#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206780.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206780_Fobs loop_ _publ_author_name 'Li, Chuan-Bi' 'Liu, Bo' 'Gao, Guang-Gang' 'Che, Guang-Bo' _publ_section_title ; Hydrogen bonding and \p--\p stacking in di-\m-isophthalato-bis[bis(isonicotinamide)copper(II)] trihydrate ; _journal_coeditor_code RN6055 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1705 _journal_page_last m1707 _journal_volume 61 _journal_year 2005 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.643 _cell_angle_beta 99.851 _cell_angle_gamma 109.665 _cell_length_a 10.0909 _cell_length_b 12.7898 _cell_length_c 17.5601 _exptl_crystal_F_000 1024.00 _reflns_d_resolution_high 0.7499 _[local]_cod_data_source_file rn6055Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LICN10m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 368.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 3550.18 3131.47 64.02 o 4 0 0 3096.74 3078.58 73.76 o 5 0 0 168.14 147.53 23.66 o 6 0 0 5747.04 6083.40 129.43 o 7 0 0 1826.54 1787.02 79.33 o 8 0 0 1729.35 1757.80 86.29 o 9 0 0 744.09 745.99 64.02 o 10 0 0 1647.48 1621.40 96.03 o 11 0 0 902.52 826.71 76.55 o 12 0 0 25.68 23.66 34.79 o -12 1 0 5.59 -26.44 26.44 o -11 1 0 635.05 601.24 66.80 o -10 1 0 3243.30 3401.47 130.83 o -9 1 0 464.59 489.90 52.89 o -8 1 0 2404.32 2546.93 98.82 o -7 1 0 1774.96 1824.60 77.94 o -6 1 0 1687.23 1735.53 69.59 o -5 1 0 2027.61 2225.43 69.59 o -4 1 0 12939.11 14410.32 153.09 o -3 1 0 6201.30 7670.02 67.90 o -2 1 0 38.83 36.89 5.90 o -1 1 0 19978.50 20862.54 135.00 o 0 1 0 23822.71 23223.80 541.40 o 1 1 0 131.94 109.95 11.13 o 2 1 0 4028.21 4354.83 69.59 o 3 1 0 2866.14 2822.50 65.41 o 4 1 0 6829.60 7373.56 119.69 o 5 1 0 739.48 776.60 45.93 o 6 1 0 3936.94 4115.45 111.34 o 7 1 0 3096.46 3259.51 108.56 o 8 1 0 625.20 642.99 57.06 o 9 1 0 655.10 627.69 61.24 o 10 1 0 2690.33 2597.03 121.08 o 11 1 0 715.69 634.64 70.98 o 12 1 0 2.80 -9.74 33.40 o -12 2 0 8.35 6.96 27.84 o -11 2 0 1102.24 1152.38 83.51 o -10 2 0 1549.24 1402.90 86.29 o -9 2 0 511.07 524.69 52.89 o -8 2 0 2951.10 3086.93 105.77 o -7 2 0 2007.77 1945.69 77.94 o -6 2 0 1252.87 1309.65 59.85 o -5 2 0 3477.21 3812.04 87.68 o -4 2 0 1895.03 1863.31 38.86 o -3 2 0 7433.50 8853.01 102.99 o -2 2 0 42.72 12.53 6.96 o -1 2 0 957.59 1400.11 27.84 o 0 2 0 26668.24 28048.71 427.97 o 1 2 0 2853.06 2615.12 51.50 o 2 2 0 1998.69 2002.75 54.28 o 3 2 0 717.21 477.37 32.01 o 4 2 0 5662.12 5675.61 111.34 o 5 2 0 7043.58 7720.11 143.35 o 6 2 0 7235.63 7853.72 158.66 o 7 2 0 1903.05 1937.33 89.07 o 8 2 0 11.06 -2.78 22.27 o 9 2 0 903.05 862.89 72.37 o 10 2 0 480.62 521.91 64.02 o 11 2 0 33.78 21.33 20.73 o -12 3 0 113.95 101.60 41.75 o -11 3 0 1113.28 1089.75 80.72 o -10 3 0 140.25 137.78 36.19 o -9 3 0 236.27 279.74 41.75 o -8 3 0 1192.17 1252.59 69.59 o -7 3 0 1905.74 1951.25 77.94 o -6 3 0 101.89 88.85 16.01 o -5 3 0 9399.44 10933.11 113.43 o -4 3 0 8670.55 10054.10 128.04 o -3 3 0 2221.97 2719.51 59.85 o -2 3 0 29.15 122.05 16.01 o -1 3 0 3551.80 3683.51 51.95 o 0 3 0 1499.83 1499.78 42.44 o 1 3 0 1614.92 2126.61 40.36 o 2 3 0 507.63 385.52 29.23 o 3 3 0 6945.95 7149.49 122.48 o 4 3 0 3761.28 3728.53 97.42 o 5 3 0 4640.08 4841.95 121.08 o 6 3 0 6797.47 6665.16 153.09 o 7 3 0 1680.40 1675.68 87.68 o 8 3 0 10.64 4.18 26.44 o 9 3 0 97.44 114.12 38.97 o 10 3 0 167.60 205.35 32.87 o 11 3 0 104.03 106.27 30.32 o -12 4 0 195.98 187.89 47.32 o -11 4 0 681.50 649.95 65.41 o -10 4 0 120.56 126.65 34.79 o -9 4 0 2802.30 2999.25 111.34 o -8 4 0 40.96 51.50 22.27 o -7 4 0 2243.24 2272.05 59.05 o -6 4 0 379.79 409.73 48.71 o -5 4 0 5868.50 6516.24 116.91 o -4 4 0 18746.39 21936.98 196.24 o -3 4 0 517.97 496.86 29.23 o -2 4 0 300.86 283.62 15.23 o -1 4 0 21070.71 22457.34 234.26 o 0 4 0 3200.60 3891.12 77.81 o 1 4 0 291.67 423.01 17.25 o 2 4 0 11563.81 12231.48 455.80 o 3 4 0 9190.78 8985.23 147.53 o 4 4 0 296.27 296.45 34.79 o 5 4 0 7671.98 7441.76 158.66 o 6 4 0 3328.30 3629.72 121.08 o 7 4 0 0.76 9.74 25.05 o 8 4 0 274.01 272.18 32.30 o 9 4 0 323.99 346.61 36.82 o 10 4 0 165.67 134.53 30.89 o -12 5 0 771.48 875.42 79.33 o -11 5 0 1030.18 993.72 76.55 o -10 5 0 560.22 584.54 57.06 o -9 5 0 1626.38 1750.84 86.29 o -8 5 0 503.02 547.30 33.94 o -7 5 0 219.21 204.71 29.23 o -6 5 0 2641.37 2723.68 84.90 o -5 5 0 8020.58 8553.78 137.78 o -4 5 0 5589.75 6519.02 112.73 o -3 5 0 36.14 55.43 9.69 o -2 5 0 154.76 234.76 15.75 o -1 5 0 3145.88 3400.69 31.29 o 0 5 0 2153.18 2156.02 79.67 o 2 5 0 2811.30 2690.06 158.66 o 3 5 0 417.69 392.13 29.23 o 4 5 0 429.87 429.42 32.01 o 5 5 0 2784.59 2774.44 85.59 o 6 5 0 1407.32 1385.07 54.29 o 7 5 0 22.28 13.33 15.69 o 8 5 0 217.52 248.62 31.88 o 9 5 0 344.41 391.64 40.31 o 10 5 0 373.02 378.56 65.41 o -12 6 0 238.31 288.10 51.50 o -11 6 0 28.69 32.01 25.05 o -10 6 0 381.03 340.98 47.32 o -9 6 0 4375.28 4619.84 96.93 o -8 6 0 510.82 493.76 32.96 o -7 6 0 71.09 80.72 23.66 o -6 6 0 139.49 141.96 25.05 o -5 6 0 3152.48 3414.00 91.86 o -4 6 0 467.78 405.65 22.00 o -3 6 0 596.66 535.81 50.10 o -2 6 0 5864.75 5529.78 217.81 o -1 6 0 513.77 501.04 26.44 o 0 6 0 242.22 220.70 11.26 o 1 6 0 1673.06 1388.85 32.88 o 2 6 0 2847.64 2604.76 152.40 o 3 6 0 259.34 229.09 21.74 o 4 6 0 2382.64 2314.69 105.08 o 5 6 0 425.06 413.40 32.08 o 6 6 0 136.65 156.84 24.39 o 7 6 0 9.37 -2.78 26.44 o 8 6 0 1124.99 1298.52 93.25 o 9 6 0 317.37 364.64 61.24 o -12 7 0 154.43 139.18 43.14 o -11 7 0 6.92 9.74 22.27 o -10 7 0 741.98 805.06 46.74 o -9 7 0 2150.58 2288.56 91.16 o -8 7 0 313.14 307.58 38.97 o -7 7 0 128.96 102.99 25.05 o -6 7 0 2326.73 2221.25 82.11 o -5 7 0 23.55 6.26 8.86 o -4 7 0 1497.48 1562.31 83.51 o -3 7 0 108.31 83.45 18.09 o -2 7 0 1913.08 1854.83 46.13 o -1 7 0 377.76 327.50 22.99 o 0 7 0 1176.06 1052.27 55.09 o 1 7 0 2585.44 2523.27 87.68 o 2 7 0 1909.85 1633.93 76.55 o 3 7 0 251.21 204.59 36.19 o 4 7 0 461.54 488.51 54.28 o 5 7 0 10.55 47.32 29.23 o 6 7 0 1.45 -1.39 23.66 o 7 7 0 257.24 296.45 52.89 o 8 7 0 1098.65 1215.01 93.25 o 9 7 0 36.40 59.85 41.75 o -12 8 0 385.84 367.43 55.67 o -11 8 0 15.82 11.10 17.63 o -10 8 0 1969.16 1932.40 69.85 o -8 8 0 103.08 128.04 30.62 o -7 8 0 696.72 727.09 35.67 o -6 8 0 1574.91 1507.33 96.73 o -5 8 0 1792.32 1740.80 164.92 o -4 8 0 5447.73 5768.41 203.20 o -3 8 0 744.98 686.23 54.28 o -2 8 0 2297.64 2168.40 53.47 o -1 8 0 229.73 221.99 21.14 o 0 8 0 907.44 867.40 38.34 o 1 8 0 2590.67 2648.53 96.03 o 2 8 0 1327.14 1306.87 73.76 o 3 8 0 503.64 542.79 55.67 o 4 8 0 1488.00 1369.50 82.11 o 5 8 0 53.80 25.05 26.44 o 6 8 0 46.31 54.28 32.01 o 7 8 0 696.29 768.25 75.16 o 8 8 0 719.27 725.11 79.33 o -12 9 0 0.77 19.48 30.62 o -11 9 0 954.57 988.17 55.54 o -10 9 0 735.68 863.59 49.21 o -9 9 0 75.97 109.95 32.01 o -8 9 0 64.54 44.54 23.66 o -7 9 0 2299.22 2275.29 68.20 o -6 9 0 1371.88 1377.91 47.36 o -5 9 0 120.78 99.48 17.03 o -4 9 0 5556.99 5882.05 91.94 o -3 9 0 3806.02 3704.12 116.91 o -2 9 0 408.77 375.94 27.50 o -1 9 0 93.80 81.70 17.71 o 0 9 0 2980.17 3035.80 73.27 o 1 9 0 709.65 750.16 59.85 o 2 9 0 6.28 -4.18 19.48 o 3 9 0 243.50 219.90 41.75 o 4 9 0 245.01 300.62 47.32 o 5 9 0 354.66 395.26 55.67 o 6 9 0 70.06 100.21 38.97 o 7 9 0 485.43 563.66 69.59 o -12 10 0 181.80 175.47 38.97 o -11 10 0 1024.91 1022.59 59.15 o -10 10 0 1351.36 1220.58 84.90 o -9 10 0 2.60 -13.92 16.70 o -8 10 0 31.91 34.79 22.27 o -7 10 0 1231.12 1203.88 72.37 o -6 10 0 1404.08 1398.52 50.33 o -5 10 0 114.13 137.75 20.01 o -4 10 0 2077.72 1988.91 57.84 o -3 10 0 1335.22 1385.64 50.07 o -2 10 0 139.62 137.27 20.67 o -1 10 0 290.23 297.16 27.93 o 0 10 0 919.34 884.14 44.15 o 1 10 0 1308.07 1394.55 82.11 o 2 10 0 213.16 229.64 41.75 o 3 10 0 731.88 736.24 66.80 o 4 10 0 1142.00 1085.58 82.11 o 5 10 0 57.23 66.80 30.62 o 6 10 0 170.30 167.01 47.32 o -11 11 0 742.44 718.94 49.63 o -10 11 0 250.79 222.68 44.54 o -9 11 0 107.10 87.68 32.01 o -8 11 0 96.03 123.87 34.79 o -7 11 0 1336.64 1262.33 77.94 o -6 11 0 16.06 20.88 19.48 o -5 11 0 116.56 108.56 20.60 o -4 11 0 17.01 10.76 16.01 o -3 11 0 890.43 866.60 43.27 o -2 11 0 818.71 840.03 43.27 o -1 11 0 37.53 48.67 17.03 o 0 11 0 102.45 122.48 34.79 o 1 11 0 636.68 528.87 57.06 o 2 11 0 360.27 413.35 54.28 o 3 11 0 631.84 679.18 68.20 o 4 11 0 207.51 297.84 52.89 o 5 11 0 0.76 9.74 26.44 o -11 12 0 199.28 192.06 45.93 o -10 12 0 137.71 146.14 40.36 o -9 12 0 186.62 178.15 41.75 o -8 12 0 143.99 160.05 38.97 o -7 12 0 121.61 100.21 32.01 o -6 12 0 32.02 23.66 22.27 o -5 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