#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/45/2204574.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204574_Fobs loop_ _publ_author_name 'Akitsu, Takashiro' 'Einaga, Yasuaki' _publ_section_title ; Bis[2-(quinolin-3-yliminomethyl)phenolato-\k^2^N,O]copper(II) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1552 _journal_page_last m1554 _journal_volume 60 _journal_year 2004 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yab' _symmetry_space_group_name_H-M 'P 1 21/a 1' _[local]_cod_data_source_file tk6188Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma 2 0 0 2934.79 2839.81 15.35 4 0 0 267.77 327.36 10.27 6 0 0 130.11 115.10 7.68 8 0 0 26.00 19.93 9.66 10 0 0 401.32 380.28 24.44 12 0 0 911.33 830.41 31.92 14 0 0 56.63 42.31 13.24 16 0 0 12.36 6.71 25.65 1 1 0 2918.32 2912.28 15.47 2 1 0 893.08 926.33 13.95 3 1 0 45.66 71.36 4.42 4 1 0 44.89 55.78 4.87 5 1 0 2183.23 2151.82 13.63 6 1 0 310.78 309.46 9.77 7 1 0 1462.92 1424.79 24.78 8 1 0 3.83 8.04 17.03 9 1 0 634.75 605.47 24.32 10 1 0 6.31 21.03 20.99 11 1 0 638.54 616.82 29.01 12 1 0 46.44 35.71 14.24 13 1 0 442.82 425.02 30.48 14 1 0 1.03 32.41 22.30 15 1 0 164.37 185.23 17.96 16 1 0 0.00 8.58 25.65 0 2 0 5284.48 5857.15 19.83 1 2 0 19846.92 20652.28 98.74 2 2 0 3756.31 3653.34 29.26 3 2 0 473.56 515.08 9.02 4 2 0 3324.32 3252.10 58.92 5 2 0 81.58 99.51 9.11 6 2 0 2539.46 2482.93 29.58 7 2 0 139.59 159.04 12.91 8 2 0 1039.00 1050.27 25.87 9 2 0 20.35 3.09 20.81 10 2 0 497.08 442.50 26.30 11 2 0 17.35 17.95 24.10 12 2 0 339.36 316.18 28.27 13 2 0 73.69 36.68 27.58 14 2 0 464.94 473.48 27.35 15 2 0 6.12 26.54 25.02 16 2 0 161.89 165.04 16.19 1 3 0 2026.21 2043.48 21.72 2 3 0 5007.68 5335.71 21.80 3 3 0 1990.46 1918.15 13.82 4 3 0 1857.41 2116.28 21.10 5 3 0 1121.74 1039.82 23.12 6 3 0 180.76 211.53 19.33 7 3 0 1100.17 1042.79 26.61 8 3 0 25.28 16.09 20.95 9 3 0 387.65 388.82 26.02 10 3 0 120.66 117.93 14.30 11 3 0 218.24 238.96 19.33 12 3 0 0.02 6.00 25.64 13 3 0 89.30 106.32 13.93 14 3 0 12.33 1.27 24.36 15 3 0 143.00 151.00 15.85 0 4 0 738.06 732.76 20.69 1 4 0 298.61 320.58 19.04 2 4 0 2078.63 2095.34 28.24 3 4 0 964.73 979.63 23.51 4 4 0 219.90 201.01 19.64 5 4 0 25.22 -3.88 19.43 6 4 0 887.18 928.79 26.87 7 4 0 0.87 17.19 21.83 8 4 0 903.86 928.35 30.50 9 4 0 19.48 21.71 14.15 10 4 0 252.94 290.98 27.74 11 4 0 16.01 12.55 26.80 12 4 0 93.07 126.80 13.55 13 4 0 0.03 -24.06 24.06 14 4 0 78.48 85.31 15.30 15 4 0 75.37 57.81 16.21 1 5 0 195.71 197.28 14.74 2 5 0 371.72 372.70 22.95 3 5 0 3067.21 3210.04 38.99 4 5 0 90.20 70.12 13.08 5 5 0 133.99 151.55 13.73 6 5 0 7.64 17.51 23.79 7 5 0 350.05 359.93 27.31 8 5 0 0.85 -2.45 25.14 9 5 0 751.85 791.36 32.32 10 5 0 58.57 43.05 16.17 11 5 0 100.48 99.87 13.95 12 5 0 10.90 2.97 24.52 13 5 0 89.91 91.95 15.15 14 5 0 2.64 19.50 27.07 0 6 0 54.80 3.80 24.52 1 6 0 13.85 35.13 23.60 2 6 0 194.08 264.14 25.53 3 6 0 8.97 12.05 24.42 4 6 0 1716.66 1714.90 37.23 5 6 0 4.13 25.52 25.11 6 6 0 76.20 100.53 15.10 7 6 0 57.70 -0.44 26.53 8 6 0 244.52 263.59 20.81 9 6 0 121.44 132.68 13.81 10 6 0 107.83 141.09 14.24 11 6 0 7.79 8.31 25.13 12 6 0 15.86 9.19 26.83 1 7 0 181.62 182.26 15.77 2 7 0 10.22 28.03 25.90 3 7 0 71.36 95.85 15.55 4 7 0 7.08 38.02 26.77 5 7 0 813.72 802.96 34.52 6 7 0 17.45 -10.84 29.12 7 7 0 162.13 172.95 14.35 8 7 0 16.98 15.69 24.50 9 7 0 43.43 55.75 14.67 10 7 0 18.28 38.06 25.64 11 7 0 99.64 114.36 16.38 0 8 0 44.45 54.90 13.56 1 8 0 43.54 23.42 23.27 2 8 0 34.54 43.59 13.72 3 8 0 43.02 22.95 24.33 4 8 0 24.53 -24.82 24.82 5 8 0 31.37 1.85 25.38 6 8 0 224.05 233.49 19.36 7 8 0 58.76 20.05 26.56 8 8 0 91.81 104.02 16.07 9 8 0 2.08 -28.31 28.31 1 9 0 395.19 424.96 30.13 2 9 0 7.40 6.05 26.26 3 9 0 160.33 177.52 16.58 4 9 0 6.68 20.75 26.99 5 9 0 1.90 -27.74 27.74 -16 0 1 39.99 27.33 26.39 -14 0 1 231.47 235.75 17.71 -12 0 1 646.08 594.35 30.33 -10 0 1 1506.47 1461.88 32.75 -8 0 1 1370.77 1339.18 26.50 -6 0 1 412.39 368.27 14.79 -4 0 1 6.26 3.33 7.68 -2 0 1 3956.57 3972.76 19.53 2 0 1 8453.61 8330.41 25.48 4 0 1 1252.83 1143.40 12.63 6 0 1 7.11 12.19 8.59 8 0 1 352.99 334.77 19.41 10 0 1 646.15 625.71 26.11 12 0 1 793.43 688.25 30.92 14 0 1 73.67 84.73 13.33 16 0 1 15.30 14.10 18.04 -16 1 1 36.25 1.96 27.52 -15 1 1 73.86 70.37 14.41 -14 1 1 4.54 -3.02 22.95 -13 1 1 259.80 289.76 28.84 -12 1 1 24.94 5.08 25.24 -11 1 1 558.32 570.17 28.26 -10 1 1 3.68 -21.92 21.92 -9 1 1 1003.96 978.84 27.12 -8 1 1 69.00 73.85 10.50 -7 1 1 606.71 540.39 19.70 -6 1 1 329.58 373.53 10.32 -5 1 1 129.17 85.78 4.84 -4 1 1 368.73 404.68 14.74 -3 1 1 186.71 153.39 6.96 -2 1 1 6043.01 6354.27 26.68 -1 1 1 10982.74 11048.40 29.30 0 1 1 321.61 335.26 6.43 1 1 1 1475.66 1517.27 13.40 2 1 1 24339.89 24507.39 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53.67 13.44 14 3 1 8.91 -18.34 24.31 15 3 1 155.40 106.60 15.96 -15 4 1 12.45 18.19 27.34 -14 4 1 162.23 174.22 15.95 -13 4 1 23.24 21.43 24.55 -12 4 1 39.96 28.63 23.45 -11 4 1 3.58 3.44 18.79 -10 4 1 151.58 192.53 18.92 -9 4 1 43.95 26.17 24.71 -8 4 1 499.63 556.98 27.39 -7 4 1 149.98 156.92 13.41 -6 4 1 819.91 841.14 26.27 -5 4 1 47.39 41.16 11.48 -4 4 1 2200.20 2116.23 30.81 -3 4 1 88.37 95.57 10.47 -2 4 1 4.97 24.38 17.15 -1 4 1 647.07 727.11 21.06 0 4 1 1341.37 1399.14 17.34 1 4 1 60.81 46.15 9.90 2 4 1 5117.11 5339.82 40.33 3 4 1 737.30 776.66 23.27 4 4 1 104.56 75.45 10.96 5 4 1 28.78 37.81 11.62 6 4 1 1046.78 1074.64 28.25 7 4 1 2.82 -10.53 22.16 8 4 1 1037.51 1087.93 31.84 9 4 1 115.99 123.73 14.36 10 4 1 249.84 230.50 19.38 11 4 1 20.11 6.52 26.85 12 4 1 211.85 206.61 17.52 13 4 1 4.16 -6.65 24.37 14 4 1 103.60 113.46 15.08 15 4 1 19.43 35.50 26.38 -14 5 1 9.93 0.92 27.65 -13 5 1 178.70 228.94 19.18 -12 5 1 50.59 15.31 25.44 -11 5 1 29.90 27.66 13.73 -10 5 1 59.79 36.92 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224.33 218.51 18.10 3 6 1 150.10 171.15 14.70 4 6 1 447.25 422.68 29.23 5 6 1 76.78 28.83 25.55 6 6 1 660.10 654.88 31.34 7 6 1 48.14 67.58 15.43 8 6 1 404.20 389.69 31.30 9 6 1 109.12 113.85 13.83 10 6 1 72.24 31.62 24.74 11 6 1 1.48 10.59 24.38 12 6 1 35.14 51.08 15.50 -11 7 1 56.19 52.68 16.48 -10 7 1 0.02 -26.70 26.70 -9 7 1 40.57 64.85 14.60 -8 7 1 0.20 -17.23 23.96 -7 7 1 347.61 395.47 26.56 -6 7 1 22.57 -29.01 29.01 -5 7 1 948.81 887.84 36.43 -4 7 1 155.26 134.56 16.48 -3 7 1 259.70 302.32 28.36 -2 7 1 0.85 22.94 25.57 -1 7 1 158.08 176.87 15.67 0 7 1 106.64 97.50 10.73 1 7 1 115.17 100.10 15.56 2 7 1 11.23 30.76 25.75 3 7 1 8.00 26.52 25.85 4 7 1 4.54 14.09 26.78 5 7 1 17.71 14.12 27.02 6 7 1 22.15 29.06 28.16 7 7 1 358.16 339.46 26.38 8 7 1 16.06 -5.63 24.04 9 7 1 109.62 110.62 15.51 10 7 1 73.73 28.42 26.95 11 7 1 20.48 34.88 27.48 -9 8 1 0.67 -15.47 28.03 -8 8 1 25.58 25.98 27.52 -7 8 1 9.77 -1.87 26.00 -6 8 1 315.88 308.57 28.93 -5 8 1 0.50 -1.48 24.72 -4 8 1 1.36 -19.31 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123.28 13.48 16 0 2 197.48 186.62 16.01 -16 1 2 0.33 -8.56 26.66 -15 1 2 68.59 27.24 25.68 -14 1 2 85.62 34.54 13.82 -13 1 2 480.59 565.59 31.23 -12 1 2 8.81 8.69 24.90 -11 1 2 1000.96 991.21 32.31 -10 1 2 24.14 15.92 23.13 -9 1 2 808.13 814.11 26.72 -8 1 2 10.20 4.67 17.94 -7 1 2 1389.64 1343.89 24.93 -6 1 2 1.11 -9.11 9.11 -5 1 2 1012.74 1003.95 11.56 -4 1 2 260.23 271.77 8.68 -3 1 2 655.97 639.74 9.39 -2 1 2 251.44 272.78 8.27 -1 1 2 1789.61 1814.41 17.88 0 1 2 198.93 243.18 8.67 1 1 2 8762.33 8699.45 30.38 2 1 2 2090.09 2062.19 175.08 3 1 2 10353.44 10339.04 77.58 4 1 2 244.74 301.87 12.50 5 1 2 1376.76 1279.91 11.75 6 1 2 345.41 362.94 9.88 7 1 2 292.58 283.61 18.21 8 1 2 492.12 589.86 21.86 9 1 2 208.94 178.94 14.83 10 1 2 0.98 15.80 20.79 11 1 2 387.41 351.32 26.11 12 1 2 0.26 -24.65 24.65 13 1 2 200.43 205.55 16.13 14 1 2 17.42 24.41 22.46 15 1 2 150.46 144.33 14.79 16 1 2 9.10 -0.85 25.83 -16 2 2 230.09 312.49 29.45 -15 2 2 36.88 25.89 14.76 -14 2 2 30.95 32.87 14.07 -13 2 2 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21.53 -7 3 2 1126.62 1165.94 27.73 -6 3 2 199.40 180.36 14.14 -5 3 2 3177.48 3353.19 34.23 -4 3 2 19.85 24.24 7.72 -3 3 2 4214.17 4275.67 28.39 -2 3 2 273.75 279.28 9.12 -1 3 2 2869.26 2841.24 39.62 0 3 2 323.76 342.57 7.90 1 3 2 1410.80 1315.17 52.62 2 3 2 506.25 535.63 29.31 3 3 2 4.87 8.82 8.38 4 3 2 4673.56 5047.93 37.60 5 3 2 30.86 9.66 16.74 6 3 2 228.73 200.58 19.82 7 3 2 569.07 528.80 23.52 8 3 2 189.67 211.90 16.04 9 3 2 908.73 887.92 30.48 10 3 2 114.68 76.10 14.18 11 3 2 214.35 197.83 19.36 12 3 2 4.13 25.16 14.91 13 3 2 236.62 212.70 17.66 14 3 2 11.11 -23.83 23.83 15 3 2 124.82 152.77 15.51 -14 4 2 282.94 258.12 20.24 -13 4 2 12.19 12.40 24.76 -12 4 2 248.59 257.81 25.15 -11 4 2 65.16 18.97 27.35 -10 4 2 250.82 221.50 19.77 -9 4 2 7.31 26.01 24.84 -8 4 2 68.67 -1.88 24.96 -7 4 2 108.10 96.79 13.74 -6 4 2 851.39 901.69 27.25 -5 4 2 9.69 -1.55 20.52 -4 4 2 1577.41 1630.16 28.77 -3 4 2 11.47 18.35 17.86 -2 4 2 660.39 589.21 21.42 -1 4 2 316.31 334.46 19.45 0 4 2 1023.52 1005.82 20.82 1 4 2 466.04 513.58 20.36 2 4 2 1286.74 1303.14 25.41 3 4 2 343.29 362.36 20.45 4 4 2 597.76 569.96 22.57 5 4 2 9.06 -11.96 20.05 6 4 2 819.48 836.71 26.79 7 4 2 194.64 246.18 16.84 8 4 2 469.69 444.68 27.83 9 4 2 114.41 95.72 14.59 10 4 2 587.94 608.90 30.96 11 4 2 55.74 41.25 15.58 12 4 2 185.65 206.75 17.33 13 4 2 0.32 5.21 24.00 14 4 2 154.26 152.95 15.70 -14 5 2 2.65 9.03 27.78 -13 5 2 58.34 34.71 26.79 -12 5 2 22.59 25.05 25.18 -11 5 2 60.73 93.84 13.89 -10 5 2 0.46 -21.36 27.50 -9 5 2 243.71 290.34 28.97 -8 5 2 41.74 40.25 14.88 -7 5 2 19.08 -1.21 25.23 -6 5 2 132.21 156.87 14.66 -5 5 2 545.47 530.66 27.51 -4 5 2 5.90 34.75 12.94 -3 5 2 258.87 235.00 22.97 -2 5 2 51.68 52.63 12.06 -1 5 2 437.76 433.34 23.02 0 5 2 7.15 19.28 10.06 1 5 2 490.26 481.73 23.84 2 5 2 126.74 146.38 12.49 3 5 2 358.20 353.79 24.82 4 5 2 38.49 -7.35 22.60 5 5 2 1855.06 1874.68 36.25 6 5 2 0.06 24.46 24.18 7 5 2 1023.45 1050.22 32.65 8 5 2 16.07 -17.98 25.75 9 5 2 432.53 392.20 29.95 10 5 2 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2363.39 93.35 4 1 3 89.15 82.34 4.68 5 1 3 1323.58 1271.77 12.45 6 1 3 7.97 17.30 15.00 7 1 3 1199.81 1168.26 24.38 8 1 3 90.70 95.40 10.92 9 1 3 572.57 558.58 24.24 10 1 3 6.89 15.10 21.85 11 1 3 502.17 501.71 27.53 12 1 3 36.06 3.07 24.49 13 1 3 115.77 123.60 15.77 14 1 3 128.85 116.19 13.90 15 1 3 227.33 254.98 18.32 16 1 3 15.51 37.25 15.01 -15 2 3 120.79 92.20 15.73 -14 2 3 238.41 244.05 18.98 -13 2 3 41.76 23.75 16.29 -12 2 3 27.73 40.22 15.30 -11 2 3 32.78 51.73 14.43 -10 2 3 12.68 -7.19 24.24 -9 2 3 147.44 162.87 13.49 -8 2 3 3468.08 3544.73 39.92 -7 2 3 531.14 605.67 22.72 -6 2 3 2231.17 2145.81 30.62 -5 2 3 680.81 706.43 11.98 -4 2 3 980.51 905.97 11.79 -3 2 3 0.04 1.94 8.14 -2 2 3 1935.62 1942.91 15.57 -1 2 3 315.53 348.17 8.78 0 2 3 2650.45 2486.25 57.09 1 2 3 179.73 190.42 12.80 2 2 3 5031.77 4751.50 322.15 3 2 3 616.04 623.78 42.86 4 2 3 5559.97 5329.76 356.25 5 2 3 46.73 61.58 10.57 6 2 3 1910.18 1874.85 27.92 7 2 3 54.13 48.84 10.70 8 2 3 233.51 224.08 21.20 9 2 3 54.10 51.63 12.56 10 2 3 89.11 79.49 13.73 11 2 3 77.92 44.35 14.11 12 2 3 33.03 54.81 14.61 13 2 3 34.78 19.38 22.39 14 2 3 43.23 36.28 13.85 15 2 3 9.07 -7.43 24.78 -15 3 3 201.86 187.38 16.69 -14 3 3 26.11 7.70 18.28 -13 3 3 115.86 118.18 14.31 -12 3 3 0.97 -28.26 28.26 -11 3 3 1083.29 1072.58 35.70 -10 3 3 2.90 -25.01 25.01 -9 3 3 28.30 21.27 24.28 -8 3 3 3.37 19.69 22.59 -7 3 3 813.41 752.23 26.61 -6 3 3 168.32 168.13 14.57 -5 3 3 982.21 1044.46 24.55 -4 3 3 54.04 61.43 10.02 -3 3 3 1635.05 1584.66 19.89 -2 3 3 2.28 -4.73 8.53 -1 3 3 1361.92 1307.77 12.59 0 3 3 335.54 340.08 11.11 1 3 3 3152.33 3034.86 159.78 2 3 3 45.72 53.50 8.37 3 3 3 249.62 199.50 18.97 4 3 3 15.88 10.29 16.77 5 3 3 1624.94 1607.68 27.86 6 3 3 23.35 4.90 19.18 7 3 3 744.63 649.99 25.27 8 3 3 0.08 -21.98 21.98 9 3 3 758.13 696.36 29.26 10 3 3 0.09 -9.62 24.33 11 3 3 43.23 73.84 14.85 12 3 3 9.96 9.78 26.28 13 3 3 246.19 259.61 24.95 14 3 3 0.38 38.73 13.66 15 3 3 83.78 132.22 15.25 -14 4 3 15.46 25.50 26.73 -13 4 3 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885.45 918.06 28.29 -2 5 3 42.08 48.92 12.51 -1 5 3 1579.96 1546.08 31.68 0 5 3 252.85 258.15 16.31 1 5 3 633.26 617.82 25.39 2 5 3 72.91 72.48 12.67 3 5 3 410.67 448.79 25.53 4 5 3 521.07 504.72 26.69 5 5 3 91.98 96.16 14.20 6 5 3 170.96 179.86 14.68 7 5 3 377.42 406.42 28.03 8 5 3 40.82 -21.37 26.22 9 5 3 229.79 260.55 20.19 10 5 3 137.63 143.21 16.49 11 5 3 480.76 465.00 27.57 12 5 3 14.30 28.28 24.81 13 5 3 156.43 165.61 15.90 -12 6 3 66.38 63.33 16.23 -11 6 3 4.28 -12.17 25.92 -10 6 3 88.29 120.90 14.73 -9 6 3 101.88 91.55 14.03 -8 6 3 86.96 98.44 16.86 -7 6 3 232.89 247.67 20.76 -6 6 3 149.82 151.73 16.00 -5 6 3 88.72 90.02 15.03 -4 6 3 504.51 526.31 29.28 -3 6 3 73.80 62.19 14.28 -2 6 3 660.73 604.63 30.32 -1 6 3 1.52 -5.15 24.15 0 6 3 179.25 203.24 12.90 1 6 3 127.53 146.32 14.80 2 6 3 52.65 51.14 14.38 3 6 3 40.70 23.97 17.52 4 6 3 88.93 98.33 14.74 5 6 3 120.12 65.12 15.39 6 6 3 252.43 251.12 20.21 7 6 3 61.09 37.24 15.93 8 6 3 363.16 342.14 31.24 9 6 3 75.95 55.11 13.85 10 6 3 351.45 306.89 28.16 11 6 3 9.02 -19.13 25.37 12 6 3 87.89 71.78 16.48 -10 7 3 7.16 27.94 26.92 -9 7 3 89.78 123.71 15.34 -8 7 3 5.84 -14.22 24.86 -7 7 3 117.55 140.94 14.42 -6 7 3 324.04 366.89 26.12 -5 7 3 437.95 406.03 32.86 -4 7 3 6.44 -2.85 27.02 -3 7 3 221.58 219.49 20.72 -2 7 3 36.27 26.46 27.07 -1 7 3 79.29 83.50 15.47 0 7 3 0.21 -13.79 18.38 1 7 3 470.82 542.76 31.07 2 7 3 39.52 57.26 15.57 3 7 3 848.62 762.90 35.69 4 7 3 206.64 233.12 20.71 5 7 3 378.33 362.62 31.92 6 7 3 4.14 24.04 16.20 7 7 3 89.93 84.50 14.42 8 7 3 28.59 17.67 17.64 9 7 3 4.13 -23.43 25.80 10 7 3 18.02 30.86 27.50 -8 8 3 73.67 87.22 16.47 -7 8 3 5.86 17.62 26.77 -6 8 3 8.14 2.87 26.14 -5 8 3 72.98 23.37 18.21 -4 8 3 394.49 321.07 28.92 -3 8 3 7.54 34.36 24.17 -2 8 3 131.18 150.87 14.39 -1 8 3 13.67 19.89 23.57 0 8 3 43.27 53.19 26.56 1 8 3 8.96 21.33 23.70 2 8 3 318.92 304.61 27.07 3 8 3 22.90 -3.58 25.21 4 8 3 98.36 77.61 15.07 5 8 3 1.11 17.60 14.41 6 8 3 75.10 45.42 15.59 7 8 3 0.04 16.91 26.17 8 8 3 6.32 37.63 27.91 -4 9 3 2.25 -28.66 28.66 -3 9 3 161.41 165.25 16.80 -2 9 3 3.44 14.62 26.97 -1 9 3 66.82 67.91 16.11 0 9 3 1.14 -7.52 24.62 1 9 3 43.58 53.62 15.91 2 9 3 0.47 11.53 18.98 3 9 3 26.63 23.61 27.95 4 9 3 0.99 20.59 27.55 -16 0 4 64.73 65.72 15.94 -14 0 4 191.18 215.68 18.15 -12 0 4 39.82 49.67 15.20 -10 0 4 6345.69 6175.37 58.60 -8 0 4 963.27 940.10 26.69 -6 0 4 20.60 70.59 9.95 -4 0 4 4055.67 4213.62 82.62 -2 0 4 383.58 284.48 11.19 0 0 4 326.24 245.33 11.09 2 0 4 662.18 647.92 11.96 4 0 4 886.55 898.89 13.59 6 0 4 289.89 280.68 17.14 8 0 4 1804.84 1740.86 29.59 10 0 4 427.97 414.36 25.26 12 0 4 116.82 120.42 14.90 14 0 4 385.23 383.30 26.51 16 0 4 161.01 175.02 15.89 -16 1 4 1.39 1.30 27.36 -15 1 4 87.66 78.08 15.21 -14 1 4 0.30 -19.50 24.40 -13 1 4 2.29 -21.15 27.73 -12 1 4 29.82 -2.37 27.50 -11 1 4 98.66 114.14 15.06 -10 1 4 815.62 821.29 30.30 -9 1 4 1806.06 1845.01 34.89 -8 1 4 379.89 390.47 22.73 -7 1 4 1231.46 1209.65 26.84 -6 1 4 478.12 530.17 20.71 -5 1 4 2625.91 2655.07 17.20 -4 1 4 2002.33 2269.05 30.83 -3 1 4 3457.85 3614.47 48.59 -2 1 4 262.90 266.84 9.13 -1 1 4 660.73 635.47 9.91 0 1 4 298.33 298.22 7.89 1 1 4 2514.29 2353.98 131.63 2 1 4 213.59 226.92 8.67 3 1 4 3913.36 3799.31 167.41 4 1 4 17.85 13.49 6.39 5 1 4 1931.32 1919.33 14.85 6 1 4 40.11 44.65 9.39 7 1 4 1167.37 1142.75 24.88 8 1 4 36.54 25.58 19.13 9 1 4 473.18 464.80 23.99 10 1 4 9.20 32.72 21.85 11 1 4 114.23 122.85 14.09 12 1 4 10.63 -20.21 24.78 13 1 4 200.08 202.71 20.08 14 1 4 0.24 17.66 23.28 15 1 4 146.79 161.77 15.11 -15 2 4 2.14 18.15 25.70 -14 2 4 251.12 273.04 26.87 -13 2 4 81.84 75.40 13.94 -12 2 4 276.13 300.09 29.92 -11 2 4 421.71 429.61 29.37 -10 2 4 11.79 8.54 24.21 -9 2 4 301.64 325.88 25.42 -8 2 4 1282.46 1270.35 30.41 -7 2 4 58.36 66.37 11.87 -6 2 4 2291.44 2264.96 32.61 -5 2 4 268.52 296.65 19.49 -4 2 4 1130.60 1054.12 12.92 -3 2 4 1077.82 1188.86 19.76 -2 2 4 1962.11 2010.96 14.10 -1 2 4 120.25 115.96 6.04 0 2 4 1238.82 1155.87 21.46 1 2 4 2.74 3.76 7.98 2 2 4 1453.99 1340.45 94.83 3 2 4 49.69 60.26 5.07 4 2 4 1557.69 1491.75 99.65 5 2 4 10.63 -1.57 16.24 6 2 4 1785.70 1719.79 28.12 7 2 4 33.12 15.11 19.29 8 2 4 219.55 215.24 15.89 9 2 4 54.59 66.83 12.98 10 2 4 138.24 133.03 14.26 11 2 4 1.50 -24.32 24.32 12 2 4 224.92 290.30 27.12 13 2 4 56.73 52.58 13.09 14 2 4 85.74 84.60 14.24 15 2 4 0.97 6.77 24.98 -15 3 4 209.09 209.32 16.98 -14 3 4 102.37 65.51 15.58 -13 3 4 387.23 457.83 28.02 -12 3 4 117.14 71.12 16.98 -11 3 4 496.49 490.11 31.75 -10 3 4 107.58 122.95 15.12 -9 3 4 100.90 105.62 14.58 -8 3 4 549.47 501.95 27.68 -7 3 4 208.41 178.55 16.70 -6 3 4 455.61 453.57 23.99 -5 3 4 619.82 614.54 23.08 -4 3 4 238.05 231.35 19.80 -3 3 4 1099.44 1148.45 24.18 -2 3 4 529.85 552.31 11.27 -1 3 4 692.19 611.49 14.18 0 3 4 558.98 618.46 20.17 1 3 4 243.32 179.45 17.34 2 3 4 718.39 720.88 49.23 3 3 4 869.74 830.42 21.66 4 3 4 66.19 87.23 10.35 5 3 4 2840.45 2829.79 33.99 6 3 4 16.90 30.11 11.33 7 3 4 2070.39 2064.52 33.87 8 3 4 217.82 243.61 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220.97 223.40 18.96 -10 5 4 0.10 -20.76 23.56 -9 5 4 79.29 63.74 16.32 -8 5 4 240.49 233.04 20.72 -7 5 4 1058.66 1073.47 33.94 -6 5 4 21.83 7.93 25.33 -5 5 4 148.75 117.07 14.63 -4 5 4 2.45 18.67 13.57 -3 5 4 507.35 525.07 27.13 -2 5 4 12.38 8.37 22.36 -1 5 4 3405.71 3532.63 42.43 0 5 4 61.67 79.54 21.45 1 5 4 1242.03 1235.42 30.34 2 5 4 4.36 -11.66 22.31 3 5 4 124.86 118.99 13.93 4 5 4 99.30 103.24 13.99 5 5 4 78.58 51.29 14.16 6 5 4 0.07 -18.43 24.28 7 5 4 15.23 2.87 24.96 8 5 4 84.25 57.58 15.25 9 5 4 51.97 34.32 27.89 10 5 4 4.52 20.52 22.71 11 5 4 595.60 559.85 28.96 12 5 4 33.42 -22.56 25.51 13 5 4 291.24 289.92 28.82 -12 6 4 96.94 90.99 16.71 -11 6 4 3.89 -26.87 26.87 -10 6 4 11.10 9.60 25.35 -9 6 4 13.27 19.98 24.28 -8 6 4 26.24 55.28 16.18 -7 6 4 4.52 -3.81 27.39 -6 6 4 747.10 767.26 33.89 -5 6 4 0.88 19.83 25.53 -4 6 4 184.45 181.39 15.84 -3 6 4 7.81 20.44 24.71 -2 6 4 107.39 89.45 14.98 -1 6 4 20.83 -24.55 24.55 0 6 4 416.80 438.81 19.58 1 6 4 66.61 17.75 25.43 2 6 4 96.57 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7 9.50 -20.31 25.19 8 4 7 247.30 248.11 19.89 9 4 7 20.10 44.59 15.60 10 4 7 619.46 622.37 27.82 11 4 7 39.79 25.72 17.40 12 4 7 40.31 24.75 17.87 13 4 7 40.52 22.81 15.28 -12 5 7 0.40 6.94 27.83 -11 5 7 312.97 335.63 29.54 -10 5 7 1.02 15.25 25.34 -9 5 7 298.63 280.32 27.34 -8 5 7 21.41 -29.13 29.13 -7 5 7 59.24 81.95 16.10 -6 5 7 96.08 44.15 16.18 -5 5 7 11.61 6.33 26.18 -4 5 7 11.27 28.84 14.83 -3 5 7 43.55 46.40 14.81 -2 5 7 0.40 -20.31 25.35 -1 5 7 255.26 258.75 19.49 0 5 7 87.94 86.96 10.57 1 5 7 912.06 918.24 32.74 2 5 7 58.88 53.62 14.84 3 5 7 1048.48 1102.45 33.50 4 5 7 50.50 -4.93 26.04 5 5 7 37.51 59.76 14.94 6 5 7 6.47 -24.65 26.81 7 5 7 317.39 329.72 30.32 8 5 7 59.79 52.75 16.25 9 5 7 139.64 129.05 14.37 10 5 7 91.85 103.05 14.46 11 5 7 73.51 64.68 15.31 12 5 7 48.98 26.79 27.21 -11 6 7 10.64 30.08 28.64 -10 6 7 37.90 55.52 15.89 -9 6 7 10.93 3.98 26.45 -8 6 7 152.14 161.57 15.39 -7 6 7 16.98 6.41 24.64 -6 6 7 484.38 458.61 28.25 -5 6 7 0.05 -28.91 28.91 -4 6 7 409.60 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8 3.59 14.71 19.70 5 1 8 838.85 876.38 26.98 6 1 8 43.90 27.74 12.82 7 1 8 111.54 125.17 13.62 8 1 8 73.97 69.96 13.85 9 1 8 528.86 547.23 29.03 10 1 8 246.45 235.28 19.74 11 1 8 295.13 299.86 21.13 12 1 8 18.86 -3.13 23.59 13 1 8 10.53 22.24 24.21 14 1 8 6.07 18.96 25.38 -14 2 8 75.61 68.73 16.40 -13 2 8 23.52 27.50 25.97 -12 2 8 197.62 184.81 15.55 -11 2 8 5.86 4.55 23.36 -10 2 8 53.95 72.57 16.22 -9 2 8 61.61 14.07 27.25 -8 2 8 137.88 154.84 15.67 -7 2 8 21.62 32.01 25.36 -6 2 8 141.86 182.69 18.19 -5 2 8 19.82 21.34 13.45 -4 2 8 1228.05 1275.85 32.40 -3 2 8 43.69 53.36 12.89 -2 2 8 1226.02 1319.17 30.20 -1 2 8 13.14 3.26 20.59 0 2 8 907.08 934.91 18.98 1 2 8 0.03 -14.21 20.07 2 2 8 784.49 825.97 26.16 3 2 8 35.18 30.49 20.79 4 2 8 927.31 873.76 28.34 5 2 8 80.55 93.57 12.89 6 2 8 182.94 181.61 17.26 7 2 8 146.03 150.65 14.29 8 2 8 1354.16 1371.48 35.07 9 2 8 481.53 448.17 29.79 10 2 8 55.88 38.60 27.16 11 2 8 33.78 17.28 22.91 12 2 8 2.62 30.43 23.15 13 2 8 34.08 27.45 25.33 14 2 8 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27.42 26.96 4 2 16 37.38 94.39 16.11 -2 3 16 2.73 -10.90 29.56 -1 3 16 5.39 3.60 20.50 0 3 16 2.66 13.28 21.85 1 3 16 55.84 75.11 16.62 2 3 16 20.12 26.97 28.53 0 0 17 77.12 72.58 14.64