#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/61/2206104.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206104_Fobs loop_ _publ_author_name 'Lei, Ke-Wei' 'Liu, Wei-Sheng' 'Yu, Kai-Bei' _publ_section_title ; [N,N-Diisopropyl-2,2'-(2,3-naphthalenedioxy)diacetamide]trinitratoneodymium(III) acetone solvate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1159 _journal_page_last m1160 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.150 _cell_angle_gamma 90.000 _cell_length_a 13.4570 _cell_length_b 19.8070 _cell_length_c 14.0800 _exptl_crystal_F_000 1700.00 _reflns_d_resolution_high 0.8332 _[local]_cod_data_source_file xu6004Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C:\XSCANS\Y1682 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 428.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5087.61 4990.88 42.55 o 4 0 0 3813.77 3898.75 53.58 o 6 0 0 29068.01 28703.29 186.85 o 8 0 0 7283.29 7107.30 116.78 o 10 0 0 5800.87 5352.53 118.47 o 12 0 0 193.72 231.10 89.05 o 14 0 0 3750.94 3931.61 139.31 o 16 0 0 14.77 -21.20 93.27 o 1 1 0 17690.70 17549.38 60.16 o 2 1 0 80707.91 79980.70 938.27 o 3 1 0 2351.88 2483.00 37.43 o 4 1 0 157.18 194.05 18.03 o 5 1 0 6648.22 6787.56 79.64 o 6 1 0 21616.16 21581.18 158.94 o 7 1 0 1118.57 1179.77 52.03 o 8 1 0 23395.40 22645.77 196.20 o 9 1 0 248.94 277.79 43.47 o 10 1 0 183.06 160.08 47.71 o 11 1 0 608.34 596.06 63.64 o 12 1 0 10101.08 9829.92 186.32 o 13 1 0 680.16 643.78 79.54 o 14 1 0 30.36 8.48 79.49 o 15 1 0 104.94 103.88 75.26 o 16 1 0 1489.28 1694.69 117.79 o 0 2 0 69734.78 76537.14 618.84 o 1 2 0 2483.66 2631.48 25.87 o 2 2 0 9677.66 9879.50 62.07 o 3 2 0 9142.77 9646.36 72.19 o 4 2 0 6635.58 6598.59 69.07 o 5 2 0 694.26 678.34 33.97 o 6 2 0 11288.57 11200.93 113.68 o 7 2 0 25197.79 25564.98 188.69 o 8 2 0 2566.54 2505.47 75.54 o 9 2 0 1056.06 1009.37 56.25 o 10 2 0 3437.15 3233.21 94.72 o 11 2 0 4192.00 4048.28 113.93 o 12 2 0 49.70 87.98 69.96 o 13 2 0 1095.35 1276.39 92.31 o 14 2 0 2332.83 2349.38 116.83 o 15 2 0 328.33 258.69 80.57 o 1 3 0 18216.55 18669.06 80.88 o 2 3 0 4185.87 4447.71 44.20 o 3 3 0 64915.49 61561.52 1830.13 o 4 3 0 5657.70 5571.01 64.53 o 5 3 0 37552.25 38135.10 192.10 o 6 3 0 742.01 731.28 39.27 o 7 3 0 611.35 536.84 44.56 o 8 3 0 4345.34 4221.38 88.52 o 9 3 0 4470.76 4494.49 97.01 o 10 3 0 574.30 530.31 59.39 o 11 3 0 255.93 322.30 68.91 o 12 3 0 131.67 199.29 63.60 o 13 3 0 2110.29 2065.61 107.26 o 14 3 0 55.41 89.04 73.14 o 15 3 0 1461.79 1631.07 112.49 o 0 4 0 1300.04 1303.54 24.51 o 1 4 0 1377.16 1301.36 25.58 o 2 4 0 198.40 205.76 16.97 o 3 4 0 75864.87 72491.14 971.09 o 4 4 0 3181.39 3525.73 54.47 o 5 4 0 5882.47 5947.37 78.31 o 6 4 0 1841.81 1830.12 51.04 o 7 4 0 9727.18 9561.30 117.30 o 8 4 0 1093.86 1158.14 53.08 o 9 4 0 2202.50 2248.00 78.65 o 10 4 0 974.31 957.12 62.61 o 11 4 0 13189.06 13581.05 193.48 o 12 4 0 9.68 -26.50 57.24 o 13 4 0 3812.94 3602.70 130.83 o 14 4 0 35.48 12.72 69.96 o 15 4 0 160.18 241.69 80.56 o 1 5 0 7726.08 8045.68 66.30 o 2 5 0 8149.30 8567.14 72.72 o 3 5 0 11263.72 11173.34 90.51 o 4 5 0 1803.21 1684.61 43.63 o 5 5 0 29530.46 28418.33 173.52 o 6 5 0 443.97 458.23 35.00 o 7 5 0 930.93 1062.47 47.76 o 8 5 0 1.58 6.36 32.86 o 9 5 0 10157.83 10301.68 143.82 o 10 5 0 279.00 306.41 55.13 o 11 5 0 4882.15 5086.17 129.98 o 12 5 0 750.75 849.61 75.31 o 13 5 0 1219.84 1113.09 93.38 o 14 5 0 11.62 19.08 61.47 o 15 5 0 1819.06 1641.08 111.46 o 0 6 0 190.05 183.46 15.91 o 1 6 0 4301.34 4599.52 54.71 o 2 6 0 3790.32 4051.07 54.59 o 3 6 0 22565.42 21935.76 134.84 o 4 6 0 8405.49 8455.25 90.57 o 5 6 0 4710.31 4909.03 76.97 o 6 6 0 910.00 978.69 44.58 o 7 6 0 9533.48 9563.82 119.29 o 8 6 0 1328.90 1296.44 57.34 o 9 6 0 1598.54 1553.66 71.15 o 10 6 0 1452.85 1484.16 78.56 o 11 6 0 5193.49 5398.55 132.14 o 12 6 0 22.98 19.08 63.60 o 13 6 0 1951.58 1824.17 105.12 o 14 6 0 782.07 807.13 88.03 o 15 6 0 136.54 152.64 79.50 o 1 7 0 19477.47 19681.01 123.10 o 2 7 0 11314.98 11333.80 96.75 o 3 7 0 2701.87 2696.77 53.30 o 4 7 0 1818.46 1882.52 51.05 o 5 7 0 25309.33 25427.80 175.72 o 6 7 0 7506.64 7534.56 105.08 o 7 7 0 4993.88 5103.09 91.79 o 8 7 0 5215.17 5075.87 101.37 o 9 7 0 3329.14 3359.34 93.64 o 10 7 0 1993.41 1947.06 86.04 o 11 7 0 407.90 378.54 68.92 o 12 7 0 2804.77 2736.60 110.53 o 13 7 0 686.57 683.00 80.60 o 14 7 0 24.68 55.12 75.25 o 15 7 0 1117.32 1130.88 100.78 o 0 8 0 29883.88 28710.63 158.90 o 1 8 0 1051.19 1093.10 36.12 o 2 8 0 1560.38 1593.86 43.59 o 3 8 0 24433.89 25388.03 161.82 o 4 8 0 9763.46 9541.33 106.72 o 5 8 0 3806.71 3925.41 76.78 o 6 8 0 5169.94 5334.52 91.85 o 7 8 0 659.05 642.87 44.56 o 8 8 0 4949.82 4880.00 102.38 o 9 8 0 643.79 695.81 59.40 o 10 8 0 6139.37 6115.34 131.23 o 11 8 0 1060.94 1178.80 77.46 o 12 8 0 105.24 139.92 71.02 o 13 8 0 598.89 639.46 78.47 o 14 8 0 2223.95 2163.08 116.81 o 15 8 0 4.95 11.66 79.49 o 1 9 0 4.77 7.42 23.32 o 2 9 0 25556.40 26178.87 168.55 o 3 9 0 473.08 473.11 37.13 o 4 9 0 5448.97 5173.25 83.41 o 5 9 0 5871.06 5857.56 95.17 o 6 9 0 9881.82 9807.89 126.79 o 7 9 0 258.03 307.47 41.35 o 8 9 0 6014.15 5918.48 115.30 o 9 9 0 47.09 58.30 46.64 o 10 9 0 659.05 554.71 70.00 o 11 9 0 40.91 10.60 58.30 o 12 9 0 4283.27 4290.47 131.95 o 13 9 0 166.77 146.29 73.14 o 14 9 0 60.26 50.88 80.56 o 0 10 0 21888.36 20812.33 153.99 o 1 10 0 1865.35 1978.86 54.23 o 2 10 0 1938.87 2040.59 56.36 o 3 10 0 1501.45 1543.75 53.12 o 4 10 0 6854.11 6849.37 97.45 o 5 10 0 1469.20 1414.74 58.42 o 6 10 0 6763.77 6509.38 110.15 o 7 10 0 154.33 157.96 45.58 o 8 10 0 2044.40 1950.58 80.74 o 9 10 0 322.75 296.88 54.07 o 10 10 0 3822.38 3865.60 115.98 o 11 10 0 135.49 114.48 59.36 o 12 10 0 273.73 288.36 73.15 o 13 10 0 11.86 -23.32 73.13 o 14 10 0 1997.22 2198.66 117.84 o 1 11 0 8657.76 8661.66 108.51 o 2 11 0 9916.59 9833.08 116.21 o 3 11 0 3322.99 3332.81 72.43 o 4 11 0 340.30 364.78 38.17 o 5 11 0 2418.04 2522.22 72.31 o 6 11 0 5851.04 5881.97 111.04 o 7 11 0 593.86 666.09 59.40 o 8 11 0 3836.21 4013.96 103.25 o 9 11 0 1913.56 1943.51 82.84 o 10 11 0 409.23 326.58 63.62 o 11 11 0 284.61 266.11 66.79 o 12 11 0 3260.48 3357.94 125.43 o 13 11 0 62.62 74.20 75.26 o 14 11 0 285.98 295.78 81.63 o 0 12 0 9119.79 9227.26 117.07 o 1 12 0 4342.88 4295.27 83.20 o 2 12 0 3156.78 3163.18 75.59 o 3 12 0 2138.82 2129.27 63.78 o 4 12 0 2734.78 2717.88 74.46 o 5 12 0 611.65 641.74 53.04 o 6 12 0 4659.86 4464.69 104.45 o 7 12 0 4878.34 4702.12 110.84 o 8 12 0 3077.63 2855.23 98.90 o 9 12 0 561.36 569.49 64.69 o 10 12 0 1761.36 1795.33 92.37 o 11 12 0 1439.78 1549.49 91.27 o 12 12 0 170.95 204.59 75.26 o 13 12 0 1008.46 1019.42 95.47 o 1 13 0 5416.62 5031.94 96.09 o 2 13 0 1512.24 1446.49 58.41 o 3 13 0 513.37 527.12 45.61 o 4 13 0 1344.19 1351.52 60.52 o 5 13 0 9903.88 9914.42 145.85 o 6 13 0 2258.79 2269.79 83.95 o 7 13 0 31.38 32.86 54.06 o 8 13 0 882.10 892.19 70.02 o 9 13 0 3696.27 3892.25 112.76 o 10 13 0 83.04 24.38 62.54 o 11 13 0 1133.09 1071.58 91.24 o 12 13 0 754.34 906.80 83.79 o 13 13 0 734.34 885.55 97.57 o 0 14 0 243.56 220.53 42.41 o 1 14 0 5629.89 5603.01 105.68 o 2 14 0 262.73 267.18 45.59 o 3 14 0 4746.77 4586.01 101.27 o 4 14 0 313.56 371.10 51.95 o 5 14 0 659.02 610.96 60.46 o 6 14 0 906.91 850.88 66.84 o 7 14 0 8202.23 8081.16 147.51 o 8 14 0 7.29 -1.06 58.29 o 9 14 0 471.61 497.32 73.17 o 10 14 0 402.28 389.13 73.16 o 11 14 0 1912.20 2081.92 106.17 o 12 14 0 93.86 54.06 63.60 o 1 15 0 4104.96 4153.77 96.92 o 2 15 0 150.95 180.21 48.76 o 3 15 0 2079.12 1894.32 81.81 o 4 15 0 106.46 85.86 50.88 o 5 15 0 10207.39 10353.32 160.73 o 6 15 0 450.49 434.76 61.50 o 7 15 0 78.63 137.80 60.42 o 8 15 0 92.16 72.08 61.48 o 9 15 0 4969.09 5012.83 140.55 o 10 15 0 130.21 216.24 72.08 o 11 15 0 780.33 926.97 93.33 o 12 15 0 177.01 184.45 76.32 o 0 16 0 2306.39 2359.09 83.95 o 1 16 0 4093.50 3985.40 103.28 o 2 16 0 818.39 843.39 66.83 o 3 16 0 7078.15 7043.77 136.71 o 4 16 0 2007.08 2089.27 86.03 o 5 16 0 131.44 149.47 58.30 o 6 16 0 1077.00 1010.11 76.39 o 7 16 0 5610.61 5318.50 136.40 o 8 16 0 711.11 722.27 79.54 o 9 16 0 401.55 475.01 82.70 o 10 16 0 826.97 916.40 90.16 o 11 16 0 851.79 896.25 91.22 o 1 17 0 2947.05 2853.68 99.94 o 2 17 0 7029.52 7097.12 138.80 o 3 17 0 78.37 92.22 61.48 o 4 17 0 143.23 172.79 57.24 o 5 17 0 1186.05 1224.56 77.46 o 6 17 0 2180.21 2355.77 99.84 o 7 17 0 262.12 234.29 73.15 o 8 17 0 2124.23 2058.00 107.25 o 9 17 0 1702.87 1538.06 102.96 o 10 17 0 240.19 203.54 77.39 o 11 17 0 453.44 432.60 85.88 o 0 18 0 10470.37 10417.51 174.59 o 1 18 0 3.47 21.20 62.53 o 2 18 0 252.19 255.50 63.61 o 3 18 0 888.48 908.07 71.08 o 4 18 0 2738.90 2862.94 104.15 o 5 18 0 1.19 44.52 63.59 o 6 18 0 2635.39 2484.06 112.62 o 7 18 0 51.31 28.62 65.72 o 8 18 0 726.93 746.64 83.78 o 9 18 0 398.96 359.43 76.34 o 10 18 0 2195.92 2391.17 121.04 o 1 19 0 0.19 11.66 54.05 o 2 19 0 5238.11 4980.89 136.35 o 3 19 0 14.50 14.84 58.30 o 4 19 0 940.72 945.20 81.68 o 5 19 0 156.24 140.99 61.48 o 6 19 0 2115.33 1935.83 107.25 o 7 19 0 13.65 -2.12 63.59 o 8 19 0 1274.43 1377.23 93.37 o 9 19 0 163.46 115.54 71.02 o 0 20 0 1389.69 1330.82 85.96 o 1 20 0 382.04 366.85 59.38 o 2 20 0 304.96 330.78 71.03 o 3 20 0 190.89 170.67 64.67 o 4 20 0 2407.97 2496.12 112.59 o 5 20 0 123.74 153.70 73.14 o 6 20 0 1075.60 1171.21 96.54 o 7 20 0 626.20 646.88 79.53 o 8 20 0 439.01 393.36 77.40 o 1 21 0 56.72 34.98 60.42 o 2 21 0 1101.63 1216.88 89.12 o 3 21 0 100.99 97.52 71.02 o 4 21 0 1215.94 1203.18 96.55 o 5 21 0 1123.98 1272.03 94.42 o 6 21 0 145.45 130.38 74.20 o 7 21 0 0.74 41.34 69.95 o 0 22 0 385.20 362.61 66.80 o 1 22 0 582.43 554.60 78.47 o 2 22 0 40.07 16.96 67.84 o 3 22 0 1500.10 1473.00 104.00 o 4 22 0 433.24 512.12 85.88 o 5 22 0 52.47 46.64 75.26 o 6 22 0 322.16 394.38 80.57 o 1 23 0 989.72 1036.37 94.41 o 2 23 0 1.28 43.46 73.13 o 3 23 0 526.15 635.15 82.71 o 4 23 0 103.62 49.82 76.32 o -15 0 1 1019.58 925.03 102.90 o -13 0 1 3320.46 3263.19 129.72 o -11 0 1 1612.14 1570.41 81.76 o -9 0 1 8546.92 8399.09 131.86 o -7 0 1 1373.37 1476.71 65.87 o -5 0 1 66361.12 62811.06 257.55 o -3 0 1 4876.48 4956.60 52.90 o -1 0 1 75747.18 77333.04 1265.51 o 1 0 1 54650.95 57923.33 534.37 o 3 0 1 11606.20 11193.64 79.43 o 5 0 1 56752.17 53565.57 236.43 o 7 0 1 10002.64 10337.57 127.12 o 9 0 1 12546.29 12038.61 160.50 o 11 0 1 1503.00 1595.64 90.24 o 13 0 1 2179.60 2166.65 115.77 o 15 0 1 2698.49 2715.24 135.97 o -16 1 1 0.59 32.86 74.19 o -15 1 1 914.21 896.31 99.71 o -14 1 1 600.44 641.59 89.08 o -13 1 1 2485.70 2383.02 117.93 o -12 1 1 1100.58 1065.34 91.25 o -11 1 1 3236.24 3067.74 99.99 o -10 1 1 34.16 57.24 42.40 o -9 1 1 5.61 63.59 44.52 o -8 1 1 4547.09 4693.05 93.90 o -7 1 1 48284.40 46575.64 260.73 o -6 1 1 2407.53 2430.13 58.57 o -5 1 1 5147.72 5145.29 72.94 o -4 1 1 3778.42 3912.83 54.64 o -3 1 1 3891.20 3958.20 47.31 o -2 1 1 3491.62 3637.07 37.77 o -1 1 1 64744.82 66038.51 1200.37 o 0 1 1 22710.11 24678.17 869.32 o 1 1 1 2353.81 2600.66 25.87 o 2 1 1 1684.42 1624.10 25.64 o 3 1 1 9869.04 9778.84 73.43 o 4 1 1 1777.53 1865.97 38.34 o 5 1 1 1876.39 1896.67 47.90 o 6 1 1 11030.88 11087.87 114.68 o 7 1 1 29841.06 29123.44 204.38 o 8 1 1 962.81 949.94 56.25 o 9 1 1 1643.78 1553.96 72.23 o 10 1 1 971.48 978.35 61.55 o 11 1 1 8309.64 8302.30 156.14 o 12 1 1 448.41 454.90 74.23 o 13 1 1 4558.05 4447.28 141.57 o 14 1 1 315.34 442.10 77.39 o 15 1 1 215.44 149.47 93.29 o -16 2 1 605.99 663.82 94.38 o -15 2 1 1303.00 1248.88 100.80 o -14 2 1 10.25 -4.24 68.89 o -13 2 1 3253.85 3294.83 128.65 o -12 2 1 6521.49 6271.59 148.31 o -11 2 1 661.45 721.26 63.64 o -10 2 1 621.19 650.21 57.28 o -9 2 1 10391.43 10187.79 143.97 o -8 2 1 3621.63 3539.83 85.25 o -7 2 1 126.36 126.15 41.34 o -6 2 1 17452.91 17861.82 143.46 o -5 2 1 17947.01 17782.88 130.09 o -4 2 1 727.33 788.03 29.74 o -3 2 1 2511.92 2653.85 40.63 o -2 2 1 14986.03 16081.57 81.48 o -1 2 1 10209.96 11119.10 57.40 o 0 2 1 7226.64 7601.11 31.07 o 1 2 1 35413.80 35377.23 458.98 o 2 2 1 30799.55 31207.98 118.16 o 3 2 1 6449.78 6419.35 59.53 o 4 2 1 13862.62 13990.50 102.12 o 5 2 1 15054.77 14968.53 118.18 o 6 2 1 6546.45 6852.81 91.18 o 7 2 1 1974.10 2007.50 61.67 o 8 2 1 10253.90 10525.48 134.43 o 9 2 1 8075.45 8001.04 128.51 o 10 2 1 200.18 190.83 50.89 o 11 2 1 3031.74 3203.98 102.08 o 12 2 1 6318.15 6096.83 147.19 o 13 2 1 200.95 196.12 77.39 o 14 2 1 125.70 104.94 73.14 o 15 2 1 2239.36 2060.06 122.12 o -15 3 1 50.46 48.76 78.44 o -14 3 1 1566.44 1619.67 101.89 o -13 3 1 760.49 842.17 85.91 o -12 3 1 1783.21 1771.12 98.75 o -11 3 1 2904.35 2774.08 103.14 o -10 3 1 4987.21 4992.99 110.88 o -9 3 1 2015.35 1921.36 75.45 o -8 3 1 8330.10 8418.47 124.43 o -7 3 1 9798.89 10054.17 119.53 o -6 3 1 1540.52 1508.34 48.90 o -5 3 1 270.96 270.43 26.51 o -4 3 1 35273.85 34244.70 164.98 o -3 3 1 11763.82 11637.31 83.54 o -2 3 1 1449.32 1654.48 28.78 o -1 3 1 94706.59 94089.41 906.12 o 0 3 1 50497.09 52592.58 492.23 o 1 3 1 16734.23 16389.01 79.79 o 2 3 1 4653.14 4774.36 48.53 o 3 3 1 977.82 878.09 26.58 o 4 3 1 20184.97 19726.38 123.46 o 5 3 1 2648.47 2762.57 54.36 o 6 3 1 13638.17 13589.21 127.04 o 7 3 1 2486.20 2333.55 63.85 o 8 3 1 577.01 518.72 47.73 o 9 3 1 121.27 99.65 44.52 o 10 3 1 4916.21 4946.13 112.99 o 11 3 1 17.59 10.60 58.30 o 12 3 1 488.27 559.90 76.35 o 13 3 1 1061.27 1013.21 80.63 o 14 3 1 1349.21 1286.12 97.63 o 15 3 1 19.44 66.77 74.19 o -15 4 1 157.14 122.96 78.44 o -14 4 1 45.87 27.56 75.26 o -13 4 1 352.36 354.12 69.98 o -12 4 1 4006.55 4103.45 124.51 o -11 4 1 1496.88 1487.33 82.81 o -10 4 1 329.74 399.74 57.26 o -9 4 1 1783.94 1717.79 72.24 o -8 4 1 13230.95 13030.99 151.16 o -7 4 1 61.86 32.86 32.86 o -6 4 1 25988.34 26328.60 178.49 o -5 4 1 1822.49 2144.86 48.94 o -4 4 1 95.24 133.58 23.32 o -3 4 1 5073.33 5318.51 60.22 o -2 4 1 45677.72 44903.51 163.92 o -1 4 1 30352.98 31074.15 123.79 o 0 4 1 13601.54 13538.72 54.51 o 1 4 1 7673.80 8131.37 62.15 o 2 4 1 20447.00 20704.64 107.25 o 3 4 1 64.78 97.53 16.96 o 4 4 1 13816.32 13724.81 106.09 o 5 4 1 190.19 258.71 27.57 o 6 4 1 2199.43 2150.30 56.39 o 7 4 1 133.15 204.60 31.80 o 8 4 1 6948.96 6904.23 109.15 o 9 4 1 302.03 373.23 45.59 o 10 4 1 577.52 494.24 62.58 o 11 4 1 569.87 546.18 64.69 o 12 4 1 4767.37 4572.68 128.85 o 13 4 1 21.53 30.74 60.42 o 14 4 1 881.35 1009.80 95.46 o 15 4 1 459.16 403.98 85.88 o -15 5 1 81.38 32.86 74.20 o -14 5 1 2456.71 2364.43 117.90 o -13 5 1 802.88 791.28 78.49 o -12 5 1 4.01 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