#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/68/2206826.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2206826_Fobs loop_ _publ_author_name 'Gao, Jian' 'Liu, Yu' _publ_section_title ; Diaquabis(vanillinato-\k^2^O,O')manganese(II) ; _journal_coeditor_code XU6038 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1692 _journal_page_last m1693 _journal_volume 61 _journal_year 2005 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.564 _cell_angle_gamma 90.000 _cell_length_a 22.4629 _cell_length_b 10.5743 _cell_length_c 7.8600 _exptl_crystal_F_000 812.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file xu6038Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' liuy1 in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 245.62 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4160.98 0.64 0.64 o 4 0 0 9.44 29.26 4.24 o 6 0 0 37.10 30.32 3.18 o 8 0 0 5311.32 6140.26 127.01 o 10 0 0 6435.09 6319.01 33.71 o 12 0 0 859.37 711.82 19.30 o 14 0 0 3574.96 3748.02 46.22 o 16 0 0 3282.09 3317.16 42.20 o 18 0 0 3864.06 3963.03 44.53 o 20 0 0 412.17 431.71 14.63 o 22 0 0 1655.78 1682.12 38.59 o 24 0 0 221.25 229.00 18.02 o 26 0 0 67.92 56.19 14.21 o 1 1 0 4963.35 103.26 81.74 o 3 1 0 7797.16 7372.52 96.05 o 5 1 0 7989.08 8038.66 129.56 o 7 1 0 239.11 262.44 2.97 o 9 1 0 563.27 655.70 8.09 o 11 1 0 12.56 7.34 4.08 o 13 1 0 406.51 441.97 7.45 o 15 1 0 896.44 919.42 11.26 o 17 1 0 2345.71 2334.21 17.27 o 19 1 0 780.14 797.76 11.23 o 21 1 0 486.75 493.83 14.01 o 23 1 0 95.26 102.96 9.55 o 25 1 0 21.94 21.20 10.14 o 27 1 0 58.72 62.95 9.02 o 0 2 0 20738.18 20701.08 290.50 o 2 2 0 4430.26 4717.49 83.01 o 4 2 0 2336.53 2451.81 43.04 o 6 2 0 155.99 125.53 3.07 o 8 2 0 6292.98 6842.96 32.02 o 10 2 0 1105.60 1138.02 12.09 o 12 2 0 7.04 11.77 3.03 o 14 2 0 201.31 176.36 4.44 o 16 2 0 8.15 9.70 4.63 o 18 2 0 26.75 27.08 6.32 o 20 2 0 933.34 931.82 8.60 o 22 2 0 132.97 136.50 9.02 o 24 2 0 333.59 325.86 14.41 o 26 2 0 260.25 246.98 11.77 o 1 3 0 1849.23 1762.30 7.65 o 3 3 0 26799.66 27441.46 279.57 o 5 3 0 8716.37 8574.80 75.38 o 7 3 0 25011.93 25594.84 26.32 o 9 3 0 1648.81 1494.97 16.65 o 11 3 0 933.79 949.33 12.09 o 13 3 0 737.84 706.42 4.76 o 15 3 0 91.91 107.97 6.82 o 17 3 0 553.04 586.75 6.19 o 19 3 0 1532.14 1446.20 17.16 o 21 3 0 2177.46 2215.21 37.43 o 23 3 0 768.57 726.55 17.28 o 25 3 0 496.88 527.33 24.07 o 27 3 0 156.00 142.59 20.36 o 0 4 0 2519.56 2646.80 20.46 o 2 4 0 1109.02 1240.57 12.33 o 4 4 0 6831.82 7390.49 48.98 o 6 4 0 5775.55 6135.43 32.97 o 8 4 0 435.46 385.31 9.44 o 10 4 0 5255.71 5765.38 87.78 o 12 4 0 2199.96 2306.34 26.61 o 14 4 0 313.49 350.98 7.32 o 16 4 0 270.15 281.70 5.30 o 18 4 0 724.73 669.64 6.45 o 20 4 0 179.33 165.81 7.57 o 22 4 0 527.08 475.08 21.95 o 24 4 0 605.04 576.31 31.17 o 26 4 0 101.52 102.20 22.05 o 1 5 0 1000.39 945.95 13.46 o 3 5 0 5946.63 6338.75 38.38 o 5 5 0 129.62 152.52 4.86 o 7 5 0 47.44 53.59 2.42 o 9 5 0 1232.76 1297.78 8.27 o 11 5 0 470.98 544.02 10.18 o 13 5 0 62.30 68.20 3.09 o 15 5 0 1.78 0.67 3.09 o 17 5 0 269.25 261.74 5.19 o 19 5 0 606.17 547.60 18.02 o 21 5 0 344.17 331.54 20.57 o 23 5 0 66.76 55.33 5.77 o 25 5 0 16.84 23.32 18.87 o 0 6 0 3454.01 3309.14 7.42 o 2 6 0 9813.21 10159.16 24.55 o 4 6 0 3589.84 3794.38 19.25 o 6 6 0 69.51 75.42 5.82 o 8 6 0 519.58 476.49 3.89 o 10 6 0 596.23 618.59 4.01 o 12 6 0 420.77 449.92 6.57 o 14 6 0 2007.07 2046.00 13.04 o 16 6 0 2785.44 2668.28 10.21 o 18 6 0 753.38 722.20 22.58 o 20 6 0 381.57 386.62 17.39 o 22 6 0 4.57 6.15 18.66 o 24 6 0 490.06 492.78 26.29 o 1 7 0 629.46 608.86 6.16 o 3 7 0 3373.43 3537.55 14.84 o 5 7 0 12.95 25.43 6.62 o 7 7 0 1724.81 1871.26 36.68 o 9 7 0 917.31 961.81 12.51 o 11 7 0 1164.68 1127.31 5.42 o 13 7 0 1049.58 1011.56 12.62 o 15 7 0 1911.59 1781.39 19.61 o 17 7 0 135.84 149.91 21.20 o 19 7 0 226.57 194.36 28.52 o 21 7 0 154.41 166.66 18.66 o 23 7 0 20.62 22.26 21.20 o 0 8 0 210.82 187.06 11.77 o 2 8 0 167.76 180.14 6.21 o 4 8 0 268.96 270.57 5.55 o 6 8 0 26.30 26.93 4.05 o 8 8 0 113.40 114.28 5.47 o 10 8 0 1.21 1.71 3.27 o 12 8 0 243.48 225.05 3.40 o 14 8 0 10.11 8.86 2.52 o 16 8 0 341.96 272.13 5.25 o 18 8 0 6.19 14.63 14.21 o 20 8 0 7.60 8.69 21.63 o 22 8 0 17.41 36.90 22.69 o 1 9 0 547.20 549.16 10.18 o 3 9 0 338.20 340.39 7.00 o 5 9 0 1578.93 1571.76 8.43 o 7 9 0 563.27 555.56 5.43 o 9 9 0 847.10 836.71 11.34 o 11 9 0 883.45 821.83 9.25 o 13 9 0 704.02 655.94 14.52 o 15 9 0 107.91 106.23 16.33 o 17 9 0 146.29 162.63 16.54 o 19 9 0 164.22 140.79 25.23 o 21 9 0 238.46 245.33 24.17 o 0 10 0 131.33 125.93 5.62 o 2 10 0 268.76 266.56 7.02 o 4 10 0 188.39 165.60 8.48 o 6 10 0 644.64 627.61 11.03 o 8 10 0 1719.19 1612.16 24.28 o 10 10 0 664.76 653.46 6.41 o 12 10 0 623.65 555.72 43.47 o 14 10 0 208.42 203.13 27.78 o 16 10 0 35.61 47.71 16.75 o 18 10 0 177.36 178.33 19.72 o 1 11 0 8.16 11.66 9.54 o 3 11 0 32.74 24.20 6.26 o 5 11 0 141.80 136.38 6.79 o 7 11 0 40.05 36.04 5.67 o 9 11 0 17.10 17.97 5.62 o 11 11 0 9.89 3.60 17.60 o 13 11 0 2.70 18.45 17.81 o 15 11 0 140.22 175.78 18.66 o 0 12 0 260.64 254.87 9.97 o 2 12 0 245.64 226.67 12.72 o 4 12 0 8.98 19.51 13.15 o 6 12 0 129.34 125.53 17.60 o 8 12 0 598.60 557.45 15.90 o 10 12 0 249.56 268.02 19.08 o 12 12 0 155.66 162.42 16.75 o 1 13 0 328.45 298.13 11.66 o 3 13 0 2.92 7.21 11.66 o 5 13 0 409.97 372.77 24.38 o 7 13 0 69.21 90.33 13.78 o 9 13 0 344.15 342.44 29.26 o -27 1 1 351.23 344.50 14.31 o -25 1 1 589.82 599.01 18.28 o -23 1 1 1150.99 1144.84 19.93 o -21 1 1 16.98 24.99 6.83 o -19 1 1 110.23 112.88 8.06 o -17 1 1 872.83 812.77 7.25 o -15 1 1 62.18 48.98 3.67 o -13 1 1 2001.70 2050.68 56.19 o -11 1 1 17318.21 18528.08 133.37 o -9 1 1 1527.25 1449.08 9.97 o -7 1 1 996.18 1000.32 2.23 o -5 1 1 1084.02 1119.64 10.22 o -3 1 1 23694.38 23107.96 88.21 o -1 1 1 48269.73 43888.79 225.86 o 1 1 1 726.20 651.47 7.21 o 3 1 1 3460.80 3447.43 21.48 o 5 1 1 34.61 48.71 3.65 o 7 1 1 54.44 42.81 9.65 o 9 1 1 89.11 48.98 5.55 o 11 1 1 4283.41 4217.10 57.57 o 13 1 1 4357.81 4506.72 23.84 o 15 1 1 2678.07 2760.41 21.02 o 17 1 1 6291.38 6469.25 45.77 o 19 1 1 7.05 8.59 6.91 o 21 1 1 44.88 48.73 7.34 o 23 1 1 384.63 381.23 8.25 o 25 1 1 149.15 154.15 9.01 o -28 2 1 352.65 365.94 22.05 o -26 2 1 234.81 233.69 12.23 o -24 2 1 131.27 147.02 11.75 o -22 2 1 1578.08 1561.48 28.41 o -20 2 1 425.02 420.88 7.21 o -18 2 1 541.96 572.72 20.36 o -16 2 1 1425.86 1381.87 22.48 o -14 2 1 2049.16 2107.45 9.97 o -12 2 1 10.21 24.07 3.90 o -10 2 1 7241.87 7484.16 44.00 o -8 2 1 1278.09 1400.92 25.66 o -6 2 1 20113.25 20146.33 198.68 o -4 2 1 60331.19 57920.46 398.32 o -2 2 1 3298.21 3803.47 10.89 o 0 2 1 13298.29 13153.22 15.63 o 2 2 1 178.01 172.22 6.25 o 4 2 1 2846.11 2640.94 38.49 o 6 2 1 8837.84 8937.33 115.03 o 8 2 1 1780.83 1694.93 17.74 o 10 2 1 3534.78 3821.98 26.70 o 12 2 1 1476.53 1549.03 8.26 o 14 2 1 1426.14 1442.36 13.03 o 16 2 1 525.20 523.29 6.89 o 18 2 1 3939.67 3938.84 41.16 o 20 2 1 998.05 997.55 9.43 o 22 2 1 345.58 348.25 8.34 o 24 2 1 166.44 169.24 9.97 o 26 2 1 1.25 6.29 9.31 o -27 3 1 3.37 8.98 8.64 o -25 3 1 148.97 145.58 9.19 o -23 3 1 0.15 0.64 15.27 o -21 3 1 31.39 29.07 6.47 o -19 3 1 412.96 390.79 6.83 o -17 3 1 303.23 318.62 5.86 o -15 3 1 711.70 762.46 6.69 o -13 3 1 143.46 162.62 5.94 o -11 3 1 427.94 370.45 8.91 o -9 3 1 128.35 177.81 3.77 o -7 3 1 412.25 420.14 13.57 o -5 3 1 1348.26 1387.46 26.29 o -3 3 1 36625.49 36700.08 129.98 o -1 3 1 7091.75 7549.83 20.04 o 1 3 1 6712.00 7337.02 23.22 o 3 3 1 700.40 823.62 5.52 o 5 3 1 3973.59 4118.91 46.12 o 7 3 1 74.43 75.36 4.14 o 9 3 1 70.04 73.06 6.42 o 11 3 1 236.09 266.82 4.41 o 13 3 1 103.83 110.95 4.04 o 15 3 1 127.01 128.69 3.61 o 17 3 1 55.62 52.71 4.55 o 19 3 1 113.48 114.86 8.78 o 21 3 1 418.55 401.81 8.68 o 23 3 1 84.18 96.72 8.28 o 25 3 1 110.07 118.70 10.32 o -26 4 1 246.73 246.08 14.16 o -24 4 1 595.57 582.59 9.14 o -22 4 1 490.90 462.58 7.85 o -20 4 1 1227.31 1138.23 9.09 o -18 4 1 2.01 -1.87 8.50 o -16 4 1 4.19 4.19 4.82 o -14 4 1 202.90 193.62 8.66 o -12 4 1 82.05 55.16 6.77 o -10 4 1 680.73 664.31 8.38 o -8 4 1 13341.63 14830.30 27.35 o -6 4 1 15783.41 17105.50 78.67 o -4 4 1 13051.74 13803.49 133.16 o -2 4 1 887.24 852.18 4.43 o 0 4 1 1523.85 1657.76 32.76 o 2 4 1 458.89 455.02 11.45 o 4 4 1 1859.12 1746.93 33.40 o 6 4 1 994.51 873.24 6.57 o 8 4 1 1213.96 1118.51 9.12 o 10 4 1 4604.34 5141.92 68.81 o 12 4 1 356.58 387.93 7.26 o 14 4 1 1258.65 1223.49 12.02 o 16 4 1 567.27 532.13 6.32 o 18 4 1 373.34 373.17 11.78 o 20 4 1 2056.32 2036.99 31.61 o 22 4 1 3.71 11.70 7.50 o 24 4 1 103.11 131.04 19.30 o -25 5 1 557.11 497.51 28.41 o -23 5 1 128.55 133.15 12.62 o -21 5 1 471.20 522.26 7.60 o -19 5 1 1430.02 1352.80 22.37 o -17 5 1 761.75 793.72 7.16 o -15 5 1 402.11 391.25 5.67 o -13 5 1 1045.85 1063.54 13.68 o -11 5 1 1382.61 1494.20 7.26 o -9 5 1 2501.36 2666.84 24.38 o -7 5 1 15695.72 16933.86 83.01 o -5 5 1 16.80 16.26 3.37 o -3 5 1 1664.62 1684.60 10.39 o -1 5 1 5999.85 6267.31 89.91 o 1 5 1 4018.91 3783.92 15.36 o 3 5 1 5466.46 5514.32 77.50 o 5 5 1 129.81 97.03 4.79 o 7 5 1 3848.18 3916.36 75.59 o 9 5 1 1952.40 1969.16 13.78 o 11 5 1 2661.36 2694.82 29.05 o 13 5 1 2756.52 2728.68 23.50 o 15 5 1 1786.85 1773.83 20.81 o 17 5 1 66.94 65.78 3.18 o 19 5 1 26.97 23.55 3.48 o 21 5 1 889.93 867.03 46.44 o 23 5 1 284.31 314.88 37.11 o 25 5 1 310.29 338.20 24.60 o -24 6 1 4.67 3.39 20.99 o -22 6 1 159.24 170.90 28.84 o -20 6 1 1.37 1.13 5.27 o -18 6 1 244.40 241.80 5.97 o -16 6 1 225.12 226.20 5.22 o -14 6 1 369.36 369.98 5.22 o -12 6 1 445.48 456.96 5.10 o -10 6 1 74.78 86.17 4.66 o -8 6 1 257.30 278.28 4.11 o -6 6 1 1563.67 1695.52 7.53 o -4 6 1 1116.98 1173.98 5.70 o -2 6 1 207.84 178.87 4.88 o 0 6 1 41.15 41.54 4.58 o 2 6 1 971.30 994.25 7.74 o 4 6 1 43.57 58.13 5.04 o 6 6 1 2374.49 2483.63 31.38 o 8 6 1 2057.82 2125.85 168.89 o 10 6 1 183.87 176.31 7.34 o 12 6 1 95.35 79.52 9.54 o 14 6 1 168.08 158.18 25.44 o 16 6 1 244.55 203.13 10.81 o 18 6 1 9.99 14.42 17.60 o 20 6 1 28.90 20.36 15.05 o 22 6 1 2.46 2.97 16.12 o 24 6 1 401.52 446.56 33.29 o -23 7 1 16.28 20.57 19.30 o -21 7 1 17.50 23.20 8.38 o -19 7 1 171.33 160.30 24.60 o -17 7 1 680.68 601.30 6.57 o -15 7 1 343.00 336.92 5.55 o -13 7 1 621.98 630.12 5.79 o -11 7 1 34.12 39.66 4.19 o -9 7 1 1104.84 1186.15 7.63 o -7 7 1 630.02 636.65 5.70 o -5 7 1 49.13 66.98 4.72 o -3 7 1 2201.27 2220.65 8.34 o -1 7 1 2871.00 2879.09 9.84 o 1 7 1 5373.76 5605.50 22.37 o 3 7 1 511.02 507.07 6.42 o 5 7 1 441.26 477.74 7.89 o 7 7 1 225.95 230.01 7.72 o 9 7 1 22.75 31.53 8.36 o 11 7 1 38.08 50.89 10.39 o 13 7 1 1953.94 1939.11 39.65 o 15 7 1 1338.84 1321.43 25.44 o 17 7 1 145.99 151.18 20.36 o 19 7 1 154.96 155.00 14.42 o 21 7 1 114.08 118.95 17.39 o 23 7 1 94.59 107.08 22.26 o -22 8 1 206.23 216.49 28.84 o -20 8 1 377.51 380.82 27.14 o -18 8 1 490.73 456.93 6.50 o -16 8 1 850.33 861.81 7.44 o -14 8 1 1533.24 1540.68 54.71 o -12 8 1 1666.78 1624.55 9.50 o -10 8 1 231.85 233.37 5.12 o -8 8 1 727.97 727.69 6.07 o -6 8 1 81.48 79.99 4.62 o -4 8 1 809.36 823.28 15.90 o -2 8 1 2557.38 2567.22 14.84 o 0 8 1 1425.25 1335.80 13.68 o 2 8 1 3742.85 3927.96 29.26 o 4 8 1 2334.84 2291.56 13.18 o 6 8 1 1282.46 1292.14 11.02 o 8 8 1 789.53 798.92 9.56 o 10 8 1 683.74 678.95 12.93 o 12 8 1 399.85 381.04 17.81 o 14 8 1 562.31 568.48 20.57 o 16 8 1 465.29 463.52 21.20 o 18 8 1 346.05 342.23 18.66 o -21 9 1 110.33 117.68 22.69 o -19 9 1 225.56 230.70 38.59 o -17 9 1 162.42 141.67 14.84 o -15 9 1 590.39 547.20 6.90 o -13 9 1 269.96 256.10 10.60 o -11 9 1 289.97 298.80 5.94 o -9 9 1 112.28 111.97 5.35 o -7 9 1 25.47 30.35 8.12 o -5 9 1 5.18 11.80 5.77 o -3 9 1 317.29 344.28 6.51 o -1 9 1 129.15 139.54 6.93 o 1 9 1 1.37 4.79 6.35 o 3 9 1 2227.17 2267.68 16.22 o 5 9 1 1223.11 1244.38 12.09 o 7 9 1 221.10 218.49 13.89 o 9 9 1 187.50 198.26 20.57 o 11 9 1 117.16 130.62 14.63 o 13 9 1 285.11 260.81 17.18 o 15 9 1 64.81 67.22 14.84 o 17 9 1 122.50 114.08 17.18 o 19 9 1 192.06 199.74 23.54 o -18 10 1 1.49 5.73 31.38 o -16 10 1 3.95 18.45 13.99 o -14 10 1 3.85 6.00 14.31 o -12 10 1 47.36 48.97 8.86 o -10 10 1 262.08 254.87 6.28 o -8 10 1 85.04 90.73 6.39 o -6 10 1 2141.29 2251.21 51.53 o -4 10 1 91.22 76.44 7.74 o -2 10 1 1.75 9.76 7.17 o 0 10 1 24.35 22.93 7.13 o 2 10 1 64.68 68.48 8.09 o 4 10 1 658.95 639.09 25.44 o 6 10 1 135.28 142.16 10.71 o 8 10 1 182.51 162.42 16.96 o 10 10 1 559.15 534.13 17.39 o 12 10 1 348.79 339.05 25.44 o 14 10 1 24.05 17.39 24.81 o 16 10 1 26.61 29.05 26.29 o 18 10 1 13.93 35.62 22.05 o -17 11 1 197.61 202.71 28.20 o -15 11 1 370.21 361.53 30.75 o -13 11 1 175.80 146.45 22.48 o -11 11 1 383.58 345.93 6.82 o -9 11 1 577.22 535.68 8.37 o -7 11 1 7.74 10.79 6.55 o -5 11 1 1313.51 1338.47 23.54 o -3 11 1 622.53 606.74 10.71 o -1 11 1 132.38 132.41 8.22 o 1 11 1 119.10 112.82 8.63 o 3 11 1 230.07 242.19 19.61 o 5 11 1 1424.31 1453.70 67.64 o 7 11 1 1008.73 931.70 45.38 o 9 11 1 1039.20 1003.16 17.81 o 11 11 1 221.65 214.58 18.87 o 13 11 1 46.63 45.38 14.84 o 15 11 1 48.53 56.40 27.14 o -14 12 1 71.29 78.67 27.99 o -12 12 1 160.43 179.17 19.08 o -10 12 1 182.63 181.37 13.10 o -8 12 1 251.11 248.36 8.17 o -6 12 1 2.31 5.69 6.77 o -4 12 1 15.85 22.56 8.02 o -2 12 1 202.38 196.47 8.92 o 0 12 1 218.67 209.74 9.82 o 2 12 1 103.95 120.35 14.42 o 4 12 1 71.08 72.94 19.30 o 6 12 1 176.54 188.93 16.75 o 8 12 1 304.40 296.43 17.18 o 10 12 1 52.01 53.01 18.66 o 12 12 1 109.59 109.62 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16.36 o -13 1 9 75.39 68.78 15.02 o -11 1 9 154.86 163.51 19.72 o -9 1 9 371.54 377.15 22.85 o -7 1 9 244.52 242.39 15.16 o -5 1 9 99.93 101.45 15.11 o -3 1 9 249.54 263.33 17.96 o -1 1 9 25.44 21.22 13.88 o 1 1 9 54.25 51.15 15.63 o 3 1 9 236.70 259.04 20.00 o 5 1 9 27.39 29.37 13.45 o -18 2 9 168.21 154.12 15.11 o -16 2 9 6.05 12.15 15.60 o -14 2 9 152.22 148.90 12.90 o -12 2 9 83.38 104.99 13.85 o -10 2 9 104.50 110.78 13.77 o -8 2 9 750.23 741.42 19.46 o -6 2 9 144.61 159.20 14.05 o -4 2 9 248.71 235.82 16.46 o -2 2 9 103.44 113.02 15.59 o 0 2 9 144.26 145.94 17.62 o 2 2 9 0.80 4.64 15.21 o 4 2 9 47.03 53.84 17.06 o -19 3 9 39.21 55.49 14.83 o -17 3 9 6.78 13.61 11.62 o -15 3 9 0.25 1.29 14.26 o -13 3 9 0.39 -1.24 11.97 o -11 3 9 26.72 32.98 12.82 o -9 3 9 2.57 -0.86 12.99 o -7 3 9 32.56 30.82 14.12 o -5 3 9 61.64 60.99 14.38 o -3 3 9 0.16 11.04 11.41 o -1 3 9 3.28 0.05 15.13 o 1 3 9 64.33 55.67 12.52 o 3 3 9 8.37 9.65 11.55 o -16 4 9 61.09 83.84 11.77 o -14 4 9 1.30 6.94 12.10 o 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36.84 48.28 13.59 o -6 2 10 5.79 16.72 18.70 o