#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:13:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180985 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/65/2206557.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206557_Fobs loop_ _publ_author_name 'Shang, Xian-Mei' 'Meng, Xiang-Gao' 'Wu, Ji-Zhou' 'Li, Qing-Shan' _publ_section_title ; 3,4-Difluorobenzohydroxamic acid ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2328 _journal_page_last o2329 _journal_volume 61 _journal_year 2005 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.9983 _cell_length_b 5.5158 _cell_length_c 26.4179 _exptl_crystal_F_000 352.00 _reflns_d_resolution_high 0.8094 _cod_data_source_file su6205Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 050603dm in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 79.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 865.89 692.64 372.45 o 4 0 0 233.70 231.85 7.87 o 6 0 0 46.12 46.99 8.37 o 1 1 0 37.42 36.90 8.27 o 2 1 0 274.69 307.67 5.43 o 3 1 0 29.12 30.18 1.61 o 4 1 0 51.99 55.60 2.86 o 5 1 0 188.03 89.51 66.81 o 6 1 0 22.86 27.30 4.45 o 0 2 0 850.77 926.21 15.36 o 1 2 0 2.31 3.50 0.61 o 2 2 0 2507.22 2727.12 29.66 o 3 2 0 133.52 123.50 4.38 o 4 2 0 292.34 284.15 5.77 o 5 2 0 6.11 6.48 1.34 o 1 3 0 0.07 0.72 0.36 o 2 3 0 176.71 182.77 4.04 o 3 3 0 125.06 132.99 4.04 o 4 3 0 13.16 14.03 1.81 o 5 3 0 26.90 24.21 2.68 o 0 4 0 288.15 288.37 12.47 o 1 4 0 21.58 21.24 3.02 o 2 4 0 14.26 13.18 2.92 o 3 4 0 0.02 1.24 2.32 o 4 4 0 2.03 3.16 1.77 o 5 4 0 1.28 1.55 1.97 o 1 5 0 0.04 0.29 0.98 o 2 5 0 25.43 31.14 4.15 o 3 5 0 6.27 5.24 1.80 o 4 5 0 16.20 17.41 3.36 o 0 6 0 20.95 20.69 4.93 o 1 6 0 0.32 0.78 1.23 o 2 6 0 3.07 5.72 1.85 o 1 0 1 1830.75 1638.29 14.50 o 2 0 1 9.10 7.43 0.61 o 3 0 1 57.42 54.83 3.89 o 4 0 1 0.01 0.04 0.55 o 5 0 1 51.31 61.16 5.03 o 6 0 1 16.24 13.54 3.17 o 0 1 1 502.29 583.90 4.53 o 1 1 1 1510.64 1427.77 76.41 o 2 1 1 389.60 391.99 3.95 o 3 1 1 37.06 38.34 1.24 o 4 1 1 8.66 6.41 1.24 o 5 1 1 2.95 1.70 0.80 o 6 1 1 0.89 0.95 0.95 o 0 2 1 898.12 889.53 16.46 o 1 2 1 147.82 168.49 2.90 o 2 2 1 107.02 112.57 2.49 o 3 2 1 53.90 65.83 2.09 o 4 2 1 0.16 1.47 0.51 o 5 2 1 1.60 1.80 0.68 o 0 3 1 61.29 51.31 3.19 o 1 3 1 194.99 215.35 2.58 o 2 3 1 8.21 9.25 0.82 o 3 3 1 0.44 0.52 0.42 o 4 3 1 36.66 36.02 2.04 o 5 3 1 12.02 11.81 1.27 o 0 4 1 0.23 0.04 1.01 o 1 4 1 3.40 4.39 1.03 o 2 4 1 18.93 17.74 2.03 o 3 4 1 77.07 76.75 3.56 o 4 4 1 11.72 10.70 1.82 o 0 5 1 5.19 2.78 1.35 o 1 5 1 16.36 15.15 2.04 o 2 5 1 6.37 7.96 1.48 o 3 5 1 2.64 4.21 1.38 o 4 5 1 7.79 13.53 2.14 o 0 6 1 20.47 19.03 3.39 o 1 6 1 10.23 10.18 1.80 o 2 6 1 7.00 5.49 1.32 o 0 0 2 511.48 317.12 4.54 o 1 0 2 2271.68 2521.79 12.44 o 2 0 2 2093.51 2000.74 22.50 o 3 0 2 16.75 18.40 0.99 o 4 0 2 488.82 477.19 8.41 o 5 0 2 3.70 3.43 1.65 o 6 0 2 1.27 -1.15 1.19 o 0 1 2 397.35 440.29 3.27 o 1 1 2 2535.10 2479.39 122.40 o 2 1 2 301.81 355.11 4.13 o 3 1 2 375.03 341.90 19.65 o 4 1 2 18.08 17.24 1.49 o 5 1 2 76.12 72.50 3.41 o 6 1 2 8.39 6.53 1.50 o 0 2 2 3371.79 3554.59 44.34 o 1 2 2 760.84 858.52 5.70 o 2 2 2 491.50 538.65 5.32 o 3 2 2 2.10 2.16 0.55 o 4 2 2 61.56 58.15 1.98 o 5 2 2 16.33 14.19 1.64 o 0 3 2 1.86 1.98 0.49 o 1 3 2 72.23 69.78 1.36 o 2 3 2 7.48 9.89 0.85 o 3 3 2 13.59 16.12 1.22 o 4 3 2 27.45 25.95 1.91 o 5 3 2 17.05 18.53 1.68 o 0 4 2 54.77 47.59 3.65 o 1 4 2 21.35 19.44 2.07 o 2 4 2 62.29 77.18 3.41 o 3 4 2 17.85 18.66 2.21 o 4 4 2 5.89 6.29 1.61 o 0 5 2 19.53 22.63 4.77 o 1 5 2 1.15 1.11 0.82 o 2 5 2 59.45 59.13 3.37 o 3 5 2 10.15 9.25 1.88 o 4 5 2 0.56 -0.08 1.29 o 0 6 2 17.26 12.78 2.91 o 1 6 2 2.06 1.37 1.22 o 2 6 2 9.95 8.51 1.69 o 1 0 3 1.93 0.94 0.23 o 2 0 3 476.09 494.73 6.72 o 3 0 3 5.82 7.08 0.68 o 4 0 3 0.42 1.45 0.71 o 5 0 3 71.21 75.19 5.60 o 6 0 3 0.57 2.05 1.44 o 0 1 3 5.89 19.21 0.66 o 1 1 3 4596.64 4370.39 190.47 o 2 1 3 84.85 67.79 2.41 o 3 1 3 67.88 75.89 1.88 o 4 1 3 61.16 61.08 2.29 o 5 1 3 28.38 29.13 2.69 o 6 1 3 2.06 1.15 1.08 o 0 2 3 21.60 33.30 1.54 o 1 2 3 16.27 17.02 0.72 o 2 2 3 383.41 324.81 37.55 o 3 2 3 128.45 109.92 3.64 o 4 2 3 45.27 46.72 1.88 o 5 2 3 12.26 14.45 1.70 o 0 3 3 0.40 0.96 0.41 o 1 3 3 59.40 55.11 1.24 o 2 3 3 9.04 10.76 0.88 o 3 3 3 6.80 7.30 0.88 o 4 3 3 15.46 16.52 1.54 o 5 3 3 26.92 22.65 1.95 o 0 4 3 22.16 18.22 2.76 o 1 4 3 3.00 3.17 0.93 o 2 4 3 1.16 0.39 0.66 o 3 4 3 30.80 29.96 2.85 o 4 4 3 7.03 8.05 1.58 o 0 5 3 36.91 48.42 7.11 o 1 5 3 29.00 27.52 2.75 o 2 5 3 1.05 0.80 0.85 o 3 5 3 8.83 7.64 1.59 o 4 5 3 1.67 1.95 1.01 o 0 6 3 23.70 17.99 3.37 o 1 6 3 15.66 18.44 2.48 o 2 6 3 1.70 3.64 1.33 o 0 0 4 6.26 0.18 0.25 o 1 0 4 2.37 5.88 0.45 o 2 0 4 700.56 757.97 7.93 o 3 0 4 106.79 117.30 2.66 o 4 0 4 0.56 1.08 0.87 o 5 0 4 177.24 165.80 8.34 o 6 0 4 6.39 7.00 2.10 o 0 1 4 6327.38 6290.22 157.71 o 1 1 4 1851.94 1638.42 201.05 o 2 1 4 491.12 497.64 4.39 o 3 1 4 296.93 292.39 3.90 o 4 1 4 98.73 90.27 2.78 o 5 1 4 67.44 60.75 3.12 o 6 1 4 14.21 13.67 2.08 o 0 2 4 1899.27 1891.21 26.49 o 1 2 4 110.98 123.10 2.03 o 2 2 4 43.31 52.29 1.36 o 3 2 4 82.82 74.01 2.25 o 4 2 4 0.77 1.34 0.50 o 5 2 4 41.30 37.90 2.76 o 0 3 4 99.25 90.68 4.33 o 1 3 4 291.18 314.63 3.04 o 2 3 4 206.48 189.62 3.39 o 3 3 4 102.07 93.08 2.63 o 4 3 4 74.98 72.81 2.44 o 5 3 4 4.19 5.75 1.11 o 0 4 4 37.22 44.79 3.56 o 1 4 4 67.54 61.06 2.95 o 2 4 4 103.48 98.74 3.84 o 3 4 4 16.34 18.76 2.28 o 4 4 4 10.57 11.51 1.84 o 0 5 4 48.74 42.79 4.21 o 1 5 4 50.06 46.72 3.29 o 2 5 4 36.97 36.82 3.18 o 3 5 4 2.61 3.44 1.08 o 4 5 4 1.48 0.87 1.15 o 0 6 4 15.89 21.96 3.67 o 1 6 4 28.76 26.61 2.85 o 2 6 4 1.39 1.93 1.01 o 1 0 5 312.58 405.39 4.50 o 2 0 5 92.04 83.65 1.86 o 3 0 5 258.53 307.80 5.24 o 4 0 5 64.74 60.21 3.53 o 5 0 5 21.08 21.79 3.66 o 6 0 5 4.84 1.00 3.10 o 0 1 5 1390.79 1401.61 19.20 o 1 1 5 2396.95 1602.14 345.57 o 2 1 5 91.97 87.98 1.80 o 3 1 5 332.71 359.74 4.68 o 4 1 5 43.06 45.99 2.08 o 5 1 5 47.76 47.90 3.15 o 6 1 5 2.36 4.92 1.46 o 0 2 5 551.80 506.28 4.32 o 1 2 5 419.79 462.53 3.43 o 2 2 5 192.07 191.60 2.47 o 3 2 5 86.61 65.29 8.48 o 4 2 5 34.08 33.36 1.90 o 5 2 5 1.58 2.41 0.84 o 0 3 5 51.77 56.17 2.35 o 1 3 5 343.86 370.25 3.80 o 2 3 5 96.71 88.19 1.95 o 3 3 5 26.06 30.06 1.82 o 4 3 5 16.95 16.58 1.54 o 5 3 5 9.56 13.64 1.66 o 0 4 5 137.93 125.49 11.56 o 1 4 5 78.97 81.62 3.40 o 2 4 5 14.52 13.43 1.60 o 3 4 5 11.89 13.11 1.96 o 4 4 5 11.43 14.43 2.01 o 0 5 5 42.20 47.57 4.45 o 1 5 5 26.57 26.41 2.71 o 2 5 5 2.96 1.85 0.83 o 3 5 5 0.37 1.90 0.92 o 4 5 5 0.22 1.14 1.01 o 0 6 5 1.11 1.11 1.39 o 1 6 5 5.37 5.92 1.38 o 2 6 5 4.56 3.78 1.22 o 0 0 6 2082.67 1721.22 11.95 o 1 0 6 1582.93 1506.94 19.98 o 2 0 6 213.87 222.65 4.81 o 3 0 6 11.12 15.43 1.19 o 4 0 6 14.46 16.62 2.32 o 5 0 6 31.42 27.46 4.14 o 6 0 6 8.02 8.09 2.45 o 0 1 6 700.38 690.25 5.33 o 1 1 6 4.26 7.77 0.93 o 2 1 6 683.87 691.43 7.05 o 3 1 6 110.98 104.90 2.56 o 4 1 6 333.28 306.73 5.18 o 5 1 6 10.74 11.25 1.70 o 6 1 6 2.10 0.89 0.92 o 0 2 6 15.83 22.28 1.03 o 1 2 6 110.07 118.74 1.79 o 2 2 6 351.53 343.68 4.01 o 3 2 6 39.63 39.91 1.58 o 4 2 6 14.57 14.97 1.41 o 5 2 6 26.12 25.00 2.25 o 0 3 6 823.00 833.08 11.93 o 1 3 6 89.94 88.51 1.60 o 2 3 6 124.97 136.39 2.94 o 3 3 6 2.33 1.96 0.61 o 4 3 6 11.38 9.59 1.20 o 5 3 6 10.70 10.17 1.53 o 0 4 6 75.89 76.10 8.20 o 1 4 6 20.64 24.40 2.06 o 2 4 6 2.57 3.28 0.86 o 3 4 6 28.63 27.23 2.78 o 4 4 6 3.00 1.85 0.95 o 0 5 6 30.02 32.92 4.22 o 1 5 6 18.91 20.68 2.15 o 2 5 6 29.15 28.64 2.93 o 3 5 6 7.51 6.86 1.48 o 4 5 6 1.13 0.85 1.05 o 0 6 6 5.25 4.77 1.58 o 1 6 6 0.49 0.37 0.71 o 2 6 6 10.68 6.70 1.58 o 1 0 7 1391.63 1404.36 14.57 o 2 0 7 499.81 497.00 7.12 o 3 0 7 4.45 5.26 0.74 o 4 0 7 107.54 108.64 6.02 o 5 0 7 6.64 5.97 2.03 o 6 0 7 4.90 4.16 1.64 o 0 1 7 384.38 368.67 23.68 o 1 1 7 563.38 458.24 6.57 o 2 1 7 62.43 58.52 1.51 o 3 1 7 33.91 32.73 1.60 o 4 1 7 57.29 58.72 2.31 o 5 1 7 1.31 0.63 0.69 o 0 2 7 307.83 325.64 4.30 o 1 2 7 139.94 137.82 1.98 o 2 2 7 437.56 444.90 6.74 o 3 2 7 151.45 149.95 3.00 o 4 2 7 96.18 97.50 3.53 o 5 2 7 30.69 27.59 2.42 o 0 3 7 91.41 105.19 2.26 o 1 3 7 119.22 123.22 1.96 o 2 3 7 151.80 156.34 2.60 o 3 3 7 7.58 7.07 1.05 o 4 3 7 15.08 13.11 1.39 o 5 3 7 12.75 17.13 1.90 o 0 4 7 468.48 445.71 14.30 o 1 4 7 40.78 38.97 2.68 o 2 4 7 76.18 77.37 3.09 o 3 4 7 3.39 2.15 0.92 o 4 4 7 28.58 27.75 2.94 o 0 5 7 90.47 92.47 4.72 o 1 5 7 8.17 11.34 1.44 o 2 5 7 3.70 3.13 1.12 o 3 5 7 6.06 6.64 1.46 o 0 6 7 17.54 19.27 2.84 o 1 6 7 2.96 2.83 0.89 o 2 6 7 16.49 16.18 2.31 o 0 0 8 28.54 35.37 1.98 o 1 0 8 1215.22 1154.22 15.96 o 2 0 8 329.72 334.03 6.98 o 3 0 8 34.92 40.30 1.95 o 4 0 8 2.06 3.57 1.53 o 5 0 8 9.46 9.95 2.37 o 0 1 8 1321.95 815.37 362.78 o 1 1 8 61.78 48.33 1.01 o 2 1 8 129.85 139.30 2.59 o 3 1 8 88.90 98.95 2.77 o 4 1 8 27.65 27.29 2.05 o 5 1 8 47.36 47.90 3.11 o 0 2 8 426.52 539.50 5.52 o 1 2 8 548.24 556.67 4.10 o 2 2 8 140.69 127.32 4.46 o 3 2 8 5.70 6.82 0.85 o 4 2 8 19.04 20.03 1.85 o 5 2 8 10.04 7.07 1.22 o 0 3 8 0.33 0.63 0.38 o 1 3 8 16.14 17.42 0.88 o 2 3 8 30.15 30.56 1.36 o 3 3 8 113.61 100.36 2.85 o 4 3 8 35.95 24.67 5.03 o 5 3 8 2.09 4.53 1.20 o 0 4 8 24.60 23.64 2.64 o 1 4 8 31.58 35.32 4.26 o 2 4 8 111.68 112.67 4.38 o 3 4 8 30.77 29.47 2.90 o 4 4 8 0.79 2.91 1.05 o 0 5 8 3.66 6.61 1.62 o 1 5 8 36.38 36.57 2.51 o 2 5 8 18.29 21.68 2.97 o 3 5 8 16.78 18.77 2.43 o 0 6 8 18.48 17.40 2.60 o 1 6 8 5.61 9.92 1.43 o 2 6 8 14.88 14.64 2.32 o 1 0 9 10.13 15.60 0.85 o 2 0 9 1250.82 1303.48 11.17 o 3 0 9 0.43 0.13 0.42 o 4 0 9 0.33 0.30 1.28 o 5 0 9 9.86 5.63 2.61 o 0 1 9 3.08 1.12 0.60 o 1 1 9 135.42 149.02 1.84 o 2 1 9 111.00 95.02 2.21 o 3 1 9 61.10 63.19 2.66 o 4 1 9 23.53 22.11 1.76 o 5 1 9 0.23 0.83 0.70 o 0 2 9 1749.76 1884.08 10.66 o 1 2 9 43.05 41.04 1.16 o 2 2 9 210.26 216.45 6.16 o 3 2 9 35.55 35.31 1.78 o 4 2 9 113.82 110.99 3.92 o 5 2 9 15.54 16.57 2.06 o 0 3 9 256.87 246.75 3.92 o 1 3 9 145.09 142.01 2.71 o 2 3 9 294.14 289.79 4.29 o 3 3 9 24.89 22.31 1.66 o 4 3 9 15.59 18.93 1.78 o 5 3 9 7.20 8.20 1.43 o 0 4 9 75.44 65.29 3.56 o 1 4 9 114.33 107.48 3.57 o 2 4 9 165.79 174.22 5.51 o 3 4 9 10.60 6.32 1.32 o 4 4 9 32.39 34.82 3.34 o 0 5 9 19.72 23.91 2.95 o 1 5 9 21.36 22.87 2.05 o 2 5 9 1.40 2.09 0.95 o 3 5 9 10.78 11.38 1.98 o 0 6 9 23.89 18.22 2.79 o 1 6 9 0.78 0.61 1.00 o 2 6 9 17.53 18.56 2.54 o 0 0 10 999.94 1047.05 16.17 o 1 0 10 18.76 13.73 0.93 o 2 0 10 33.05 44.56 2.13 o 3 0 10 25.99 29.73 1.99 o 4 0 10 22.68 15.86 2.32 o 5 0 10 0.98 0.56 1.09 o 0 1 10 1.47 0.39 0.35 o 1 1 10 330.49 330.23 2.87 o 2 1 10 4.65 3.72 0.58 o 3 1 10 5.43 5.98 0.95 o 4 1 10 0.88 2.18 0.70 o 5 1 10 24.93 25.65 2.32 o 0 2 10 62.20 69.53 2.06 o 1 2 10 273.40 299.73 3.18 o 2 2 10 100.67 73.45 11.52 o 3 2 10 91.24 80.57 2.48 o 4 2 10 96.91 98.56 3.42 o 5 2 10 10.03 12.11 1.57 o 0 3 10 75.30 74.01 2.25 o 1 3 10 66.00 65.49 1.56 o 2 3 10 24.35 26.22 1.53 o 3 3 10 47.98 40.99 6.06 o 4 3 10 2.93 3.57 0.89 o 5 3 10 13.17 12.59 1.74 o 0 4 10 17.59 21.54 2.51 o 1 4 10 159.96 145.25 4.17 o 2 4 10 115.89 101.23 4.24 o 3 4 10 0.79 2.14 0.90 o 4 4 10 4.43 6.95 2.03 o 0 5 10 52.52 46.98 3.59 o 1 5 10 26.83 27.40 2.24 o 2 5 10 0.63 3.41 1.07 o 3 5 10 22.45 25.10 2.98 o 0 6 10 4.72 4.67 1.42 o 1 6 10 0.97 2.14 1.00 o 2 6 10 15.43 17.96 2.48 o 1 0 11 34.73 31.29 1.33 o 2 0 11 65.66 84.27 2.99 o 3 0 11 2.07 2.49 0.79 o 4 0 11 8.40 9.81 1.87 o 5 0 11 9.45 8.05 2.31 o 0 1 11 394.60 354.54 4.93 o 1 1 11 245.41 239.96 2.90 o 2 1 11 59.95 67.72 1.94 o 3 1 11 20.17 20.14 1.69 o 4 1 11 4.03 4.66 0.90 o 5 1 11 2.82 2.43 0.83 o 0 2 11 148.86 157.08 3.18 o 1 2 11 329.92 339.83 4.23 o 2 2 11 103.02 60.07 14.21 o 3 2 11 17.20 17.84 1.45 o 4 2 11 27.40 27.86 2.25 o 5 2 11 0.67 2.04 0.84 o 0 3 11 118.84 125.18 3.03 o 1 3 11 30.34 34.66 1.20 o 2 3 11 94.83 98.84 2.62 o 3 3 11 189.62 182.60 4.32 o 4 3 11 6.40 5.80 1.08 o 5 3 11 0.14 1.60 1.05 o 0 4 11 14.94 13.09 2.02 o 1 4 11 3.48 3.66 0.77 o 2 4 11 54.45 52.86 3.10 o 3 4 11 13.78 14.60 2.09 o 4 4 11 8.10 8.82 2.44 o 0 5 11 4.69 4.64 1.66 o 1 5 11 2.66 2.14 0.85 o 2 5 11 3.84 2.77 1.11 o 3 5 11 4.42 3.21 1.20 o 0 6 11 4.85 8.44 1.84 o 1 6 11 0.74 0.74 0.93 o 2 6 11 3.25 5.28 1.24 o 0 0 12 203.72 205.25 8.20 o 1 0 12 28.89 26.78 1.95 o 2 0 12 129.95 151.70 4.71 o 3 0 12 32.49 28.31 2.32 o 4 0 12 42.78 45.29 3.07 o 5 0 12 7.97 12.09 2.69 o 0 1 12 499.17 531.24 6.29 o 1 1 12 837.98 986.68 6.38 o 2 1 12 8.32 11.72 1.01 o 3 1 12 36.25 38.31 2.13 o 4 1 12 2.15 3.49 0.79 o 5 1 12 32.68 33.81 2.72 o 0 2 12 266.60 263.71 4.26 o 1 2 12 76.90 66.81 5.08 o 2 2 12 44.48 35.74 3.24 o 3 2 12 59.74 63.53 2.54 o 4 2 12 15.05 14.32 1.63 o 5 2 12 3.32 3.07 1.51 o 0 3 12 23.29 32.25 1.70 o 1 3 12 122.40 117.98 2.32 o 2 3 12 39.59 34.91 1.71 o 3 3 12 212.56 232.40 6.71 o 4 3 12 1.28 1.53 0.74 o 5 3 12 8.48 8.10 1.60 o 0 4 12 40.62 38.42 3.10 o 1 4 12 111.64 95.11 13.74 o 2 4 12 23.60 24.92 2.65 o 3 4 12 6.02 5.22 1.40 o 4 4 12 12.24 10.33 2.67 o 0 5 12 5.61 4.92 1.39 o 1 5 12 51.87 52.29 3.13 o 2 5 12 1.78 3.21 1.12 o 3 5 12 12.05 15.11 2.19 o 0 6 12 4.20 5.66 1.62 o 1 6 12 0.09 0.85 0.87 o 1 0 13 36.80 42.39 2.38 o 2 0 13 3.25 8.83 1.48 o 3 0 13 0.10 0.89 0.65 o 4 0 13 32.32 29.03 2.71 o 5 0 13 13.17 12.05 2.81 o 0 1 13 1548.80 1564.17 13.53 o 1 1 13 17.73 21.14 1.25 o 2 1 13 21.85 20.29 1.26 o 3 1 13 4.54 4.67 0.90 o 4 1 13 7.66 7.10 1.05 o 5 1 13 2.12 2.72 0.88 o 0 2 13 0.87 0.81 0.45 o 1 2 13 75.96 65.94 6.79 o 2 2 13 28.02 31.24 1.43 o 3 2 13 28.08 29.28 2.09 o 4 2 13 3.99 5.63 1.07 o 5 2 13 9.47 10.08 1.53 o 0 3 13 51.31 55.28 2.58 o 1 3 13 81.39 72.42 4.11 o 2 3 13 210.46 215.56 4.02 o 3 3 13 157.01 152.65 3.71 o 4 3 13 16.30 16.58 1.99 o 0 4 13 3.04 4.97 1.27 o 1 4 13 16.28 11.71 1.86 o 2 4 13 84.24 80.35 3.87 o 3 4 13 18.38 20.97 2.85 o 4 4 13 16.16 20.22 3.77 o 0 5 13 36.22 39.21 3.79 o 1 5 13 6.68 6.39 1.19 o 2 5 13 28.59 24.89 2.84 o 3 5 13 4.61 5.74 1.44 o 0 6 13 6.79 7.74 2.34 o 1 6 13 1.60 2.28 1.04 o 0 0 14 218.72 201.09 8.85 o 1 0 14 242.13 199.28 5.29 o 2 0 14 98.38 83.50 6.42 o 3 0 14 2.11 3.58 0.97 o 4 0 14 37.48 32.31 2.91 o 5 0 14 11.13 14.91 3.15 o 0 1 14 638.57 743.04 8.04 o 1 1 14 68.00 75.16 5.92 o 2 1 14 104.37 96.75 3.28 o 3 1 14 23.85 26.72 2.04 o 4 1 14 46.78 46.54 2.45 o 5 1 14 8.19 7.12 1.29 o 0 2 14 322.18 336.66 5.12 o 1 2 14 43.09 41.16 1.96 o 2 2 14 121.95 117.10 2.90 o 3 2 14 78.59 93.92 3.19 o 4 2 14 14.73 16.50 1.76 o 5 2 14 7.97 11.25 1.52 o 0 3 14 0.50 0.57 0.47 o 1 3 14 33.99 32.55 2.43 o 2 3 14 54.54 37.59 6.08 o 3 3 14 12.97 15.18 1.59 o 4 3 14 11.80 11.00 1.67 o 0 4 14 21.91 17.99 2.70 o 1 4 14 29.03 28.34 2.67 o 2 4 14 4.28 4.86 1.18 o 3 4 14 10.20 13.02 2.00 o 4 4 14 4.70 7.20 2.31 o 0 5 14 7.15 8.30 1.71 o 1 5 14 8.03 8.15 1.37 o 2 5 14 11.27 8.78 1.68 o 3 5 14 1.96 3.08 1.22 o 0 6 14 0.35 1.18 1.67 o 1 6 14 1.26 2.40 1.04 o 1 0 15 2.17 2.74 0.94 o 2 0 15 105.49 100.62 5.87 o 3 0 15 8.19 6.44 1.23 o 4 0 15 2.45 2.53 0.99 o 5 0 15 0.29 -0.68 1.18 o 0 1 15 27.08 15.09 1.49 o 1 1 15 6.79 3.38 0.67 o 2 1 15 26.26 27.31 1.88 o 3 1 15 14.40 19.38 1.77 o 4 1 15 16.89 19.67 1.81 o 5 1 15 1.12 -0.12 0.74 o 0 2 15 234.44 231.69 4.37 o 1 2 15 15.40 7.99 3.31 o 2 2 15 127.20 121.76 3.01 o 3 2 15 55.78 62.26 2.66 o 4 2 15 22.51 22.99 2.08 o 5 2 15 0.80 2.08 0.90 o 0 3 15 3.66 3.63 0.92 o 1 3 15 48.82 37.99 5.53 o 2 3 15 221.53 219.01 4.58 o 3 3 15 15.70 16.27 1.84 o 4 3 15 0.69 0.38 1.18 o 0 4 15 0.00 1.98 0.91 o 1 4 15 19.18 16.88 1.77 o 2 4 15 88.29 82.75 4.00 o 3 4 15 15.40 10.65 2.11 o 4 4 15 8.88 8.39 2.47 o 0 5 15 42.90 53.25 5.48 o 1 5 15 9.52 10.46 1.57 o 2 5 15 3.10 4.23 1.27 o 3 5 15 5.21 4.08 2.28 o 0 6 15 7.95 5.02 3.34 o 0 0 16 323.48 303.82 11.77 o 1 0 16 263.44 296.30 6.89 o 2 0 16 226.54 232.67 6.52 o 3 0 16 22.63 29.49 2.59 o 4 0 16 20.04 26.60 2.73 o 5 0 16 38.11 37.29 5.17 o 0 1 16 148.62 126.24 3.55 o 1 1 16 26.19 24.63 1.18 o 2 1 16 58.93 67.33 2.51 o 3 1 16 35.40 39.98 2.51 o 4 1 16 27.30 28.74 2.20 o 5 1 16 12.41 10.03 1.66 o 0 2 16 29.21 32.74 5.38 o 1 2 16 2.42 1.70 0.83 o 2 2 16 236.32 224.13 4.37 o 3 2 16 63.00 65.68 2.78 o 4 2 16 27.49 26.95 2.32 o 5 2 16 12.51 13.29 1.67 o 0 3 16 223.34 229.85 6.06 o 1 3 16 16.78 13.70 3.08 o 2 3 16 36.29 36.76 2.13 o 3 3 16 32.58 31.60 2.63 o 4 3 16 5.37 7.00 1.58 o 0 4 16 59.17 55.83 5.74 o 1 4 16 2.17 2.26 0.81 o 2 4 16 13.79 15.32 2.08 o 3 4 16 1.86 2.87 1.19 o 0 5 16 3.29 3.67 1.59 o 1 5 16 22.88 22.42 2.63 o 2 5 16 6.13 8.50 1.67 o 1 0 17 262.29 258.43 9.53 o 2 0 17 134.41 127.11 4.94 o 3 0 17 1.90 2.42 0.88 o 4 0 17 15.97 18.90 2.31 o 5 0 17 16.46 14.01 2.98 o 0 1 17 5.48 3.59 1.04 o 1 1 17 52.47 50.66 1.56 o 2 1 17 17.43 16.96 1.59 o 3 1 17 33.07 34.21 2.39 o 4 1 17 18.21 21.35 1.90 o 5 1 17 2.30 2.14 1.03 o 0 2 17 0.02 -0.16 0.44 o 1 2 17 42.52 34.40 2.49 o 2 2 17 96.69 92.69 3.07 o 3 2 17 113.68 102.48 3.51 o 4 2 17 2.68 4.27 1.03 o 0 3 17 1.78 2.86 0.83 o 1 3 17 18.43 17.62 2.49 o 2 3 17 9.54 9.33 1.36 o 3 3 17 2.03 3.63 1.15 o 4 3 17 7.74 9.30 1.80 o 0 4 17 92.67 85.35 5.54 o 1 4 17 13.00 13.99 1.74 o 2 4 17 0.20 0.32 0.79 o 3 4 17 3.31 5.39 1.92 o 0 5 17 7.91 7.62 2.14 o 1 5 17 8.21 9.74 1.70 o 2 5 17 4.48 4.36 1.32 o 0 0 18 8.51 3.54 2.04 o 1 0 18 20.28 30.10 3.43 o 2 0 18 31.63 29.15 2.94 o 3 0 18 25.95 20.43 2.30 o 4 0 18 21.33 21.76 3.04 o 5 0 18 17.35 16.78 3.32 o 0 1 18 348.32 363.28 7.90 o 1 1 18 50.72 44.36 1.50 o 2 1 18 44.77 42.33 2.19 o 3 1 18 37.03 38.51 2.48 o 4 1 18 14.70 13.29 1.50 o 5 1 18 2.52 1.02 0.92 o 0 2 18 68.26 56.99 3.05 o 1 2 18 4.87 4.64 0.73 o 2 2 18 72.54 81.61 2.95 o 3 2 18 41.96 42.75 2.72 o 4 2 18 1.21 0.50 0.72 o 0 3 18 0.19 0.00 0.62 o 1 3 18 5.02 3.40 0.75 o 2 3 18 14.27 14.17 1.96 o 3 3 18 12.18 16.18 2.23 o 4 3 18 9.62 14.20 2.17 o 0 4 18 10.58 10.20 2.32 o 1 4 18 25.48 25.90 2.34 o 2 4 18 2.00 1.21 0.83 o 3 4 18 1.51 3.27 1.70 o 0 5 18 12.86 13.88 3.01 o 1 5 18 12.01 15.17 2.10 o 2 5 18 2.44 2.88 1.14 o 1 0 19 24.83 38.34 3.59 o 2 0 19 13.44 16.07 2.26 o 3 0 19 26.06 27.66 2.66 o 4 0 19 11.27 9.68 1.96 o 5 0 19 3.05 7.20 1.99 o 0 1 19 32.74 18.98 2.28 o 1 1 19 166.39 157.38 3.40 o 2 1 19 5.64 6.64 1.10 o 3 1 19 117.13 117.48 3.84 o 4 1 19 8.38 9.66 1.37 o 0 2 19 15.04 13.99 1.47 o 1 2 19 71.74 62.49 2.09 o 2 2 19 25.00 33.43 2.32 o 3 2 19 10.18 10.89 1.45 o 4 2 19 0.66 0.38 0.71 o 0 3 19 15.27 23.72 2.76 o 1 3 19 60.32 55.75 2.27 o 2 3 19 2.46 1.78 0.98 o 3 3 19 25.31 26.71 3.24 o 4 3 19 1.48 3.22 1.12 o 0 4 19 0.40 3.05 1.24 o 1 4 19 1.63 1.39 0.76 o 2 4 19 5.53 6.69 1.40 o 3 4 19 5.42 5.76 1.99 o 0 5 19 1.69 1.18 1.53 o 1 5 19 1.65 1.14 0.98 o 2 5 19 8.83 9.63 1.77 o 0 0 20 183.88 147.41 9.24 o 1 0 20 74.14 86.10 5.08 o 2 0 20 24.01 24.21 2.81 o 3 0 20 82.28 83.17 4.51 o 4 0 20 6.60 3.70 1.33 o 0 1 20 14.51 11.59 1.86 o 1 1 20 78.93 82.93 3.21 o 2 1 20 205.37 198.23 4.72 o 3 1 20 8.97 9.74 1.39 o 4 1 20 17.63 17.34 1.89 o 0 2 20 2.87 2.52 0.86 o 1 2 20 14.01 19.84 1.48 o 2 2 20 20.99 23.22 2.02 o 3 2 20 5.65 5.08 1.02 o 4 2 20 5.08 4.55 1.07 o 0 3 20 22.36 20.22 2.59 o 1 3 20 61.95 54.22 2.32 o 2 3 20 15.99 15.83 2.17 o 3 3 20 6.33 5.17 1.40 o 4 3 20 6.44 5.33 1.54 o 0 4 20 11.44 15.12 2.32 o 1 4 20 3.66 5.39 0.98 o 2 4 20 3.95 3.01 1.17 o 3 4 20 1.26 1.58 1.78 o 0 5 20 0.91 1.74 1.56 o 1 5 20 2.52 2.51 1.24 o 1 0 21 5.77 5.11 1.60 o 2 0 21 2.50 4.95 1.71 o 3 0 21 2.31 4.76 1.38 o 4 0 21 10.49 13.93 2.48 o 0 1 21 15.22 17.85 2.41 o 1 1 21 270.89 260.78 5.80 o 2 1 21 8.81 9.65 1.48 o 3 1 21 15.29 20.41 2.18 o 4 1 21 9.03 6.34 1.24 o 0 2 21 1.37 1.55 0.87 o 1 2 21 11.79 15.24 1.30 o 2 2 21 24.18 27.93 2.23 o 3 2 21 1.28 1.63 0.72 o 4 2 21 9.57 8.26 1.34 o 0 3 21 13.44 12.24 2.35 o 1 3 21 27.97 19.00 3.02 o 2 3 21 2.97 4.31 1.22 o 3 3 21 0.69 2.26 1.11 o 0 4 21 0.05 -0.47 0.95 o 1 4 21 0.05 0.35 0.62 o 2 4 21 1.47 1.80 0.95 o 3 4 21 9.11 10.59 2.82 o 0 5 21 0.03 -0.03 1.23 o 1 5 21 6.48 4.67 1.44 o 0 0 22 1.74 10.56 3.46 o 1 0 22 144.13 136.30 6.80 o 2 0 22 2.47 2.32 1.28 o 3 0 22 22.99 22.22 2.91 o 4 0 22 16.77 17.37 2.69 o 0 1 22 209.96 193.73 9.33 o 1 1 22 12.19 16.21 1.83 o 2 1 22 114.55 122.20 4.27 o 3 1 22 5.70 7.55 1.31 o 4 1 22 3.33 5.09 1.16 o 0 2 22 3.44 3.07 0.89 o 1 2 22 12.91 13.81 1.40 o 2 2 22 16.90 17.16 1.77 o 3 2 22 3.82 3.87 1.00 o 4 2 22 0.58 1.19 0.89 o 0 3 22 31.44 28.11 3.27 o 1 3 22 7.21 5.64 1.08 o 2 3 22 6.32 5.86 1.50 o 3 3 22 3.14 3.67 1.27 o 0 4 22 0.38 1.15 1.06 o 1 4 22 0.01 -0.52 0.74 o 2 4 22 2.01 1.59 0.99 o 0 5 22 1.36 0.98 1.35 o 1 0 23 16.75 20.67 3.42 o 2 0 23 10.54 11.25 2.57 o 3 0 23 16.66 12.36 2.21 o 4 0 23 2.40 1.39 1.10 o 0 1 23 11.29 8.10 1.72 o 1 1 23 14.41 16.14 1.84 o 2 1 23 21.91 26.34 2.51 o 3 1 23 2.60 2.61 0.87 o 4 1 23 4.33 3.32 1.02 o 0 2 23 23.93 22.71 2.34 o 1 2 23 10.93 9.37 1.16 o 2 2 23 23.13 23.91 2.17 o 3 2 23 9.09 5.88 1.15 o 0 3 23 7.77 8.04 2.33 o 1 3 23 1.68 1.52 0.87 o 2 3 23 0.00 0.29 0.91 o 3 3 23 3.56 3.68 1.38 o 0 4 23 0.03 0.68 1.12 o 1 4 23 1.62 1.31 0.99 o 2 4 23 3.13 4.55 1.28 o 0 0 24 462.65 493.92 18.93 o 1 0 24 0.93 1.77 1.65 o 2 0 24 6.00 5.44 1.75 o 3 0 24 7.43 6.97 1.63 o 4 0 24 0.29 1.01 1.04 o 0 1 24 3.13 2.95 1.26 o 1 1 24 3.89 4.66 1.09 o 2 1 24 24.87 26.62 2.51 o 3 1 24 6.98 10.21 1.64 o 4 1 24 0.58 0.59 0.79 o 0 2 24 4.89 4.54 2.25 o 1 2 24 3.31 5.12 0.91 o 2 2 24 7.61 8.32 1.25 o 3 2 24 8.55 6.97 1.21 o 0 3 24 1.04 0.86 1.03 o 1 3 24 1.58 2.83 0.93 o 2 3 24 1.12 1.15 1.14 o 3 3 24 0.13 1.08 1.09 o 0 4 24 0.00 1.77 1.13 o 1 4 24 1.04 1.67 0.99 o 2 4 24 6.04 7.34 1.41 o 1 0 25 121.16 109.59 6.60 o 2 0 25 1.71 2.35 1.44 o 3 0 25 18.45 18.48 3.47 o 0 1 25 15.53 17.31 3.15 o 1 1 25 13.15 13.31 1.72 o 2 1 25 7.94 8.28 1.41 o 3 1 25 0.78 0.72 0.87 o 0 2 25 0.22 -0.06 1.01 o 1 2 25 40.79 37.73 2.62 o 2 2 25 0.01 0.28 0.70 o 3 2 25 16.34 18.05 2.03 o 0 3 25 0.75 1.22 1.56 o 1 3 25 12.19 14.93 1.89 o 2 3 25 1.63 2.88 1.15 o 0 4 25 0.88 0.03 1.13 o 1 4 25 2.58 3.13 1.19 o 0 0 26 43.16 48.80 7.46 o 1 0 26 26.89 31.07 4.31 o 2 0 26 0.39 0.29 1.12 o 3 0 26 1.63 2.56 2.20 o 0 1 26 0.10 1.03 1.28 o 1 1 26 25.71 29.52 2.65 o 2 1 26 7.50 7.95 1.61 o 3 1 26 1.43 1.40 0.98 o 0 2 26 0.07 0.39 0.97 o 1 2 26 14.41 16.54 1.79 o 2 2 26 3.13 4.86 1.10 o 3 2 26 0.36 0.19 0.87 o 0 3 26 2.13 3.71 1.34 o 1 3 26 1.60 1.85 0.84 o 2 3 26 0.49 1.62 1.05 o 0 4 26 2.39 3.15 1.83 o 1 0 27 8.71 8.81 3.75 o 2 0 27 5.43 9.03 2.18 o 3 0 27 8.53 11.58 2.65 o 0 1 27 8.89 9.17 2.41 o 1 1 27 15.98 15.16 1.94 o 2 1 27 7.55 7.67 1.45 o 3 1 27 0.76 2.15 1.00 o 0 2 27 1.84 2.21 1.18 o 1 2 27 4.61 6.60 1.27 o 2 2 27 3.30 2.45 0.97 o 0 3 27 1.44 2.09 1.45 o 1 3 27 0.44 -0.12 0.93 o 2 3 27 10.98 10.32 2.49 o 0 0 28 0.00 1.76 1.64 o 1 0 28 0.23 0.70 1.09 o 2 0 28 5.74 7.09 2.20 o 3 0 28 2.22 1.80 1.50 o 0 1 28 18.27 19.08 3.57 o 1 1 28 6.39 10.61 1.89 o 2 1 28 1.95 1.44 0.89 o 3 1 28 3.86 5.09 1.24 o 0 2 28 4.15 4.65 1.43 o 1 2 28 1.51 1.62 0.90 o 2 2 28 6.78 5.16 1.30 o 0 3 28 0.29 -0.10 3.05 o 1 3 28 1.28 1.27 0.98 o 1 0 29 5.35 5.80 1.80 o 2 0 29 0.02 0.65 1.33 o 0 1 29 11.56 12.86 2.93 o 1 1 29 1.85 2.19 1.12 o 2 1 29 0.62 1.45 1.44 o 0 2 29 2.47 1.12 1.98 o 1 2 29 0.85 0.85 0.94 o 2 2 29 4.34 5.45 1.28 o 0 3 29 0.59 -0.46 1.34 o 0 0 30 0.44 -2.26 1.70 o 1 0 30 4.39 3.06 1.73 o 2 0 30 0.91 1.33 1.35 o 0 1 30 0.19 1.65 1.54 o 1 1 30 2.18 1.57 1.03 o 2 1 30 2.21 3.42 1.23 o 0 2 30 0.69 2.03 1.65 o 1 2 30 4.57 3.44 1.04 o 1 0 31 1.84 2.93 2.02 o 0 1 31 0.19 3.00 1.50 o 1 1 31 0.56 1.97 1.10 o 0 2 31 0.08 0.70 1.54 o 0 0 32 0.22 2.94 1.90 o 1 0 32 1.97 1.91 1.25 o 0 1 32 1.28 1.58 1.65 o