#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206567.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206567_Fobs loop_ _publ_author_name 'Bellabarba, Ronan M.' 'Nieuwenhuyzen, Mark' 'Saunders, Graham C.' _publ_section_title ; (Acetonitrile-\kN){1,2-bis[bis(pentafluorophenyl)phosphino]ethane-\k^2^P,P}(\h^5^-pentamethylcyclopentadienyl)ruthenium(II) hexafluorophosphate ; _journal_coeditor_code WK6052 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1588 _journal_page_last m1589 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.062 _cell_angle_gamma 90.000 _cell_length_a 12.5380 _cell_length_b 10.6157 _cell_length_c 31.7596 _exptl_crystal_F_000 2320.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file wk6052Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gcs16m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 368.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 484.02 1016.47 69.35 o 4 0 0 34730.79 36536.43 397.32 o 6 0 0 16835.08 17043.46 327.56 o 8 0 0 26866.54 25550.28 459.61 o 10 0 0 2458.14 2802.04 315.30 o 12 0 0 3011.33 3286.87 450.76 o 14 0 0 980.99 842.59 335.86 o 16 0 0 1013.72 1213.81 430.14 o 1 1 0 10337.22 10801.53 124.43 o 2 1 0 28383.15 29437.02 234.00 o 3 1 0 10902.50 12543.01 208.37 o 4 1 0 508.25 544.48 55.91 o 5 1 0 361.49 445.22 56.06 o 6 1 0 16425.87 13406.19 1637.77 o 7 1 0 1781.70 1557.52 363.94 o 8 1 0 1510.19 1629.78 113.15 o 9 1 0 122.25 86.98 78.41 o 10 1 0 6431.94 6522.57 235.80 o 11 1 0 3.14 -53.03 88.91 o 12 1 0 1938.43 2185.21 249.18 o 13 1 0 760.94 854.73 189.83 o 14 1 0 2.31 27.23 129.95 o 15 1 0 10.80 -46.40 166.50 o 16 1 0 33.91 -220.00 238.64 o 0 2 0 3892.94 3580.62 95.77 o 1 2 0 15885.06 16737.53 161.32 o 2 2 0 471.51 533.13 50.35 o 3 2 0 19320.11 20165.70 260.20 o 4 2 0 612.74 845.90 76.93 o 5 2 0 23883.16 23465.50 275.74 o 6 2 0 4342.86 3956.43 114.62 o 7 2 0 3277.21 3258.05 117.83 o 8 2 0 786.16 665.44 104.11 o 9 2 0 730.53 709.90 109.86 o 10 2 0 324.07 311.42 101.61 o 11 2 0 1192.72 628.44 364.59 o 12 2 0 2101.77 2013.96 251.56 o 13 2 0 338.91 504.38 171.07 o 14 2 0 33.60 -161.30 123.39 o 15 2 0 1038.91 1169.31 238.78 o 1 3 0 1377.45 1535.47 63.56 o 2 3 0 34871.14 36112.79 264.08 o 3 3 0 13571.01 12412.45 215.40 o 4 3 0 554.12 610.78 72.09 o 5 3 0 4292.34 3975.51 135.13 o 6 3 0 5205.61 4907.52 157.67 o 7 3 0 151.82 161.28 70.13 o 8 3 0 21.13 60.96 72.32 o 9 3 0 2312.44 2412.01 202.54 o 10 3 0 1536.02 1431.65 181.27 o 11 3 0 1935.10 1712.44 193.06 o 12 3 0 51.22 105.03 117.37 o 13 3 0 557.72 317.48 153.52 o 14 3 0 1670.31 1569.39 261.81 o 15 3 0 114.93 50.08 198.82 o 0 4 0 9379.11 9382.79 187.32 o 1 4 0 3588.40 3069.76 321.26 o 2 4 0 724.56 730.64 52.26 o 3 4 0 6429.74 6550.01 162.85 o 4 4 0 17269.71 16946.46 225.49 o 5 4 0 1681.58 1890.27 122.44 o 6 4 0 1044.34 1382.53 110.50 o 7 4 0 24.58 78.43 91.02 o 8 4 0 7134.81 6860.42 276.93 o 9 4 0 3274.14 3566.21 236.14 o 10 4 0 2850.76 3306.55 253.45 o 11 4 0 1649.59 1708.39 197.86 o 12 4 0 2560.15 2867.59 278.11 o 13 4 0 700.68 705.52 187.96 o 14 4 0 227.65 19.34 152.54 o 15 4 0 8.26 -174.31 164.97 o 1 5 0 866.40 894.27 167.71 o 2 5 0 18431.83 16544.51 179.29 o 3 5 0 442.42 476.01 82.62 o 4 5 0 117.50 3.58 52.62 o 5 5 0 1304.69 1554.95 179.27 o 6 5 0 11141.39 10691.37 317.79 o 7 5 0 900.98 813.03 146.52 o 8 5 0 9.39 3.64 108.53 o 9 5 0 1.16 30.10 108.58 o 10 5 0 7010.50 6693.67 308.03 o 11 5 0 238.26 199.60 121.12 o 12 5 0 47.07 -0.43 115.47 o 13 5 0 51.50 -95.43 120.62 o 14 5 0 1474.66 1509.85 213.11 o 15 5 0 91.38 -164.98 271.04 o 0 6 0 210.27 446.24 103.59 o 1 6 0 1479.26 1708.20 95.78 o 2 6 0 22.33 32.63 53.78 o 3 6 0 1024.88 1080.40 82.96 o 4 6 0 3809.91 3947.85 213.50 o 5 6 0 496.92 584.42 134.70 o 6 6 0 570.12 611.51 151.99 o 7 6 0 551.63 645.61 153.55 o 8 6 0 297.91 149.45 114.22 o 9 6 0 5470.60 5390.95 283.35 o 10 6 0 2.66 -10.21 110.34 o 11 6 0 836.90 915.82 193.91 o 12 6 0 335.50 352.19 147.00 o 13 6 0 19.29 -95.95 132.48 o 14 6 0 101.93 170.77 143.21 o 1 7 0 1341.46 1614.33 118.45 o 2 7 0 2761.23 2809.80 158.18 o 3 7 0 68.82 86.02 81.12 o 4 7 0 4274.31 4488.79 242.77 o 5 7 0 14.93 -111.93 109.66 o 6 7 0 82.58 -17.68 115.29 o 7 7 0 6421.40 6205.92 296.12 o 8 7 0 374.64 268.97 133.67 o 9 7 0 3520.75 4300.47 287.88 o 10 7 0 821.95 762.25 172.88 o 11 7 0 366.02 347.19 143.70 o 12 7 0 861.46 748.04 170.19 o 13 7 0 1480.94 1421.34 229.38 o 0 8 0 788.28 811.25 147.25 o 1 8 0 1385.15 1588.64 153.39 o 2 8 0 2152.76 1422.93 386.25 o 3 8 0 72.12 56.57 112.54 o 4 8 0 91.54 169.68 122.22 o 5 8 0 830.01 666.15 176.05 o 6 8 0 390.95 305.17 138.54 o 7 8 0 4.60 -22.13 107.07 o 8 8 0 4944.19 4959.96 292.37 o 9 8 0 1531.69 1374.79 201.70 o 10 8 0 122.70 26.65 127.03 o 11 8 0 719.36 762.48 180.09 o 12 8 0 230.26 88.61 147.91 o 1 9 0 151.42 90.00 113.29 o 2 9 0 4234.05 4406.77 350.40 o 3 9 0 606.06 534.27 163.29 o 4 9 0 1.52 -60.80 109.96 o 5 9 0 488.59 338.59 133.69 o 6 9 0 7447.69 7357.96 329.31 o 7 9 0 603.38 900.12 182.85 o 8 9 0 629.71 483.93 159.55 o 9 9 0 98.25 46.43 128.51 o 10 9 0 1288.81 1524.36 286.11 o 11 9 0 3.35 -143.24 135.46 o 0 10 0 111.81 21.18 155.86 o 1 10 0 327.34 309.15 167.96 o 2 10 0 612.80 501.09 182.01 o 3 10 0 1790.07 1949.90 284.19 o 4 10 0 5011.01 4792.94 289.41 o 5 10 0 951.75 742.77 179.45 o 6 10 0 22.56 -10.30 130.98 o 7 10 0 722.05 527.96 164.95 o 8 10 0 304.57 192.08 140.66 o 9 10 0 100.60 -67.87 125.16 o 10 10 0 128.94 220.73 144.86 o 1 11 0 170.64 297.67 177.95 o 2 11 0 46.42 -116.72 140.38 o 3 11 0 1090.53 1029.46 225.25 o 4 11 0 29.35 -29.24 154.26 o 5 11 0 2435.79 2592.55 258.10 o 6 11 0 241.78 133.07 146.83 o 7 11 0 2.50 -15.40 131.48 o 8 11 0 5.91 38.60 135.39 o 9 11 0 179.49 241.35 168.71 o 0 12 0 1779.32 1791.25 506.73 o 1 12 0 129.72 -114.96 193.71 o 2 12 0 5.40 -81.92 142.15 o 3 12 0 441.60 390.94 189.46 o 4 12 0 965.88 937.74 334.50 o 5 12 0 1104.26 1154.86 247.72 o 6 12 0 948.02 891.94 233.75 o 7 12 0 935.56 1172.93 216.83 o 1 13 0 6.42 -40.93 230.99 o 2 13 0 3397.55 3703.69 499.14 o 3 13 0 1.13 -115.09 171.30 o 4 13 0 100.90 -43.21 183.30 o 5 13 0 112.11 117.85 324.07 o -15 0 1 163.91 -64.81 276.94 o -13 0 1 3197.96 3180.51 360.38 o -11 0 1 3825.83 3658.18 307.56 o -9 0 1 9576.39 9479.94 310.31 o -7 0 1 9534.51 9265.10 267.05 o -5 0 1 2470.12 2469.12 139.54 o -3 0 1 38070.73 37757.19 686.18 o -1 0 1 1585.07 1026.31 521.95 o 1 0 1 15443.18 17267.57 147.90 o 3 0 1 2410.30 2334.74 127.32 o 5 0 1 2973.25 3160.96 148.57 o 7 0 1 1037.94 1125.46 127.75 o 9 0 1 2224.33 2312.58 193.68 o 11 0 1 1548.56 1414.14 245.72 o 13 0 1 112.59 178.63 162.65 o 15 0 1 82.51 11.78 259.26 o -16 1 1 650.33 1044.33 296.14 o -15 1 1 470.17 482.85 228.97 o -14 1 1 108.54 68.00 136.19 o -13 1 1 113.88 0.39 127.74 o -12 1 1 496.47 634.74 203.77 o -11 1 1 1772.01 1706.58 181.27 o -10 1 1 0.87 34.55 86.29 o -9 1 1 16168.60 14928.68 266.59 o -8 1 1 4922.77 4905.60 235.80 o -7 1 1 10972.80 9211.46 1468.96 o -6 1 1 3049.22 3055.58 111.89 o -5 1 1 101.34 37.55 43.67 o -4 1 1 9899.02 9960.88 147.56 o -3 1 1 6141.31 6573.28 116.66 o -2 1 1 784.13 909.97 49.57 o -1 1 1 86471.78 91064.48 1000.55 o 0 1 1 2843.95 2693.13 47.25 o 1 1 1 22550.20 24207.84 185.91 o 2 1 1 49122.02 54139.40 324.20 o 3 1 1 8356.02 9508.55 145.96 o 4 1 1 3211.81 3294.52 97.19 o 5 1 1 1733.91 1556.40 99.82 o 6 1 1 429.87 228.53 47.29 o 7 1 1 3.95 4.69 42.78 o 8 1 1 377.14 417.73 73.44 o 9 1 1 566.22 411.71 103.25 o 10 1 1 1576.04 1759.34 155.93 o 11 1 1 735.55 539.38 128.97 o 12 1 1 5.92 -127.29 112.16 o 13 1 1 703.92 533.54 169.63 o 14 1 1 642.41 649.99 185.95 o 15 1 1 870.93 913.25 259.18 o -16 2 1 0.41 40.19 216.61 o -15 2 1 112.73 172.59 171.87 o -14 2 1 1589.16 1575.89 237.47 o -13 2 1 413.12 153.26 147.84 o -12 2 1 7.75 23.21 119.60 o -11 2 1 11.19 -0.40 85.62 o -10 2 1 4827.73 4451.04 207.18 o -9 2 1 1022.95 1013.31 122.89 o -8 2 1 707.86 609.29 97.97 o -7 2 1 4617.75 4285.19 130.43 o -6 2 1 855.25 586.23 72.03 o -5 2 1 1168.53 1227.06 75.53 o -4 2 1 5442.22 5113.90 108.13 o -3 2 1 13509.58 13388.49 154.43 o -2 2 1 24713.84 24639.53 192.33 o -1 2 1 24828.42 25995.16 192.80 o 0 2 1 19767.84 19113.91 1100.11 o 1 2 1 346.95 508.89 40.44 o 2 2 1 8434.68 9469.63 238.98 o 3 2 1 37566.90 39780.35 373.50 o 4 2 1 672.40 750.36 67.26 o 5 2 1 1112.95 1291.47 97.62 o 6 2 1 553.10 451.04 57.57 o 7 2 1 3353.20 3012.69 115.35 o 8 2 1 476.03 427.02 90.34 o 9 2 1 4511.24 4278.95 188.50 o 10 2 1 745.04 659.47 189.66 o 11 2 1 25.37 4.60 77.69 o 12 2 1 1568.31 1627.05 225.34 o 13 2 1 512.74 232.37 163.27 o 14 2 1 1257.59 1322.90 227.88 o 15 2 1 55.49 74.04 158.01 o -15 3 1 16.33 -109.38 141.58 o -14 3 1 98.07 40.83 143.99 o -13 3 1 2786.30 2639.54 286.84 o -12 3 1 5483.20 5455.05 281.72 o -11 3 1 1588.87 1420.96 179.28 o -10 3 1 920.71 922.09 151.70 o -9 3 1 166.12 112.37 101.00 o -8 3 1 128.15 50.28 70.50 o -7 3 1 316.28 264.19 76.53 o -6 3 1 65.50 57.28 62.03 o -5 3 1 20388.98 20480.74 292.77 o -4 3 1 3072.71 2917.27 89.42 o -3 3 1 29860.97 31182.48 292.15 o -2 3 1 159.11 215.99 42.84 o -1 3 1 1.47 13.01 49.68 o 0 3 1 341.63 507.26 55.05 o 1 3 1 8381.90 7965.57 127.53 o 2 3 1 7906.26 7322.68 134.62 o 3 3 1 20863.02 21540.74 320.82 o 4 3 1 2162.93 2148.61 91.85 o 5 3 1 673.92 657.18 75.43 o 6 3 1 5398.75 5385.02 163.68 o 7 3 1 3021.95 3032.64 154.00 o 8 3 1 257.47 226.86 103.52 o 9 3 1 650.94 777.96 148.54 o 10 3 1 145.19 180.95 115.84 o 11 3 1 2234.44 2541.03 224.07 o 12 3 1 1161.56 987.75 165.42 o 13 3 1 0.22 -60.03 129.72 o 14 3 1 387.99 462.61 176.46 o 15 3 1 402.96 323.66 172.31 o -15 4 1 836.06 832.54 228.40 o -14 4 1 4.64 -213.14 142.09 o -13 4 1 116.73 -52.48 111.53 o -12 4 1 224.69 207.51 122.08 o -11 4 1 1835.60 1925.27 221.12 o -10 4 1 177.92 156.56 109.50 o -9 4 1 66.86 78.35 110.96 o -8 4 1 50.17 -98.94 86.85 o -7 4 1 3433.37 3436.23 209.15 o -6 4 1 12978.94 13187.24 244.35 o -5 4 1 10336.00 10652.87 197.42 o -4 4 1 9749.51 9476.52 222.67 o -3 4 1 43638.67 42710.25 380.75 o -2 4 1 41258.39 43216.34 523.17 o -1 4 1 1840.09 1466.25 198.89 o 0 4 1 3810.98 3675.40 102.24 o 1 4 1 1727.71 1656.68 79.67 o 2 4 1 11685.54 11641.54 206.09 o 3 4 1 985.66 971.76 75.70 o 4 4 1 46.43 90.78 70.44 o 5 4 1 59946.32 58115.09 963.59 o 6 4 1 537.27 634.95 114.44 o 7 4 1 12.20 -71.82 78.46 o 8 4 1 572.71 703.21 147.98 o 9 4 1 2595.11 2903.29 232.86 o 10 4 1 964.30 623.20 144.32 o 11 4 1 2167.60 1882.95 205.61 o 12 4 1 427.78 359.73 129.86 o 13 4 1 4636.69 4987.88 309.19 o 14 4 1 300.46 301.29 175.72 o 15 4 1 556.85 440.19 230.95 o -15 5 1 383.04 149.88 256.31 o -14 5 1 439.51 528.68 164.38 o -13 5 1 1567.41 1703.24 216.02 o -12 5 1 70.09 -8.66 110.66 o -11 5 1 81.20 11.09 105.03 o -10 5 1 1707.89 1441.78 234.41 o -9 5 1 28.28 -48.66 93.17 o -8 5 1 64.65 121.75 107.80 o -7 5 1 831.06 886.23 151.35 o -6 5 1 2260.40 2432.61 194.20 o -5 5 1 4249.86 3755.64 199.85 o -4 5 1 2316.86 2541.47 128.14 o -3 5 1 216.88 165.71 42.22 o -2 5 1 22.43 -8.91 37.70 o -1 5 1 4459.03 4379.08 114.94 o 0 5 1 615.86 439.29 58.45 o 1 5 1 1691.37 1130.85 321.39 o 2 5 1 22.60 46.47 40.76 o 3 5 1 30973.36 29474.82 322.88 o 4 5 1 4809.74 4673.48 189.64 o 5 5 1 4554.51 4913.96 224.86 o 6 5 1 298.78 216.54 107.97 o 7 5 1 14612.63 15084.47 449.77 o 8 5 1 7466.76 7147.60 294.98 o 9 5 1 2012.60 2461.03 227.05 o 10 5 1 348.45 234.08 121.81 o 11 5 1 1308.50 1227.30 181.63 o 12 5 1 32.52 -86.28 109.48 o 13 5 1 704.00 652.35 166.77 o 14 5 1 546.95 603.88 211.51 o -14 6 1 535.40 377.08 166.03 o -13 6 1 97.02 143.77 170.77 o -12 6 1 10.56 -69.56 115.93 o -11 6 1 90.78 177.90 124.06 o -10 6 1 758.43 788.15 211.77 o -9 6 1 5.11 -136.84 104.26 o -8 6 1 1324.62 1188.55 177.57 o -7 6 1 49.94 10.30 108.84 o -6 6 1 3.93 -27.76 101.72 o -5 6 1 326.36 312.91 119.88 o -4 6 1 160.57 105.44 72.72 o -3 6 1 149.97 97.27 44.40 o -2 6 1 8567.30 7881.96 153.78 o -1 6 1 1619.64 1840.49 99.80 o 0 6 1 557.16 499.00 67.33 o 1 6 1 650.32 398.76 82.59 o 2 6 1 3573.73 3347.42 113.55 o 3 6 1 111.87 64.69 70.01 o 4 6 1 2.50 14.50 86.60 o 5 6 1 133.57 124.26 105.18 o 6 6 1 6646.46 6254.29 273.39 o 7 6 1 4995.18 4666.57 259.54 o 8 6 1 10101.99 9804.85 352.28 o 9 6 1 92.22 98.01 110.97 o 10 6 1 874.21 650.12 157.47 o 11 6 1 1.85 -51.65 118.77 o 12 6 1 398.99 184.82 135.47 o 13 6 1 835.36 896.12 185.26 o 14 6 1 176.14 -4.04 145.84 o -13 7 1 51.09 -40.74 147.66 o -12 7 1 239.07 203.10 139.28 o -11 7 1 580.39 431.95 148.25 o -10 7 1 1060.13 1221.29 192.13 o -9 7 1 478.13 388.47 144.77 o -8 7 1 2663.32 2680.99 235.40 o -7 7 1 142.26 68.75 116.56 o -6 7 1 730.28 905.85 165.19 o -5 7 1 3385.48 3822.67 264.50 o -4 7 1 18.08 -0.73 105.98 o -3 7 1 1226.77 1203.62 128.37 o -2 7 1 1254.79 1248.10 178.27 o -1 7 1 9416.60 9499.45 202.68 o 0 7 1 12146.47 12279.62 220.06 o 1 7 1 145.76 81.44 62.56 o 2 7 1 3.32 -41.05 70.66 o 3 7 1 392.66 413.61 95.59 o 4 7 1 3365.63 3711.06 330.83 o 5 7 1 304.04 334.82 127.86 o 6 7 1 585.07 523.04 143.36 o 7 7 1 0.70 -54.65 107.81 o 8 7 1 1704.96 1827.65 210.26 o 9 7 1 16.41 19.25 113.28 o 10 7 1 2809.14 2328.76 236.90 o 11 7 1 845.95 792.92 179.29 o 12 7 1 406.57 316.16 153.72 o 13 7 1 12.88 -30.88 135.53 o -12 8 1 20.50 -20.86 136.10 o -11 8 1 1345.76 1608.74 227.87 o -10 8 1 304.27 144.30 123.60 o -9 8 1 67.77 66.91 123.36 o -8 8 1 0.50 -92.02 104.29 o -7 8 1 95.89 47.57 111.20 o -6 8 1 432.20 320.83 128.92 o -5 8 1 676.52 616.45 151.33 o -4 8 1 3871.18 3930.15 256.11 o -3 8 1 2897.82 3071.89 225.26 o -2 8 1 683.80 448.78 127.57 o -1 8 1 2718.01 3121.23 187.83 o 0 8 1 3.77 -9.22 67.51 o 1 8 1 6576.71 6625.27 232.56 o 2 8 1 3823.16 3211.75 321.08 o 3 8 1 314.56 275.94 129.09 o 4 8 1 1547.08 1499.30 193.57 o 5 8 1 13299.68 13445.53 405.60 o 6 8 1 606.82 464.81 145.43 o 7 8 1 1499.56 1451.51 191.36 o 8 8 1 2761.99 2794.71 256.89 o 9 8 1 1582.23 1653.43 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