#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2206822.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206822_Fobs loop_ _publ_author_name 'Zhang, Jun-Hong' 'Wang, Da-Qi' 'Dou, Jian-Min' _publ_section_title ; Bis[2,5,8,11,14-pentaoxabicyclo[13.4.0]nonadeca-1(15),16,18-triene]potassium(I) bis(2-thioxo-4,5-dihydro-1,3-dithiole-4,5-dithiolato)nickel(III) ; _journal_coeditor_code XU6034 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1699 _journal_page_last m1700 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 110.648 _cell_angle_gamma 90.000 _cell_length_a 18.2703 _cell_length_b 11.8005 _cell_length_c 21.9275 _exptl_crystal_F_000 2124.00 _reflns_d_resolution_high 0.8400 _[local]_cod_data_source_file xu6034Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 010428b in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 478.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 25340.60 26629.49 762.37 o 4 0 0 28461.57 28604.47 340.95 o 6 0 0 163.27 63.07 72.58 o 8 0 0 5548.30 5485.35 171.11 o 10 0 0 11000.08 11035.24 263.45 o 12 0 0 456.68 430.23 114.99 o 14 0 0 504.90 490.68 295.49 o 16 0 0 1672.57 1642.84 374.11 o 18 0 0 32.15 -10.84 298.21 o 20 0 0 162.46 -35.24 325.32 o 1 1 0 3847.00 3837.13 62.55 o 2 1 0 3394.24 3339.62 89.21 o 3 1 0 7239.26 7248.45 93.84 o 4 1 0 1853.25 1676.96 69.81 o 5 1 0 1280.54 1260.14 66.50 o 6 1 0 6856.26 6641.80 120.35 o 7 1 0 4.12 -0.79 49.43 o 8 1 0 2082.72 1970.61 83.82 o 9 1 0 4.12 -11.82 55.37 o 10 1 0 3312.25 3349.76 112.79 o 11 1 0 5395.17 5219.21 143.76 o 12 1 0 251.23 287.19 78.96 o 13 1 0 602.52 486.85 96.27 o 14 1 0 80.24 128.44 197.42 o 15 1 0 207.51 0.59 193.35 o 16 1 0 70.51 117.93 197.44 o 17 1 0 584.01 836.33 237.70 o 18 1 0 127.05 165.56 216.81 o 19 1 0 27.85 51.23 223.32 o 20 1 0 31.31 8.45 223.89 o 0 2 0 559.85 443.86 69.95 o 1 2 0 34513.54 36330.24 337.58 o 2 2 0 1781.47 1725.84 106.82 o 3 2 0 914.65 884.60 114.10 o 4 2 0 5056.86 4921.35 115.29 o 5 2 0 1883.38 1881.69 88.75 o 6 2 0 4234.96 3940.96 102.59 o 7 2 0 5663.94 5224.35 119.68 o 8 2 0 471.49 415.50 63.55 o 9 2 0 14471.73 14811.77 211.58 o 10 2 0 6537.74 6439.28 152.14 o 11 2 0 2881.30 2952.56 119.14 o 12 2 0 207.75 230.03 92.85 o 13 2 0 740.89 801.43 107.73 o 14 2 0 964.49 1304.78 177.04 o 15 2 0 316.40 350.32 185.99 o 16 2 0 157.58 21.80 235.85 o 17 2 0 490.75 662.17 237.33 o 18 2 0 14.27 -55.60 190.55 o 19 2 0 291.53 361.05 242.03 o 20 2 0 12.43 14.64 212.85 o 1 3 0 2108.26 2061.96 103.98 o 2 3 0 16.85 65.41 71.32 o 3 3 0 7193.09 7264.03 188.99 o 4 3 0 1839.79 1865.66 88.46 o 5 3 0 92.86 164.66 64.78 o 6 3 0 1820.68 1814.30 94.09 o 7 3 0 67.54 30.04 56.40 o 8 3 0 2136.15 2232.94 96.59 o 9 3 0 13457.08 13632.90 210.70 o 10 3 0 25.75 46.87 68.09 o 11 3 0 2402.41 2208.16 111.24 o 12 3 0 1969.10 2258.85 140.43 o 13 3 0 10.59 -7.24 87.13 o 14 3 0 70.62 48.21 110.86 o 15 3 0 402.16 411.44 205.74 o 16 3 0 28.07 136.30 189.52 o 17 3 0 81.56 141.49 200.26 o 18 3 0 24.53 114.85 195.64 o 19 3 0 18.18 -88.66 195.66 o 0 4 0 4283.90 4532.87 203.17 o 1 4 0 4191.88 3987.76 136.26 o 2 4 0 7.30 71.98 76.86 o 3 4 0 258.24 340.94 80.66 o 4 4 0 2472.55 2165.03 108.12 o 5 4 0 716.31 745.28 76.61 o 6 4 0 9.37 -4.96 66.68 o 7 4 0 5115.06 5250.64 155.88 o 8 4 0 901.98 835.96 93.62 o 9 4 0 681.47 510.02 78.35 o 10 4 0 5498.12 5354.99 155.91 o 11 4 0 273.82 243.27 97.52 o 12 4 0 62.32 19.60 97.96 o 13 4 0 30.76 117.98 113.97 o 14 4 0 33.20 -76.98 108.94 o 15 4 0 65.45 38.59 179.70 o 16 4 0 105.91 85.41 185.47 o 17 4 0 599.69 719.67 221.47 o 18 4 0 705.14 1023.85 264.32 o 19 4 0 207.97 202.71 229.02 o 1 5 0 6955.39 6666.38 201.12 o 2 5 0 4613.38 4347.86 156.56 o 3 5 0 275.43 230.84 95.29 o 4 5 0 212.59 91.77 77.72 o 5 5 0 95.86 75.24 68.61 o 6 5 0 2511.43 2311.64 117.11 o 7 5 0 2224.67 2165.74 118.39 o 8 5 0 93.89 155.62 82.17 o 9 5 0 472.01 273.30 92.28 o 10 5 0 2599.95 2680.54 130.14 o 11 5 0 1176.26 1172.56 124.95 o 12 5 0 1212.55 1109.40 131.16 o 13 5 0 1001.34 1178.33 145.57 o 14 5 0 106.71 -41.03 110.73 o 15 5 0 314.92 317.03 151.76 o 16 5 0 204.65 178.34 193.97 o 17 5 0 0.30 172.17 202.76 o 18 5 0 80.98 -9.88 207.66 o 19 5 0 50.27 -108.71 204.15 o 0 6 0 11719.03 11255.32 405.29 o 1 6 0 1193.99 1223.87 116.52 o 2 6 0 974.40 994.90 107.57 o 3 6 0 261.80 231.47 101.40 o 4 6 0 5557.67 5298.44 223.82 o 5 6 0 3161.58 3035.43 129.11 o 6 6 0 436.43 347.67 84.59 o 7 6 0 54.79 68.83 86.69 o 8 6 0 15.43 67.43 91.50 o 9 6 0 151.64 178.19 99.61 o 10 6 0 13.30 81.29 97.38 o 11 6 0 3142.18 2968.86 170.56 o 12 6 0 883.78 1287.70 134.85 o 13 6 0 116.30 -7.60 115.66 o 14 6 0 1146.72 1034.44 146.48 o 15 6 0 25.00 -27.76 141.71 o 16 6 0 193.81 -86.63 190.67 o 17 6 0 20.23 223.09 203.99 o 18 6 0 295.75 509.93 318.54 o 1 7 0 1129.51 1119.90 120.67 o 2 7 0 368.13 240.22 103.54 o 3 7 0 455.22 486.33 85.43 o 4 7 0 697.87 576.20 100.49 o 5 7 0 47.62 37.36 87.25 o 6 7 0 2063.22 2138.10 130.07 o 7 7 0 158.74 82.74 90.01 o 8 7 0 1884.75 1872.14 138.21 o 9 7 0 2022.32 2041.05 145.48 o 10 7 0 1912.59 2099.35 153.46 o 11 7 0 38.45 38.77 102.48 o 12 7 0 1.48 62.49 107.50 o 13 7 0 549.87 462.94 129.88 o 14 7 0 2.82 -29.39 119.20 o 15 7 0 0.00 -131.51 138.09 o 16 7 0 67.99 -157.24 260.25 o 17 7 0 21.25 -105.73 246.70 o 0 8 0 40.61 -13.55 149.52 o 1 8 0 10487.44 10272.37 294.81 o 2 8 0 391.38 442.91 119.49 o 3 8 0 4248.70 4840.82 262.33 o 4 8 0 1939.20 1780.76 187.69 o 5 8 0 3026.70 2929.50 218.30 o 6 8 0 46.39 108.05 144.74 o 7 8 0 682.62 525.95 163.68 o 8 8 0 88.42 35.79 112.92 o 9 8 0 38.31 -57.91 106.26 o 10 8 0 355.25 354.55 119.37 o 11 8 0 852.39 884.99 147.52 o 12 8 0 110.66 13.98 132.64 o 13 8 0 634.93 633.19 160.07 o 14 8 0 26.63 62.14 148.34 o 15 8 0 85.57 290.67 151.56 o 16 8 0 95.63 265.48 189.12 o 1 9 0 318.33 383.47 134.63 o 2 9 0 6534.75 7038.19 315.02 o 3 9 0 988.47 1006.92 173.36 o 4 9 0 1.37 92.42 150.97 o 5 9 0 3.75 -112.00 147.40 o 6 9 0 292.80 219.00 148.89 o 7 9 0 684.14 663.76 177.04 o 8 9 0 123.01 77.40 143.40 o 9 9 0 33.51 -18.21 140.53 o 10 9 0 68.39 62.59 144.41 o 11 9 0 28.78 23.85 143.95 o 12 9 0 2.75 -50.20 179.92 o 13 9 0 8.86 131.32 184.98 o 14 9 0 6.37 -33.15 178.86 o 15 9 0 272.17 250.54 205.74 o 0 10 0 748.29 522.80 215.52 o 1 10 0 8.08 5.58 147.91 o 2 10 0 2416.55 2623.79 238.20 o 3 10 0 680.09 410.07 166.80 o 4 10 0 334.57 188.89 160.63 o 5 10 0 1792.05 1682.95 206.13 o 6 10 0 604.32 630.00 169.44 o 7 10 0 46.56 70.19 152.86 o 8 10 0 2424.12 2567.02 245.12 o 9 10 0 33.48 -19.09 152.70 o 10 10 0 1179.63 1421.38 208.31 o 11 10 0 209.29 161.70 172.92 o 12 10 0 8.22 -99.47 284.65 o 13 10 0 18.84 -46.98 200.26 o 14 10 0 14.41 -45.21 198.01 o 1 11 0 228.15 170.06 142.39 o 2 11 0 128.47 36.45 147.46 o 3 11 0 177.59 219.73 158.71 o 4 11 0 58.47 35.92 139.29 o 5 11 0 129.75 121.41 157.03 o 6 11 0 196.60 177.43 164.82 o 7 11 0 103.05 19.61 149.64 o 8 11 0 550.96 992.85 222.22 o 9 11 0 44.67 -3.61 166.01 o 10 11 0 89.18 228.69 170.99 o 11 11 0 67.00 -87.77 195.64 o 12 11 0 110.33 180.19 216.50 o 0 12 0 80.13 124.70 268.39 o 1 12 0 125.96 230.04 177.08 o 2 12 0 2.78 -2.81 156.64 o 3 12 0 3.27 -53.06 162.96 o 4 12 0 5.43 -133.17 165.99 o 5 12 0 7.13 122.14 171.81 o 6 12 0 293.02 308.49 171.72 o 7 12 0 901.51 864.06 203.47 o 8 12 0 131.48 93.67 176.44 o 9 12 0 765.66 1000.78 208.82 o 10 12 0 2.68 -53.59 165.89 o 1 13 0 202.22 608.67 249.11 o 2 13 0 71.79 214.32 172.81 o 3 13 0 71.83 187.01 176.61 o 4 13 0 3.79 -13.28 178.60 o 5 13 0 14.81 23.02 179.78 o 6 13 0 5.14 -60.59 181.05 o 7 13 0 54.38 8.38 175.06 o 0 14 0 484.76 1043.72 422.91 o 1 14 0 15.96 -5.54 242.49 o -19 0 1 1.13 -119.28 298.21 o -17 0 1 1.42 233.14 284.65 o -15 0 1 2438.94 2960.37 425.62 o -13 0 1 3236.70 3208.48 251.42 o -11 0 1 16166.90 16601.24 329.76 o -9 0 1 40.14 144.73 85.98 o -7 0 1 3075.23 2885.37 124.20 o -5 0 1 19460.67 20063.45 371.33 o -3 0 1 12726.90 12644.91 178.54 o -1 0 1 25701.52 26312.58 365.98 o 1 0 1 15195.19 16639.87 276.52 o 3 0 1 27210.31 28177.14 345.65 o 5 0 1 12329.53 12778.46 208.66 o 7 0 1 1013.11 1190.19 99.60 o 9 0 1 10754.15 10780.88 250.96 o 11 0 1 164.33 140.00 101.31 o 13 0 1 1214.09 886.48 298.21 o 15 0 1 1403.91 1648.26 357.85 o 17 0 1 365.73 287.36 281.94 o 19 0 1 202.47 138.26 325.32 o -20 1 1 9.87 -107.66 248.05 o -19 1 1 8.31 -90.52 195.92 o -18 1 1 402.75 438.20 265.67 o -17 1 1 378.61 314.26 203.14 o -16 1 1 1.97 -40.23 173.09 o -15 1 1 160.46 154.52 197.44 o -14 1 1 280.09 285.63 112.13 o -13 1 1 21.49 0.90 100.34 o -12 1 1 489.07 581.44 94.53 o -11 1 1 5392.25 5545.62 144.13 o -10 1 1 512.48 485.89 69.87 o -9 1 1 4221.00 4140.75 114.98 o -8 1 1 3071.66 3058.82 96.65 o -7 1 1 841.89 734.56 61.40 o -6 1 1 30248.09 30254.40 236.03 o -5 1 1 23609.05 23171.51 190.95 o -4 1 1 2655.24 2677.49 72.45 o -3 1 1 329.78 358.56 47.74 o -2 1 1 9445.58 9047.51 185.06 o -1 1 1 7.52 13.66 23.89 o 0 1 1 8397.14 8249.25 185.26 o 1 1 1 486.85 530.71 40.95 o 2 1 1 22905.94 24085.15 292.69 o 3 1 1 14642.26 14583.95 145.64 o 4 1 1 2094.38 2011.49 79.92 o 5 1 1 2576.66 2366.47 78.37 o 6 1 1 2206.16 2066.60 79.54 o 7 1 1 2146.08 2103.76 82.59 o 8 1 1 63.47 115.85 58.18 o 9 1 1 4600.53 4546.20 122.46 o 10 1 1 186.16 210.90 65.71 o 11 1 1 2648.20 2385.68 110.61 o 12 1 1 792.79 956.62 89.27 o 13 1 1 2366.26 1874.19 309.64 o 14 1 1 322.07 408.59 189.86 o 15 1 1 187.88 198.85 190.55 o 16 1 1 80.85 -19.02 184.62 o 17 1 1 4.05 43.02 204.15 o 18 1 1 156.54 -1.64 213.58 o 19 1 1 90.95 20.49 217.52 o -20 2 1 223.00 -12.17 230.51 o -19 2 1 20.99 -120.90 194.15 o -18 2 1 60.45 78.92 194.76 o -17 2 1 0.27 -3.66 199.11 o -16 2 1 212.89 328.01 198.06 o -15 2 1 486.08 601.14 153.66 o -14 2 1 1292.34 1403.04 148.07 o -13 2 1 975.79 808.46 112.16 o -12 2 1 2315.11 2375.45 136.24 o -11 2 1 734.62 727.93 79.96 o -10 2 1 1250.94 1097.12 83.21 o -9 2 1 2090.82 1974.98 92.21 o -8 2 1 7562.12 7534.87 143.85 o -7 2 1 111.93 115.55 53.80 o -6 2 1 32.04 3.87 49.81 o -5 2 1 1992.82 1761.07 87.22 o -4 2 1 27408.80 28201.30 249.43 o -3 2 1 71.34 102.02 63.06 o -2 2 1 2506.91 2473.84 66.39 o -1 2 1 1152.12 1134.10 63.83 o 0 2 1 48082.83 49398.92 372.12 o 1 2 1 24758.27 24492.17 303.64 o 2 2 1 74481.01 76963.35 440.21 o 3 2 1 9251.18 8939.76 151.54 o 4 2 1 4970.41 5133.66 129.62 o 5 2 1 8356.80 8495.96 146.14 o 6 2 1 16381.08 15927.98 202.17 o 7 2 1 1125.02 986.81 71.14 o 8 2 1 7554.76 7507.40 150.12 o 9 2 1 313.70 405.66 68.02 o 10 2 1 664.46 747.59 80.09 o 11 2 1 5376.64 5427.69 153.65 o 12 2 1 960.84 872.31 104.07 o 13 2 1 874.51 802.34 128.22 o 14 2 1 1042.83 1186.81 238.65 o 15 2 1 994.56 778.37 216.51 o 16 2 1 1364.33 1496.71 344.29 o 17 2 1 24.28 -83.63 189.52 o 18 2 1 133.42 197.64 217.52 o 19 2 1 26.19 -201.41 201.41 o -20 3 1 12.80 -112.08 222.34 o -19 3 1 2.36 -155.38 207.00 o -18 3 1 0.02 -53.94 203.82 o -17 3 1 119.57 172.55 279.23 o -16 3 1 33.47 -143.56 176.33 o -15 3 1 1960.56 2109.55 199.98 o -14 3 1 23.22 136.01 111.35 o -13 3 1 650.63 669.55 112.18 o -12 3 1 471.10 365.33 99.17 o -11 3 1 4202.75 4012.26 159.84 o -10 3 1 2914.72 2644.73 110.46 o -9 3 1 40.62 1.67 61.14 o -8 3 1 8523.19 8486.11 159.42 o -7 3 1 4628.22 4616.90 138.97 o -6 3 1 2729.14 2656.48 107.25 o -5 3 1 1432.79 1314.14 82.95 o -4 3 1 5495.01 5481.56 126.97 o -3 3 1 155.87 269.85 58.43 o -2 3 1 4461.65 4058.17 101.25 o -1 3 1 38.60 -49.57 49.57 o 0 3 1 2067.64 1940.99 106.60 o 1 3 1 3001.45 2984.75 95.31 o 2 3 1 11433.88 11385.96 205.48 o 3 3 1 4345.27 4180.52 122.14 o 4 3 1 9584.58 9298.92 174.91 o 5 3 1 9960.67 9875.82 190.99 o 6 3 1 453.20 465.73 69.46 o 7 3 1 486.13 499.07 67.31 o 8 3 1 98.15 66.44 61.67 o 9 3 1 1286.38 1121.74 85.96 o 10 3 1 2191.28 2046.13 106.10 o 11 3 1 81.44 79.33 75.50 o 12 3 1 1473.25 1443.09 120.64 o 13 3 1 1.99 40.80 110.92 o 14 3 1 13.68 89.53 137.48 o 15 3 1 17.80 165.37 174.44 o 16 3 1 17.65 -84.05 173.09 o 17 3 1 64.74 -94.86 188.81 o 18 3 1 2.46 3.26 197.23 o 19 3 1 12.65 -202.23 202.23 o -19 4 1 155.83 170.95 221.40 o -18 4 1 315.82 97.45 217.52 o -17 4 1 29.76 -191.79 191.79 o -16 4 1 102.54 11.32 193.83 o -15 4 1 113.39 -5.29 131.61 o -14 4 1 82.67 87.19 115.95 o -13 4 1 1592.19 1840.26 168.57 o -12 4 1 2069.92 2317.80 145.84 o -11 4 1 1680.91 1593.19 126.30 o -10 4 1 954.28 856.38 87.68 o -9 4 1 5247.27 5199.75 144.96 o -8 4 1 9219.42 9110.75 204.22 o -7 4 1 920.07 962.34 92.68 o -6 4 1 225.38 187.74 73.05 o -5 4 1 1884.76 1792.15 97.05 o -4 4 1 1439.57 1490.68 87.80 o -3 4 1 27988.03 27966.17 260.36 o -2 4 1 252.01 196.13 55.14 o -1 4 1 51.07 142.91 47.18 o 0 4 1 5570.99 5253.03 154.72 o 1 4 1 23781.44 24322.01 360.55 o 2 4 1 5588.63 5459.81 135.81 o 3 4 1 2024.07 2037.18 102.19 o 4 4 1 17148.38 17329.42 255.79 o 5 4 1 6344.76 6299.46 172.00 o 6 4 1 47.28 8.85 65.56 o 7 4 1 11567.90 12147.61 248.65 o 8 4 1 219.47 165.39 67.54 o 9 4 1 521.75 429.33 80.25 o 10 4 1 122.79 185.08 78.39 o 11 4 1 139.53 56.63 93.67 o 12 4 1 35.60 72.51 107.55 o 13 4 1 2162.22 2161.01 168.59 o 14 4 1 1425.62 1606.98 192.50 o 15 4 1 126.77 220.81 230.43 o 16 4 1 5.03 -59.93 167.88 o 17 4 1 42.73 14.93 190.55 o 18 4 1 103.77 -43.57 203.61 o 19 4 1 37.62 209.51 231.74 o -19 5 1 85.74 -116.11 199.07 o -18 5 1 11.51 -51.56 208.71 o -17 5 1 46.63 119.64 202.52 o -16 5 1 808.12 739.21 218.51 o -15 5 1 321.13 257.02 145.23 o -14 5 1 354.26 485.24 122.66 o -13 5 1 34.96 132.43 107.63 o -12 5 1 157.21 128.63 103.56 o -11 5 1 163.46 172.92 101.99 o -10 5 1 92.40 102.96 100.01 o -9 5 1 1034.22 1128.91 113.49 o -8 5 1 1895.37 2146.38 126.05 o -7 5 1 442.29 348.53 85.65 o -6 5 1 6865.37 7107.75 176.44 o -5 5 1 649.41 748.49 84.25 o -4 5 1 974.52 911.20 81.29 o -3 5 1 4272.14 3849.75 120.99 o -2 5 1 147.86 114.28 53.94 o -1 5 1 7875.22 7699.95 135.03 o 0 5 1 17288.21 17246.27 285.31 o 1 5 1 269.57 238.99 80.95 o 2 5 1 311.70 337.68 97.19 o 3 5 1 4970.58 4699.31 184.30 o 4 5 1 1315.79 1372.37 106.52 o 5 5 1 3493.97 4005.62 155.05 o 6 5 1 4148.16 4142.70 142.68 o 7 5 1 1100.65 1134.51 100.86 o 8 5 1 30.29 41.50 85.53 o 9 5 1 1486.95 1485.48 119.40 o 10 5 1 32.12 -44.88 75.36 o 11 5 1 9.07 -33.41 97.16 o 12 5 1 250.06 289.18 120.99 o 13 5 1 503.89 372.86 121.76 o 14 5 1 452.35 419.63 148.28 o 15 5 1 3.03 -35.05 131.95 o 16 5 1 38.08 45.12 199.53 o 17 5 1 0.15 -20.33 193.61 o 18 5 1 175.89 8.70 209.90 o -18 6 1 4.38 117.51 217.26 o -17 6 1 25.76 -49.32 189.05 o -16 6 1 1.04 -15.72 185.66 o -15 6 1 741.07 988.37 152.44 o -14 6 1 6.18 -77.00 101.96 o -13 6 1 1759.40 1759.97 146.35 o -12 6 1 1741.10 1736.56 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