#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:07:34 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180965 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/45/2204595.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2204595_Fobs loop_ _publ_author_name 'Cline, Daniel J.' 'Schnieder, Joel P.' 'Thorpe, Colin' 'Yap, Glenn P. A.' _publ_section_title ; 1-Benzylsulfanyl-2-(benzylsulfanylmethyl)propanaminium chloride ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o1972 _journal_page_last o1974 _journal_volume 60 _journal_year 2004 _space_group_IT_number 18 _symmetry_space_group_name_Hall 'P 2 2ab' _symmetry_space_group_name_H-M 'P 21 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.3957 _cell_length_b 31.6333 _cell_length_c 7.1438 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.7494 _cod_data_source_file ya6215Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' joes003a in P2(1)2(1)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 460.72 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5464.96 5574.20 73.47 o 4 0 0 212260.80 240021.52 3399.51 o 6 0 0 540.38 556.63 21.94 o 8 0 0 430.08 382.31 13.12 o 10 0 0 416.66 393.98 23.83 o 12 0 0 680.07 675.48 31.38 o 14 0 0 26.89 40.11 12.02 o 16 0 0 641.06 711.64 36.69 o 18 0 0 268.26 254.90 24.75 o 20 0 0 4.14 5.22 14.16 o 2 1 0 5.60 4.97 2.06 o 3 1 0 2890.04 3254.85 30.64 o 4 1 0 1043.18 1046.48 18.24 o 5 1 0 36663.62 39928.19 278.57 o 6 1 0 921.87 959.08 14.39 o 7 1 0 46567.53 52449.41 365.56 o 8 1 0 46.08 40.84 5.60 o 9 1 0 36656.46 40356.32 309.66 o 10 1 0 520.13 550.90 14.35 o 11 1 0 9218.97 8986.99 100.98 o 12 1 0 48.34 55.85 9.65 o 13 1 0 912.97 917.28 26.58 o 14 1 0 13.86 23.42 7.51 o 15 1 0 1946.80 1718.36 38.97 o 16 1 0 11.79 20.50 12.85 o 17 1 0 8.03 17.37 7.03 o 18 1 0 80.32 75.28 9.16 o 19 1 0 95.47 120.83 14.32 o 20 1 0 74.53 105.37 16.04 o 21 1 0 19.65 38.44 11.80 o 1 2 0 9.95 3.03 1.36 o 2 2 0 2285.24 2350.24 22.48 o 3 2 0 0.22 -3.41 3.41 o 4 2 0 173.14 259.38 8.73 o 5 2 0 9.55 8.99 4.76 o 6 2 0 1849.16 1820.67 24.80 o 7 2 0 50.90 48.63 6.04 o 8 2 0 1834.78 2205.37 30.40 o 9 2 0 111.17 93.55 7.77 o 10 2 0 371.24 406.33 16.19 o 11 2 0 7.66 8.77 7.20 o 12 2 0 2506.38 2330.36 51.45 o 13 2 0 82.03 79.83 10.62 o 14 2 0 1176.91 1180.30 30.85 o 15 2 0 41.34 50.00 8.84 o 16 2 0 1354.92 1266.12 34.11 o 17 2 0 11.76 24.34 8.57 o 18 2 0 2741.35 2460.70 51.14 o 19 2 0 1.03 5.28 12.38 o 20 2 0 413.09 424.17 29.09 o 21 2 0 84.17 100.28 39.25 o 1 3 0 318.59 375.40 5.99 o 2 3 0 25.33 28.21 2.91 o 3 3 0 17361.85 20255.19 143.71 o 4 3 0 1694.47 1734.58 19.71 o 5 3 0 3181.71 3760.54 38.90 o 6 3 0 35.81 45.83 6.28 o 7 3 0 5789.47 5826.03 57.52 o 8 3 0 46.27 48.08 6.62 o 9 3 0 1812.27 2024.33 30.11 o 10 3 0 108.60 111.16 8.34 o 11 3 0 3037.66 2690.99 44.45 o 12 3 0 133.29 109.81 12.34 o 13 3 0 7.56 10.42 6.78 o 14 3 0 140.94 154.32 13.31 o 15 3 0 231.71 192.44 15.56 o 16 3 0 188.55 173.57 15.03 o 17 3 0 254.90 274.11 18.61 o 18 3 0 39.98 65.13 8.49 o 19 3 0 667.11 590.81 33.63 o 20 3 0 92.64 98.68 22.77 o 21 3 0 0.40 -1.65 23.72 o 0 4 0 22014.12 25299.89 381.22 o 1 4 0 40.03 39.85 2.71 o 2 4 0 3258.40 3689.16 31.11 o 3 4 0 3.87 -1.20 3.72 o 4 4 0 9962.07 10937.44 83.09 o 5 4 0 11.48 10.98 3.91 o 6 4 0 5308.37 5802.27 56.06 o 7 4 0 498.17 507.09 14.48 o 8 4 0 131.24 147.52 9.12 o 9 4 0 311.11 330.44 12.94 o 10 4 0 81.92 55.77 7.08 o 11 4 0 930.20 843.24 24.46 o 12 4 0 2349.97 2186.43 40.80 o 13 4 0 1.44 8.46 6.80 o 14 4 0 249.58 220.92 15.81 o 15 4 0 369.21 325.50 18.98 o 16 4 0 948.53 821.16 27.34 o 17 4 0 56.07 81.35 12.37 o 18 4 0 1327.95 1283.76 35.49 o 19 4 0 22.89 78.91 21.55 o 20 4 0 1524.88 1277.14 44.50 o 21 4 0 17.42 16.89 14.90 o 1 5 0 8133.94 8871.02 105.49 o 2 5 0 9.70 -3.54 3.54 o 3 5 0 1120.76 1230.27 16.11 o 4 5 0 185.59 206.32 7.63 o 5 5 0 266.39 395.58 10.48 o 6 5 0 59.09 63.89 5.26 o 7 5 0 871.12 1124.11 20.84 o 8 5 0 158.80 179.60 10.06 o 9 5 0 1763.38 1843.22 29.33 o 10 5 0 6.05 1.59 5.06 o 11 5 0 1966.32 1852.50 49.67 o 12 5 0 28.73 33.36 8.81 o 13 5 0 402.09 377.32 18.91 o 14 5 0 354.60 350.37 19.05 o 15 5 0 0.83 11.51 6.56 o 16 5 0 0.06 10.18 9.29 o 17 5 0 78.78 83.33 10.76 o 18 5 0 603.91 612.21 27.81 o 19 5 0 88.14 126.39 15.88 o 20 5 0 3.94 40.72 18.21 o 0 6 0 9061.11 10444.77 111.97 o 1 6 0 141.20 144.45 5.28 o 2 6 0 16757.01 18071.80 129.23 o 3 6 0 70.27 74.03 5.43 o 4 6 0 91.36 95.06 6.21 o 5 6 0 0.14 0.24 4.40 o 6 6 0 1387.46 1618.91 21.85 o 7 6 0 1.52 0.37 3.55 o 8 6 0 5608.22 5791.05 60.27 o 9 6 0 252.81 238.24 11.68 o 10 6 0 51.19 34.98 6.95 o 11 6 0 17.40 35.40 8.13 o 12 6 0 4049.95 3821.77 57.11 o 13 6 0 154.56 120.47 12.69 o 14 6 0 33.24 60.38 9.62 o 15 6 0 460.89 434.00 21.59 o 16 6 0 225.55 232.28 17.39 o 17 6 0 7.96 23.30 9.90 o 18 6 0 714.27 690.84 26.95 o 19 6 0 275.07 261.41 22.94 o 20 6 0 149.32 202.00 20.46 o 1 7 0 10.54 32.56 4.19 o 2 7 0 229.88 211.65 9.83 o 3 7 0 5052.25 5332.86 45.58 o 4 7 0 56.26 61.28 5.75 o 5 7 0 50.82 27.72 5.31 o 6 7 0 589.17 610.18 13.65 o 7 7 0 2399.61 2329.82 28.57 o 8 7 0 173.84 209.44 12.45 o 9 7 0 1.20 -4.08 5.01 o 10 7 0 129.15 156.54 10.78 o 11 7 0 2770.61 2661.19 39.71 o 12 7 0 597.25 530.63 21.08 o 13 7 0 2061.36 1763.66 37.78 o 14 7 0 151.35 146.46 13.93 o 15 7 0 1731.84 1474.37 36.03 o 16 7 0 229.43 185.67 15.69 o 17 7 0 2684.78 2422.07 50.06 o 18 7 0 208.43 217.69 16.36 o 19 7 0 404.28 450.92 29.80 o 20 7 0 2.56 35.78 16.21 o 0 8 0 18478.15 21042.18 231.33 o 1 8 0 430.11 446.69 9.73 o 2 8 0 259.38 295.42 8.84 o 3 8 0 306.47 338.86 10.28 o 4 8 0 9773.99 11171.07 88.77 o 5 8 0 179.50 183.46 8.28 o 6 8 0 2968.48 3230.29 37.12 o 7 8 0 206.97 198.08 9.01 o 8 8 0 2508.64 2393.49 29.94 o 9 8 0 0.72 4.68 5.01 o 10 8 0 379.14 420.70 15.68 o 11 8 0 231.20 220.59 12.72 o 12 8 0 3745.24 3550.28 55.83 o 13 8 0 191.14 166.12 13.97 o 14 8 0 469.35 510.06 21.66 o 15 8 0 181.42 179.88 15.04 o 16 8 0 267.64 272.73 18.50 o 17 8 0 425.65 446.76 23.14 o 18 8 0 2966.86 2714.25 54.43 o 19 8 0 0.22 27.89 23.90 o 20 8 0 495.07 479.79 35.63 o 1 9 0 10767.94 11666.98 88.25 o 2 9 0 545.69 591.81 14.87 o 3 9 0 2713.35 2880.08 29.91 o 4 9 0 633.84 655.10 14.02 o 5 9 0 13841.65 14806.10 113.51 o 6 9 0 492.17 505.82 13.59 o 7 9 0 8109.68 8041.53 70.37 o 8 9 0 36.22 60.71 6.11 o 9 9 0 2223.85 2153.83 33.37 o 10 9 0 0.96 7.62 5.99 o 11 9 0 6630.05 6431.36 71.50 o 12 9 0 74.40 50.28 9.74 o 13 9 0 0.15 6.81 6.53 o 14 9 0 83.72 78.38 10.81 o 15 9 0 8.11 9.39 8.52 o 16 9 0 59.09 68.14 9.97 o 17 9 0 698.45 739.16 27.18 o 18 9 0 0.09 32.65 13.09 o 19 9 0 501.48 528.76 44.18 o 20 9 0 161.33 173.73 18.60 o 0 10 0 114159.64 128186.66 1473.70 o 1 10 0 3628.12 3723.41 34.99 o 2 10 0 386.56 425.07 12.89 o 3 10 0 2306.24 2299.41 26.37 o 4 10 0 25664.76 27273.32 196.38 o 5 10 0 3.29 -0.04 4.58 o 6 10 0 741.83 655.77 15.20 o 7 10 0 23.89 22.97 5.55 o 8 10 0 50.43 95.05 7.12 o 9 10 0 100.06 130.60 10.12 o 10 10 0 3488.38 3334.04 45.62 o 11 10 0 9.02 15.46 6.62 o 12 10 0 1586.12 1585.63 34.84 o 13 10 0 2.04 10.34 6.75 o 14 10 0 339.80 345.94 19.19 o 15 10 0 0.49 1.47 6.61 o 16 10 0 1152.27 1123.79 32.46 o 17 10 0 14.36 22.56 8.57 o 18 10 0 468.00 530.64 25.48 o 19 10 0 145.12 181.26 20.90 o 20 10 0 492.59 553.09 34.08 o 1 11 0 22771.71 24817.85 178.36 o 2 11 0 1823.22 1830.09 28.13 o 3 11 0 27.67 36.08 5.20 o 4 11 0 1651.81 1603.11 22.39 o 5 11 0 28804.52 31572.26 227.28 o 6 11 0 3.74 4.65 4.43 o 7 11 0 19566.30 20405.14 155.49 o 8 11 0 2173.07 2097.62 29.22 o 9 11 0 5260.31 5163.03 58.85 o 10 11 0 525.52 504.07 17.13 o 11 11 0 6756.58 6481.41 109.49 o 12 11 0 590.27 576.68 24.23 o 13 11 0 3027.44 2733.07 53.49 o 14 11 0 9.61 15.00 7.48 o 15 11 0 29.11 38.47 9.96 o 16 11 0 0.83 19.27 7.47 o 17 11 0 709.93 713.19 52.93 o 18 11 0 50.82 75.95 24.90 o 19 11 0 81.35 93.96 17.84 o 20 11 0 8.46 55.51 27.66 o 0 12 0 22485.16 24334.01 356.09 o 1 12 0 1066.43 1184.17 34.02 o 2 12 0 111.20 104.37 6.49 o 3 12 0 1326.45 1323.92 19.75 o 4 12 0 8432.44 8485.88 71.77 o 5 12 0 395.27 385.44 12.28 o 6 12 0 388.52 464.02 13.35 o 7 12 0 485.15 482.76 17.85 o 8 12 0 1481.07 1341.28 23.11 o 9 12 0 136.95 165.99 11.02 o 10 12 0 1374.42 1362.88 27.47 o 11 12 0 0.06 7.11 6.36 o 12 12 0 113.63 140.70 11.09 o 13 12 0 81.56 89.09 10.67 o 14 12 0 1.40 17.02 6.40 o 15 12 0 500.29 473.56 21.07 o 16 12 0 3516.80 3145.47 63.26 o 17 12 0 15.97 23.51 11.19 o 18 12 0 681.69 761.60 42.34 o 19 12 0 122.48 177.96 19.89 o 20 12 0 1053.32 1020.17 73.53 o 1 13 0 773.93 707.68 13.47 o 2 13 0 94.42 81.47 6.07 o 3 13 0 103.26 177.76 8.17 o 4 13 0 44.11 43.96 5.87 o 5 13 0 885.13 918.54 17.88 o 6 13 0 623.26 565.39 14.91 o 7 13 0 3093.62 3021.38 36.81 o 8 13 0 529.87 531.73 14.96 o 9 13 0 209.27 252.66 12.92 o 10 13 0 198.65 159.84 11.68 o 11 13 0 4679.17 4262.70 80.81 o 12 13 0 1230.56 1083.83 26.01 o 13 13 0 1721.49 1519.48 34.65 o 14 13 0 56.31 75.50 9.53 o 15 13 0 387.93 376.27 22.81 o 16 13 0 321.16 325.79 22.02 o 17 13 0 126.42 152.75 14.80 o 18 13 0 30.50 89.81 24.06 o 19 13 0 17.31 19.82 13.17 o 20 13 0 81.80 131.40 24.59 o 0 14 0 401.39 529.05 16.48 o 1 14 0 20.00 15.76 4.00 o 2 14 0 18.28 64.87 6.78 o 3 14 0 5.59 2.40 4.31 o 4 14 0 5793.17 6714.92 61.08 o 5 14 0 452.34 452.56 13.30 o 6 14 0 849.80 659.11 16.15 o 7 14 0 317.63 279.01 11.57 o 8 14 0 1809.52 1896.53 28.73 o 9 14 0 223.55 233.14 12.84 o 10 14 0 4870.48 4336.43 79.62 o 11 14 0 1031.66 927.69 30.85 o 12 14 0 787.03 814.38 26.13 o 13 14 0 176.96 189.48 14.08 o 14 14 0 4973.11 4683.80 77.19 o 15 14 0 976.38 938.74 32.10 o 16 14 0 10.68 23.89 8.84 o 17 14 0 173.56 196.53 17.77 o 18 14 0 1258.75 1152.22 41.00 o 19 14 0 310.50 331.46 27.85 o 20 14 0 1266.61 1300.85 84.21 o 1 15 0 11549.69 12318.44 106.09 o 2 15 0 3180.40 3000.87 33.53 o 3 15 0 9532.58 9997.48 83.37 o 4 15 0 150.99 171.93 8.80 o 5 15 0 11571.27 12395.51 101.71 o 6 15 0 1349.29 1369.35 23.36 o 7 15 0 1123.25 1141.84 21.80 o 8 15 0 192.97 193.38 11.58 o 9 15 0 30.81 46.84 8.70 o 10 15 0 241.15 236.23 13.57 o 11 15 0 2927.66 2691.28 42.25 o 12 15 0 19.00 17.53 6.43 o 13 15 0 1446.80 1289.35 35.82 o 14 15 0 50.33 64.75 10.80 o 15 15 0 1893.05 1750.69 44.76 o 16 15 0 11.46 12.21 7.68 o 17 15 0 891.65 861.15 31.91 o 18 15 0 283.71 318.49 29.15 o 19 15 0 57.81 77.68 13.29 o 20 15 0 18.50 39.74 15.65 o 0 16 0 317.13 314.15 13.46 o 1 16 0 7.36 38.74 9.83 o 2 16 0 585.54 591.56 15.31 o 3 16 0 61.70 53.14 6.79 o 4 16 0 35.81 40.98 5.81 o 5 16 0 115.17 99.54 7.86 o 6 16 0 1447.96 1213.39 22.08 o 7 16 0 334.91 286.20 12.10 o 8 16 0 49.94 63.98 8.34 o 9 16 0 1638.08 1443.94 30.99 o 10 16 0 5047.89 4659.64 58.63 o 11 16 0 248.60 206.92 13.41 o 12 16 0 51.97 83.65 10.26 o 13 16 0 528.96 533.79 24.13 o 14 16 0 1303.86 1213.68 35.93 o 15 16 0 177.98 192.90 17.26 o 16 16 0 141.07 184.13 19.63 o 17 16 0 14.36 32.23 10.85 o 18 16 0 332.43 338.59 31.87 o 19 16 0 192.09 163.00 37.88 o 20 16 0 368.05 405.63 32.29 o 1 17 0 446.19 421.60 11.21 o 2 17 0 42.67 50.32 5.62 o 3 17 0 1.87 2.56 4.48 o 4 17 0 35.96 37.55 5.76 o 5 17 0 820.47 779.31 17.35 o 6 17 0 60.98 78.35 7.57 o 7 17 0 444.09 526.06 15.53 o 8 17 0 0.02 2.17 5.40 o 9 17 0 395.49 396.48 15.79 o 10 17 0 783.44 718.58 20.97 o 11 17 0 1968.09 1937.83 39.59 o 12 17 0 15.23 21.31 6.97 o 13 17 0 2415.77 2066.69 47.02 o 14 17 0 476.04 454.85 24.48 o 15 17 0 5.12 26.86 8.53 o 16 17 0 150.23 195.30 17.10 o 17 17 0 3303.41 2929.12 62.68 o 18 17 0 720.85 680.86 29.23 o 19 17 0 417.00 473.34 56.01 o 0 18 0 391.24 363.31 19.25 o 1 18 0 464.97 454.77 11.70 o 2 18 0 1594.26 1678.21 24.28 o 3 18 0 220.91 281.15 10.63 o 4 18 0 0.05 13.07 5.59 o 5 18 0 176.03 184.60 9.85 o 6 18 0 2144.82 2205.28 31.66 o 7 18 0 1.46 5.53 4.88 o 8 18 0 5350.48 5042.48 89.31 o 9 18 0 131.87 146.98 11.08 o 10 18 0 316.20 331.80 15.27 o 11 18 0 66.40 75.46 10.27 o 12 18 0 2890.60 2713.15 48.79 o 13 18 0 30.65 51.01 10.57 o 14 18 0 678.39 746.22 28.74 o 15 18 0 212.00 267.68 19.92 o 16 18 0 166.66 208.59 16.93 o 17 18 0 357.09 353.52 26.71 o 18 18 0 1905.31 1927.71 63.24 o 19 18 0 360.85 342.54 43.47 o 1 19 0 2666.56 2586.81 31.62 o 2 19 0 257.56 273.66 11.19 o 3 19 0 78.78 94.49 7.21 o 4 19 0 1.26 13.48 4.92 o 5 19 0 59.37 104.57 8.11 o 6 19 0 330.82 337.87 12.75 o 7 19 0 1282.17 1252.93 23.84 o 8 19 0 131.32 143.93 10.53 o 9 19 0 2054.33 1972.93 34.67 o 10 19 0 2297.44 2105.40 40.86 o 11 19 0 5538.16 5260.48 72.58 o 12 19 0 19.50 26.26 6.80 o 13 19 0 370.91 396.74 21.12 o 14 19 0 326.62 340.39 20.13 o 15 19 0 442.50 433.56 27.46 o 16 19 0 168.70 161.53 27.07 o 17 19 0 845.35 772.93 32.26 o 18 19 0 16.98 47.31 10.08 o 19 19 0 333.98 494.81 38.00 o 0 20 0 6219.57 6367.28 85.34 o 1 20 0 913.91 998.39 25.37 o 2 20 0 448.66 484.35 18.18 o 3 20 0 1812.37 1741.40 33.81 o 4 20 0 5223.87 5092.56 190.76 o 5 20 0 49.44 75.28 11.71 o 6 20 0 1285.02 1251.35 29.79 o 7 20 0 92.10 127.11 10.28 o 8 20 0 99.21 102.95 13.59 o 9 20 0 715.72 683.19 26.15 o 10 20 0 401.88 376.86 21.50 o 11 20 0 11.08 26.59 9.84 o 12 20 0 1105.79 1061.21 32.92 o 13 20 0 36.10 58.96 13.44 o 14 20 0 240.51 291.39 22.47 o 15 20 0 0.21 17.02 8.05 o 16 20 0 238.73 318.18 23.66 o 17 20 0 266.89 284.16 27.61 o 18 20 0 376.47 504.64 36.76 o 1 21 0 2141.25 2270.31 39.78 o 2 21 0 1562.41 1393.91 30.65 o 3 21 0 77.48 90.31 10.54 o 4 21 0 2499.32 2337.49 40.66 o 5 21 0 6359.65 6247.21 76.43 o 6 21 0 201.91 220.12 14.04 o 7 21 0 3294.10 2956.26 55.41 o 8 21 0 4602.60 4015.72 75.20 o 9 21 0 7014.54 6341.93 90.21 o 10 21 0 29.99 54.21 11.87 o 11 21 0 1868.22 1722.08 42.42 o 12 21 0 1968.72 1728.79 47.50 o 13 21 0 2981.02 2539.28 54.53 o 14 21 0 0.46 13.21 16.42 o 15 21 0 404.40 423.49 27.06 o 16 21 0 278.26 309.58 22.48 o 17 21 0 117.14 164.60 36.69 o 18 21 0 29.42 28.32 13.66 o 0 22 0 33234.59 32536.02 681.10 o 1 22 0 6143.53 5672.29 116.73 o 2 22 0 112.51 143.94 12.66 o 3 22 0 3395.11 3029.05 48.36 o 4 22 0 8780.98 8582.82 105.81 o 5 22 0 1629.20 1565.55 50.30 o 6 22 0 32.19 58.29 11.70 o 7 22 0 2399.43 2131.51 46.07 o 8 22 0 1839.26 1741.11 46.95 o 9 22 0 374.13 371.09 24.34 o 10 22 0 343.51 348.69 24.24 o 11 22 0 207.53 229.19 20.83 o 12 22 0 272.69 293.64 22.90 o 13 22 0 112.35 132.70 14.46 o 14 22 0 47.30 50.62 13.16 o 15 22 0 127.02 139.97 16.38 o 16 22 0 162.62 187.61 19.34 o 17 22 0 2.43 13.52 28.44 o 18 22 0 2.98 -12.92 12.92 o 1 23 0 1049.31 1038.11 32.85 o 2 23 0 77.94 72.93 10.05 o 3 23 0 516.13 501.22 19.98 o 4 23 0 746.79 700.92 32.67 o 5 23 0 927.44 951.23 26.06 o 6 23 0 433.88 416.52 26.05 o 7 23 0 884.87 794.51 28.47 o 8 23 0 309.43 281.87 22.25 o 9 23 0 1532.20 1356.61 42.44 o 10 23 0 18.66 25.61 10.58 o 11 23 0 402.68 396.60 27.26 o 12 23 0 283.15 308.82 23.56 o 13 23 0 704.69 733.67 31.20 o 14 23 0 5.23 20.22 10.55 o 15 23 0 291.59 335.12 27.49 o 16 23 0 213.62 256.30 23.06 o 17 23 0 433.67 484.62 54.90 o 18 23 0 13.67 -13.66 13.66 o 0 24 0 12.75 18.77 10.58 o 1 24 0 0.63 46.40 9.01 o 2 24 0 1543.82 1544.80 34.28 o 3 24 0 2750.22 2465.73 44.58 o 4 24 0 929.09 891.76 30.73 o 5 24 0 24.56 29.74 9.20 o 6 24 0 2724.80 2495.36 51.43 o 7 24 0 2132.53 1753.75 60.52 o 8 24 0 82.35 93.79 15.03 o 9 24 0 187.65 192.11 19.30 o 10 24 0 2135.97 1986.92 53.83 o 11 24 0 406.32 392.37 26.91 o 12 24 0 181.41 180.28 19.26 o 13 24 0 118.47 142.75 21.33 o 14 24 0 684.98 636.78 35.29 o 15 24 0 194.52 197.81 21.58 o 16 24 0 254.67 232.69 19.70 o 17 24 0 7.41 2.24 13.91 o 1 25 0 2820.79 2734.16 47.61 o 2 25 0 5160.29 4568.88 65.33 o 3 25 0 3324.24 3085.92 51.48 o 4 25 0 1.63 -4.02 7.45 o 5 25 0 2346.06 2097.81 47.35 o 6 25 0 3260.24 2773.18 55.79 o 7 25 0 933.62 933.49 31.04 o 8 25 0 23.96 11.92 10.76 o 9 25 0 33.20 37.91 10.54 o 10 25 0 173.05 183.69 26.93 o 11 25 0 182.50 166.09 18.32 o 12 25 0 19.31 25.77 9.86 o 13 25 0 383.67 412.65 26.82 o 14 25 0 194.10 218.00 22.91 o 15 25 0 43.75 103.64 28.06 o 16 25 0 6.54 52.44 11.66 o 17 25 0 1113.38 1116.05 70.05 o 0 26 0 2181.52 2150.71 60.02 o 1 26 0 104.29 151.33 13.89 o 2 26 0 696.18 742.42 24.30 o 3 26 0 19.94 34.88 8.06 o 4 26 0 21.85 22.19 8.97 o 5 26 0 527.26 480.64 28.99 o 6 26 0 1704.14 1563.83 40.96 o 7 26 0 91.44 96.42 15.81 o 8 26 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