#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206562.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206562_Fobs loop_ _publ_author_name 'Klausmeyer, Kevin K.' 'Yaklin, Marsha M.' 'Adrian, Rafael A.' _publ_section_title ; Pentakis(tetraethylammonium) diaqua-\m~4~-malonato-tetramalonatodi-\m~3~-oxo-di-\m-oxo-tetraoxopotassiumtetramolybdenum acetonitrile disolvate ; _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1607 _journal_page_last m1609 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.592 _cell_angle_gamma 90.000 _cell_length_a 10.6052 _cell_length_b 24.2012 _cell_length_c 30.7783 _exptl_crystal_F_000 3800.00 _reflns_d_resolution_high 0.7985 _[local]_cod_data_source_file su6217Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kk63 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 823.02 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 209512.23 216107.19 5567.91 o 4 0 0 14614.24 13266.65 454.44 o 5 0 0 20765.26 22752.83 774.33 o 6 0 0 4971.56 4728.18 190.35 o 7 0 0 150856.89 153612.89 3994.22 o 8 0 0 38016.09 38002.89 1154.62 o 9 0 0 17708.05 16951.57 586.24 o 10 0 0 48352.29 49377.07 1643.01 o 11 0 0 14389.51 14474.88 695.63 o 12 0 0 2909.65 3395.07 370.53 o 13 0 0 4215.34 3348.00 520.37 o 2 1 0 262683.63 273977.09 4983.69 o 3 1 0 329.13 190.09 27.74 o 4 1 0 38251.63 41919.05 893.14 o 5 1 0 534.36 285.65 34.82 o 6 1 0 24286.79 25061.51 518.32 o 7 1 0 1.33 -26.25 47.64 o 8 1 0 32670.99 32605.16 701.90 o 9 1 0 29479.15 29466.22 698.83 o 10 1 0 6.83 26.71 91.61 o 11 1 0 505.90 298.43 149.54 o 12 1 0 6233.36 6329.94 379.41 o 13 1 0 3929.29 4508.23 414.72 o 1 2 0 3153.17 1472.57 206.64 o 2 2 0 25443.97 27017.98 440.08 o 3 2 0 57894.00 58483.08 1027.52 o 4 2 0 72472.88 73035.60 1371.77 o 5 2 0 10893.16 11855.75 240.52 o 6 2 0 2515.00 2645.31 68.54 o 7 2 0 4168.97 4280.63 142.45 o 8 2 0 402.82 217.24 69.19 o 9 2 0 1233.34 1120.36 78.98 o 10 2 0 23377.04 23685.75 645.46 o 11 2 0 7384.77 7507.28 272.09 o 12 2 0 2.44 -61.79 217.64 o 13 2 0 482.19 140.23 293.64 o 1 3 0 116729.98 124024.37 2450.93 o 2 3 0 635987.56 644007.94 10283.38 o 3 3 0 31684.22 34193.45 586.63 o 4 3 0 1711.61 2436.12 53.50 o 5 3 0 115001.42 113866.27 2065.48 o 6 3 0 50531.21 49276.91 966.42 o 7 3 0 435.04 486.12 53.13 o 8 3 0 68306.47 67893.70 1677.51 o 9 3 0 62098.37 62898.31 1470.23 o 10 3 0 115.84 -66.30 97.85 o 11 3 0 11998.02 11997.60 416.85 o 12 3 0 21478.66 21274.49 971.97 o 13 3 0 14292.17 15453.18 866.65 o 0 4 0 530055.31 558887.50 16232.65 o 1 4 0 79114.10 82076.20 1299.75 o 2 4 0 1220.49 1592.89 64.44 o 3 4 0 84259.90 82571.35 1442.16 o 4 4 0 99058.13 94810.23 1663.81 o 5 4 0 21864.31 21833.74 389.53 o 6 4 0 6292.43 6153.16 128.51 o 7 4 0 66405.88 65764.12 1334.83 o 8 4 0 7896.93 8395.72 222.39 o 9 4 0 1071.83 1281.09 177.75 o 10 4 0 21555.94 21095.63 583.92 o 11 4 0 11775.23 12170.10 695.62 o 12 4 0 599.64 690.90 228.99 o 13 4 0 59.84 37.27 273.63 o 1 5 0 231.50 326.15 22.54 o 2 5 0 12510.29 12453.92 215.27 o 3 5 0 172.35 212.22 21.11 o 4 5 0 1.47 30.61 28.51 o 5 5 0 1149.13 1077.47 45.53 o 6 5 0 2074.11 2080.36 61.83 o 7 5 0 70.60 77.40 48.68 o 8 5 0 10527.44 10576.59 255.93 o 9 5 0 855.66 864.50 130.73 o 10 5 0 946.51 713.95 109.71 o 11 5 0 30.66 39.80 160.04 o 12 5 0 2.54 -111.32 255.73 o 0 6 0 677356.63 708994.56 16672.02 o 1 6 0 9499.13 8238.45 144.86 o 2 6 0 76565.15 81987.10 1403.52 o 3 6 0 69094.53 68149.13 1245.26 o 4 6 0 117289.45 119922.59 2155.73 o 5 6 0 5484.01 5936.67 126.88 o 6 6 0 66106.07 66866.37 1297.37 o 7 6 0 84143.41 84170.79 1699.69 o 8 6 0 11133.39 11199.08 336.08 o 9 6 0 4790.49 5149.42 226.31 o 10 6 0 23842.65 23487.69 800.10 o 11 6 0 12702.18 13733.67 767.45 o 12 6 0 2309.91 2316.57 343.55 o 1 7 0 102776.95 100118.34 1825.45 o 2 7 0 129213.05 122563.31 2104.51 o 3 7 0 13996.85 14850.43 262.38 o 4 7 0 35962.08 37915.23 728.40 o 5 7 0 89463.47 91470.49 1822.76 o 6 7 0 35112.10 33377.13 632.02 o 7 7 0 751.19 928.89 87.43 o 8 7 0 26542.96 26036.39 622.37 o 9 7 0 29571.51 30065.55 1010.41 o 10 7 0 2359.11 2647.63 162.47 o 11 7 0 721.25 673.43 196.49 o 12 7 0 12883.64 13032.15 797.11 o 0 8 0 1998.26 2174.57 81.88 o 1 8 0 39660.02 41632.74 763.71 o 2 8 0 42741.92 42065.80 724.74 o 3 8 0 1879.56 1637.68 66.10 o 4 8 0 445.64 402.93 31.20 o 5 8 0 4767.80 4653.04 122.78 o 6 8 0 230.66 308.62 54.61 o 7 8 0 288.97 321.67 62.87 o 8 8 0 357.58 348.31 86.11 o 9 8 0 2634.47 2738.66 133.90 o 10 8 0 44.20 -21.21 118.86 o 11 8 0 3866.25 4280.62 464.42 o 12 8 0 805.07 729.15 424.39 o 1 9 0 68552.87 73390.59 1384.36 o 2 9 0 14300.76 14010.24 243.36 o 3 9 0 36396.69 40275.22 697.07 o 4 9 0 27523.02 27848.27 499.51 o 5 9 0 39652.71 37784.39 704.23 o 6 9 0 47187.51 47303.42 917.78 o 7 9 0 99.57 -68.55 68.55 o 8 9 0 30473.18 31127.71 720.92 o 9 9 0 20390.06 19904.59 624.87 o 10 9 0 5.95 -98.52 109.19 o 11 9 0 2674.85 3099.53 254.68 o 12 9 0 6145.98 6518.02 411.60 o 0 10 0 7659.19 6194.98 200.37 o 1 10 0 13.08 136.62 40.87 o 2 10 0 47606.55 49132.54 936.12 o 3 10 0 158207.36 158346.30 2990.03 o 4 10 0 70782.82 71101.06 1346.83 o 5 10 0 13337.46 13279.38 260.08 o 6 10 0 10938.70 11536.00 271.00 o 7 10 0 42542.91 42653.68 1039.92 o 8 10 0 5381.05 5502.19 177.13 o 9 10 0 1229.14 1108.99 152.48 o 10 10 0 14522.79 15237.63 699.55 o 11 10 0 12314.33 13812.47 577.18 o 12 10 0 15.67 74.55 303.33 o 1 11 0 34.25 202.55 44.37 o 2 11 0 34240.37 34667.93 665.03 o 3 11 0 5771.68 6021.94 135.86 o 4 11 0 3523.17 3769.30 147.48 o 5 11 0 1029.77 1008.41 62.37 o 6 11 0 424.14 485.90 68.83 o 7 11 0 107.00 113.03 74.35 o 8 11 0 113.92 149.65 86.25 o 9 11 0 512.70 259.84 132.69 o 10 11 0 2040.30 2143.26 285.42 o 11 11 0 544.31 528.02 154.85 o 12 11 0 1868.32 2094.04 644.59 o 0 12 0 121427.45 125061.08 3595.02 o 1 12 0 1275.78 1296.04 79.69 o 2 12 0 22629.74 22368.79 490.92 o 3 12 0 410.37 545.56 53.32 o 4 12 0 2021.45 1917.31 119.63 o 5 12 0 304.38 295.33 50.16 o 6 12 0 7735.35 7779.44 206.70 o 7 12 0 32732.61 33826.61 835.79 o 8 12 0 7016.02 6934.02 220.94 o 9 12 0 1718.60 1881.98 205.09 o 10 12 0 1412.06 1751.72 225.19 o 11 12 0 32.94 -244.28 244.28 o 12 12 0 1250.60 1240.10 463.93 o 1 13 0 35858.45 36878.42 758.58 o 2 13 0 45669.03 44218.84 910.29 o 3 13 0 8436.88 9270.52 202.23 o 4 13 0 18679.39 18038.44 377.08 o 5 13 0 20355.55 20523.49 438.31 o 6 13 0 9666.49 9306.66 253.63 o 7 13 0 385.00 481.68 105.76 o 8 13 0 11021.13 11086.01 375.97 o 9 13 0 5608.77 5762.50 357.46 o 10 13 0 99.03 162.83 206.26 o 11 13 0 3694.14 4335.17 369.25 o 0 14 0 5578.34 6052.23 229.87 o 1 14 0 4231.74 4124.22 145.91 o 2 14 0 762.59 825.92 80.77 o 3 14 0 6185.66 6201.53 152.90 o 4 14 0 7956.52 8725.53 195.04 o 5 14 0 9.39 92.35 63.66 o 6 14 0 451.38 441.92 97.15 o 7 14 0 67.29 10.39 109.47 o 8 14 0 1.32 100.70 125.12 o 9 14 0 1042.17 737.85 342.42 o 10 14 0 101.31 -90.46 213.20 o 11 14 0 983.87 751.00 264.10 o 1 15 0 118.79 225.33 62.32 o 2 15 0 357.34 364.36 65.42 o 3 15 0 107.38 94.29 63.72 o 4 15 0 1232.27 1202.34 77.22 o 5 15 0 5015.79 4895.56 136.38 o 6 15 0 1110.93 1382.47 110.02 o 7 15 0 2316.65 2425.31 146.96 o 8 15 0 3044.97 2915.59 179.71 o 9 15 0 2091.24 2073.21 244.83 o 10 15 0 581.05 863.87 238.77 o 11 15 0 4168.47 4892.98 378.17 o 0 16 0 5290.28 5850.70 212.25 o 1 16 0 938.41 1145.22 88.25 o 2 16 0 696.25 624.61 72.16 o 3 16 0 6838.54 6739.95 170.11 o 4 16 0 2176.27 2378.71 102.19 o 5 16 0 1332.93 1407.43 94.47 o 6 16 0 9967.35 10819.91 332.38 o 7 16 0 12129.58 12310.58 478.32 o 8 16 0 145.50 314.82 146.58 o 9 16 0 1005.33 1321.41 268.46 o 10 16 0 3648.23 4621.60 429.89 o 11 16 0 95.92 311.28 279.79 o 1 17 0 192.60 209.63 73.87 o 2 17 0 2072.20 2399.56 116.31 o 3 17 0 864.10 965.28 88.06 o 4 17 0 403.41 186.12 82.80 o 5 17 0 5.49 -66.20 82.79 o 6 17 0 373.80 447.62 82.62 o 7 17 0 325.45 304.19 126.47 o 8 17 0 42.37 108.57 156.65 o 9 17 0 223.06 233.03 238.57 o 10 17 0 7.61 -163.85 261.79 o 0 18 0 24.97 226.26 110.15 o 1 18 0 20.61 -10.23 77.42 o 2 18 0 354.37 266.92 83.77 o 3 18 0 576.35 626.16 89.91 o 4 18 0 1449.28 1616.78 106.41 o 5 18 0 1104.47 1156.10 101.53 o 6 18 0 526.46 343.46 89.78 o 7 18 0 620.30 576.37 135.41 o 8 18 0 1409.73 1220.60 178.22 o 9 18 0 3718.28 4272.40 652.63 o 10 18 0 1204.27 1170.47 297.20 o 1 19 0 582.42 667.92 93.68 o 2 19 0 8.69 270.33 93.09 o 3 19 0 97.80 207.53 98.26 o 4 19 0 3255.17 3240.17 141.24 o 5 19 0 5981.10 5849.73 215.74 o 6 19 0 158.24 53.87 95.85 o 7 19 0 1924.79 2414.93 166.97 o 8 19 0 1.40 99.70 176.56 o 9 19 0 1192.69 896.22 283.89 o 10 19 0 2486.31 2816.97 353.05 o 0 20 0 9321.02 9365.15 327.86 o 1 20 0 2078.83 2477.13 188.89 o 2 20 0 525.42 377.27 99.95 o 3 20 0 0.29 3.03 102.11 o 4 20 0 545.96 508.81 108.76 o 5 20 0 1135.62 892.40 121.48 o 6 20 0 42.01 152.12 106.87 o 7 20 0 2017.32 2480.60 180.15 o 8 20 0 1054.02 1250.06 206.04 o 9 20 0 1164.05 1341.87 294.75 o 1 21 0 120.86 114.62 100.64 o 2 21 0 1873.91 1961.60 119.10 o 3 21 0 616.05 578.09 115.24 o 4 21 0 210.78 226.28 118.83 o 5 21 0 319.96 386.76 127.38 o 6 21 0 16.91 -92.77 123.19 o 7 21 0 3216.91 3825.90 228.44 o 8 21 0 7482.40 7335.64 356.85 o 9 21 0 2618.39 2511.48 343.22 o 0 22 0 2088.99 2008.75 185.53 o 1 22 0 31.41 -6.22 107.43 o 2 22 0 8.63 192.22 116.68 o 3 22 0 14.63 -115.22 115.22 o 4 22 0 46.00 37.61 126.09 o 5 22 0 1262.49 1137.17 172.08 o 6 22 0 940.10 933.07 142.17 o 7 22 0 76.22 16.29 178.59 o 8 22 0 813.74 1180.13 306.72 o 9 22 0 2051.37 3193.23 749.15 o 1 23 0 5644.12 5602.57 197.01 o 2 23 0 10196.91 10197.60 365.50 o 3 23 0 1876.90 1816.78 189.85 o 4 23 0 59.99 127.53 129.81 o 5 23 0 5516.86 5711.42 243.66 o 6 23 0 8497.61 8774.03 303.01 o 7 23 0 1585.10 1481.70 201.94 o 8 23 0 406.83 517.26 272.80 o 0 24 0 1689.90 2546.59 221.33 o 1 24 0 1442.26 1365.01 147.71 o 2 24 0 1179.05 1294.40 150.16 o 3 24 0 9033.05 8749.84 308.27 o 4 24 0 3417.37 3696.02 207.28 o 5 24 0 1589.26 1654.81 171.70 o 6 24 0 1085.25 830.48 163.27 o 7 24 0 4499.84 4409.63 343.12 o 1 25 0 395.05 373.65 149.04 o 2 25 0 2386.45 2396.56 228.63 o 3 25 0 6.11 82.07 150.99 o 4 25 0 367.89 457.43 158.25 o 5 25 0 165.32 158.32 164.56 o 6 25 0 79.62 141.81 168.99 o 7 25 0 1531.54 1569.07 239.44 o 0 26 0 23745.04 23839.58 933.28 o 1 26 0 3451.36 3815.27 267.86 o 2 26 0 17.85 66.63 159.30 o 3 26 0 2788.58 2470.73 199.55 o 4 26 0 6369.32 6712.34 264.21 o 5 26 0 434.81 609.22 178.47 o 6 26 0 1451.85 1117.94 191.12 o 1 27 0 10056.06 9863.12 320.47 o 2 27 0 10113.28 9460.57 415.67 o 3 27 0 1824.26 2421.95 205.58 o 4 27 0 1123.91 1280.61 193.34 o 5 27 0 9034.92 9233.72 319.79 o 0 28 0 754.35 514.03 275.85 o 1 28 0 2126.94 2022.40 211.22 o 2 28 0 206.45 332.20 194.62 o 3 28 0 6.15 -96.66 184.65 o 4 28 0 92.15 346.22 209.77 o 5 28 0 1337.45 1715.76 1054.94 o 1 29 0 5190.79 5201.42 327.23 o 2 29 0 9505.93 9504.88 450.51 o 3 29 0 63.79 338.31 223.12 o 0 30 0 11869.40 12673.67 760.54 o 1 30 0 4453.96 3951.33 369.52 o -13 1 1 405.16 437.24 297.47 o -12 1 1 1244.85 1049.05 209.66 o -11 1 1 8710.88 8962.22 337.21 o -10 1 1 7203.83 7288.22 213.62 o -9 1 1 141.15 -16.87 62.62 o -8 1 1 878.79 748.73 67.83 o -7 1 1 8943.19 8374.83 195.78 o -6 1 1 5.06 -23.77 45.32 o -5 1 1 1002.12 1180.93 76.13 o -4 1 1 1567.58 1900.51 79.55 o -3 1 1 6588.50 7509.91 152.94 o -2 1 1 178.46 175.91 12.81 o -1 1 1 1777.21 570.98 214.20 o 1 1 1 95.63 -18.07 18.07 o 2 1 1 383.09 362.21 15.88 o 3 1 1 5418.24 5858.71 99.67 o 4 1 1 2094.46 2092.49 46.88 o 5 1 1 3286.28 3024.70 96.37 o 6 1 1 473.62 308.28 37.43 o 7 1 1 705.35 521.57 52.90 o 8 1 1 2022.30 2087.54 103.19 o 9 1 1 2272.11 2202.01 98.65 o 10 1 1 1691.22 1628.08 166.48 o 11 1 1 2059.38 1789.99 201.60 o 12 1 1 1596.85 2040.31 366.38 o 13 1 1 1350.42 1518.19 340.98 o -13 2 1 5372.98 5518.98 404.66 o -12 2 1 1798.79 1986.95 229.32 o -11 2 1 889.36 568.70 180.40 o -10 2 1 349.19 197.22 92.94 o -9 2 1 20410.83 20787.70 568.86 o -8 2 1 12208.44 12375.96 308.94 o -7 2 1 93.58 98.07 47.18 o -6 2 1 5140.86 5397.72 124.16 o -5 2 1 863.93 1094.56 46.75 o -4 2 1 3168.57 3578.51 75.86 o -3 2 1 25074.06 25968.17 444.68 o -2 2 1 2542.47 2105.21 40.45 o -1 2 1 7.68 -7.88 7.88 o 0 2 1 501.85 213.21 44.22 o 1 2 1 83.17 -10.65 10.65 o 2 2 1 3519.97 3137.08 53.67 o 3 2 1 4322.91 4332.13 78.21 o 4 2 1 825.80 747.79 49.04 o 5 2 1 2438.98 2253.35 72.18 o 6 2 1 5290.46 5366.38 142.29 o 7 2 1 1603.25 1613.55 73.09 o 8 2 1 566.39 478.14 87.77 o 9 2 1 7144.23 7128.26 196.50 o 10 2 1 8335.04 8697.53 251.78 o 11 2 1 811.30 619.07 246.20 o 12 2 1 220.74 12.79 236.12 o 13 2 1 506.66 1057.72 367.85 o -13 3 1 303.35 587.71 264.67 o -12 3 1 77.10 -14.74 267.52 o -11 3 1 10.77 48.38 130.86 o -10 3 1 1.48 -5.36 87.42 o -9 3 1 4432.52 4714.02 185.15 o -8 3 1 2799.31 3066.37 134.56 o -7 3 1 177.53 171.18 47.61 o -6 3 1 4540.29 4828.53 108.48 o -5 3 1 20299.67 19182.67 355.24 o 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