#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/65/2206559.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206559_Fobs loop_ _publ_author_name 'Dong, Min' 'Sun, Liang-Dong' _publ_section_title ; 4-Methylthiazole-5-carbaldehyde ; _journal_coeditor_code SU6210 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2712 _journal_page_last o2713 _journal_volume 61 _journal_year 2005 _space_group_IT_number 33 _symmetry_space_group_name_Hall 'P 2c -2n' _symmetry_space_group_name_H-M 'P n a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 22.5740 _cell_length_b 3.9269 _cell_length_c 6.6260 _exptl_crystal_F_000 264.00 _reflns_d_resolution_high 0.8000 _[local]_cod_data_source_file su6210Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50610D in Pna2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 79.96 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 1 -4 474.70 508.25 16.58 o 1 2 -4 135.45 144.02 4.86 o 2 2 -4 69.71 63.93 2.33 o 3 2 -4 23.46 20.75 0.93 o 4 2 -4 120.56 120.95 4.17 o 1 3 -4 15.81 15.80 0.85 o 2 3 -4 138.30 164.71 43.69 o 3 3 -4 66.50 59.75 2.23 o 4 3 -4 65.40 62.00 2.35 o 5 3 -4 14.56 13.61 0.83 o 1 4 -4 26.48 30.43 1.43 o 2 4 -4 1.94 4.60 1.43 o 3 4 -4 0.01 -1.94 1.94 o 4 4 -4 2.52 5.90 0.68 o 8 0 -3 1481.42 1784.28 56.96 o 2 1 -3 93.46 98.01 3.44 o 3 1 -3 82.53 82.12 2.88 o 4 1 -3 58.04 60.89 2.17 o 5 1 -3 410.53 414.09 13.75 o 6 1 -3 422.14 464.33 15.67 o 7 1 -3 446.87 483.20 15.65 o 8 1 -3 165.34 135.07 34.45 o 9 1 -3 76.80 70.32 11.11 o 10 1 -3 25.26 27.76 1.18 o 11 1 -3 197.64 212.77 7.21 o 2 2 -3 85.39 77.53 2.75 o 3 2 -3 7.08 7.06 0.50 o 4 2 -3 133.12 121.18 4.12 o 5 2 -3 46.47 48.18 1.81 o 6 2 -3 29.47 26.89 1.15 o 8 2 -3 142.27 146.62 5.00 o 9 2 -3 204.46 211.60 6.99 o 10 2 -3 87.71 93.56 3.40 o 11 2 -3 133.66 130.69 4.63 o 12 2 -3 2.51 3.07 0.56 o 0 3 -3 83.23 84.09 3.05 o 1 3 -3 268.87 254.43 28.89 o 2 3 -3 7.92 10.99 3.37 o 3 3 -3 18.08 13.72 0.82 o 4 3 -3 26.69 24.62 1.15 o 5 3 -3 81.31 82.49 3.01 o 6 3 -3 73.64 76.76 2.88 o 7 3 -3 7.26 6.19 0.67 o 8 3 -3 12.87 11.63 0.82 o 9 3 -3 0.71 -0.48 0.48 o 10 3 -3 16.02 15.94 0.95 o 11 3 -3 1.54 1.36 0.55 o 12 3 -3 58.08 60.26 2.36 o 13 3 -3 9.12 11.33 0.83 o 1 4 -3 52.77 53.65 8.41 o 2 4 -3 4.33 8.42 3.73 o 3 4 -3 113.18 143.68 73.70 o 4 4 -3 19.30 39.10 76.70 o 5 4 -3 4.10 3.60 0.70 o 6 4 -3 13.50 12.42 0.87 o 7 4 -3 9.05 9.19 0.88 o 8 4 -3 2.25 2.45 0.62 o 9 4 -3 4.33 2.72 0.67 o 10 4 -3 4.21 3.51 0.70 o 11 4 -3 5.46 4.69 0.71 o 12 4 -3 0.39 0.82 0.65 o 6 0 -2 1395.80 1472.04 50.07 o 8 0 -2 945.84 1127.78 38.12 o 10 0 -2 199.12 208.33 7.23 o 12 0 -2 714.09 735.83 23.97 o 14 0 -2 772.92 732.00 24.16 o 16 0 -2 45.99 44.15 1.83 o 18 0 -2 535.64 459.51 15.24 o 2 1 -2 3.34 3.09 0.26 o 3 1 -2 897.58 809.08 28.98 o 4 1 -2 419.49 498.91 16.50 o 5 1 -2 902.45 761.59 212.06 o 6 1 -2 71.05 70.13 14.48 o 7 1 -2 286.08 304.82 38.76 o 8 1 -2 333.57 347.27 33.86 o 9 1 -2 1461.12 1559.34 84.94 o 10 1 -2 194.70 221.35 7.38 o 11 1 -2 65.56 68.66 1.82 o 12 1 -2 28.71 29.56 2.56 o 13 1 -2 12.59 12.47 0.96 o 14 1 -2 43.92 45.89 1.65 o 15 1 -2 179.96 203.49 7.48 o 16 1 -2 202.28 208.73 7.32 o 17 1 -2 100.62 110.80 4.14 o 18 1 -2 0.98 0.78 0.79 o 0 2 -2 1196.14 1032.13 34.13 o 1 2 -2 279.18 264.41 9.02 o 2 2 -2 292.15 269.77 9.23 o 3 2 -2 21.65 19.31 0.90 o 4 2 -2 224.20 240.67 8.10 o 5 2 -2 160.56 167.67 5.83 o 6 2 -2 354.60 378.85 12.80 o 7 2 -2 396.40 326.66 73.08 o 8 2 -2 57.45 43.77 5.61 o 9 2 -2 14.93 16.68 2.95 o 10 2 -2 18.96 20.47 3.42 o 11 2 -2 81.62 77.97 6.14 o 12 2 -2 107.95 97.48 4.53 o 13 2 -2 97.89 103.17 2.73 o 14 2 -2 126.21 128.38 3.54 o 15 2 -2 20.61 18.33 1.38 o 16 2 -2 16.14 18.33 1.05 o 17 2 -2 2.81 2.78 0.62 o 1 3 -2 32.90 32.15 0.95 o 2 3 -2 180.30 172.90 12.04 o 3 3 -2 95.10 83.37 3.07 o 4 3 -2 135.92 124.35 4.48 o 5 3 -2 69.10 67.74 2.57 o 6 3 -2 3.07 4.77 0.67 o 7 3 -2 1.96 0.73 0.52 o 8 3 -2 54.24 58.58 2.33 o 9 3 -2 55.98 56.27 2.24 o 10 3 -2 65.49 66.29 2.57 o 11 3 -2 38.11 36.83 3.18 o 12 3 -2 21.83 19.86 1.06 o 13 3 -2 11.05 12.16 1.54 o 14 3 -2 27.13 28.04 1.08 o 15 3 -2 43.46 41.45 1.41 o 16 3 -2 54.02 53.99 2.25 o 17 3 -2 15.51 17.04 1.03 o 18 3 -2 3.35 3.55 0.69 o 19 3 -2 1.21 0.93 0.70 o 0 4 -2 19.07 18.17 0.99 o 1 4 -2 50.99 46.02 3.60 o 2 4 -2 7.95 9.59 2.02 o 3 4 -2 10.57 11.98 5.72 o 4 4 -2 4.21 6.94 4.10 o 5 4 -2 26.65 44.14 104.49 o 6 4 -2 2.49 5.63 0.76 o 7 4 -2 42.05 43.79 1.91 o 8 4 -2 3.15 1.88 0.64 o 9 4 -2 2.77 1.89 0.67 o 10 4 -2 1.37 0.77 0.69 o 11 4 -2 19.98 23.50 1.27 o 12 4 -2 1.66 1.79 0.68 o 13 4 -2 32.02 35.69 1.71 o 14 4 -2 3.50 6.48 0.90 o 4 0 -1 1115.05 1076.79 38.07 o 6 0 -1 1923.91 1774.86 63.14 o 8 0 -1 3515.62 3588.30 126.13 o 10 0 -1 422.15 440.30 15.25 o 12 0 -1 6.82 47.29 70.65 o 14 0 -1 326.83 291.22 101.00 o 16 0 -1 834.79 760.38 24.41 o 18 0 -1 15.06 12.17 36.63 o 20 0 -1 127.83 85.82 69.25 o 22 0 -1 189.75 176.75 68.17 o 24 0 -1 18.81 -122.05 122.05 o 1 1 -1 4204.55 4165.97 141.09 o 2 1 -1 711.53 758.63 24.76 o 3 1 -1 789.35 700.73 153.39 o 4 1 -1 147.79 132.02 23.59 o 5 1 -1 273.85 245.77 48.04 o 6 1 -1 3.52 3.29 0.43 o 7 1 -1 1089.70 1164.32 141.43 o 8 1 -1 35.35 36.94 3.83 o 9 1 -1 43.80 52.42 3.28 o 10 1 -1 249.10 275.01 35.21 o 11 1 -1 70.68 68.68 11.87 o 12 1 -1 232.81 271.68 40.66 o 13 1 -1 447.00 438.08 54.48 o 14 1 -1 113.82 118.72 6.21 o 15 1 -1 86.36 88.11 6.97 o 16 1 -1 50.44 53.13 3.48 o 17 1 -1 236.16 204.45 96.26 o 18 1 -1 160.05 137.90 41.03 o 19 1 -1 109.36 35.27 100.01 o 20 1 -1 12.23 16.22 21.16 o 21 1 -1 16.75 26.64 103.01 o 22 1 -1 3.45 1.95 6.20 o 23 1 -1 7.85 5.51 12.12 o 24 1 -1 7.08 -90.60 90.60 o 25 1 -1 30.05 -61.40 93.10 o 26 1 -1 1.01 -0.08 0.65 o 27 1 -1 11.69 -100.27 100.27 o 1 2 -1 606.10 559.09 18.58 o 2 2 -1 488.78 501.36 16.82 o 3 2 -1 293.67 293.03 9.98 o 4 2 -1 1025.27 797.68 197.16 o 5 2 -1 71.73 61.61 14.45 o 6 2 -1 78.04 86.50 15.89 o 7 2 -1 76.36 76.29 18.75 o 8 2 -1 431.56 403.33 29.73 o 9 2 -1 140.46 114.82 17.49 o 10 2 -1 335.76 318.70 26.64 o 11 2 -1 5.69 5.26 1.95 o 12 2 -1 7.27 8.33 8.59 o 13 2 -1 10.31 11.97 0.86 o 14 2 -1 95.34 96.57 2.60 o 15 2 -1 82.71 89.63 3.54 o 16 2 -1 14.38 12.88 1.16 o 17 2 -1 28.66 32.02 1.82 o 20 2 -1 0.50 0.03 0.48 o 21 2 -1 26.65 27.62 1.48 o 22 2 -1 54.05 54.89 2.37 o 23 2 -1 11.09 13.24 1.09 o 24 2 -1 1.93 1.23 0.72 o 25 2 -1 1.28 2.14 0.74 o 0 3 -1 233.72 182.65 6.31 o 1 3 -1 18.25 16.79 0.62 o 2 3 -1 93.96 80.33 2.42 o 3 3 -1 0.74 0.95 0.28 o 4 3 -1 11.14 11.97 1.29 o 5 3 -1 73.31 76.31 2.86 o 6 3 -1 250.28 279.75 9.66 o 7 3 -1 61.75 60.65 2.41 o 8 3 -1 82.82 75.35 10.44 o 9 3 -1 18.04 18.73 1.47 o 10 3 -1 16.76 15.36 1.59 o 11 3 -1 41.01 33.40 6.29 o 12 3 -1 61.39 59.75 7.78 o 13 3 -1 106.57 88.06 2.46 o 14 3 -1 22.24 23.20 4.09 o 15 3 -1 1.67 1.21 0.53 o 16 3 -1 4.68 6.48 1.77 o 17 3 -1 38.98 33.63 4.09 o 18 3 -1 4.17 5.29 0.66 o 19 3 -1 18.66 17.33 0.95 o 20 3 -1 22.67 26.66 1.14 o 21 3 -1 3.16 3.92 0.70 o 1 4 -1 5.39 5.15 0.42 o 2 4 -1 4.34 5.56 0.93 o 3 4 -1 38.74 40.26 4.22 o 4 4 -1 2.55 4.96 0.73 o 5 4 -1 21.51 24.09 9.07 o 6 4 -1 0.22 -0.91 1.89 o 7 4 -1 7.94 7.57 0.85 o 8 4 -1 9.29 10.11 0.93 o 9 4 -1 51.10 49.01 2.12 o 10 4 -1 6.27 6.13 0.78 o 11 4 -1 35.86 37.27 1.76 o 12 4 -1 4.67 6.29 0.82 o 13 4 -1 5.31 5.81 0.87 o 14 4 -1 1.28 3.25 1.57 o 15 4 -1 42.53 42.94 2.09 o 4 0 0 1547.70 1425.94 184.07 o 6 0 0 939.87 867.94 99.16 o 8 0 0 837.35 851.09 113.61 o 10 0 0 15.05 -0.28 54.91 o 12 0 0 140.97 168.44 30.58 o 14 0 0 769.61 627.89 88.22 o 16 0 0 22.07 15.00 2.87 o 18 0 0 283.90 62.42 108.01 o 20 0 0 27.97 23.21 5.13 o 22 0 0 4.49 3.54 39.57 o 24 0 0 24.91 -111.72 111.72 o 26 0 0 33.39 -95.91 95.91 o 28 0 0 1.24 0.66 0.78 o 1 1 0 726.14 903.51 30.31 o 2 1 0 6393.17 5871.23 1101.49 o 3 1 0 551.71 570.89 19.22 o 4 1 0 150.86 219.67 7.49 o 5 1 0 2224.52 2364.09 245.71 o 6 1 0 497.62 505.64 41.63 o 7 1 0 21.19 19.62 3.86 o 8 1 0 23.22 24.78 3.49 o 9 1 0 1553.57 1453.51 128.46 o 10 1 0 136.52 147.55 52.89 o 11 1 0 4.62 15.34 32.29 o 12 1 0 45.35 44.01 11.39 o 13 1 0 1.69 1.49 1.35 o 14 1 0 103.64 120.48 39.57 o 15 1 0 420.65 373.49 90.06 o 16 1 0 39.77 31.92 9.11 o 17 1 0 147.13 122.99 39.99 o 18 1 0 1.44 26.63 61.78 o 19 1 0 8.24 10.80 5.27 o 20 1 0 3.58 3.36 2.87 o 21 1 0 162.06 12.73 64.82 o 22 1 0 1.44 3.29 9.61 o 23 1 0 78.47 -62.24 62.24 o 24 1 0 6.02 1.95 28.19 o 25 1 0 1.89 1.43 23.52 o 26 1 0 0.00 -1.22 30.82 o 27 1 0 3.27 1.36 1.17 o 0 2 0 8.06 7.57 0.48 o 1 2 0 390.21 330.59 18.05 o 2 2 0 15.23 13.08 1.74 o 3 2 0 0.95 0.68 0.28 o 4 2 0 30.55 25.72 8.12 o 5 2 0 22.88 23.56 5.25 o 6 2 0 236.41 226.62 53.66 o 7 2 0 304.30 294.47 28.82 o 8 2 0 131.91 107.50 11.81 o 9 2 0 4.41 4.95 2.57 o 10 2 0 51.69 45.37 6.19 o 11 2 0 20.35 26.27 4.72 o 12 2 0 570.63 548.37 54.79 o 13 2 0 50.07 62.38 5.39 o 14 2 0 146.32 166.06 16.89 o 15 2 0 14.26 14.74 3.50 o 16 2 0 79.99 84.23 8.41 o 17 2 0 142.67 152.96 10.76 o 18 2 0 72.00 83.73 40.01 o 19 2 0 113.57 111.45 66.24 o 20 2 0 35.62 38.79 28.71 o 21 2 0 2.20 4.73 20.95 o 22 2 0 0.01 0.27 0.52 o 23 2 0 19.25 19.39 3.94 o 24 2 0 20.46 16.11 1.57 o 25 2 0 3.35 4.07 1.66 o 1 3 0 1.85 2.40 0.72 o 2 3 0 44.18 41.45 1.57 o 3 3 0 155.08 154.67 5.45 o 4 3 0 76.37 74.45 3.30 o 5 3 0 80.16 83.76 4.58 o 6 3 0 6.44 8.35 1.62 o 7 3 0 81.00 68.47 10.65 o 8 3 0 82.48 71.09 17.10 o 9 3 0 169.49 146.77 31.53 o 10 3 0 88.68 79.89 14.78 o 11 3 0 22.74 21.87 3.27 o 12 3 0 0.91 1.05 0.50 o 13 3 0 5.68 6.90 2.83 o 14 3 0 111.21 102.82 17.99 o 15 3 0 0.02 0.53 0.52 o 16 3 0 37.01 38.21 6.54 o 17 3 0 0.21 0.00 1.10 o 18 3 0 0.00 0.25 1.92 o 19 3 0 21.82 18.67 1.67 o 20 3 0 5.68 7.57 2.00 o 21 3 0 0.23 -0.12 0.75 o 22 3 0 31.09 33.04 1.33 o 0 4 0 24.86 22.45 1.08 o 1 4 0 53.02 45.89 1.31 o 2 4 0 0.37 1.59 0.34 o 3 4 0 6.76 6.64 0.48 o 4 4 0 12.28 12.89 1.27 o 5 4 0 76.36 80.41 7.22 o 6 4 0 4.85 9.54 3.15 o 7 4 0 101.06 140.23 77.76 o 8 4 0 5.59 7.32 0.86 o 9 4 0 0.14 -0.58 0.58 o 10 4 0 1.68 0.70 0.65 o 11 4 0 32.09 26.35 8.14 o 12 4 0 3.64 3.64 0.66 o 13 4 0 11.39 12.38 2.44 o 14 4 0 17.63 20.54 3.15 o 15 4 0 0.00 1.03 0.57 o 16 4 0 1.32 1.08 0.93 o 2 0 1 4264.48 4042.93 135.81 o 4 0 1 1067.08 1068.61 55.66 o 6 0 1 1923.35 1722.81 126.26 o 8 0 1 3538.28 3840.20 196.21 o 10 0 1 440.50 461.46 26.04 o 12 0 1 7.46 29.79 55.48 o 14 0 1 337.96 469.43 104.03 o 16 0 1 839.11 538.53 121.09 o 18 0 1 14.47 20.12 90.62 o 20 0 1 126.53 80.19 88.47 o 22 0 1 190.45 102.54 105.81 o 24 0 1 18.20 -77.64 77.64 o 26 0 1 10.96 5.70 65.71 o 28 0 1 2.83 -76.22 106.44 o 0 1 1 4048.35 3983.40 314.05 o 1 1 1 4198.17 4417.07 248.93 o 2 1 1 705.89 717.34 40.19 o 3 1 1 787.95 843.93 62.55 o 4 1 1 145.53 148.62 17.95 o 5 1 1 276.74 286.66 25.63 o 6 1 1 3.87 2.58 2.97 o 7 1 1 1105.04 1160.09 101.93 o 8 1 1 36.13 38.01 2.03 o 9 1 1 42.27 49.36 5.46 o 10 1 1 249.91 261.24 18.67 o 11 1 1 71.08 64.88 6.48 o 12 1 1 238.49 261.12 12.93 o 13 1 1 447.79 428.73 19.49 o 14 1 1 114.86 117.69 12.97 o 15 1 1 86.96 91.44 16.26 o 16 1 1 50.83 50.87 6.03 o 17 1 1 234.14 240.84 74.16 o 18 1 1 159.57 133.55 20.24 o 19 1 1 105.91 91.26 24.08 o 20 1 1 12.37 19.17 24.35 o 21 1 1 17.17 19.14 15.58 o 22 1 1 3.46 3.03 8.94 o 23 1 1 7.75 8.53 7.83 o 24 1 1 7.21 8.21 33.90 o 25 1 1 30.08 28.80 35.37 o 26 1 1 0.97 0.53 24.62 o 27 1 1 11.68 13.91 55.06 o 1 2 1 607.00 587.08 35.02 o 2 2 1 506.30 478.20 30.47 o 3 2 1 292.97 276.98 22.91 o 4 2 1 1029.14 937.53 114.08 o 5 2 1 72.04 71.11 12.82 o 6 2 1 78.42 98.89 13.13 o 7 2 1 78.70 87.07 13.84 o 8 2 1 430.50 448.06 50.16 o 9 2 1 144.47 136.58 8.78 o 10 2 1 330.59 333.04 30.57 o 11 2 1 5.64 6.28 1.92 o 12 2 1 7.63 16.84 3.42 o 13 2 1 10.02 15.50 3.17 o 14 2 1 91.68 95.30 8.70 o 15 2 1 81.50 91.13 23.55 o 16 2 1 14.73 17.64 8.38 o 17 2 1 27.64 26.97 5.61 o 18 2 1 24.16 25.23 15.57 o 19 2 1 24.33 22.40 18.29 o 20 2 1 0.44 0.99 5.88 o 21 2 1 25.60 26.54 14.52 o 22 2 1 53.56 51.55 18.65 o 23 2 1 11.05 12.92 21.94 o 24 2 1 1.90 0.44 18.90 o 25 2 1 1.30 1.01 0.56 o 0 3 1 239.36 199.78 6.92 o 1 3 1 18.45 18.22 0.68 o 2 3 1 93.41 84.51 11.43 o 3 3 1 0.76 0.93 0.29 o 4 3 1 12.08 9.82 1.69 o 5 3 1 71.20 68.35 10.56 o 6 3 1 250.90 237.07 29.27 o 7 3 1 60.24 54.41 6.72 o 8 3 1 83.02 76.78 15.60 o 9 3 1 18.29 19.61 3.06 o 10 3 1 16.54 17.26 4.03 o 11 3 1 40.65 35.75 7.86 o 12 3 1 59.79 62.89 19.05 o 13 3 1 106.79 101.93 18.69 o 14 3 1 23.18 24.99 4.81 o 15 3 1 1.76 1.82 0.55 o 16 3 1 4.49 5.68 0.74 o 17 3 1 39.87 37.36 7.72 o 18 3 1 4.05 2.58 0.66 o 19 3 1 19.66 18.91 7.09 o 20 3 1 22.37 26.65 1.62 o 21 3 1 3.02 0.84 0.61 o 1 4 1 5.47 5.95 0.44 o 2 4 1 4.17 3.84 0.40 o 3 4 1 37.92 36.20 2.41 o 4 4 1 2.66 5.08 0.46 o 5 4 1 21.15 18.43 0.73 o 6 4 1 0.23 -0.35 0.39 o 7 4 1 7.60 9.71 0.68 o 8 4 1 9.25 16.96 2.92 o 9 4 1 50.49 61.56 33.01 o 10 4 1 6.15 8.24 2.49 o 11 4 1 35.95 37.66 8.89 o 12 4 1 4.57 5.96 1.32 o 13 4 1 5.24 8.26 0.79 o 14 4 1 1.35 3.11 0.76 o 15 4 1 43.25 42.03 11.11 o 0 0 2 3025.89 2958.80 99.37 o 2 0 2 203.70 215.25 5.98 o 4 0 2 443.81 444.68 13.72 o 6 0 2 1439.53 1340.66 60.19 o 8 0 2 957.04 1057.83 60.78 o 10 0 2 200.48 189.09 8.67 o 12 0 2 709.86 660.26 19.58 o 14 0 2 773.08 683.50 46.42 o 16 0 2 45.51 39.88 6.51 o 18 0 2 521.99 399.69 35.58 o 20 0 2 19.88 22.60 19.37 o 22 0 2 9.51 7.67 14.55 o 24 0 2 26.12 23.13 13.58 o 26 0 2 23.27 24.16 33.05 o 1 1 2 288.77 322.59 14.48 o 2 1 2 3.92 3.98 1.25 o 3 1 2 872.79 928.62 38.34 o 4 1 2 427.68 492.72 19.44 o 5 1 2 904.88 957.20 54.90 o 6 1 2 71.11 84.01 5.10 o 7 1 2 287.07 315.91 12.89 o 8 1 2 337.00 343.63 19.78 o 9 1 2 1469.75 1525.19 75.69 o 10 1 2 195.50 204.13 9.25 o 11 1 2 64.96 62.66 6.22 o 12 1 2 29.07 27.48 2.24 o 13 1 2 11.89 13.39 2.74 o 14 1 2 43.34 43.31 2.94 o 15 1 2 185.31 191.24 16.58 o 16 1 2 199.14 178.21 27.25 o 17 1 2 99.41 98.10 17.03 o 18 1 2 1.04 -0.90 14.80 o 19 1 2 7.13 8.99 7.39 o 20 1 2 92.23 75.61 21.35 o 21 1 2 48.08 43.76 17.27 o 22 1 2 0.53 1.75 6.90 o 23 1 2 38.67 33.48 11.69 o 24 1 2 2.03 4.08 24.08 o 25 1 2 6.67 4.64 9.52 o 26 1 2 3.60 4.14 24.06 o 0 2 2 1201.44 1149.78 125.53 o 1 2 2 270.50 290.14 17.13 o 2 2 2 285.35 297.45 20.08 o 3 2 2 21.52 21.41 2.18 o 4 2 2 224.32 225.48 14.96 o 5 2 2 157.35 151.25 13.63 o 6 2 2 345.28 321.36 31.77 o 7 2 2 400.44 386.26 47.24 o 8 2 2 56.06 48.35 4.73 o 9 2 2 14.62 18.34 2.61 o 10 2 2 20.11 25.02 4.44 o 11 2 2 82.57 85.22 11.91 o 12 2 2 106.33 105.81 11.01 o 13 2 2 101.55 116.35 9.93 o 14 2 2 128.59 137.35 11.50 o 15 2 2 20.53 22.43 6.50 o 16 2 2 16.33 17.82 5.55 o 17 2 2 3.24 2.95 13.52 o 18 2 2 111.80 108.10 29.78 o 19 2 2 12.51 13.78 10.80 o 20 2 2 22.35 26.53 19.95 o 21 2 2 4.62 5.46 5.90 o 22 2 2 1.58 -1.25 22.98 o 23 2 2 4.95 7.94 25.88 o 24 2 2 6.84 5.67 26.39 o 1 3 2 34.47 39.63 1.57 o 2 3 2 180.87 176.99 17.78 o 3 3 2 98.74 87.18 7.58 o 4 3 2 131.46 117.42 11.98 o 5 3 2 68.84 62.50 5.87 o 6 3 2 2.93 4.79 1.64 o 7 3 2 1.84 1.89 0.58 o 8 3 2 54.97 58.72 4.86 o 9 3 2 54.46 58.11 6.14 o 10 3 2 64.44 61.24 7.81 o 11 3 2 36.81 37.55 9.92 o 12 3 2 21.90 24.27 17.45 o 13 3 2 10.86 12.82 3.68 o 14 3 2 27.25 31.09 9.19 o 15 3 2 42.53 43.64 15.28 o 16 3 2 55.71 56.00 13.99 o 17 3 2 15.91 19.10 6.85 o 18 3 2 3.24 6.85 2.88 o 19 3 2 1.22 2.43 0.62 o 20 3 2 5.56 4.91 0.80 o 21 3 2 20.18 22.09 2.27 o 0 4 2 19.19 18.07 1.00 o 1 4 2 53.20 45.07 1.34 o 2 4 2 8.21 8.83 1.68 o 3 4 2 10.50 10.25 1.12 o 4 4 2 4.09 4.85 0.45 o 5 4 2 27.24 28.04 2.83 o 6 4 2 2.56 3.88 0.70 o 7 4 2 41.48 45.07 3.32 o 8 4 2 3.31 4.95 1.01 o 9 4 2 2.67 5.32 1.66 o 10 4 2 1.33 2.05 1.02 o 11 4 2 19.30 34.29 14.19 o 12 4 2 1.65 1.57 1.78 o 13 4 2 31.16 36.60 9.53 o 14 4 2 3.37 3.71 2.26 o 2 0 3 550.97 523.69 13.98 o 4 0 3 2057.02 2099.20 54.86 o 6 0 3 150.00 144.19 8.38 o 8 0 3 1486.20 1501.79 50.93 o 10 0 3 957.82 864.62 28.68 o 12 0 3 2.49 2.44 2.31 o 14 0 3 60.34 53.29 2.56 o 16 0 3 11.50 6.58 6.15 o 18 0 3 74.74 65.96 8.94 o 20 0 3 18.54 13.41 17.36 o 22 0 3 59.40 53.73 7.69 o 24 0 3 12.50 9.24 24.90 o 26 0 3 24.60 20.43 39.16 o 0 1 3 132.09 143.70 8.42 o 1 1 3 379.44 374.29 10.98 o 2 1 3 93.65 105.97 4.15 o 3 1 3 81.98 89.40 4.84 o 4 1 3 57.20 62.82 2.17 o 5 1 3 401.49 407.08 16.75 o 6 1 3 422.72 449.95 18.14 o 7 1 3 455.54 453.67 17.34 o 8 1 3 163.92 156.10 7.40 o 9 1 3 76.15 75.44 4.07 o 10 1 3 25.06 28.47 1.54 o 11 1 3 195.45 192.90 12.64 o 12 1 3 19.29 20.11 1.25 o 13 1 3 547.28 545.45 36.25 o 14 1 3 1.09 2.77 3.26 o 15 1 3 33.45 30.68 8.50 o 16 1 3 64.63 58.20 5.03 o 17 1 3 108.45 94.45 26.43 o 18 1 3 56.36 49.45 11.37 o 19 1 3 62.68 63.18 15.11 o 20 1 3 12.70 16.48 9.44 o 21 1 3 5.20 6.98 5.83 o 22 1 3 8.01 5.13 16.09 o 23 1 3 7.35 4.68 19.92 o 24 1 3 3.12 0.51 6.62 o 25 1 3 15.89 17.97 10.94 o 1 2 3 6.51 6.95 1.18 o 2 2 3 89.42 93.35 5.42 o 3 2 3 6.15 7.81 0.67 o 4 2 3 129.75 125.07 9.86 o 5 2 3 48.38 55.11 2.53 o 6 2 3 30.09 31.24 2.83 o 7 2 3 15.00 16.87 2.26 o 8 2 3 143.63 142.30 10.99 o 9 2 3 203.60 203.72 15.60 o 10 2 3 87.32 91.64 7.50 o 11 2 3 133.19 134.71 15.19 o 12 2 3 2.49 3.59 1.23 o 13 2 3 12.40 13.86 3.65 o 14 2 3 97.72 100.71 22.84 o 15 2 3 111.23 120.51 34.46 o 16 2 3 158.30 167.94 49.31 o 17 2 3 23.20 31.30 13.29 o 18 2 3 18.21 25.82 21.10 o 19 2 3 2.22 2.57 11.39 o 20 2 3 48.61 44.60 22.08 o 21 2 3 4.97 8.86 8.22 o 22 2 3 49.41 52.17 23.61 o 23 2 3 2.39 3.27 5.36 o 0 3 3 86.81 101.92 14.81 o 1 3 3 269.78 297.88 13.86 o 2 3 3 7.52 11.82 1.30 o 3 3 3 17.93 20.61 1.54 o 4 3 3 26.31 27.57 3.13 o 5 3 3 81.27 82.24 6.31 o 6 3 3 73.55 72.41 6.64 o 7 3 3 6.88 9.73 1.38 o 8 3 3 13.57 13.90 1.09 o 9 3 3 0.67 1.13 0.37 o 10 3 3 16.07 18.27 2.47 o 11 3 3 1.65 1.54 1.12 o 12 3 3 56.86 57.16 7.38 o 13 3 3 8.59 13.10 9.13 o 14 3 3 36.85 40.04 11.84 o 15 3 3 6.60 7.58 6.19 o 16 3 3 1.19 -0.36 6.35 o 17 3 3 5.45 8.87 3.53 o 18 3 3 38.94 43.95 17.53 o 19 3 3 10.39 11.77 16.65 o 1 4 3 53.07 55.23 1.63 o 2 4 3 4.13 7.26 0.84 o 3 4 3 113.03 112.36 8.57 o 4 4 3 19.38 21.81 1.31 o 5 4 3 3.88 4.96 0.47 o 6 4 3 13.51 15.34 1.61 o 7 4 3 9.00 10.41 1.80 o 8 4 3 2.27 3.50 0.55 o 9 4 3 4.50 8.36 0.91 o 10 4 3 4.29 5.86 2.15 o 11 4 3 5.26 6.88 1.04 o 12 4 3 0.36 -0.39 1.02 o 0 0 4 86.30 62.55 12.01 o 2 0 4 170.81 147.17 4.68 o 4 0 4 243.49 231.00 6.44 o 6 0 4 313.93 299.94 8.25 o 8 0 4 109.25 103.92 11.38 o 10 0 4 15.05 12.82 2.95 o 12 0 4 607.08 598.06 15.87 o 14 0 4 96.02 93.94 17.25 o 16 0 4 150.97 146.35 12.23 o 18 0 4 115.43 112.90 14.67 o 20 0 4 56.20 63.63 28.27 o 22 0 4 11.33 9.34 24.93 o 24 0 4 18.65 16.84 24.36 o 1 1 4 65.40 62.47 1.81 o 2 1 4 57.99 64.50 1.95 o 3 1 4 477.26 475.04 22.24 o 4 1 4 22.73 24.05 2.57 o 5 1 4 350.11 342.33 16.69 o 6 1 4 4.58 4.60 1.07 o 7 1 4 76.23 82.26 5.04 o 8 1 4 29.64 29.06 2.07 o 9 1 4 376.13 342.01 15.79 o 10 1 4 90.54 87.31 7.03 o 11 1 4 116.30 108.17 7.02 o 12 1 4 19.48 19.77 3.89 o 13 1 4 42.00 40.25 3.87 o 14 1 4 133.58 127.93 12.37 o 15 1 4 46.47 47.02 6.14 o 16 1 4 15.43 18.43 6.57 o 17 1 4 51.15 51.28 14.70 o 18 1 4 0.37 1.23 5.95 o 19 1 4 2.57 4.22 6.34 o 20 1 4 16.72 16.35 4.70 o 21 1 4 38.85 40.02 21.61 o 22 1 4 23.18 24.20 14.06 o 23 1 4 24.01 23.78 13.11 o 0 2 4 769.83 770.54 37.96 o 1 2 4 139.52 154.53 6.15 o 2 2 4 68.90 70.51 2.29 o 3 2 4 23.56 25.79 2.85 o 4 2 4 120.41 120.22 6.47 o 5 2 4 98.02 94.17 5.70 o 6 2 4 107.69 102.69 5.75 o 7 2 4 91.03 89.41 5.96 o 8 2 4 57.64 57.14 2.14 o 9 2 4 13.00 13.93 1.69 o 10 2 4 26.67 25.46 2.76 o 11 2 4 60.94 60.58 4.60 o 12 2 4 45.86 48.84 3.39 o 13 2 4 21.00 21.12 3.99 o 14 2 4 84.75 86.42 21.32 o 15 2 4 4.74 7.48 7.85 o 16 2 4 1.05 0.31 3.43 o 17 2 4 0.32 0.39 10.35 o 18 2 4 42.07 41.18 25.04 o 19 2 4 8.09 13.42 21.10 o 20 2 4 11.28 13.07 21.76 o 21 2 4 7.37 8.64 2.15 o 1 3 4 15.34 18.96 2.12 o 2 3 4 138.76 161.30 9.60 o 3 3 4 64.19 60.94 7.97 o 4 3 4 65.55 66.28 4.07 o 5 3 4 14.42 15.79 1.77 o 6 3 4 12.66 12.58 1.85 o 7 3 4 6.35 8.63 2.31 o 8 3 4 13.00 13.80 2.03 o 9 3 4 38.48 38.68 5.12 o 10 3 4 32.54 33.91 3.90 o 11 3 4 6.53 4.79 1.35 o 12 3 4 15.31 16.46 1.46 o 13 3 4 0.43 1.69 0.69 o 14 3 4 5.67 10.48 34.12 o 15 3 4 15.91 16.89 27.87 o 16 3 4 22.19 28.26 56.00 o 17 3 4 14.37 16.95 12.20 o 0 4 4 4.55 -0.89 3.54 o 1 4 4 25.56 33.04 6.03 o 2 4 4 1.85 2.81 1.48 o 3 4 4 0.01 -0.52 1.10 o 4 4 4 2.62 3.11 2.23 o 5 4 4 18.54 20.65 4.53 o 6 4 4 2.94 4.99 1.67 o 7 4 4 17.41 22.50 3.03 o 8 4 4 2.18 3.01 0.94 o 9 4 4 0.43 1.69 2.81 o 2 0 5 189.99 190.14 9.92 o 4 0 5 750.40 753.63 36.39 o 6 0 5 13.15 12.65 1.42 o 8 0 5 52.11 47.71 3.70 o 10 0 5 290.35 263.82 7.47 o 12 0 5 23.41 22.96 4.80 o 14 0 5 115.41 117.76 4.07 o 16 0 5 44.67 44.48 12.74 o 18 0 5 26.35 33.10 10.91 o 20 0 5 32.16 38.14 21.45 o 22 0 5 55.26 57.15 51.41 o 0 1 5 175.70 182.50 15.39 o 1 1 5 346.51 323.95 27.16 o 2 1 5 110.48 109.55 4.86 o 3 1 5 4.27 4.71 1.86 o 4 1 5 24.53 23.05 3.80 o 5 1 5 249.89 217.75 11.18 o 6 1 5 28.05 28.33 1.55 o 7 1 5 46.53 44.95 2.15 o 8 1 5 15.87 13.91 1.01 o 9 1 5 33.47 34.88 2.09 o 10 1 5 36.14 32.57 2.54 o 11 1 5 36.89 40.79 3.89 o 12 1 5 50.65 50.99 7.30 o 13 1 5 113.08 119.41 14.68 o 14 1 5 1.66 1.43 3.83 o 15 1 5 1.54 2.11 2.66 o 16 1 5 4.91 6.40 4.51 o 17 1 5 33.96 33.36 13.62 o 18 1 5 11.30 15.37 8.32 o 19 1 5 37.56 42.56 7.81 o 20 1 5 11.09 14.51 10.16 o 21 1 5 2.80 4.93 13.00 o 1 2 5 10.58 13.31 2.43 o 2 2 5 101.82 94.49 7.61 o 3 2 5 148.72 126.80 13.86 o 4 2 5 118.61 93.94 7.92 o 5 2 5 17.08 19.01 1.81 o 6 2 5 9.78 9.94 1.02 o 7 2 5 4.11 3.33 0.60 o 8 2 5 110.28 105.11 7.44 o 9 2 5 6.14 7.66 1.47 o 10 2 5 56.47 57.08 4.61 o 11 2 5 13.27 13.06 1.39 o 12 2 5 12.03 11.77 0.94 o 13 2 5 7.57 12.16 2.05 o 14 2 5 9.99 14.40 17.35 o 15 2 5 19.14 23.24 6.18 o 16 2 5 15.88 20.83 8.09 o 17 2 5 2.53 4.76 16.29 o 18 2 5 10.12 11.18 2.47 o 19 2 5 1.22 0.57 4.33 o 0 3 5 44.50 51.53 12.77 o 1 3 5 9.48 10.75 3.55 o 2 3 5 20.54 24.36 3.66 o 3 3 5 4.83 3.17 0.83 o 4 3 5 6.33 7.47 2.00 o 5 3 5 6.75 5.94 2.09 o 6 3 5 39.42 31.30 3.98 o 7 3 5 16.71 17.09 1.92 o 8 3 5 14.06 16.56 2.01 o 9 3 5 3.80 3.28 1.89 o 10 3 5 15.63 15.41 1.66 o 11 3 5 8.25 8.85 1.48 o 12 3 5 15.21 17.84 1.93 o 13 3 5 35.53 34.77 3.01 o 14 3 5 2.02 3.45 1.43 o 0 0 6 438.83 448.94 29.94 o 2 0 6 247.81 269.27 13.70 o 4 0 6 212.02 216.09 11.41 o 6 0 6 125.09 134.24 8.01 o 8 0 6 19.87 28.37 3.92 o 10 0 6 30.13 36.31 10.41 o 12 0 6 55.70 69.13 6.87 o 14 0 6 20.48 23.47 2.97 o 16 0 6 1.22 1.11 15.12 o 18 0 6 17.84 21.27 10.22 o 1 1 6 0.14 -1.31 2.13 o 2 1 6 76.77 76.21 7.92 o 3 1 6 139.97 146.07 7.44 o 4 1 6 90.11 96.69 9.14 o 5 1 6 70.41 74.48 6.26 o 6 1 6 43.30 51.38 4.50 o 7 1 6 18.90 24.97 2.84 o 8 1 6 4.63 5.02 2.08 o 9 1 6 73.90 78.65 5.71 o 10 1 6 0.82 -1.90 1.90 o 11 1 6 38.61 39.02 3.67 o 12 1 6 5.70 5.61 9.67 o 13 1 6 15.73 15.75 9.68 o 14 1 6 1.14 0.67 4.24 o 15 1 6 25.90 27.88 7.82 o 16 1 6 1.39 1.22 8.10 o 17 1 6 26.11 30.13 19.46 o 18 1 6 2.67 5.03 16.06 o 0 2 6 24.94 37.07 5.06 o 1 2 6 9.97 7.25 3.27 o 2 2 6 1.89 1.59 2.13 o 3 2 6 12.09 9.45 3.92 o 4 2 6 9.11 7.85 2.30 o 5 2 6 22.58 21.72 2.87 o 6 2 6 24.21 26.76 3.55 o 7 2 6 5.22 4.00 2.14 o 8 2 6 33.60 36.23 5.09 o 9 2 6 4.18 3.03 2.32 o 10 2 6 6.56 2.34 1.97 o 11 2 6 7.76 2.87 2.06 o 12 2 6 58.04 48.40 3.94 o 13 2 6 19.86 17.40 1.20 o 14 2 6 18.63 22.24 38.27 o 15 2 6 0.97 2.21 23.64 o 1 3 6 4.89 2.57 2.80 o 2 3 6 8.81 9.20 2.74 o 3 3 6 16.57 11.85 7.15 o 4 3 6 11.40 11.50 4.42 o 5 3 6 11.64 6.76 5.68 o 6 3 6 1.53 -0.13 2.26 o 7 3 6 5.28 2.83 2.62 o 8 3 6 10.57 7.73 3.91 o 9 3 6 27.04 29.21 3.25 o 2 0 7 28.64 32.00 4.59 o 4 0 7 86.25 89.63 6.66 o 6 0 7 18.30 11.77 3.78 o 8 0 7 25.81 20.75 3.84 o 10 0 7 48.67 62.20 6.37 o 12 0 7 1.81 34.63 46.90 o 14 0 7 27.68 19.31 8.79 o 0 1 7 13.26 13.51 3.78 o 1 1 7 67.76 71.73 4.94 o 2 1 7 3.16 0.34 2.22 o 3 1 7 1.31 1.56 2.15 o 4 1 7 12.38 9.36 2.60 o 5 1 7 73.67 82.51 9.33 o 6 1 7 1.20 -0.29 2.23 o 7 1 7 10.04 9.69 2.56 o 8 1 7 9.33 7.01 2.39 o 9 1 7 8.10 3.87 2.20 o 10 1 7 0.59 -1.07 2.37 o 11 1 7 10.15 1.77 2.52 o 12 1 7 16.15 22.69 23.34 o 13 1 7 40.77 147.88 68.67 o 1 2 7 4.93 4.38 2.48 o 2 2 7 12.21 11.09 4.31 o 3 2 7 36.62 39.29 5.24 o 4 2 7 44.46 51.74 7.73 o 5 2 7 0.30 0.09 2.34 o 6 2 7 15.33 9.86 6.05 o 7 2 7 7.75 6.70 2.65 o 8 2 7 26.70 23.49 3.10 o 9 2 7 2.90 0.24 2.25 o 0 0 8 25.06 22.18 6.06 o 2 0 8 13.05 14.61 4.12 o 4 0 8 18.66 23.31 4.56 o 6 0 8 20.17 21.51 4.35 o 1 1 8 2.34 -3.36 3.78 o 2 1 8 1.59 -2.01 2.54 o 3 1 8 32.11 35.08 4.56 o 4 1 8 5.33 8.05 3.73 o