#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2205813.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2205813_Fobs loop_ _publ_author_name 'Yarovenko, Vladimir N.' 'Shirokov, Alexander V.' 'Kondrashev, Pavel A.' 'Rybakov, Victor B.' 'Zavarzin, Igor V.' 'Krayushkin, Mikhail M.' _publ_section_title ; {N-Anilino-2-[(2-oxidophenyl)methylenehydrazono]-2-sulfidoacetamide}pyridinenickel(II) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m964 _journal_page_last m966 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 126.870 _cell_angle_gamma 90.000 _cell_length_a 41.9082 _cell_length_b 3.9518 _cell_length_c 28.8401 _exptl_crystal_F_000 1792.00 _reflns_d_resolution_high 0.7838 _[local]_cod_data_source_file su61713sup2.hkl _[local]_cod_data_source_block 3 #BEGIN Tags that were not found in dictionaries: _shelx_title ' shir in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 471.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 333.06 37744.66 19875.12 o 4 0 0 221938.05 211360.63 7637.42 o 6 0 0 8007.81 8440.42 341.81 o 8 0 0 34723.39 37286.84 1342.08 o 10 0 0 5935.33 5849.33 133.15 o 12 0 0 3343.27 3548.08 116.16 o 14 0 0 1134.06 938.87 155.82 o 16 0 0 14106.52 15321.15 345.14 o 18 0 0 154.56 34.24 116.25 o 20 0 0 666.08 503.76 120.37 o 22 0 0 11681.04 12625.00 553.91 o 24 0 0 1594.81 1099.78 343.43 o 26 0 0 31632.26 34591.76 1607.80 o 28 0 0 5968.11 5839.73 710.75 o 30 0 0 5867.40 6084.43 275.71 o 32 0 0 7253.47 7183.26 427.05 o 34 0 0 1904.28 1650.66 297.19 o 36 0 0 3326.40 3221.30 654.31 o 38 0 0 52.26 -108.24 108.24 o 40 0 0 1079.05 941.94 239.75 o 42 0 0 27.44 -25.08 85.60 o 1 1 0 12546.27 13010.63 154.33 o 3 1 0 736.98 631.61 101.50 o 5 1 0 25426.06 26057.83 220.72 o 7 1 0 3090.26 3217.85 109.05 o 9 1 0 4436.55 4537.67 171.82 o 11 1 0 408.97 355.44 76.95 o 13 1 0 8682.75 8790.43 169.51 o 15 1 0 317.26 445.75 221.77 o 17 1 0 26.56 141.96 83.68 o 19 1 0 2626.90 2521.74 129.26 o 21 1 0 1836.01 1929.78 131.67 o 23 1 0 1880.13 1867.87 353.63 o 25 1 0 1346.35 1230.23 202.29 o 27 1 0 21.07 -35.66 147.34 o 29 1 0 1370.11 1277.19 130.06 o 31 1 0 547.25 545.11 258.73 o 33 1 0 1214.78 1156.87 323.16 o 35 1 0 61.35 193.92 95.24 o 37 1 0 187.59 364.61 97.54 o 39 1 0 153.80 104.33 141.35 o 41 1 0 125.80 203.90 129.36 o 0 2 0 11196.56 11707.62 304.68 o 2 2 0 82.15 -74.88 99.53 o 4 2 0 5511.64 5493.09 160.33 o 6 2 0 296.44 304.86 97.41 o 8 2 0 18775.39 18653.31 274.04 o 10 2 0 1750.13 1609.42 122.52 o 12 2 0 2398.81 2148.18 144.35 o 14 2 0 7626.52 7152.50 201.55 o 16 2 0 5560.98 5579.71 304.68 o 18 2 0 15766.21 15396.13 296.04 o 20 2 0 200.56 182.11 117.15 o 22 2 0 14264.32 14136.76 309.35 o 24 2 0 1242.31 996.11 147.95 o 26 2 0 4784.26 4553.69 203.90 o 28 2 0 309.50 382.50 139.85 o 30 2 0 444.58 706.22 121.88 o 32 2 0 258.13 332.80 112.07 o 34 2 0 101.26 -26.81 118.37 o 36 2 0 4.53 44.14 85.48 o 38 2 0 516.35 565.98 103.00 o 1 3 0 2817.68 2796.24 192.80 o 3 3 0 120.07 250.85 203.78 o 5 3 0 2875.13 2876.72 212.77 o 7 3 0 1784.39 1790.92 289.19 o 9 3 0 854.87 772.93 218.77 o 11 3 0 1732.46 1612.22 179.81 o 13 3 0 7.04 109.64 142.97 o 15 3 0 492.11 578.55 153.32 o 17 3 0 447.38 467.34 168.22 o 19 3 0 991.48 673.65 177.22 o 21 3 0 347.98 400.11 153.33 o 23 3 0 223.10 321.94 146.84 o 25 3 0 2975.10 2705.70 418.06 o 27 3 0 87.32 149.15 140.85 o 29 3 0 273.33 401.97 133.36 o 31 3 0 470.26 337.24 138.57 o 33 3 0 211.97 186.17 128.24 o 0 4 0 2646.36 2562.29 322.66 o 2 4 0 810.57 1096.66 187.51 o 4 4 0 5436.21 4917.91 278.65 o 6 4 0 1400.97 1385.26 209.33 o 8 4 0 486.79 324.40 227.26 o 10 4 0 1107.67 938.11 181.25 o 12 4 0 304.62 253.72 163.11 o 14 4 0 74.82 108.66 185.80 o 16 4 0 218.66 325.40 153.60 o 18 4 0 331.32 252.07 175.35 o 20 4 0 543.99 564.50 181.24 o 22 4 0 2102.72 1702.22 216.89 o 24 4 0 296.29 586.78 396.08 o 26 4 0 1587.85 1761.12 188.41 o 1 5 0 11.72 -40.04 187.46 o 3 5 0 68.82 27.98 176.23 o 5 5 0 59.58 -202.62 252.23 o -41 1 1 428.17 279.70 166.82 o -39 1 1 1997.08 1922.97 216.77 o -37 1 1 144.75 174.82 165.82 o -35 1 1 2296.32 2273.60 220.77 o -33 1 1 16.46 -94.90 177.81 o -31 1 1 9346.11 9568.88 393.58 o -29 1 1 0.56 -177.81 177.81 o -27 1 1 17961.09 19358.53 483.49 o -25 1 1 220.62 319.66 162.83 o -23 1 1 9380.43 9089.39 322.66 o -21 1 1 2171.20 1986.90 192.80 o -19 1 1 14419.42 14173.01 348.63 o -17 1 1 1189.86 1028.91 136.86 o -15 1 1 1021.38 890.06 124.87 o -13 1 1 11461.17 11315.89 252.73 o -11 1 1 462.21 413.56 115.88 o -9 1 1 15385.16 15586.52 275.71 o -7 1 1 48372.27 49677.46 429.55 o -5 1 1 88096.00 90821.95 555.41 o -3 1 1 6561.32 6946.65 181.81 o -1 1 1 40412.02 42402.16 365.61 o 1 1 1 179087.30 181903.64 0.10 o 3 1 1 4951.06 4922.79 161.83 o 5 1 1 940.87 980.96 113.88 o 7 1 1 11372.47 11859.46 237.75 o 9 1 1 9178.55 9080.40 224.76 o 11 1 1 9198.68 9182.29 234.75 o 13 1 1 1079.69 1024.56 121.87 o 15 1 1 406.37 385.01 110.88 o 17 1 1 30754.20 31202.00 490.48 o 19 1 1 730.35 920.03 149.84 o 21 1 1 16446.56 17069.95 407.57 o 23 1 1 409.45 122.87 164.83 o 25 1 1 10981.09 11913.40 374.60 o 27 1 1 1048.72 992.95 179.81 o 29 1 1 106.58 143.85 140.85 o 31 1 1 151.76 31.97 152.84 o 33 1 1 637.16 822.13 141.85 o 35 1 1 284.12 423.55 126.87 o 37 1 1 187.51 247.74 122.87 o 39 1 1 696.02 671.98 139.85 o 41 1 1 137.56 -88.91 135.86 o -40 2 1 234.55 446.53 154.84 o -38 2 1 135.30 319.66 159.83 o -36 2 1 293.94 374.60 181.81 o -34 2 1 249.43 482.49 162.83 o -32 2 1 1241.17 1203.73 211.78 o -30 2 1 1.48 -148.84 174.82 o -28 2 1 24.52 -179.81 181.81 o -26 2 1 666.60 824.13 181.81 o -24 2 1 120.08 -75.92 181.81 o -22 2 1 45.84 223.76 169.82 o -20 2 1 45.42 -185.80 185.80 o -18 2 1 282.70 422.55 174.82 o -16 2 1 0.09 -73.92 158.83 o -14 2 1 1974.81 2203.67 213.77 o -12 2 1 709.53 793.16 177.81 o -10 2 1 1183.34 1442.47 173.82 o -8 2 1 9282.35 9026.45 286.70 o -6 2 1 1446.67 1366.55 170.82 o -4 2 1 25.07 212.77 132.86 o -2 2 1 2169.38 2424.44 184.80 o 0 2 1 597.63 692.27 146.84 o 2 2 1 211.16 252.73 131.86 o 4 2 1 531.76 744.21 135.86 o 6 2 1 600.20 686.27 145.85 o 8 2 1 3124.41 3333.47 203.78 o 10 2 1 582.96 505.47 137.85 o 12 2 1 816.87 566.40 169.82 o 14 2 1 101.62 170.82 143.85 o 16 2 1 227.82 8.99 167.82 o 18 2 1 125.45 -45.95 160.83 o 20 2 1 875.15 886.06 176.81 o 22 2 1 72.61 304.68 166.82 o 24 2 1 586.23 562.18 171.82 o 26 2 1 1422.29 1217.71 199.79 o 28 2 1 168.83 349.63 143.85 o 30 2 1 199.94 159.83 131.86 o 32 2 1 171.48 100.89 117.88 o 34 2 1 1069.34 1165.77 167.82 o 36 2 1 248.06 223.76 109.88 o 38 2 1 64.51 182.81 111.88 o -35 3 1 844.99 1262.66 216.77 o -33 3 1 132.45 13.99 197.79 o -31 3 1 1401.15 1418.50 230.76 o -29 3 1 5.06 -207.78 207.78 o -27 3 1 894.60 1358.56 246.74 o -25 3 1 562.77 492.48 252.73 o -23 3 1 3017.26 3289.52 312.67 o -21 3 1 2311.32 2621.23 302.68 o -19 3 1 2435.26 3132.69 298.68 o -17 3 1 885.14 1315.61 246.74 o -15 3 1 1624.89 1671.23 247.74 o -13 3 1 707.54 421.55 225.76 o -11 3 1 916.93 660.30 239.75 o -9 3 1 9275.54 8670.83 375.60 o -7 3 1 508.74 479.49 235.75 o -5 3 1 11663.24 11255.10 423.55 o -3 3 1 27.10 -135.86 208.78 o -1 3 1 13280.42 13570.65 449.52 o 1 3 1 20.15 240.75 203.78 o 3 3 1 9526.06 9255.21 396.58 o 5 3 1 2267.31 2198.67 242.74 o 7 3 1 2881.70 3257.56 275.71 o 9 3 1 3337.03 3767.02 292.69 o 11 3 1 803.16 1196.73 222.76 o 13 3 1 1362.61 1502.41 216.77 o 15 3 1 193.10 49.95 197.79 o 17 3 1 6692.00 6771.84 368.61 o 19 3 1 8.31 -179.81 179.81 o 21 3 1 2697.46 2411.45 278.71 o 23 3 1 80.38 109.88 191.80 o 25 3 1 657.54 782.17 205.78 o 27 3 1 484.66 445.53 164.83 o 29 3 1 1213.36 1312.61 213.77 o 31 3 1 1457.76 1054.88 229.76 o 33 3 1 1558.41 1484.03 203.78 o -26 4 1 0.30 -228.76 254.73 o -24 4 1 4.66 484.49 279.70 o -22 4 1 261.29 226.76 260.72 o -20 4 1 595.56 230.76 280.70 o -18 4 1 142.49 181.81 231.75 o -16 4 1 56.30 -27.97 218.77 o -14 4 1 1054.72 950.99 237.75 o -12 4 1 39.23 58.94 230.76 o -10 4 1 133.27 -241.74 241.74 o -8 4 1 21.53 -61.93 240.75 o -6 4 1 137.26 430.54 265.72 o -4 4 1 396.86 749.21 264.72 o -2 4 1 325.24 691.27 272.71 o 0 4 1 354.06 288.69 268.72 o 2 4 1 1.39 78.92 279.70 o 4 4 1 5.87 -111.88 284.70 o 6 4 1 135.23 209.78 255.73 o 8 4 1 1.77 -217.77 248.74 o 10 4 1 5.50 100.89 241.74 o 12 4 1 825.21 751.21 268.72 o 14 4 1 1.28 378.60 195.79 o 16 4 1 60.02 51.95 216.77 o 18 4 1 411.29 33.96 235.75 o 20 4 1 495.52 393.58 240.75 o 22 4 1 31.54 -169.82 220.77 o 24 4 1 2.50 32.97 200.79 o -5 5 1 986.87 1133.80 280.70 o -3 5 1 9.94 403.57 286.70 o -1 5 1 676.58 240.75 301.68 o 1 5 1 14.07 467.51 259.73 o 3 5 1 459.81 582.38 264.72 o -44 0 2 78.28 63.93 119.87 o -42 0 2 112.53 64.93 145.85 o -40 0 2 100.25 166.82 153.84 o -38 0 2 69.20 -151.84 166.82 o -36 0 2 1638.33 2176.70 214.77 o -34 0 2 126.43 -227.76 227.76 o -32 0 2 14942.83 15701.40 498.47 o -30 0 2 1125.86 1022.17 270.71 o -28 0 2 26341.99 26432.84 590.38 o -26 0 2 9007.44 9815.62 360.62 o -24 0 2 27082.07 27050.39 516.45 o -22 0 2 3482.03 2970.86 205.78 o -20 0 2 1238.15 1334.33 149.84 o -18 0 2 7235.24 6991.51 221.77 o -16 0 2 6194.88 6500.13 207.78 o -14 0 2 5566.86 5447.24 179.81 o -12 0 2 772.70 775.18 121.87 o -10 0 2 3123.50 3223.59 139.85 o -8 0 2 122179.32 122628.32 0.10 o -6 0 2 12651.59 13534.69 173.82 o -4 0 2 379.90 380.90 64.93 o -2 0 2 196041.38 188984.14 0.10 o 0 0 2 18602.59 18560.61 158.83 o 2 0 2 16602.39 16712.99 185.80 o 4 0 2 1628.81 1497.42 100.89 o 6 0 2 7918.64 7992.23 184.80 o 8 0 2 21331.28 21660.09 295.69 o 10 0 2 2231.33 2293.57 136.86 o 12 0 2 7385.53 7235.35 216.77 o 14 0 2 0.12 -104.89 104.89 o 16 0 2 1557.25 1646.26 142.85 o 18 0 2 2.79 114.88 107.89 o 20 0 2 12729.61 12077.23 337.64 o 22 0 2 50.55 -139.85 139.85 o 24 0 2 24687.06 23823.81 504.47 o 26 0 2 3355.61 2836.00 259.73 o 28 0 2 6385.64 6584.04 311.67 o 30 0 2 579.62 418.56 157.83 o 32 0 2 3547.58 3675.11 254.73 o 34 0 2 6866.91 6675.94 308.67 o 36 0 2 4.19 -63.93 135.86 o 38 0 2 1851.16 1763.14 193.80 o 40 0 2 145.92 160.83 119.87 o -43 1 2 63.23 36.96 141.85 o -41 1 2 403.80 267.72 169.82 o -39 1 2 1301.52 1589.32 186.80 o -37 1 2 79.25 -169.82 169.82 o -35 1 2 515.57 585.38 180.81 o -33 1 2 553.51 660.30 195.79 o -31 1 2 673.53 735.22 174.82 o -29 1 2 79.63 184.80 148.84 o -27 1 2 1430.31 1498.42 186.80 o -25 1 2 457.16 483.49 150.84 o -23 1 2 1360.81 1446.47 168.82 o -21 1 2 1962.87 2013.87 172.82 o -19 1 2 64.42 52.94 113.88 o -17 1 2 28.81 -111.88 111.88 o -15 1 2 1775.29 1609.30 143.85 o -13 1 2 7278.25 7305.27 214.77 o -11 1 2 13024.65 13085.59 274.71 o -9 1 2 1158.04 946.00 135.86 o -7 1 2 217263.30 227091.84 0.10 o -5 1 2 12237.38 12584.69 231.75 o -3 1 2 29718.48 31754.42 327.65 o -1 1 2 8893.99 8726.77 193.80 o 1 1 2 6.17 3.00 107.89 o 3 1 2 1448.46 1458.46 123.87 o 5 1 2 7129.88 7072.52 185.80 o 7 1 2 52.01 102.89 101.89 o 9 1 2 371.46 280.70 102.89 o 11 1 2 12248.78 12398.89 282.70 o 13 1 2 197.39 322.66 101.89 o 15 1 2 4124.75 3886.89 190.80 o 17 1 2 30.84 35.96 125.87 o 19 1 2 810.24 730.23 161.83 o 21 1 2 1.08 7.99 128.86 o 23 1 2 949.19 846.11 170.82 o 25 1 2 2925.15 2830.01 215.77 o 27 1 2 3566.07 3775.01 251.73 o 29 1 2 1141.96 1306.62 179.81 o 31 1 2 131.43 107.89 128.86 o 33 1 2 31.04 98.90 127.86 o 35 1 2 8.09 43.95 102.89 o 37 1 2 30.70 128.86 117.88 o 39 1 2 120.82 113.88 120.87 o -40 2 2 2001.39 1966.92 218.77 o -38 2 2 331.25 244.74 181.81 o -36 2 2 472.26 631.33 173.82 o -34 2 2 447.14 387.59 181.81 o -32 2 2 190.92 138.85 168.82 o -30 2 2 510.49 512.46 173.82 o -28 2 2 932.67 1087.85 205.78 o -26 2 2 325.86 635.33 162.83 o -24 2 2 6029.49 5697.97 312.67 o -22 2 2 3223.87 3346.46 250.73 o -20 2 2 6207.56 6412.22 320.66 o -18 2 2 7507.04 7559.01 321.66 o -16 2 2 3902.75 3737.05 247.74 o -14 2 2 16596.34 16599.45 402.57 o -12 2 2 1518.64 1859.03 195.79 o -10 2 2 16227.23 16099.97 373.60 o -8 2 2 3831.20 4019.75 226.76 o -6 2 2 4632.59 4560.18 224.76 o -4 2 2 5497.17 5099.61 225.76 o -2 2 2 2662.23 2514.34 181.81 o 0 2 2 2248.18 2262.61 179.81 o 2 2 2 2875.67 2905.93 188.80 o 4 2 2 2610.30 2531.32 178.81 o 6 2 2 4430.08 4343.41 211.78 o 8 2 2 1597.04 1528.38 163.83 o 10 2 2 33.97 43.95 124.87 o 12 2 2 21008.57 20659.15 442.53 o 14 2 2 89.37 7.99 147.84 o 16 2 2 31008.67 30282.97 564.40 o 18 2 2 3462.39 3381.42 252.73 o 20 2 2 10414.11 10518.88 368.61 o 22 2 2 3731.82 3743.04 263.72 o 24 2 2 2762.72 2530.32 239.75 o 26 2 2 2365.46 2037.84 235.75 o 28 2 2 697.76 660.30 188.80 o 30 2 2 13.64 22.98 129.86 o 32 2 2 132.26 258.73 142.85 o 34 2 2 180.51 308.67 128.86 o 36 2 2 1.33 -20.98 123.87 o -35 3 2 53.80 -95.90 177.81 o -33 3 2 57.46 85.91 177.81 o -31 3 2 371.46 592.37 205.78 o -29 3 2 251.14 565.40 205.78 o -27 3 2 1909.97 1888.00 268.72 o -25 3 2 285.50 71.92 236.75 o -23 3 2 592.68 1072.87 233.75 o -21 3 2 1611.45 1394.53 297.69 o -19 3 2 667.18 463.51 260.72 o -17 3 2 324.56 -48.95 251.73 o -15 3 2 120.61 155.84 204.78 o -13 3 2 234.53 112.88 207.78 o -11 3 2 134.52 53.94 223.76 o -9 3 2 1618.35 1772.13 256.73 o -7 3 2 129.11 -209.78 253.73 o -5 3 2 42.12 20.98 222.76 o -3 3 2 3433.17 4106.66 287.70 o -1 3 2 497.05 614.35 235.75 o 1 3 2 10.72 455.52 194.79 o 3 3 2 1227.91 1241.69 237.75 o 5 3 2 466.93 675.29 208.78 o 7 3 2 569.34 834.12 227.76 o 9 3 2 1738.80 1853.04 231.75 o 11 3 2 508.45 398.58 187.80 o 13 3 2 412.07 584.38 201.79 o 15 3 2 152.30 -63.93 211.78 o 17 3 2 1642.08 1728.17 246.74 o 19 3 2 72.30 53.94 178.81 o 21 3 2 506.71 562.41 209.78 o 23 3 2 1603.74 1407.51 235.75 o 25 3 2 7.45 27.97 154.84 o 27 3 2 249.22 248.91 191.80 o 29 3 2 607.85 756.20 199.79 o 31 3 2 228.50 294.69 165.82 o -26 4 2 796.27 945.00 301.68 o -24 4 2 2579.79 2549.30 379.60 o -22 4 2 2425.51 2023.86 340.64 o -20 4 2 968.46 949.89 276.71 o -18 4 2 184.55 467.51 218.77 o -16 4 2 112.37 -83.91 223.76 o -14 4 2 350.00 356.62 236.75 o -12 4 2 12.00 -167.82 256.73 o -10 4 2 1307.10 977.97 314.67 o -8 4 2 9.21 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226.13 93.90 184.80 o -46 0 32 272.50 141.85 198.79 o -44 0 32 1364.00 974.97 241.74 o -42 0 32 1556.68 1949.94 258.73 o -40 0 32 470.94 196.79 203.78 o -38 0 32 5976.96 6081.57 372.61 o -36 0 32 353.57 308.67 185.80 o -34 0 32 2011.30 1995.89 275.71 o -32 0 32 1382.68 1402.52 226.76 o -30 0 32 578.44 583.38 208.78 o -28 0 32 573.10 661.30 167.82 o -26 0 32 12.20 -182.81 182.81 o -24 0 32 115.13 -54.94 177.81 o -22 0 32 151.62 54.94 155.84 o -20 0 32 320.12 217.77 181.81 o -18 0 32 1045.43 1250.68 191.80 o -16 0 32 1383.86 1282.64 238.75 o -14 0 32 1626.90 2140.74 227.76 o -12 0 32 2866.12 3204.61 271.71 o -10 0 32 32.03 171.82 141.85 o -8 0 32 1357.00 1274.65 212.77 o -47 1 32 27.51 -164.83 181.81 o -45 1 32 58.67 -147.84 186.80 o -43 1 32 231.07 310.67 208.78 o -41 1 32 0.44 31.97 202.79 o -39 1 32 109.68 390.59 175.81 o -37 1 32 184.51 276.71 176.81 o -35 1 32 393.63 360.39 205.78 o -33 1 32 569.83 150.84 194.79 o -31 1 32 957.18 849.10 220.77 o -29 1 32 11.05 14.98 181.81 o -27 1 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