#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:12:56 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180983 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/63/2206350.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206350_Fobs loop_ _publ_author_name 'Liu, Jie' 'Zhang, Jun-Hong' 'Wang, Da-Qi' 'Dou, Jian-Min' _publ_section_title ; Bis{bis[2,5,8,11,14-pentaoxabicyclo[13.4.0]nonadeca-1(15),16,18-triene]potassium(I)} bis(2-thioxo-4,5-dihydro-1,3-dithiole-4,5-dithiolato)zinc(II) ; _journal_coeditor_code BR6206 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1652 _journal_page_last m1654 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 98.832 _cell_angle_beta 94.633 _cell_angle_gamma 103.500 _cell_length_a 10.9614 _cell_length_b 16.1352 _cell_length_c 22.0263 _exptl_crystal_F_000 1680.00 _reflns_d_resolution_high 0.8400 _cod_data_source_file br6206Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 010127a in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 399.37 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10767.90 10633.41 175.89 o 2 0 0 184.19 106.30 42.69 o 3 0 0 52208.58 52286.32 659.57 o 4 0 0 11698.58 11381.18 217.24 o 5 0 0 25335.16 25412.28 363.53 o 6 0 0 9196.18 8671.92 229.98 o 7 0 0 497.27 403.39 77.43 o 8 0 0 684.40 476.27 164.36 o 9 0 0 176.56 135.11 80.50 o 10 0 0 957.24 1241.02 236.93 o 11 0 0 627.67 919.13 224.13 o 12 0 0 48.44 96.05 137.04 o -12 1 0 26.86 49.52 146.00 o -11 1 0 15.72 17.93 119.96 o -10 1 0 8.60 -19.64 110.57 o -9 1 0 3.10 -36.49 63.04 o -8 1 0 4.20 -34.26 53.61 o -7 1 0 126.55 110.68 62.12 o -6 1 0 671.39 629.98 85.03 o -5 1 0 0.15 17.50 38.27 o -4 1 0 21852.96 21204.42 289.32 o -3 1 0 18109.40 18078.71 318.90 o -2 1 0 11184.52 11103.19 267.88 o -1 1 0 73.55 57.22 13.53 o 0 1 0 667.20 661.54 24.45 o 1 1 0 11930.26 12583.94 216.44 o 2 1 0 15038.78 15465.14 306.09 o 3 1 0 474.45 510.58 90.93 o 4 1 0 5297.88 5539.98 247.18 o 5 1 0 2015.88 1734.52 158.81 o 6 1 0 916.30 1145.82 168.20 o 7 1 0 273.78 251.24 72.16 o 8 1 0 131.56 84.31 71.36 o 9 1 0 214.04 177.68 77.14 o 10 1 0 18.14 183.14 134.90 o 11 1 0 58.84 14.51 152.41 o 12 1 0 0.83 -128.07 128.07 o -12 2 0 49.31 132.34 146.86 o -11 2 0 27.96 41.41 133.62 o -10 2 0 328.14 513.57 171.19 o -9 2 0 19.58 -14.22 66.42 o -8 2 0 899.72 930.43 109.76 o -7 2 0 162.07 266.82 104.17 o -6 2 0 200.27 197.29 59.33 o -5 2 0 2895.17 2833.75 119.29 o -4 2 0 2677.00 2669.03 106.33 o -3 2 0 824.19 796.46 60.54 o -2 2 0 13365.68 13410.93 174.64 o -1 2 0 36.88 70.18 32.02 o 0 2 0 27962.08 28127.80 307.59 o 1 2 0 118.58 84.95 35.43 o 2 2 0 127599.92 133543.81 1170.15 o 3 2 0 12665.71 13341.70 344.94 o 4 2 0 3284.92 3436.60 210.89 o 5 2 0 68.53 96.05 80.69 o 6 2 0 196.63 53.36 81.11 o 7 2 0 510.56 661.71 163.08 o 8 2 0 526.10 465.46 101.43 o 9 2 0 12.63 69.33 76.50 o 10 2 0 21.64 56.35 119.11 o 11 2 0 106.27 156.67 149.84 o 12 2 0 30.77 -90.08 138.32 o -12 3 0 43.74 14.51 138.74 o -11 3 0 2.40 -4.70 116.12 o -10 3 0 90.77 17.50 109.29 o -9 3 0 85.95 133.85 87.09 o -8 3 0 777.29 661.92 101.47 o -7 3 0 2356.43 2096.12 127.40 o -6 3 0 367.47 427.65 74.85 o -5 3 0 4734.93 4943.38 157.13 o -4 3 0 334.60 356.16 55.49 o -3 3 0 1788.16 1812.31 85.03 o -2 3 0 9990.23 10747.78 417.73 o -1 3 0 7811.57 7408.03 133.11 o 0 3 0 811.72 719.53 51.32 o 1 3 0 28520.88 29514.66 321.49 o 2 3 0 9627.08 8847.65 265.96 o 3 3 0 762.54 1016.04 129.35 o 4 3 0 155.73 187.84 77.70 o 5 3 0 167.90 128.50 90.93 o 6 3 0 41.71 40.98 90.93 o 7 3 0 231.92 60.19 101.18 o 8 3 0 24.53 49.95 111.00 o 9 3 0 329.62 310.51 100.15 o 10 3 0 113.29 69.59 134.90 o 11 3 0 2.32 136.61 146.43 o -12 4 0 1.18 19.64 142.59 o -11 4 0 304.41 406.42 172.47 o -10 4 0 1.95 58.91 116.12 o -9 4 0 58.65 25.19 108.01 o -8 4 0 2.03 12.37 59.96 o -7 4 0 219.46 202.51 69.22 o -6 4 0 1550.63 1460.70 103.00 o -5 4 0 7.63 24.15 41.45 o -4 4 0 7024.55 7371.48 183.50 o -3 4 0 11.63 5.31 32.99 o -2 4 0 3025.01 2972.96 104.04 o -1 4 0 3528.15 3564.53 112.58 o 0 4 0 4466.35 4349.52 125.84 o 1 4 0 2.68 -23.71 23.71 o 2 4 0 1243.07 1218.82 119.96 o 3 4 0 18243.44 18007.80 461.06 o 4 4 0 2681.19 2992.62 218.58 o 5 4 0 840.46 807.28 149.42 o 6 4 0 4715.89 4479.96 291.15 o 7 4 0 1730.78 1990.67 256.14 o 8 4 0 165.08 172.47 130.21 o 9 4 0 184.66 193.39 137.46 o 10 4 0 223.04 71.29 132.77 o 11 4 0 34.37 -22.63 140.45 o -13 5 0 51.70 13.23 139.17 o -12 5 0 7.58 -17.50 141.31 o -11 5 0 0.70 104.17 134.05 o -10 5 0 691.16 1224.37 221.99 o -9 5 0 101.93 100.75 116.97 o -8 5 0 1095.69 1126.14 127.67 o -7 5 0 6.78 28.69 53.47 o -6 5 0 14.47 -32.56 46.17 o -5 5 0 30.81 4.69 42.71 o -4 5 0 1102.55 1044.16 83.03 o -3 5 0 6129.91 5971.41 165.40 o -2 5 0 437.89 528.24 64.73 o -1 5 0 2228.64 2202.49 99.77 o 0 5 0 26142.80 27032.06 347.67 o 1 5 0 16869.32 16577.40 202.15 o 2 5 0 971.05 977.19 135.76 o 3 5 0 2805.90 2299.75 181.86 o 4 5 0 2979.95 2657.07 206.62 o 5 5 0 3596.13 3063.49 248.03 o 6 5 0 551.17 448.68 152.83 o 7 5 0 104.63 53.36 106.30 o 8 5 0 1188.09 1346.04 242.06 o 9 5 0 232.91 -27.75 123.80 o 10 5 0 9.75 36.71 131.91 o 11 5 0 257.83 227.54 190.40 o -12 6 0 0.55 -33.30 127.65 o -11 6 0 18.42 47.81 128.50 o -10 6 0 24.29 29.46 116.97 o -9 6 0 6.60 87.52 114.84 o -8 6 0 108.30 93.25 74.73 o -7 6 0 1711.21 1793.12 131.98 o -6 6 0 0.30 -11.48 48.63 o -5 6 0 1347.50 1390.21 101.55 o -4 6 0 943.78 947.72 87.08 o -3 6 0 13685.81 13001.79 269.16 o -2 6 0 1388.59 1280.15 86.26 o -1 6 0 350.22 377.60 70.23 o 0 6 0 593.69 604.93 75.16 o 1 6 0 48.88 70.32 32.10 o 2 6 0 497.12 518.69 110.14 o 3 6 0 12.45 -54.22 65.74 o 4 6 0 1671.44 1644.02 182.29 o 5 6 0 817.69 694.15 173.32 o 6 6 0 724.44 730.01 181.01 o 7 6 0 608.31 535.77 177.17 o 8 6 0 70.73 -1.28 122.95 o 9 6 0 14.16 -95.20 125.08 o 10 6 0 0.02 63.61 153.26 o -12 7 0 13.14 14.09 151.13 o -11 7 0 152.55 158.38 149.84 o -10 7 0 68.98 111.85 128.50 o -9 7 0 1342.35 1510.82 244.62 o -8 7 0 2887.02 2952.67 174.84 o -7 7 0 522.92 710.80 107.48 o -6 7 0 756.60 657.18 95.60 o -5 7 0 1469.10 1501.56 109.69 o -4 7 0 12882.53 12410.17 278.38 o -3 7 0 964.90 858.36 92.05 o -2 7 0 6838.97 6925.58 200.28 o -1 7 0 1755.52 1650.43 105.80 o 0 7 0 320.37 210.27 51.45 o 1 7 0 4088.70 3876.60 114.54 o 2 7 0 136.69 50.80 69.59 o 3 7 0 1029.99 922.97 161.37 o 4 7 0 64.23 81.54 97.33 o 5 7 0 3595.87 3861.80 307.37 o 6 7 0 379.40 302.25 146.00 o 7 7 0 80.54 65.74 127.22 o 8 7 0 300.87 151.55 147.71 o 9 7 0 24.85 19.21 137.89 o 10 7 0 35.31 -32.02 159.24 o -12 8 0 2.01 -53.36 125.51 o -11 8 0 123.48 77.27 138.32 o -10 8 0 48.90 10.67 128.50 o -9 8 0 32.25 23.91 113.13 o -8 8 0 148.44 84.78 79.75 o -7 8 0 99.35 29.92 61.03 o -6 8 0 742.62 734.85 115.26 o -5 8 0 3544.40 3539.19 166.09 o -4 8 0 749.25 757.71 97.65 o -3 8 0 1295.06 1339.15 102.88 o -2 8 0 18919.39 18379.66 340.30 o -1 8 0 75.12 40.82 46.48 o 0 8 0 4559.96 4287.50 143.90 o 1 8 0 274.62 303.28 51.27 o 2 8 0 2.15 44.40 79.40 o 3 8 0 149.35 138.32 103.74 o 4 8 0 724.38 833.75 177.17 o 5 8 0 1665.05 1651.28 246.75 o 6 8 0 79.84 -53.36 123.38 o 7 8 0 6.30 -11.10 107.58 o 8 8 0 18.54 -104.17 133.20 o 9 8 0 279.51 395.74 186.99 o 10 8 0 153.68 241.20 200.65 o -12 9 0 22.95 183.14 161.37 o -11 9 0 251.58 359.46 178.45 o -10 9 0 615.73 588.28 181.01 o -9 9 0 0.53 -20.06 99.04 o -8 9 0 444.70 553.16 114.13 o -7 9 0 1079.47 1379.21 150.63 o -6 9 0 959.30 1154.95 129.77 o -5 9 0 1340.53 1521.39 161.37 o -4 9 0 763.75 719.11 98.34 o -3 9 0 3971.54 3548.02 166.75 o -2 9 0 4786.52 4609.22 190.74 o -1 9 0 5032.67 4723.04 192.53 o 0 9 0 1362.63 1315.04 82.50 o 1 9 0 1479.98 1335.68 87.93 o 2 9 0 2515.35 2372.75 227.54 o 3 9 0 2211.70 2115.33 228.82 o 4 9 0 2262.66 1980.42 233.09 o 5 9 0 648.39 810.70 199.37 o 6 9 0 142.46 160.52 163.08 o 7 9 0 74.31 2.13 126.36 o 8 9 0 380.12 480.27 218.15 o 9 9 0 18.26 -40.13 141.31 o -12 10 0 26.80 -48.24 140.88 o -11 10 0 12.93 -2.56 124.66 o -10 10 0 13.40 59.77 140.45 o -9 10 0 88.65 85.81 119.53 o -8 10 0 31.67 5.55 75.67 o -7 10 0 992.99 803.40 126.62 o -6 10 0 0.98 -43.03 60.28 o -5 10 0 18.49 9.65 59.59 o -4 10 0 418.06 326.00 83.14 o -3 10 0 5.17 22.15 51.88 o -2 10 0 116.08 103.45 63.00 o -1 10 0 3047.08 2901.05 164.47 o 0 10 0 14.60 0.46 41.61 o 1 10 0 1077.57 1247.26 97.15 o 2 10 0 1134.37 1229.92 213.45 o 3 10 0 465.62 335.12 141.73 o 4 10 0 246.81 324.45 146.86 o 5 10 0 2.72 4.27 116.55 o 6 10 0 77.59 63.18 130.63 o 7 10 0 32.78 70.87 134.05 o 8 10 0 199.34 296.27 195.52 o -12 11 0 33.00 121.67 165.21 o -11 11 0 23.83 3.42 140.88 o -10 11 0 55.55 40.98 131.06 o -9 11 0 114.33 95.63 131.91 o -8 11 0 78.17 5.39 75.99 o -7 11 0 25.42 97.28 82.30 o -6 11 0 465.01 517.27 108.77 o -5 11 0 138.73 88.94 70.62 o -4 11 0 846.12 963.57 175.89 o -3 11 0 658.82 811.04 117.86 o -2 11 0 1395.14 1392.81 142.37 o -1 11 0 6453.58 6399.73 247.23 o 0 11 0 182.34 128.55 52.81 o 1 11 0 1308.86 1572.32 113.28 o 2 11 0 1213.46 1098.86 203.21 o 3 11 0 218.00 181.86 134.05 o 4 11 0 87.69 124.66 137.04 o 5 11 0 712.18 956.27 227.54 o 6 11 0 4.53 -21.77 138.74 o 7 11 0 194.21 167.35 182.29 o 8 11 0 239.67 251.88 187.84 o -11 12 0 3.24 -61.90 132.77 o -10 12 0 119.54 369.27 175.03 o -9 12 0 156.83 195.95 151.98 o -8 12 0 173.37 152.91 92.30 o -7 12 0 3.30 -66.24 68.49 o -6 12 0 89.67 1.63 70.98 o -5 12 0 2304.08 2404.24 169.16 o -4 12 0 70.30 61.47 71.09 o -3 12 0 1167.11 1327.90 145.77 o -2 12 0 42.35 3.75 64.85 o -1 12 0 8.33 1.83 49.07 o 0 12 0 1155.20 1276.92 110.45 o 1 12 0 21.80 -11.04 58.92 o 2 12 0 616.52 633.53 171.62 o 3 12 0 239.77 133.20 135.33 o 4 12 0 21.88 -106.73 106.73 o 5 12 0 7.90 -10.25 126.79 o 6 12 0 106.09 49.09 166.92 o 7 12 0 85.26 70.44 157.53 o -11 13 0 22.43 -53.79 157.10 o -10 13 0 96.51 151.55 154.97 o -9 13 0 7.83 -71.72 114.84 o -8 13 0 8.21 -26.04 112.70 o -7 13 0 70.11 2.95 75.42 o -6 13 0 403.47 444.52 109.22 o -5 13 0 1409.45 1542.07 169.68 o -4 13 0 2389.84 2229.72 221.78 o -3 13 0 788.82 695.35 122.12 o -2 13 0 23.84 17.96 73.64 o -1 13 0 223.41 245.16 68.61 o 0 13 0 1832.59 1794.92 131.29 o 1 13 0 2794.43 2549.69 188.83 o 2 13 0 38.93 -18.36 108.86 o 3 13 0 404.47 523.82 184.00 o 4 13 0 56.22 29.88 137.89 o 5 13 0 67.59 85.38 158.81 o 6 13 0 232.45 171.19 201.50 o -10 14 0 14.53 41.84 134.05 o -9 14 0 49.75 23.05 124.66 o -8 14 0 1.01 -58.91 116.55 o -7 14 0 74.23 4.87 79.98 o -6 14 0 2.78 -26.89 78.34 o -5 14 0 2.93 -56.45 64.90 o -4 14 0 87.24 70.40 84.03 o -3 14 0 6.19 24.95 75.79 o -2 14 0 136.15 186.35 93.79 o -1 14 0 881.93 961.71 107.03 o 0 14 0 338.40 263.55 71.06 o 1 14 0 27.15 -24.12 91.37 o 2 14 0 362.69 500.34 186.13 o 3 14 0 18.05 50.80 143.87 o 4 14 0 128.16 277.92 178.02 o 5 14 0 354.51 448.68 203.21 o 6 14 0 0.08 -60.62 159.24 o -10 15 0 37.93 -70.44 163.08 o -9 15 0 33.06 23.91 140.03 o -8 15 0 20.41 157.10 144.72 o -7 15 0 12.03 -54.91 81.28 o -6 15 0 202.14 206.42 103.13 o -5 15 0 8.82 -10.09 82.53 o -4 15 0 203.54 223.07 94.77 o -3 15 0 10.91 -72.32 73.65 o -2 15 0 38.25 75.86 85.75 o -1 15 0 3.69 -42.30 52.26 o 0 15 0 38.41 -5.63 60.04 o 1 15 0 95.90 52.83 86.41 o 2 15 0 25.25 25.61 130.63 o 3 15 0 183.25 105.02 151.98 o 4 15 0 0.33 20.49 156.25 o 5 15 0 63.83 -38.42 157.53 o -9 16 0 24.21 160.52 158.38 o -8 16 0 13.09 -74.28 117.40 o -7 16 0 72.32 19.50 97.03 o -6 16 0 16.54 37.53 89.83 o -5 16 0 76.16 -58.82 81.30 o -4 16 0 692.01 620.52 138.67 o -3 16 0 4.27 -10.65 82.72 o -2 16 0 85.11 66.76 65.05 o -1 16 0 75.08 79.00 68.54 o 0 16 0 11.60 -18.08 71.08 o 1 16 0 8.74 -15.80 143.01 o 2 16 0 77.14 130.63 160.94 o 3 16 0 59.81 -46.53 145.15 o 4 16 0 64.47 229.25 179.73 o -8 17 0 40.51 130.21 151.55 o -7 17 0 1.06 21.02 94.88 o -6 17 0 6.41 10.99 93.25 o -5 17 0 96.49 151.81 111.68 o -4 17 0 40.19 36.32 115.48 o -3 17 0 258.70 187.41 105.55 o -2 17 0 172.37 188.42 79.88 o -1 17 0 58.34 21.13 69.25 o 0 17 0 71.48 157.67 116.50 o 1 17 0 46.52 105.87 176.74 o 2 17 0 36.05 41.84 156.25 o -7 18 0 0.09 40.98 168.63 o -6 18 0 5.39 -34.99 105.66 o -5 18 0 0.58 -17.96 101.11 o -4 18 0 6.38 -25.15 86.66 o -3 18 0 295.96 254.69 92.24 o -2 18 0 41.99 24.40 73.38 o -1 18 0 0.18 -19.07 79.71 o 0 18 0 15.66 -61.01 111.18 o 3 -19 1 153.15 172.38 93.17 o 4 -19 1 25.33 -59.39 102.20 o -1 -18 1 4.05 -110.57 166.07 o 0 -18 1 0.46 -95.54 95.54 o 1 -18 1 112.33 88.04 91.44 o 2 -18 1 1.20 -22.66 73.30 o 3 -18 1 78.50 121.02 81.18 o 4 -18 1 57.72 85.04 103.05 o 5 -18 1 14.10 -54.07 98.32 o 6 -18 1 8.95 -57.63 100.07 o 7 -18 1 1.11 75.56 169.91 o -2 -17 1 81.16 -6.40 157.96 o -1 -17 1 92.24 93.49 169.91 o 0 -17 1 602.64 743.77 129.11 o 1 -17 1 8.26 -13.10 76.96 o 2 -17 1 0.41 -8.30 65.85 o 3 -17 1 47.08 -9.85 97.37 o 4 -17 1 14.95 43.67 98.16 o 5 -17 1 443.34 391.23 191.68 o 6 -17 1 218.95 71.13 106.99 o 7 -17 1 28.19 -40.13 135.76 o 8 -17 1 12.76 -29.88 156.67 o -4 -16 1 116.88 237.36 192.96 o -3 -16 1 10.04 33.73 167.77 o -2 -16 1 769.72 1131.30 274.50 o -1 -16 1 538.89 240.67 390.41 o 0 -16 1 0.50 -41.16 67.21 o 1 -16 1 258.84 253.30 78.20 o 2 -16 1 324.70 211.69 80.05 o 3 -16 1 151.32 205.96 109.53 o 4 -16 1 35.13 -27.72 81.39 o 5 -16 1 266.95 195.65 104.29 o 6 -16 1 13.08 15.48 83.89 o 7 -16 1 2.74 -28.47 89.49 o 8 -16 1 99.70 75.14 145.15 o 9 -16 1 14.64 6.83 144.72 o -5 -15 1 61.13 98.62 173.75 o -4 -15 1 13.82 -111.00 131.06 o -3 -15 1 14.24 99.47 148.14 o -2 -15 1 695.15 790.63 221.99 o -1 -15 1 45.98 7.98 88.50 o 0 -15 1 7.40 38.97 70.86 o 1 -15 1 159.58 160.77 70.35 o 2 -15 1 64.66 17.30 83.68 o 3 -15 1 723.33 574.81 141.09 o 4 -15 1 172.21 86.68 86.90 o 5 -15 1 164.89 42.68 86.04 o 6 -15 1 184.42 19.80 86.57 o 7 -15 1 34.35 33.39 85.57 o 8 -15 1 90.34 218.15 161.37 o 9 -15 1 16.71 59.34 138.32 o 10 -15 1 3.43 -50.38 146.00 o -6 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