#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/57/2205763.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205763_Fobs loop_ _publ_author_name 'Gao, Shan' 'Huo, Li-Hua' 'Liu, Ji-Wei' 'Zhao, Hui' _publ_section_title ; catena-Poly[[aqua(2,2'-bipyridine-\k^2^N,N')manganese(II)]-\m-4-carboxylatophenoxyacetato-\k^3^O,O':O''] ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m989 _journal_page_last m991 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.005 _cell_angle_gamma 90.000 _cell_length_a 14.3789 _cell_length_b 13.2345 _cell_length_c 19.7049 _exptl_crystal_F_000 1736.00 _reflns_d_resolution_high 0.7720 _[local]_cod_data_source_file lh6411Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gao13 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 661.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 79888.76 97638.76 1555.41 o 6 0 0 5156.45 4430.55 168.99 o 8 0 0 6371.75 5006.50 251.76 o 10 0 0 5760.92 5022.59 101.16 o 3 1 0 16722.78 18106.16 41.39 o 5 1 0 90.33 52.88 27.59 o 7 1 0 0.25 36.68 45.50 o 9 1 0 508.00 395.68 71.85 o 0 2 0 67610.81 85779.51 81.62 o 2 2 0 7496.90 6790.49 350.63 o 4 2 0 6006.31 5912.44 358.10 o 6 2 0 7721.49 7574.35 354.65 o 8 2 0 9164.12 8132.97 179.34 o 10 2 0 2528.29 2247.46 151.75 o 12 2 0 611.16 462.14 198.88 o 1 3 0 14090.66 14728.64 415.00 o 5 3 0 284.58 263.78 53.46 o 7 3 0 12.34 78.04 51.85 o 9 3 0 141.70 56.33 140.25 o 11 3 0 1706.65 1542.76 83.92 o 13 3 0 1626.71 1330.08 109.21 o 15 3 0 101.84 35.64 108.06 o 17 3 0 1.13 78.25 115.57 o 0 4 0 13220.56 15429.90 78.17 o 2 4 0 69.82 55.18 62.08 o 4 4 0 1099.55 1030.04 49.43 o 6 4 0 3953.65 3536.70 166.69 o 8 4 0 9559.38 8264.90 239.69 o 10 4 0 970.61 815.20 66.32 o 12 4 0 118.69 33.34 85.07 o 14 4 0 63.41 -20.69 89.67 o 1 5 0 9451.94 9140.09 315.56 o 3 5 0 834.70 766.78 77.02 o 5 5 0 236.74 252.91 129.90 o 7 5 0 1579.14 1625.14 221.30 o 9 5 0 1660.39 1725.55 300.04 o 11 5 0 298.58 308.09 47.13 o 13 5 0 213.48 168.05 50.13 o 17 5 0 10.35 -113.81 140.25 o 2 6 0 368.38 395.46 86.22 o 4 6 0 51.61 1056.42 612.16 o 6 6 0 74.45 920.47 114.96 o 8 6 0 0.47 32.19 109.21 o 10 6 0 120.47 141.11 69.89 o 12 6 0 29.95 24.14 136.80 o 14 6 0 70.08 57.48 54.03 o 16 6 0 20.22 -19.54 195.43 o 3 7 0 745.89 935.77 95.42 o 5 7 0 1086.72 1030.04 98.87 o 7 7 0 1.41 5.75 96.57 o 9 7 0 70.21 -13.80 110.36 o 11 7 0 3.05 6.90 74.72 o 13 7 0 167.28 136.80 117.26 o 15 7 0 77.33 114.34 96.53 o 0 8 0 5035.62 5396.21 88.52 o 2 8 0 6122.47 6861.95 129.90 o 4 8 0 3713.60 4002.90 96.57 o 6 8 0 1924.68 1742.79 93.12 o 8 8 0 5049.58 5899.73 618.48 o 10 8 0 118.39 60.93 185.09 o 12 8 0 108.17 131.05 163.24 o 14 8 0 489.60 494.33 137.95 o 1 9 0 743.91 1209.38 94.27 o 3 9 0 1697.81 1469.19 312.69 o 5 9 0 1749.42 1953.17 117.26 o 7 9 0 14.08 63.23 293.15 o 9 9 0 133.78 116.11 172.44 o 11 9 0 75.10 114.96 56.33 o 13 9 0 205.94 163.24 105.76 o 0 10 0 2413.62 2721.10 109.21 o 2 10 0 2273.49 1511.72 398.91 o 4 10 0 484.26 512.72 160.94 o 6 10 0 842.85 903.58 242.57 o 8 10 0 8582.26 8641.52 158.64 o 10 10 0 742.75 656.42 190.83 o 12 10 0 21.87 -36.79 91.97 o 14 10 0 674.31 930.02 168.99 o 1 11 0 1257.53 1466.89 120.71 o 3 11 0 666.56 425.35 154.05 o 5 11 0 1.20 -97.72 142.55 o 7 11 0 149.05 325.34 132.20 o 9 11 0 434.81 280.50 164.39 o 11 11 0 20.12 -1.15 98.87 o 13 11 0 188.87 304.64 156.35 o 0 12 0 2864.04 3539.61 236.82 o 2 12 0 988.85 1257.66 164.39 o 4 12 0 1101.81 1011.65 189.68 o 8 12 0 1012.46 857.60 217.27 o 10 12 0 636.02 561.00 185.09 o 12 12 0 318.46 227.62 75.87 o 1 13 0 4.52 -18.39 155.20 o 3 13 0 336.76 293.15 254.06 o 5 13 0 127.75 -40.24 180.49 o 7 13 0 380.31 198.88 228.77 o 9 13 0 9.67 32.19 168.99 o 11 13 0 32.80 1.15 148.30 o 0 14 0 2095.35 2318.74 164.39 o 2 14 0 558.98 534.56 300.04 o 4 14 0 319.37 302.34 197.73 o 6 14 0 99.56 174.74 237.97 o 8 14 0 149.80 285.10 279.35 o 10 14 0 31.31 136.80 218.42 o 1 15 0 62.88 196.58 134.50 o 3 15 0 42.41 49.43 237.97 o 5 15 0 89.71 26.44 140.25 o 7 15 0 78.57 77.02 221.87 o 0 16 0 0.06 19.54 142.55 o 2 16 0 3.11 71.28 233.37 o 6 16 0 15.01 72.42 249.46 o 1 17 0 0.00 -63.23 191.98 o -11 1 1 1317.48 1105.05 113.81 o -9 1 1 7816.92 7468.10 204.05 o -7 1 1 24782.78 23393.16 172.44 o -5 1 1 18.32 75.22 45.98 o -3 1 1 33997.90 40358.32 705.28 o 3 1 1 79.51 131.72 34.23 o 5 1 1 924.88 959.91 83.92 o 7 1 1 24571.70 22857.98 1357.10 o 9 1 1 10466.68 8516.22 343.73 o 11 1 1 363.20 206.19 103.77 o 13 1 1 117.41 102.31 183.94 o -18 2 1 29.09 -124.16 140.25 o -16 2 1 53.10 12.65 114.96 o -12 2 1 1.18 141.40 54.03 o -10 2 1 1529.21 1250.41 182.79 o -8 2 1 7333.19 7821.70 643.77 o -6 2 1 10997.70 10413.02 651.25 o -4 2 1 1105.28 966.49 91.39 o -2 2 1 10729.34 11048.28 378.22 o 0 2 1 534.22 504.03 44.26 o 2 2 1 958.17 1059.98 19.55 o 4 2 1 5599.26 5099.07 57.09 o 6 2 1 12.98 4.31 44.36 o 8 2 1 2427.01 2085.25 172.44 o 10 2 1 3120.51 2895.41 70.13 o 12 2 1 142.76 106.91 162.09 o 14 2 1 1.19 148.30 189.68 o -15 3 1 322.28 325.34 112.66 o -11 3 1 4879.02 4440.90 219.57 o -9 3 1 10222.26 9905.24 374.19 o -7 3 1 1529.22 1293.66 152.90 o -5 3 1 810.61 855.30 254.06 o -3 3 1 1194.05 1287.55 98.87 o -1 3 1 1181.57 1324.59 37.36 o 1 3 1 71569.19 87673.46 1652.55 o 3 3 1 267.76 238.96 39.21 o 5 3 1 425.32 403.89 61.79 o 7 3 1 3407.72 3074.68 188.53 o 9 3 1 35.05 -55.73 58.25 o 11 3 1 54.94 73.57 114.96 o 13 3 1 0.22 -86.22 94.27 o 15 3 1 17.49 -11.10 94.17 o 17 3 1 107.07 183.94 128.75 o -16 4 1 26.15 -10.35 104.61 o -14 4 1 436.94 340.28 87.37 o -12 4 1 45.77 13.24 86.22 o -10 4 1 13.14 -35.64 50.58 o -8 4 1 2092.71 1782.95 62.15 o -6 4 1 12497.27 13831.96 940.37 o -4 4 1 91.46 446.04 100.01 o -2 4 1 70.55 25.53 39.81 o 0 4 1 1088.54 1140.46 60.93 o 2 4 1 12083.75 12265.06 257.51 o 4 4 1 8863.93 9539.35 194.28 o 6 4 1 11615.45 9831.36 271.30 o 8 4 1 10748.43 9406.62 587.44 o 14 4 1 1026.50 799.07 125.88 o -17 5 1 6.22 -108.06 140.25 o -15 5 1 21.47 234.52 120.71 o -13 5 1 11.21 -23.15 188.53 o -11 5 1 386.73 326.49 52.88 o -9 5 1 5.03 90.04 68.40 o -7 5 1 169.14 374.77 111.51 o -5 5 1 36.83 2687.11 1049.01 o -3 5 1 348.16 424.20 77.02 o -1 5 1 10335.34 10749.16 156.92 o 1 5 1 50460.20 56531.16 3152.77 o 3 5 1 1021.37 1071.42 89.67 o 5 5 1 29.09 16.09 39.09 o 7 5 1 150.28 170.14 194.28 o 9 5 1 741.74 588.59 77.02 o 11 5 1 217.91 255.21 52.88 o 17 5 1 0.80 318.44 113.81 o -14 6 1 26.28 78.17 119.56 o -12 6 1 249.14 88.52 91.97 o -10 6 1 347.56 251.76 63.23 o -8 6 1 1130.22 1067.86 68.35 o -6 6 1 9658.93 9586.83 534.56 o -4 6 1 10172.46 10103.46 110.94 o -2 6 1 9476.33 9115.70 83.78 o 0 6 1 3850.69 3859.90 139.10 o 2 6 1 5846.63 5415.75 246.01 o 4 6 1 3730.66 3526.97 78.17 o 8 6 1 3764.63 3464.89 97.72 o 10 6 1 1759.45 1593.34 133.35 o 16 6 1 270.58 349.48 202.33 o -15 7 1 76.06 153.06 116.55 o -13 7 1 176.84 212.68 134.50 o -9 7 1 283.84 411.84 123.01 o -7 7 1 703.42 1628.21 126.31 o -5 7 1 606.37 819.66 83.92 o -3 7 1 2053.39 2469.17 120.71 o -1 7 1 9370.24 9518.67 101.16 o 1 7 1 495.31 475.93 68.98 o 3 7 1 833.33 682.86 66.68 o 5 7 1 3.41 129.90 152.90 o 7 7 1 12.20 4.60 94.27 o 9 7 1 1259.32 1219.72 149.45 o 11 7 1 603.80 600.09 120.71 o 13 7 1 25.79 -101.16 101.16 o 15 7 1 21.50 136.80 121.86 o -12 8 1 673.27 546.88 89.62 o -8 8 1 649.68 772.85 86.77 o -6 8 1 1849.29 2090.40 71.31 o -4 8 1 1335.17 1387.41 80.30 o -2 8 1 1401.97 1392.30 183.94 o 0 8 1 1466.13 1403.66 78.17 o 2 8 1 7445.18 7575.85 241.42 o 4 8 1 1999.03 2088.82 88.52 o 6 8 1 2350.96 2346.33 70.13 o 8 8 1 1203.46 1094.42 125.31 o 12 8 1 1488.86 1495.63 87.37 o 14 8 1 323.22 421.90 63.23 o -15 9 1 410.88 652.97 86.22 o -13 9 1 41.86 12.65 168.99 o -11 9 1 195.77 447.19 91.97 o -9 9 1 277.68 301.19 167.84 o -7 9 1 2603.44 2609.59 235.67 o -5 9 1 2698.99 3074.02 341.43 o -3 9 1 1026.37 1300.19 91.97 o -1 9 1 4562.01 4990.40 198.88 o 1 9 1 10495.70 12193.78 194.28 o 3 9 1 1449.14 1809.47 106.91 o 5 9 1 3112.53 3206.23 116.11 o 7 9 1 518.15 487.43 116.11 o 9 9 1 450.69 397.76 103.46 o 11 9 1 119.98 182.79 166.69 o 15 9 1 115.93 178.19 62.08 o -14 10 1 0.01 -87.37 87.37 o -12 10 1 16.80 116.11 125.31 o -10 10 1 336.20 411.56 159.79 o -8 10 1 591.22 862.20 118.41 o -6 10 1 1932.01 2165.84 209.23 o -4 10 1 80.68 17.24 133.35 o -2 10 1 440.49 710.45 228.77 o 0 10 1 568.49 693.21 231.07 o 2 10 1 2362.45 2550.96 104.61 o 4 10 1 56.54 323.04 247.16 o 6 10 1 197.37 191.98 146.00 o 8 10 1 1323.30 1363.42 114.96 o 10 10 1 763.45 713.90 102.31 o 12 10 1 2.23 44.83 173.59 o 14 10 1 4.98 54.03 114.96 o -13 11 1 190.00 357.52 155.20 o -11 11 1 980.67 1094.42 256.36 o -9 11 1 1076.92 846.10 151.75 o -7 11 1 2902.44 3087.82 310.39 o -5 11 1 718.67 656.42 198.88 o -3 11 1 730.47 657.57 293.15 o -1 11 1 1374.02 1738.19 118.41 o 1 11 1 1806.34 1923.28 220.72 o 3 11 1 771.98 1112.81 196.58 o 5 11 1 1137.87 1130.05 246.01 o 7 11 1 222.44 132.20 203.48 o 9 11 1 69.79 255.21 147.15 o 13 11 1 123.45 137.95 170.14 o -12 12 1 17.98 -119.56 119.56 o -10 12 1 1.50 48.28 102.31 o -8 12 1 203.70 195.43 206.93 o -6 12 1 0.35 105.76 205.78 o -4 12 1 176.64 96.57 251.76 o -2 12 1 7.49 -54.03 223.02 o 0 12 1 171.72 162.09 124.16 o 2 12 1 230.37 234.52 104.61 o 4 12 1 75.41 214.97 216.12 o 6 12 1 232.32 251.76 231.07 o 8 12 1 14.77 40.24 126.46 o 10 12 1 49.63 126.46 117.26 o 12 12 1 140.30 114.96 151.75 o -11 13 1 72.13 -93.12 103.46 o -9 13 1 253.19 375.92 203.48 o -7 13 1 2020.98 2261.26 425.35 o -5 13 1 355.99 477.08 170.14 o -3 13 1 609.63 657.57 193.13 o -1 13 1 443.82 383.97 226.47 o 1 13 1 286.42 308.09 250.61 o 3 13 1 763.30 821.96 141.40 o 5 13 1 720.60 625.38 186.23 o 7 13 1 231.14 210.38 327.64 o 9 13 1 86.76 171.29 356.38 o 11 13 1 0.43 172.44 80.47 o -10 14 1 26.52 -72.42 136.80 o -8 14 1 17.55 -35.64 174.74 o -6 14 1 108.15 155.20 259.81 o -4 14 1 107.22 279.35 296.60 o -2 14 1 398.90 519.62 134.50 o 0 14 1 933.23 1130.05 300.04 o 2 14 1 297.39 147.15 255.21 o 4 14 1 156.39 367.87 228.77 o 8 14 1 139.09 159.79 166.69 o 10 14 1 24.67 108.06 141.40 o -7 15 1 257.12 362.12 229.92 o -5 15 1 45.47 64.38 259.81 o -3 15 1 6.36 -68.98 274.75 o -1 15 1 29.16 128.75 193.13 o 1 15 1 29.49 16.09 177.04 o 3 15 1 48.53 9.20 150.60 o 5 15 1 14.84 111.51 152.90 o 7 15 1 23.69 90.82 181.64 o -6 16 1 102.50 193.13 141.40 o -4 16 1 35.04 24.14 252.91 o -2 16 1 242.86 260.96 158.64 o 0 16 1 190.25 106.91 140.25 o 2 16 1 197.90 167.84 194.28 o 4 16 1 306.82 441.45 233.37 o 6 16 1 191.22 159.79 221.87 o -1 17 1 89.43 211.53 174.74 o 1 17 1 5.53 89.67 352.93 o -18 0 2 165.42 263.26 132.20 o -10 0 2 233.30 211.53 62.08 o -8 0 2 2402.73 2355.53 132.20 o -6 0 2 506.63 746.09 90.82 o -2 0 2 3069.14 3605.14 78.17 o 2 0 2 15077.30 17273.85 55.18 o 4 0 2 4978.52 4106.36 56.33 o 6 0 2 4975.49 5078.92 179.34 o 8 0 2 3281.98 3205.08 191.98 o 10 0 2 26.98 75.87 179.34 o 12 0 2 968.28 889.79 141.40 o -17 1 2 0.19 -117.26 117.26 o -13 1 2 46.82 46.24 57.91 o -11 1 2 641.91 513.05 73.42 o -9 1 2 728.84 707.65 65.53 o -7 1 2 65.10 603.77 100.59 o -5 1 2 519.03 481.29 25.67 o -3 1 2 35978.80 41788.77 319.01 o 1 1 2 4524.91 4523.83 384.54 o 3 1 2 1070.86 1153.05 40.24 o 5 1 2 2393.62 2217.67 94.84 o 7 1 2 1278.10 1131.20 108.06 o 9 1 2 1.83 -59.84 95.26 o 11 1 2 4.62 22.39 87.34 o 13 1 2 41.42 21.97 149.36 o 15 1 2 62.91 -102.31 218.42 o -16 2 2 26.82 -16.09 119.56 o -12 2 2 1471.58 1379.83 106.91 o -10 2 2 385.85 617.14 110.46 o -8 2 2 1.37 132.78 87.37 o -6 2 2 9953.15 12205.28 210.38 o -4 2 2 0.88 29.59 47.78 o -2 2 2 544.60 466.87 33.69 o 0 2 2 4575.69 4501.82 324.19 o 2 2 2 3552.95 3581.70 289.12 o 4 2 2 1014.50 1031.28 59.10 o 6 2 2 10521.62 10546.41 141.40 o 8 2 2 169.39 192.19 64.74 o 10 2 2 61.10 -9.47 75.73 o 12 2 2 211.40 231.31 61.78 o 14 2 2 1128.04 1239.27 203.48 o 16 2 2 85.25 387.41 234.52 o -15 3 2 302.24 324.19 102.31 o -13 3 2 287.95 383.97 40.24 o -11 3 2 240.19 332.23 117.26 o -9 3 2 2319.16 2193.51 54.24 o -7 3 2 3799.04 3311.99 60.93 o -5 3 2 13546.24 14145.80 144.85 o -3 3 2 2040.51 2084.66 37.77 o -1 3 2 8743.35 8173.90 45.98 o 1 3 2 88018.13 94718.10 611.01 o 3 3 2 25589.42 26111.03 605.84 o 7 3 2 1846.09 1628.48 49.16 o 9 3 2 1559.40 1297.90 114.96 o 11 3 2 1395.76 1217.42 270.16 o 13 3 2 1321.14 1503.71 72.22 o 15 3 2 251.59 297.62 95.09 o 17 3 2 169.37 334.53 135.65 o -16 4 2 35.14 28.74 91.97 o -14 4 2 4.51 3.45 108.06 o -12 4 2 534.44 574.42 150.60 o -10 4 2 587.81 930.02 108.64 o -8 4 2 120.69 446.15 246.01 o -6 4 2 270.59 746.36 161.52 o -4 4 2 3797.23 3728.72 84.85 o -2 4 2 71.70 83.37 52.74 o 0 4 2 12136.53 12658.60 97.14 o 2 4 2 258.35 226.42 37.21 o 4 4 2 67.56 29.06 54.61 o 6 4 2 3608.54 3615.74 240.84 o 8 4 2 80.37 55.30 76.16 o 10 4 2 309.99 224.38 68.91 o 12 4 2 11.55 52.49 119.31 o 14 4 2 24.62 -28.74 93.12 o 16 4 2 20.99 -150.60 221.87 o -15 5 2 1075.99 1163.39 158.64 o -11 5 2 114.97 132.20 97.72 o -9 5 2 2227.12 1816.08 212.10 o -7 5 2 11996.28 11377.57 98.87 o -5 5 2 17523.74 17337.68 382.82 o -3 5 2 2253.19 2144.79 62.28 o -1 5 2 3521.14 3478.68 125.31 o 1 5 2 46363.35 49105.06 185.09 o 3 5 2 28445.19 30107.96 317.29 o 5 5 2 5358.07 4740.94 308.09 o 7 5 2 1835.20 1796.46 67.53 o 9 5 2 7972.68 7687.59 101.23 o 11 5 2 2895.25 2675.42 123.68 o 13 5 2 928.07 912.78 74.72 o -14 6 2 37.19 -10.35 81.62 o -12 6 2 266.48 132.51 92.26 o -10 6 2 15.41 61.56 120.05 o -8 6 2 854.09 1095.58 71.98 o -6 6 2 787.96 1144.69 119.56 o -4 6 2 12455.67 13753.03 99.98 o -2 6 2 2450.31 2498.18 55.15 o 0 6 2 12806.06 13784.56 326.49 o 2 6 2 1813.41 1967.23 196.58 o 4 6 2 3424.17 3220.54 102.05 o 6 6 2 679.26 680.56 45.98 o 8 6 2 2325.61 1883.04 195.43 o 10 6 2 72.91 71.28 144.85 o 12 6 2 2.30 -17.30 69.55 o 14 6 2 28.16 5.75 91.97 o -15 7 2 161.37 142.55 114.96 o -13 7 2 1178.50 1243.86 81.62 o -11 7 2 991.34 1003.01 95.56 o -9 7 2 6266.13 5725.67 108.43 o -7 7 2 9328.99 10594.69 331.08 o -5 7 2 4391.65 4048.63 148.42 o -3 7 2 4722.63 4161.54 83.92 o -1 7 2 8236.36 7080.37 95.42 o 1 7 2 6940.67 6115.23 259.81 o 3 7 2 8921.13 9362.32 279.35 o 5 7 2 7152.61 7228.67 94.27 o 7 7 2 1473.73 1326.64 72.42 o 9 7 2 3619.06 3438.45 217.27 o 11 7 2 380.20 423.05 113.81 o 13 7 2 183.74 182.79 105.76 o -16 8 2 3.26 -66.68 110.36 o -14 8 2 3.06 -1.15 90.82 o -12 8 2 147.17 50.73 150.02 o -10 8 2 36.14 -92.54 92.54 o -8 8 2 754.31 881.74 125.31 o -6 8 2 3023.94 3253.50 170.72 o -4 8 2 1.42 110.36 91.97 o -2 8 2 601.15 865.65 78.17 o 0 8 2 438.81 390.31 113.24 o 2 8 2 221.86 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