0.53 o 2 8 1 0.00 -0.31 0.31 o 3 8 1 0.00 -0.30 0.30 o 4 8 1 0.31 -0.14 0.25 o 0 0 2 1037.91 1060.82 8.86 o 1 0 2 3978.15 4112.92 21.61 o 2 0 2 144.58 126.29 3.76 o 3 0 2 497.31 454.85 3.37 o 4 0 2 1648.56 1600.20 33.16 o 5 0 2 6.18 4.64 0.22 o 6 0 2 39.30 32.22 1.17 o 7 0 2 65.88 61.74 0.78 o 8 0 2 189.04 160.66 1.62 o 10 0 2 5.17 4.76 0.47 o 11 0 2 18.22 17.00 0.68 o 1 1 2 198.86 205.13 1.08 o 2 1 2 424.12 441.76 2.09 o 3 1 2 607.89 590.35 3.89 o 4 1 2 388.96 425.12 1.98 o 5 1 2 442.39 460.05 2.07 o 6 1 2 11.61 11.26 0.14 o 7 1 2 323.24 315.50 1.65 o 8 1 2 0.04 -0.03 0.10 o 9 1 2 157.90 154.96 1.17 o 10 1 2 5.28 6.88 0.29 o 11 1 2 10.23 13.09 0.98 o 0 2 2 2184.09 2303.01 12.69 o 1 2 2 2560.29 2606.34 12.36 o 2 2 2 52.35 65.07 0.34 o 3 2 2 152.62 134.56 0.65 o 4 2 2 886.41 926.31 4.08 o 5 2 2 8.24 9.95 0.18 o 6 2 2 21.12 20.82 0.27 o 7 2 2 34.33 32.16 0.28 o 8 2 2 126.97 113.58 0.92 o 9 2 2 0.68 1.14 0.17 o 10 2 2 2.97 2.15 0.22 o 11 2 2 10.63 10.25 0.75 o 1 3 2 157.28 162.19 0.73 o 2 3 2 0.75 0.56 0.08 o 3 3 2 147.06 130.99 0.66 o 4 3 2 264.35 273.01 1.57 o 5 3 2 78.64 73.37 0.46 o 6 3 2 2.59 4.12 0.14 o 7 3 2 207.61 208.00 1.36 o 8 3 2 0.01 -0.14 0.14 o 9 3 2 46.38 43.98 0.58 o 10 3 2 5.79 5.11 0.34 o 0 4 2 1045.73 1081.04 10.15 o 1 4 2 525.50 523.29 2.22 o 2 4 2 188.77 180.68 0.89 o 3 4 2 2.48 2.40 0.09 o 4 4 2 160.21 158.42 0.80 o 5 4 2 9.86 10.53 0.22 o 6 4 2 7.66 8.02 0.20 o 7 4 2 3.66 4.75 0.32 o 8 4 2 42.86 41.98 0.54 o 9 4 2 0.03 -0.04 0.20 o 10 4 2 0.91 -0.14 0.25 o 1 5 2 0.80 1.45 0.21 o 2 5 2 1.57 1.11 0.09 o 3 5 2 30.35 27.33 0.28 o 4 5 2 114.91 116.30 0.77 o 5 5 2 2.12 1.63 0.15 o 6 5 2 15.37 16.41 0.28 o 7 5 2 79.04 85.06 0.84 o 8 5 2 0.02 -0.21 0.21 o 9 5 2 3.45 3.59 0.29 o 0 6 2 250.85 256.82 3.49 o 1 6 2 51.22 48.75 0.38 o 2 6 2 60.40 59.07 0.48 o 3 6 2 0.03 -0.11 0.11 o 4 6 2 13.02 11.62 0.23 o 5 6 2 1.97 2.08 0.30 o 6 6 2 0.10 -0.19 0.19 o 7 6 2 0.03 -0.21 0.21 o 8 6 2 13.21 14.07 0.38 o 1 7 2 4.66 6.06 0.23 o 2 7 2 0.21 0.14 0.17 o 3 7 2 4.42 4.32 0.26 o 4 7 2 16.36 16.06 0.33 o 5 7 2 0.15 -0.20 0.20 o 6 7 2 5.63 5.22 0.30 o 0 8 2 39.73 39.55 1.13 o 1 8 2 3.82 4.26 0.32 o 2 8 2 8.15 9.20 0.49 o 3 8 2 0.13 0.59 0.25 o 4 8 2 1.22 1.13 0.27 o 1 0 3 518.78 528.34 2.78 o 2 0 3 355.58 391.95 2.31 o 3 0 3 986.96 1002.30 7.32 o 4 0 3 622.51 631.63 5.46 o 5 0 3 313.26 320.99 8.18 o 6 0 3 154.08 164.45 2.89 o 7 0 3 23.93 23.28 0.37 o 8 0 3 12.52 9.84 0.29 o 9 0 3 0.35 0.78 0.19 o 10 0 3 10.43 10.96 0.52 o 11 0 3 10.57 16.17 0.66 o 0 1 3 5880.40 5610.61 57.99 o 1 1 3 327.52 279.68 1.34 o 2 1 3 387.78 415.30 1.98 o 3 1 3 62.28 62.02 0.35 o 4 1 3 182.80 199.06 1.16 o 5 1 3 466.12 447.81 3.15 o 6 1 3 4.85 6.01 0.12 o 7 1 3 46.76 50.97 0.50 o 8 1 3 77.15 77.75 0.73 o 9 1 3 0.10 -0.16 0.16 o 10 1 3 1.31 2.21 0.18 o 11 1 3 1.50 4.49 0.37 o 1 2 3 19.53 21.70 0.16 o 2 2 3 33.54 29.25 0.20 o 3 2 3 649.47 673.86 3.17 o 4 2 3 208.12 187.29 1.02 o 5 2 3 107.04 108.22 0.66 o 6 2 3 82.03 81.84 0.69 o 7 2 3 5.17 5.52 0.16 o 8 2 3 13.47 13.09 0.29 o 9 2 3 0.51 0.17 0.17 o 10 2 3 6.86 7.89 0.26 o 11 2 3 8.08 10.71 0.58 o 0 3 3 403.86 401.32 2.28 o 1 3 3 5.30 5.15 0.08 o 2 3 3 9.79 10.95 0.12 o 3 3 3 157.97 153.27 0.75 o 4 3 3 57.31 56.76 0.36 o 5 3 3 148.06 144.82 1.01 o 6 3 3 0.42 0.03 0.10 o 7 3 3 22.06 22.70 0.28 o 8 3 3 50.13 51.90 0.50 o 9 3 3 0.67 0.66 0.17 o 10 3 3 1.17 0.89 0.21 o 1 4 3 5.21 5.72 0.12 o 2 4 3 4.67 4.77 0.10 o 3 4 3 115.72 115.00 0.57 o 4 4 3 1.40 1.46 0.13 o 5 4 3 0.10 0.05 0.09 o 6 4 3 23.35 24.11 0.28 o 7 4 3 2.65 2.88 0.30 o 8 4 3 11.85 12.24 0.27 o 9 4 3 5.82 5.73 0.29 o 10 4 3 2.44 2.22 0.53 o 0 5 3 35.39 36.62 0.38 o 1 5 3 0.32 0.48 0.08 o 2 5 3 10.08 10.01 0.18 o 3 5 3 72.53 70.05 0.48 o 4 5 3 12.07 11.54 0.20 o 5 5 3 24.08 24.81 0.29 o 6 5 3 0.29 0.30 0.14 o 7 5 3 4.76 5.26 0.22 o 8 5 3 18.86 20.50 0.40 o 9 5 3 0.09 -0.06 0.23 o 1 6 3 17.87 17.99 0.24 o 2 6 3 3.80 4.67 0.20 o 3 6 3 8.14 7.25 0.18 o 4 6 3 1.14 0.84 0.14 o 5 6 3 1.24 1.38 0.17 o 6 6 3 3.16 3.97 0.29 o 7 6 3 2.99 3.59 0.27 o 8 6 3 6.72 7.07 0.36 o 0 7 3 9.66 8.99 0.70 o 1 7 3 0.54 0.86 0.23 o 2 7 3 3.69 4.25 0.23 o 3 7 3 7.38 7.27 0.34 o 4 7 3 2.58 2.47 0.23 o 5 7 3 6.73 7.24 0.31 o 6 7 3 0.00 -0.22 0.22 o 1 8 3 10.41 12.45 0.39 o 2 8 3 0.29 -0.15 0.26 o 3 8 3 0.36 -0.06 0.25 o 4 8 3 0.00 0.35 0.35 o 0 0 4 1156.03 1159.13 8.17 o 1 0 4 154.95 169.39 0.85 o 2 0 4 684.96 669.49 3.52 o 3 0 4 2600.41 2775.10 16.04 o 4 0 4 476.44 587.27 3.46 o 5 0 4 67.43 68.20 0.58 o 6 0 4 46.94 45.54 0.40 o 7 0 4 44.50 40.92 0.45 o 8 0 4 4.73 4.30 0.39 o 9 0 4 9.89 14.25 0.35 o 10 0 4 22.97 24.95 0.76 o 11 0 4 7.36 10.63 0.58 o 1 1 4 11.69 9.06 0.08 o 2 1 4 732.70 736.24 3.46 o 3 1 4 0.95 0.78 0.05 o 4 1 4 251.80 259.57 1.40 o 5 1 4 218.87 198.84 1.99 o 6 1 4 6.86 5.61 0.13 o 7 1 4 30.47 27.80 0.31 o 8 1 4 216.75 195.22 1.43 o 9 1 4 0.71 1.03 0.17 o 10 1 4 11.14 10.30 0.28 o 11 1 4 1.75 1.11 0.24 o 0 2 4 987.96 1026.59 6.37 o 1 2 4 206.64 201.92 1.02 o 2 2 4 277.66 272.69 1.47 o 3 2 4 818.98 829.67 5.16 o 4 2 4 271.94 302.03 1.49 o 5 2 4 62.39 58.81 0.57 o 6 2 4 23.90 26.56 0.30 o 7 2 4 45.10 43.65 0.42 o 8 2 4 0.88 0.67 0.15 o 9 2 4 12.25 14.39 0.32 o 10 2 4 12.00 13.48 0.30 o 1 3 4 134.78 140.21 0.69 o 2 3 4 307.82 310.73 1.55 o 3 3 4 12.20 13.42 0.14 o 4 3 4 40.72 36.75 0.33 o 5 3 4 9.47 10.74 0.17 o 6 3 4 1.03 1.11 0.11 o 7 3 4 0.38 0.06 0.14 o 8 3 4 81.89 79.96 0.68 o 9 3 4 0.01 -0.10 0.17 o 10 3 4 4.71 5.89 0.43 o 0 4 4 203.35 187.54 1.15 o 1 4 4 96.05 89.27 0.46 o 2 4 4 18.40 19.47 0.20 o 3 4 4 26.35 31.12 0.27 o 4 4 4 82.15 86.26 0.55 o 5 4 4 50.63 45.34 0.36 o 6 4 4 7.34 8.17 0.21 o 7 4 4 26.02 27.13 0.36 o 8 4 4 0.72 0.90 0.17 o 9 4 4 9.99 10.44 0.26 o 1 5 4 23.44 24.80 0.22 o 2 5 4 48.94 46.48 0.35 o 3 5 4 26.71 27.57 0.26 o 4 5 4 0.48 0.14 0.11 o 5 5 4 14.49 13.22 0.22 o 6 5 4 0.04 0.39 0.15 o 7 5 4 2.56 3.10 0.20 o 8 5 4 16.25 16.78 0.37 o 9 5 4 0.11 -0.22 0.22 o 0 6 4 14.30 12.65 0.30 o 1 6 4 14.67 15.86 0.23 o 2 6 4 0.33 0.14 0.11 o 3 6 4 0.07 -0.12 0.12 o 4 6 4 15.25 15.40 0.25 o 5 6 4 13.43 13.40 0.26 o 6 6 4 1.40 1.01 0.18 o 7 6 4 7.15 8.26 0.33 o 1 7 4 0.53 0.58 0.17 o 2 7 4 5.54 6.42 0.32 o 3 7 4 12.46 12.66 0.26 o 4 7 4 0.09 -0.03 0.16 o 5 7 4 8.14 8.27 0.28 o 6 7 4 0.04 -0.24 0.24 o 0 8 4 0.14 1.02 0.47 o 1 8 4 0.58 1.03 0.33 o 2 8 4 0.31 0.28 0.21 o 3 8 4 0.10 0.68 0.26 o 1 0 5 21.32 20.84 0.16 o 2 0 5 547.05 577.25 3.05 o 3 0 5 73.68 82.38 0.57 o 4 0 5 98.31 99.35 0.79 o 5 0 5 4.51 3.26 0.19 o 6 0 5 280.03 267.24 1.90 o 7 0 5 155.53 155.94 1.21 o 8 0 5 185.41 186.79 1.73 o 9 0 5 10.04 10.12 0.31 o 10 0 5 10.43 12.47 0.36 o 11 0 5 0.18 0.71 0.37 o 0 1 5 2200.03 2334.33 11.17 o 1 1 5 1098.75 1170.53 4.12 o 2 1 5 238.67 226.45 1.05 o 3 1 5 30.20 43.33 0.28 o 4 1 5 230.06 262.40 1.31 o 5 1 5 191.04 183.05 1.04 o 6 1 5 287.65 276.17 1.69 o 7 1 5 35.00 33.76 0.40 o 8 1 5 36.99 32.55 0.41 o 9 1 5 2.80 1.74 0.18 o 10 1 5 6.89 7.39 0.28 o 1 2 5 65.47 65.64 0.36 o 2 2 5 381.22 401.56 2.26 o 3 2 5 41.63 45.50 0.40 o 4 2 5 56.02 54.36 0.36 o 5 2 5 5.31 6.08 0.13 o 6 2 5 153.64 143.50 0.98 o 7 2 5 62.64 61.93 0.53 o 8 2 5 104.50 114.26 0.96 o 9 2 5 4.03 4.90 0.27 o 10 2 5 7.81 9.39 0.27 o 0 3 5 449.39 461.50 2.96 o 1 3 5 153.69 153.04 0.82 o 2 3 5 61.44 58.65 0.42 o 3 3 5 58.73 57.11 0.42 o 4 3 5 131.48 149.04 0.99 o 5 3 5 23.26 21.51 0.24 o 6 3 5 135.30 135.46 0.95 o 7 3 5 24.62 22.12 0.31 o 8 3 5 8.07 7.15 0.24 o 9 3 5 1.02 0.66 0.19 o 10 3 5 0.34 0.02 0.21 o 1 4 5 33.66 30.03 0.23 o 2 4 5 74.04 68.51 0.45 o 3 4 5 1.80 2.32 0.11 o 4 4 5 32.81 29.98 0.28 o 5 4 5 9.73 11.14 0.18 o 6 4 5 29.85 26.61 0.31 o 7 4 5 0.79 0.47 0.13 o 8 4 5 24.35 26.95 0.37 o 9 4 5 0.10 -0.27 0.27 o 0 5 5 31.07 29.57 0.41 o 1 5 5 8.38 7.26 0.13 o 2 5 5 10.74 10.47 0.17 o 3 5 5 15.87 14.60 0.20 o 4 5 5 46.69 43.64 0.42 o 5 5 5 0.69 0.66 0.13 o 6 5 5 44.67 45.43 0.56 o 7 5 5 13.41 11.04 0.26 o 8 5 5 0.00 -0.18 0.18 o 1 6 5 0.20 0.18 0.13 o 2 6 5 8.05 7.44 0.18 o 3 6 5 0.38 0.37 0.13 o 4 6 5 14.44 14.34 0.24 o 5 6 5 2.32 3.95 0.19 o 6 6 5 4.41 4.61 0.28 o 7 6 5 0.99 0.91 0.23 o 0 7 5 0.93 1.26 0.29 o 1 7 5 0.25 -0.04 0.17 o 2 7 5 3.48 2.83 0.27 o 3 7 5 0.15 0.19 0.16 o 4 7 5 18.60 17.47 0.28 o 5 7 5 0.64 1.23 0.22 o 6 7 5 11.33 12.60 0.52 o 1 8 5 0.63 0.60 0.33 o 2 8 5 0.94 0.71 0.23 o 3 8 5 0.41 0.29 0.22 o 0 0 6 70.57 81.59 0.67 o 1 0 6 1942.07 1989.48 9.88 o 2 0 6 396.85 452.22 2.55 o 3 0 6 65.96 74.77 0.48 o 4 0 6 319.34 336.49 2.05 o 5 0 6 156.41 157.27 1.18 o 6 0 6 226.91 219.99 1.61 o 7 0 6 145.98 129.45 1.06 o 8 0 6 1.63 1.51 0.20 o 9 0 6 15.21 17.27 0.60 o 10 0 6 4.42 5.64 0.32 o 1 1 6 4.18 8.52 0.07 o 2 1 6 406.10 421.79 1.79 o 3 1 6 481.53 520.38 2.75 o 4 1 6 169.19 156.17 0.83 o 5 1 6 319.82 338.38 1.82 o 6 1 6 66.44 74.53 0.58 o 7 1 6 288.47 289.01 2.00 o 8 1 6 16.53 11.14 0.22 o 9 1 6 2.16 2.60 0.18 o 10 1 6 0.40 0.71 0.27 o 0 2 6 66.02 67.48 0.53 o 1 2 6 680.12 694.75 3.09 o 2 2 6 129.95 142.86 0.68 o 3 2 6 16.22 17.19 0.16 o 4 2 6 142.56 147.94 0.88 o 5 2 6 70.04 68.50 0.49 o 6 2 6 139.45 130.79 0.92 o 7 2 6 116.94 108.18 1.08 o 8 2 6 1.58 1.56 0.20 o 9 2 6 10.30 10.93 0.27 o 10 2 6 1.49 1.09 0.43 o 1 3 6 80.00 82.67 0.46 o 2 3 6 106.71 105.36 0.66 o 3 3 6 240.23 265.35 1.48 o 4 3 6 59.32 57.93 0.44 o 5 3 6 130.89 134.68 0.85 o 6 3 6 40.54 43.26 0.44 o 7 3 6 105.36 108.36 0.83 o 8 3 6 21.54 16.56 0.39 o 9 3 6 0.20 0.07 0.18 o 10 3 6 0.23 0.23 0.21 o 0 4 6 29.78 35.27 0.32 o 1 4 6 89.08 94.37 0.57 o 2 4 6 17.56 16.87 0.21 o 3 4 6 0.00 -0.06 0.09 o 4 4 6 28.13 28.94 0.30 o 5 4 6 1.67 1.80 0.16 o 6 4 6 31.37 29.55 0.37 o 7 4 6 62.51 63.69 0.63 o 8 4 6 1.68 1.37 0.19 o 9 4 6 5.32 5.72 0.38 o 1 5 6 22.68 21.47 0.23 o 2 5 6 11.94 12.79 0.19 o 3 5 6 62.98 67.28 0.48 o 4 5 6 5.48 6.19 0.16 o 5 5 6 37.48 38.61 0.39 o 6 5 6 15.98 16.92 0.27 o 7 5 6 20.07 19.67 0.33 o 8 5 6 12.54 12.54 0.29 o 0 6 6 7.03 6.58 0.25 o 1 6 6 14.58 14.35 0.25 o 2 6 6 1.74 1.95 0.15 o 3 6 6 0.06 -0.12 0.12 o 4 6 6 2.26 2.12 0.21 o 5 6 6 0.46 0.22 0.15 o 6 6 6 1.52 1.43 0.26 o 7 6 6 21.83 24.49 0.39 o 1 7 6 2.67 1.97 0.30 o 2 7 6 0.15 -0.18 0.18 o 3 7 6 12.74 11.43 0.27 o 4 7 6 0.07 -0.17 0.17 o 5 7 6 11.79 12.18 0.29 o 0 8 6 1.20 0.02 0.43 o 1 8 6 2.72 3.30 0.38 o 2 8 6 0.03 -0.24 0.25 o 1 0 7 1038.97 1080.15 5.39 o 2 0 7 556.18 690.12 3.54 o 3 0 7 7.06 4.31 0.10 o 4 0 7 26.09 23.40 0.25 o 5 0 7 26.60 21.08 0.29 o 6 0 7 22.57 21.54 0.32 o 7 0 7 26.06 24.36 0.44 o 8 0 7 18.16 19.92 0.41 o 9 0 7 59.02 61.54 0.81 o 10 0 7 0.05 -0.24 0.24 o 0 1 7 159.15 175.03 0.90 o 1 1 7 314.27 327.31 1.17 o 2 1 7 1066.80 1201.42 4.81 o 3 1 7 22.21 20.00 0.14 o 4 1 7 209.25 257.16 1.12 o 5 1 7 3.74 2.05 0.10 o 6 1 7 427.79 408.88 2.33 o 7 1 7 5.28 5.11 0.18 o 8 1 7 70.67 64.55 0.54 o 9 1 7 0.19 -0.01 0.15 o 10 1 7 2.47 2.52 0.20 o 1 2 7 279.42 262.72 1.05 o 2 2 7 384.99 437.65 2.00 o 3 2 7 1.84 1.07 0.11 o 4 2 7 21.46 19.36 0.22 o 5 2 7 23.74 20.24 0.24 o 6 2 7 32.47 27.15 0.32 o 7 2 7 11.11 10.68 0.25 o 8 2 7 24.48 23.62 0.37 o 9 2 7 40.93 43.86 0.53 o 10 2 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81.34 0.77 o 8 3 8 0.41 0.02 0.17 o 9 3 8 0.08 0.16 0.21 o 0 4 8 8.26 10.00 0.36 o 1 4 8 147.00 149.49 0.92 o 2 4 8 6.22 6.28 0.15 o 3 4 8 26.11 24.44 0.28 o 4 4 8 18.45 17.87 0.25 o 5 4 8 7.55 6.87 0.18 o 6 4 8 2.08 1.85 0.20 o 7 4 8 38.21 38.67 0.45 o 8 4 8 0.08 -0.02 0.17 o 9 4 8 0.37 0.22 0.41 o 1 5 8 5.52 5.48 0.18 o 2 5 8 0.57 0.28 0.10 o 3 5 8 4.17 4.75 0.17 o 4 5 8 5.00 4.71 0.17 o 5 5 8 6.53 7.47 0.19 o 6 5 8 7.53 7.77 0.23 o 7 5 8 31.58 32.68 0.40 o 8 5 8 0.41 0.64 0.20 o 0 6 8 4.75 5.35 0.34 o 1 6 8 28.00 29.41 0.34 o 2 6 8 7.43 6.48 0.18 o 3 6 8 7.78 6.82 0.20 o 4 6 8 9.07 8.16 0.22 o 5 6 8 2.09 1.71 0.18 o 6 6 8 3.46 4.37 0.31 o 1 7 8 2.01 1.54 0.21 o 2 7 8 0.69 0.56 0.20 o 3 7 8 0.28 0.14 0.17 o 4 7 8 2.36 2.82 0.22 o 1 0 9 2.23 4.04 0.10 o 2 0 9 1.97 2.14 0.10 o 3 0 9 37.20 31.05 0.29 o 4 0 9 0.24 1.67 0.14 o 5 0 9 36.24 33.11 0.43 o 6 0 9 222.87 220.43 2.26 o 7 0 9 0.15 -0.15 0.20 o 8 0 9 2.05 1.98 0.29 o 9 0 9 9.84 8.83 0.37 o 10 0 9 4.06 6.04 0.41 o 0 1 9 1053.16 1159.37 5.80 o 1 1 9 128.87 144.82 0.58 o 2 1 9 216.01 207.03 0.87 o 3 1 9 33.90 26.48 0.21 o 4 1 9 29.84 30.75 0.24 o 5 1 9 14.74 18.41 0.24 o 6 1 9 14.35 14.73 0.23 o 7 1 9 8.17 7.33 0.19 o 8 1 9 24.44 21.32 0.33 o 9 1 9 3.72 4.52 0.23 o 10 1 9 1.57 2.58 0.23 o 1 2 9 1.72 2.06 0.09 o 2 2 9 0.15 0.05 0.06 o 3 2 9 6.78 4.62 0.12 o 4 2 9 0.50 0.03 0.08 o 5 2 9 11.70 12.08 0.19 o 6 2 9 145.01 140.75 1.12 o 7 2 9 2.42 2.34 0.15 o 8 2 9 2.88 2.25 0.16 o 9 2 9 5.55 5.63 0.24 o 0 3 9 604.26 605.40 4.58 o 1 3 9 62.72 67.28 0.40 o 2 3 9 33.59 31.93 0.31 o 3 3 9 15.56 14.55 0.21 o 4 3 9 12.21 12.95 0.21 o 5 3 9 5.86 6.53 0.17 o 6 3 9 3.89 4.10 0.18 o 7 3 9 13.53 14.45 0.31 o 8 3 9 17.01 15.52 0.33 o 9 3 9 0.62 0.56 0.20 o 1 4 9 15.60 14.44 0.21 o 2 4 9 1.66 1.63 0.12 o 3 4 9 9.37 10.26 0.19 o 4 4 9 2.41 2.10 0.14 o 5 4 9 0.22 0.23 0.13 o 6 4 9 48.36 49.17 0.46 o 7 4 9 6.75 7.62 0.30 o 8 4 9 1.55 1.19 0.21 o 0 5 9 147.25 136.39 1.25 o 1 5 9 26.96 29.35 0.32 o 2 5 9 0.92 0.58 0.12 o 3 5 9 4.33 4.18 0.18 o 4 5 9 3.60 4.02 0.26 o 5 5 9 0.38 0.48 0.14 o 6 5 9 0.10 0.07 0.16 o 7 5 9 10.13 12.56 0.27 o 1 6 9 11.48 10.30 0.23 o 2 6 9 5.39 5.63 0.21 o 3 6 9 13.93 13.95 0.25 o 4 6 9 0.55 0.51 0.17 o 5 6 9 2.20 3.02 0.32 o 6 6 9 12.48 12.19 0.27 o 0 7 9 23.77 18.30 0.52 o 1 7 9 6.15 7.10 0.42 o 2 7 9 0.32 0.31 0.18 o 3 7 9 0.48 0.21 0.18 o 4 7 9 0.18 0.07 0.22 o 0 0 10 279.96 296.42 2.23 o 1 0 10 89.05 67.66 0.45 o 2 0 10 10.14 9.71 0.17 o 3 0 10 412.08 421.79 2.45 o 4 0 10 18.98 20.08 0.33 o 5 0 10 464.13 476.30 3.57 o 6 0 10 8.99 7.98 0.31 o 7 0 10 0.20 0.22 0.33 o 8 0 10 6.21 4.19 0.33 o 9 0 10 0.59 0.23 0.27 o 1 1 10 0.67 0.43 0.08 o 2 1 10 20.16 26.39 0.19 o 3 1 10 382.10 378.41 1.69 o 4 1 10 76.19 74.80 0.48 o 5 1 10 12.37 8.67 0.17 o 6 1 10 81.46 73.64 0.58 o 7 1 10 32.43 35.72 0.43 o 8 1 10 14.50 11.51 0.27 o 9 1 10 3.92 4.66 0.24 o 0 2 10 123.09 132.51 0.83 o 1 2 10 57.35 49.15 0.28 o 2 2 10 16.04 15.97 0.17 o 3 2 10 253.93 257.61 1.29 o 4 2 10 13.08 12.93 0.18 o 5 2 10 320.06 327.99 1.70 o 6 2 10 9.49 8.32 0.26 o 7 2 10 1.36 1.35 0.15 o 8 2 10 3.90 2.93 0.30 o 9 2 10 0.08 0.09 0.19 o 1 3 10 13.92 14.34 0.19 o 2 3 10 23.36 24.16 0.24 o 3 3 10 115.44 116.45 0.77 o 4 3 10 36.68 34.46 0.36 o 5 3 10 1.77 0.89 0.14 o 6 3 10 55.46 50.63 0.50 o 7 3 10 3.98 6.58 0.29 o 8 3 10 2.50 2.35 0.21 o 0 4 10 24.96 27.40 0.43 o 1 4 10 9.84 9.24 0.17 o 2 4 10 5.73 4.93 0.19 o 3 4 10 64.63 67.84 0.54 o 4 4 10 6.54 6.29 0.19 o 5 4 10 132.67 135.60 0.92 o 6 4 10 6.54 7.13 0.20 o 7 4 10 3.49 4.56 0.26 o 8 4 10 0.95 0.04 0.20 o 1 5 10 35.42 31.51 0.38 o 2 5 10 10.31 9.69 0.20 o 3 5 10 9.15 9.39 0.21 o 4 5 10 8.88 8.41 0.21 o 5 5 10 0.00 -0.05 0.15 o 6 5 10 22.57 23.53 0.37 o 7 5 10 0.14 0.16 0.18 o 0 6 10 5.06 5.43 0.37 o 1 6 10 0.47 0.12 0.16 o 2 6 10 0.60 0.27 0.16 o 3 6 10 7.08 8.26 0.24 o 4 6 10 1.03 0.92 0.17 o 5 6 10 38.03 41.05 0.46 o 1 7 10 18.60 18.00 0.38 o 2 7 10 2.28 2.33 0.21 o 3 7 10 0.61 0.80 0.26 o 1 0 11 12.06 15.38 0.19 o 2 0 11 0.53 0.90 0.11 o 3 0 11 54.70 52.69 0.50 o 4 0 11 193.49 175.66 1.46 o 5 0 11 38.27 30.73 0.57 o 6 0 11 2.73 2.03 0.26 o 7 0 11 56.92 49.92 0.81 o 8 0 11 0.56 0.66 0.26 o 9 0 11 1.86 2.98 0.38 o 0 1 11 286.68 268.29 1.45 o 1 1 11 312.54 313.70 1.25 o 2 1 11 16.65 17.43 0.17 o 3 1 11 64.60 59.42 0.39 o 4 1 11 307.51 323.71 1.71 o 5 1 11 5.96 5.68 0.16 o 6 1 11 49.48 47.74 0.45 o 7 1 11 33.45 31.14 0.41 o 8 1 11 36.10 38.69 0.48 o 9 1 11 0.03 -0.20 0.20 o 1 2 11 3.82 3.90 0.15 o 2 2 11 0.42 0.29 0.10 o 3 2 11 18.02 17.39 0.21 o 4 2 11 146.93 135.08 0.77 o 5 2 11 10.49 8.78 0.20 o 6 2 11 0.25 0.25 0.13 o 7 2 11 29.06 28.17 0.35 o 8 2 11 0.00 -0.17 0.17 o 9 2 11 1.04 2.18 0.22 o 0 3 11 116.96 111.65 0.84 o 1 3 11 114.85 116.62 0.68 o 2 3 11 13.61 13.45 0.19 o 3 3 11 31.90 31.21 0.30 o 4 3 11 141.62 146.16 0.95 o 5 3 11 3.44 3.57 0.16 o 6 3 11 16.81 16.70 0.26 o 7 3 11 9.50 9.06 0.21 o 8 3 11 17.08 16.66 0.30 o 1 4 11 2.00 1.60 0.13 o 2 4 11 3.47 3.47 0.17 o 3 4 11 3.13 2.70 0.16 o 4 4 11 65.94 63.93 0.54 o 5 4 11 0.45 0.62 0.15 o 6 4 11 0.96 0.73 0.15 o 7 4 11 4.72 4.89 0.28 o 0 5 11 40.77 38.48 0.56 o 1 5 11 24.69 24.93 0.35 o 2 5 11 10.04 10.37 0.22 o 3 5 11 15.42 14.13 0.25 o 4 5 11 39.50 39.87 0.43 o 5 5 11 0.60 0.36 0.18 o 6 5 11 2.49 2.94 0.20 o 1 6 11 7.12 7.37 0.26 o 2 6 11 2.01 1.78 0.19 o 3 6 11 10.22 10.34 0.24 o 4 6 11 19.14 19.64 0.31 o 5 6 11 1.18 1.83 0.26 o 0 7 11 10.48 8.93 0.49 o 1 7 11 5.52 5.76 0.31 o 0 0 12 190.88 179.52 1.45 o 1 0 12 34.26 42.11 0.34 o 2 0 12 144.53 154.94 1.02 o 3 0 12 53.94 58.35 0.55 o 4 0 12 215.85 208.62 1.49 o 5 0 12 139.76 125.95 1.46 o 6 0 12 43.71 40.05 0.70 o 7 0 12 2.34 1.96 0.29 o 8 0 12 1.33 0.70 0.29 o 1 1 12 287.92 279.11 1.13 o 2 1 12 210.56 201.27 0.95 o 3 1 12 0.09 0.27 0.11 o 4 1 12 20.75 24.60 0.29 o 5 1 12 4.17 4.62 0.18 o 6 1 12 7.06 5.91 0.24 o 7 1 12 5.52 7.76 0.26 o 8 1 12 22.14 26.09 0.43 o 0 2 12 148.87 136.78 0.93 o 1 2 12 26.10 30.44 0.26 o 2 2 12 59.17 65.76 0.44 o 3 2 12 25.03 27.43 0.27 o 4 2 12 158.57 159.87 0.89 o 5 2 12 98.14 89.77 0.63 o 6 2 12 30.28 28.99 0.35 o 7 2 12 0.19 0.19 0.15 o 8 2 12 0.89 0.67 0.19 o 1 3 12 131.61 129.87 0.75 o 2 3 12 138.32 137.07 0.85 o 3 3 12 5.87 7.01 0.20 o 4 3 12 3.18 4.40 0.24 o 5 3 12 2.48 2.32 0.16 o 6 3 12 1.95 2.08 0.17 o 7 3 12 0.76 1.47 0.17 o 8 3 12 10.89 13.02 0.32 o 0 4 12 83.19 82.41 0.88 o 1 4 12 11.17 12.41 0.22 o 2 4 12 1.07 1.96 0.15 o 3 4 12 3.80 4.57 0.19 o 4 4 12 70.33 73.02 0.60 o 5 4 12 32.64 30.95 0.37 o 6 4 12 9.86 10.24 0.23 o 7 4 12 0.43 0.90 0.22 o 1 5 12 22.80 24.95 0.36 o 2 5 12 56.63 58.85 0.58 o 3 5 12 14.72 14.79 0.27 o 4 5 12 0.00 -0.15 0.15 o 5 5 12 7.80 8.28 0.24 o 6 5 12 0.01 -0.09 0.22 o 0 6 12 26.25 29.60 0.65 o 1 6 12 1.31 1.00 0.20 o 2 6 12 1.88 1.57 0.20 o 3 6 12 1.05 1.20 0.21 o 4 6 12 20.42 23.22 0.35 o 1 0 13 189.94 174.92 1.14 o 2 0 13 1.34 1.09 0.22 o 3 0 13 237.05 216.49 1.54 o 4 0 13 33.19 28.52 0.46 o 5 0 13 0.10 0.05 0.23 o 6 0 13 0.32 -0.15 0.24 o 7 0 13 3.00 2.80 0.33 o 8 0 13 1.63 1.93 0.34 o 0 1 13 616.63 602.00 3.46 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