#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:11:14 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180977 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/57/2205779.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205779_Fobs loop_ _publ_author_name 'Nakazawa, Hiroshi' 'Itazaki, Masumi' 'Owaribe, Mari' _publ_section_title ; Chloropyridinebis[tricarbonyl(\h^5^-cyclopentadienyl)tungstenio]indium ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m945 _journal_page_last m946 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 93.826 _cell_angle_beta 94.393 _cell_angle_gamma 98.725 _cell_length_a 8.1713 _cell_length_b 8.7735 _cell_length_c 16.3845 _exptl_crystal_F_000 820.00 _reflns_d_resolution_high 0.7700 _cod_data_source_file ob6502Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I' _shelx_refln_list_code 4 _shelx_f_calc_maximum 294.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1900.06 1906.68 214.88 o 3 0 0 28984.59 27872.54 574.34 o 4 0 0 5401.79 4713.46 579.17 o 5 0 0 7122.30 7427.71 399.60 o 6 0 0 1003.98 873.91 208.87 o 7 0 0 15589.07 16533.27 742.86 o 8 0 0 1277.35 1630.29 299.14 o 9 0 0 1241.55 1639.09 283.58 o 10 0 0 5728.72 6391.94 453.27 o -10 1 0 864.30 966.11 284.65 o -9 1 0 328.61 383.07 193.31 o -8 1 0 13502.07 14087.67 608.15 o -7 1 0 3754.34 3960.51 397.99 o -6 1 0 4041.47 4023.30 314.60 o -5 1 0 2940.11 2912.72 464.76 o -4 1 0 11848.65 11717.74 328.66 o -3 1 0 3933.73 4466.80 269.52 o -2 1 0 7272.11 7225.39 288.94 o 2 1 0 15300.05 15212.52 398.75 o 3 1 0 3208.70 2739.48 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