#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/73/2207399.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2207399_Fobs
loop_
_publ_author_name
'Cui, Yun-Cheng'
'Che, Guang-Bo'
'Liu, Chun-Bo'
'Li, Chuan-Bi'
_publ_section_title
;
 Diazido[<i>N</i>,<i>N</i>-bis(2-pyridylmethyl-\k<i>N</i>)glycine-\k^2^<i>N</i>,<i>O</i>]copper(II)
 monohydrate
;
_journal_coeditor_code           WW6434
_journal_issue                   11
_journal_name_full               'Acta Crystallographica Section E'
_journal_page_first              m2355
_journal_page_last               m2356
_journal_volume                  61
_journal_year                    2005
_space_group_IT_number           9
_symmetry_space_group_name_Hall  'C -2yc'
_symmetry_space_group_name_H-M   'C 1 c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 114.072
_cell_angle_gamma                90.000
_cell_length_a                   13.5526
_cell_length_b                   9.5725
_cell_length_c                   14.3309
_exptl_crystal_F_000             868.00
_reflns_d_resolution_high        0.8257
_[local]_cod_data_source_file    ww6434Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' 2 in Cc'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            266.24
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
5 1 -17 311.87 291.63 20.51 o
7 1 -17 527.52 521.60 19.76 o
9 1 -17 209.13 205.74 11.80 o
6 2 -17 230.73 274.74 18.50 o
8 2 -17 782.74 779.64 25.93 o
6 0 -16 2667.28 2665.52 100.97 o
8 0 -16 1271.91 1307.52 53.83 o
10 0 -16 176.87 162.17 14.62 o
3 1 -16 932.06 1013.74 45.72 o
5 1 -16 1294.73 1349.22 54.24 o
7 1 -16 1379.37 1334.58 38.21 o
9 1 -16 41.13 43.24 6.78 o
11 1 -16 327.37 352.69 14.63 o
2 2 -16 511.91 516.89 27.15 o
4 2 -16 235.18 237.73 18.77 o
6 2 -16 319.06 325.89 20.18 o
8 2 -16 185.82 208.89 12.54 o
10 2 -16 107.68 126.23 9.24 o
3 3 -16 34.70 25.95 9.65 o
5 3 -16 201.87 207.29 16.49 o
7 3 -16 202.55 192.28 15.29 o
9 3 -16 61.14 61.87 7.26 o
4 4 -16 51.91 46.73 10.26 o
6 4 -16 63.74 65.57 9.86 o
8 4 -16 76.64 74.06 7.90 o
3 1 -15 487.04 461.85 24.81 o
5 1 -15 361.41 359.27 15.16 o
7 1 -15 239.16 275.95 12.93 o
9 1 -15 154.40 140.49 9.17 o
11 1 -15 193.81 193.11 9.16 o
13 1 -15 341.34 333.27 11.78 o
2 2 -15 355.22 375.23 22.79 o
4 2 -15 243.98 254.42 18.37 o
6 2 -15 320.35 328.57 20.05 o
8 2 -15 1331.29 1392.72 39.50 o
10 2 -15 324.98 341.94 11.92 o
12 2 -15 535.04 595.97 16.97 o
1 3 -15 474.05 483.98 26.01 o
3 3 -15 623.02 612.23 31.51 o
5 3 -15 408.24 442.95 24.07 o
7 3 -15 616.05 626.69 21.98 o
9 3 -15 980.43 1018.43 25.08 o
11 3 -15 567.08 590.63 16.78 o
2 4 -15 833.12 788.35 36.00 o
4 4 -15 1133.58 1112.49 47.60 o
6 4 -15 355.10 390.89 16.12 o
8 4 -15 1037.96 1050.04 31.62 o
10 4 -15 649.36 684.38 22.60 o
3 5 -15 685.22 713.39 32.25 o
5 5 -15 716.58 722.47 23.88 o
7 5 -15 897.76 911.45 28.68 o
9 5 -15 1068.88 1120.55 32.78 o
4 0 -14 775.34 794.51 33.12 o
6 0 -14 525.23 542.30 27.02 o
8 0 -14 1062.30 1110.35 45.45 o
10 0 -14 535.84 551.42 26.35 o
12 0 -14 1469.29 1487.79 42.42 o
14 0 -14 1201.75 1206.91 35.92 o
5 1 -14 759.00 773.83 23.87 o
7 1 -14 2769.14 2792.13 62.39 o
9 1 -14 292.05 323.98 11.17 o
11 1 -14 864.51 873.84 22.14 o
13 1 -14 1065.04 1030.12 22.14 o
0 2 -14 255.98 283.65 17.50 o
2 2 -14 449.66 482.90 26.28 o
4 2 -14 202.48 216.41 16.16 o
6 2 -14 600.06 635.26 17.89 o
8 2 -14 1573.31 1553.19 34.96 o
10 2 -14 545.75 556.46 12.93 o
12 2 -14 247.76 295.74 10.63 o
1 3 -14 141.24 120.76 9.15 o
3 3 -14 372.42 335.03 13.83 o
5 3 -14 552.70 546.90 13.76 o
7 3 -14 147.24 165.91 7.73 o
9 3 -14 271.93 275.26 8.16 o
11 3 -14 138.43 148.50 7.45 o
13 3 -14 127.21 134.87 10.95 o
0 4 -14 33.13 44.31 9.86 o
2 4 -14 206.78 194.15 15.22 o
4 4 -14 376.90 343.24 11.24 o
6 4 -14 230.19 235.53 8.88 o
8 4 -14 187.67 177.46 7.02 o
10 4 -14 36.59 36.15 4.62 o
12 4 -14 592.76 516.06 20.45 o
1 5 -14 324.25 323.28 20.92 o
3 5 -14 501.22 474.74 18.19 o
5 5 -14 270.32 254.67 12.13 o
7 5 -14 484.07 474.01 16.77 o
9 5 -14 284.30 248.14 10.76 o
11 5 -14 312.73 320.12 23.53 o
2 6 -14 715.79 727.95 25.05 o
4 6 -14 660.91 660.08 22.57 o
6 6 -14 952.83 976.41 30.09 o
8 6 -14 1077.08 1103.81 31.52 o
1 1 -13 535.93 569.72 27.42 o
3 1 -13 360.51 377.18 21.19 o
5 1 -13 4.95 6.41 4.19 o
7 1 -13 334.40 323.87 9.74 o
9 1 -13 911.27 913.07 20.10 o
11 1 -13 47.90 51.28 4.53 o
13 1 -13 100.66 113.73 6.02 o
2 2 -13 1634.87 1667.20 63.76 o
4 2 -13 725.13 733.94 26.39 o
6 2 -13 883.81 950.10 20.59 o
8 2 -13 1193.51 1249.54 26.04 o
10 2 -13 793.50 806.05 16.79 o
12 2 -13 325.51 352.13 11.26 o
14 2 -13 402.69 394.73 16.80 o
-1 3 -13 383.97 414.39 16.18 o
1 3 -13 705.33 724.89 22.16 o
3 3 -13 649.89 658.44 17.54 o
5 3 -13 1181.48 1164.59 23.70 o
7 3 -13 2782.18 2677.40 48.56 o
9 3 -13 1781.99 1801.30 34.23 o
11 3 -13 407.69 459.03 13.20 o
13 3 -13 761.77 819.66 27.41 o
-2 4 -13 777.84 836.08 38.62 o
0 4 -13 1182.16 1195.96 34.43 o
2 4 -13 1177.06 1203.79 27.98 o
4 4 -13 595.76 588.24 14.42 o
6 4 -13 1296.23 1264.56 28.01 o
8 4 -13 1804.12 1755.42 47.98 o
10 4 -13 1197.42 1226.56 29.24 o
12 4 -13 510.05 552.87 21.11 o
-1 5 -13 1086.04 1085.31 33.14 o
1 5 -13 1623.68 1562.47 44.00 o
3 5 -13 1073.93 1075.97 25.64 o
5 5 -13 1249.69 1243.08 28.80 o
7 5 -13 755.81 760.91 24.31 o
9 5 -13 643.59 625.43 34.73 o
11 5 -13 159.90 160.64 11.40 o
0 6 -13 741.88 735.08 25.25 o
2 6 -13 389.25 400.12 16.32 o
4 6 -13 705.00 723.46 18.33 o
6 6 -13 547.71 534.01 18.01 o
8 6 -13 225.90 220.97 20.65 o
10 6 -13 200.71 214.53 19.64 o
1 7 -13 16.11 16.07 6.86 o
3 7 -13 75.87 90.98 8.54 o
5 7 -13 119.55 127.78 8.76 o
7 7 -13 89.44 78.44 13.74 o
9 7 -13 95.35 100.76 15.22 o
2 0 -12 91.12 106.46 11.46 o
6 0 -12 2196.20 2214.27 50.01 o
8 0 -12 5628.40 5617.68 121.16 o
10 0 -12 2233.94 2185.25 58.72 o
12 0 -12 1078.99 1132.24 33.13 o
14 0 -12 727.80 819.25 25.70 o
1 1 -12 1210.49 1187.18 45.66 o
3 1 -12 230.15 227.49 10.54 o
5 1 -12 1642.69 1644.17 32.94 o
7 1 -12 4313.74 4291.02 73.23 o
9 1 -12 1542.43 1573.59 28.17 o
11 1 -12 700.72 783.52 17.25 o
13 1 -12 1568.19 1552.33 35.07 o
15 1 -12 613.82 630.91 21.62 o
-2 2 -12 432.93 461.32 25.14 o
0 2 -12 696.27 714.87 31.24 o
2 2 -12 640.06 628.18 26.82 o
4 2 -12 2040.86 2057.30 39.01 o
6 2 -12 1449.60 1477.51 29.26 o
8 2 -12 2338.99 2426.79 46.36 o
10 2 -12 860.17 891.82 17.99 o
12 2 -12 258.21 277.01 9.46 o
14 2 -12 935.38 879.85 44.42 o
-3 3 -12 293.92 267.56 18.44 o
-1 3 -12 389.67 382.47 15.30 o
1 3 -12 979.97 958.35 23.12 o
3 3 -12 391.66 384.94 10.73 o
5 3 -12 292.07 293.27 8.43 o
7 3 -12 859.93 834.87 15.86 o
9 3 -12 784.84 784.93 15.84 o
11 3 -12 270.14 247.40 8.33 o
13 3 -12 167.01 151.17 10.78 o
-2 4 -12 78.54 76.60 7.68 o
0 4 -12 350.36 355.40 11.71 o
2 4 -12 357.05 375.55 10.39 o
4 4 -12 147.53 125.71 5.71 o
6 4 -12 251.30 267.96 7.92 o
8 4 -12 329.40 316.64 10.23 o
10 4 -12 50.22 51.24 7.23 o
12 4 -12 211.17 190.79 11.68 o
14 4 -12 86.47 72.20 8.68 o
-3 5 -12 301.16 283.84 14.53 o
-1 5 -12 183.54 192.66 9.10 o
1 5 -12 66.38 64.53 5.54 o
3 5 -12 877.08 809.39 19.68 o
5 5 -12 448.87 408.34 11.16 o
7 5 -12 731.63 679.75 21.36 o
9 5 -12 369.50 369.00 24.94 o
11 5 -12 283.27 316.70 15.13 o
13 5 -12 123.91 134.71 11.20 o
-2 6 -12 797.49 777.36 26.45 o
0 6 -12 1254.18 1216.97 36.53 o
2 6 -12 1388.89 1350.82 31.02 o
4 6 -12 840.56 841.67 19.98 o
6 6 -12 765.05 772.26 24.38 o
8 6 -12 379.46 371.34 24.54 o
10 6 -12 74.31 108.94 14.41 o
12 6 -12 198.80 241.42 22.26 o
-1 7 -12 851.02 867.33 28.80 o
1 7 -12 1451.65 1449.73 42.34 o
3 7 -12 1501.28 1546.12 34.08 o
5 7 -12 979.14 1015.95 29.25 o
7 7 -12 1028.97 995.71 47.20 o
9 7 -12 168.77 248.32 20.45 o
2 8 -12 358.14 377.35 15.82 o
4 8 -12 1021.49 996.84 29.30 o
6 8 -12 1141.21 1129.45 51.35 o
1 1 -11 391.25 395.21 19.98 o
3 1 -11 692.70 774.21 17.53 o
5 1 -11 813.78 853.56 17.31 o
7 1 -11 1310.49 1252.80 20.99 o
9 1 -11 125.55 124.15 4.98 o
11 1 -11 443.99 428.60 10.79 o
13 1 -11 306.23 288.67 9.41 o
15 1 -11 113.90 133.23 12.37 o
-2 2 -11 1643.20 1682.15 63.29 o
0 2 -11 1740.71 1750.40 69.32 o
2 2 -11 4406.17 4620.28 100.12 o
4 2 -11 590.10 568.72 13.53 o
6 2 -11 2468.80 2367.80 45.31 o
8 2 -11 1330.40 1356.00 24.04 o
10 2 -11 722.33 735.64 14.89 o
12 2 -11 1895.22 1817.20 39.26 o
14 2 -11 960.06 1029.73 31.43 o
-3 3 -11 626.34 656.34 31.98 o
-1 3 -11 2107.38 2132.95 44.54 o
1 3 -11 5172.15 5011.89 91.14 o
3 3 -11 3462.17 3440.16 63.65 o
5 3 -11 3052.05 3158.20 51.67 o
7 3 -11 4321.55 4310.37 69.83 o
9 3 -11 991.14 1022.49 23.99 o
11 3 -11 1216.81 1194.61 34.70 o
13 3 -11 1533.07 1484.64 43.01 o
15 3 -11 1135.29 1169.51 35.85 o
-4 4 -11 1370.56 1405.33 56.85 o
-2 4 -11 1549.84 1567.55 34.27 o
0 4 -11 1000.34 1018.35 23.41 o
2 4 -11 3121.87 3200.59 59.49 o
4 4 -11 1850.70 1813.43 35.07 o
6 4 -11 3306.55 3341.39 61.90 o
8 4 -11 1127.76 1110.15 25.66 o
10 4 -11 547.34 585.16 20.51 o
12 4 -11 834.03 900.60 28.50 o
14 4 -11 797.31 847.41 28.01 o
-5 5 -11 720.51 743.90 37.74 o
-3 5 -11 1461.13 1431.40 33.48 o
-1 5 -11 1622.72 1653.21 36.15 o
1 5 -11 1211.95 1226.29 25.66 o
3 5 -11 642.62 658.08 14.87 o
5 5 -11 481.74 485.47 12.71 o
7 5 -11 992.66 947.73 26.34 o
9 5 -11 116.77 125.77 14.55 o
11 5 -11 500.23 533.92 21.89 o
13 5 -11 207.26 248.45 13.60 o
-4 6 -11 310.47 296.09 15.12 o
-2 6 -11 381.12 414.50 24.07 o
0 6 -11 599.50 605.53 16.39 o
2 6 -11 158.91 181.58 7.67 o
4 6 -11 260.65 262.35 8.09 o
6 6 -11 169.40 173.62 7.82 o
8 6 -11 38.65 49.34 10.46 o
10 6 -11 133.18 133.21 16.69 o
12 6 -11 339.75 328.31 16.27 o
-3 7 -11 83.19 75.78 8.96 o
-1 7 -11 28.57 28.97 6.96 o
1 7 -11 186.45 177.70 11.02 o
3 7 -11 6.03 16.42 4.90 o
5 7 -11 157.75 142.03 7.25 o
7 7 -11 80.89 76.43 13.21 o
9 7 -11 13.57 17.50 10.26 o
11 7 -11 120.76 110.08 15.49 o
0 8 -11 68.94 51.50 7.38 o
2 8 -11 216.55 209.37 11.16 o
4 8 -11 311.21 299.93 11.02 o
6 8 -11 35.42 34.33 11.20 o
8 8 -11 1.77 2.21 10.26 o
2 0 -10 2846.18 2694.06 72.31 o
4 0 -10 6578.92 6578.07 147.69 o
6 0 -10 2703.59 2446.14 54.32 o
8 0 -10 4891.96 5183.64 111.47 o
10 0 -10 609.96 687.86 21.28 o
12 0 -10 336.34 379.64 14.11 o
14 0 -10 1079.64 995.39 29.37 o
1 1 -10 3797.49 3897.22 81.89 o
3 1 -10 1930.96 1778.43 30.68 o
5 1 -10 692.72 598.10 11.15 o
7 1 -10 3886.53 3858.26 59.40 o
9 1 -10 4476.63 4481.91 74.06 o
11 1 -10 4.15 7.37 2.72 o
13 1 -10 987.06 975.34 22.87 o
15 1 -10 721.68 717.31 23.09 o
-2 2 -10 992.27 993.03 22.81 o
0 2 -10 3781.50 3868.87 81.66 o
2 2 -10 2800.81 3052.48 63.28 o
4 2 -10 2218.77 2194.05 38.75 o
6 2 -10 1296.38 1305.43 21.45 o
8 2 -10 2312.20 2296.18 35.23 o
10 2 -10 1735.92 1732.09 38.60 o
12 2 -10 554.05 572.58 19.57 o
14 2 -10 766.86 737.04 24.35 o
-3 3 -10 142.92 154.94 7.94 o
-1 3 -10 1199.86 1199.24 27.17 o
1 3 -10 1004.24 982.23 20.04 o
3 3 -10 879.21 840.34 17.23 o
5 3 -10 1260.57 1240.90 21.92 o
7 3 -10 954.58 968.49 17.63 o
9 3 -10 218.23 219.70 7.19 o
11 3 -10 78.47 82.31 7.28 o
13 3 -10 257.05 251.16 13.41 o
15 3 -10 220.37 194.58 11.77 o
-6 4 -10 157.51 147.96 16.56 o
-4 4 -10 453.39 426.64 13.45 o
-2 4 -10 745.90 747.36 18.72 o
0 4 -10 314.18 300.56 8.77 o
2 4 -10 785.82 806.22 17.23 o
4 4 -10 215.70 233.23 6.98 o
6 4 -10 218.17 214.71 6.07 o
8 4 -10 294.58 324.98 11.19 o
10 4 -10 26.67 48.07 8.58 o
12 4 -10 3.94 5.97 5.64 o
14 4 -10 60.39 48.59 7.39 o
-5 5 -10 393.86 379.62 13.17 o
-3 5 -10 332.16 329.38 11.67 o
-1 5 -10 344.98 319.63 12.03 o
1 5 -10 763.80 775.53 16.46 o
3 5 -10 1446.13 1357.44 27.39 o
5 5 -10 25.89 29.40 2.54 o
7 5 -10 259.84 226.80 16.16 o
9 5 -10 162.03 148.65 9.97 o
11 5 -10 146.58 145.96 10.00 o
13 5 -10 284.28 308.65 17.13 o
-4 6 -10 795.62 805.59 27.12 o
-2 6 -10 1093.47 1047.67 25.42 o
0 6 -10 861.01 806.82 18.03 o
2 6 -10 275.17 299.11 8.78 o
4 6 -10 77.25 61.96 5.86 o
6 6 -10 332.49 328.44 20.45 o
8 6 -10 364.93 385.16 22.59 o
10 6 -10 741.17 756.70 38.15 o
12 6 -10 418.43 434.52 18.46 o
-3 7 -10 1051.55 1065.29 33.42 o
-1 7 -10 1694.12 1668.98 47.52 o
1 7 -10 2636.33 2570.32 54.56 o
3 7 -10 603.53 592.41 19.94 o
5 7 -10 344.69 342.32 21.39 o
7 7 -10 620.06 603.18 33.52 o
9 7 -10 662.95 666.33 35.20 o
11 7 -10 934.81 985.92 46.80 o
-2 8 -10 370.35 399.19 16.98 o
0 8 -10 3434.97 3188.76 85.00 o
2 8 -10 1294.67 1359.92 38.95 o
4 8 -10 1066.86 1122.88 49.68 o
6 8 -10 978.38 937.65 44.78 o
8 8 -10 1230.75 1191.07 56.72 o
10 8 -10 1038.63 1010.92 47.60 o
1 9 -10 758.89 715.30 23.37 o
3 9 -10 512.45 601.57 34.39 o
5 9 -10 803.49 802.83 40.29 o
7 9 -10 1341.44 1305.44 59.06 o
-1 1 -9 775.89 785.94 23.63 o
1 1 -9 1490.23 1583.76 28.68 o
3 1 -9 1257.42 1195.04 20.32 o
5 1 -9 1056.68 1056.04 15.98 o
7 1 -9 2095.02 2287.74 35.26 o
9 1 -9 356.08 352.91 8.95 o
11 1 -9 235.45 237.74 7.10 o
13 1 -9 272.91 266.73 8.17 o
15 1 -9 73.68 80.07 7.31 o
-4 2 -9 1296.37 1381.20 59.60 o
-2 2 -9 4793.58 5165.91 105.24 o
0 2 -9 1343.17 1249.64 30.10 o
2 2 -9 3551.60 3518.19 58.96 o
4 2 -9 1943.85 1797.50 31.92 o
6 2 -9 4268.36 4165.24 63.75 o
8 2 -9 3617.58 3650.92 58.91 o
10 2 -9 2859.67 2884.16 60.94 o
12 2 -9 1254.71 1165.20 33.22 o
14 2 -9 412.77 429.23 16.38 o
16 2 -9 257.62 298.57 13.37 o
-5 3 -9 888.53 952.60 39.02 o
-3 3 -9 3372.52 3468.29 72.23 o
-1 3 -9 7953.06 7933.56 142.89 o
1 3 -9 6114.55 6061.60 110.43 o
3 3 -9 2423.73 2321.04 39.46 o
5 3 -9 3054.57 3085.21 47.23 o
7 3 -9 8444.94 8450.48 153.79 o
9 3 -9 2483.22 2367.89 52.91 o
11 3 -9 2577.35 2563.99 68.26 o
13 3 -9 2054.60 1953.19 54.31 o
15 3 -9 729.66 747.89 24.88 o
-8 4 -9 1149.60 1234.71 52.90 o
-6 4 -9 1029.98 1128.18 46.12 o
-4 4 -9 372.46 391.73 12.43 o
-2 4 -9 4283.75 4383.30 89.98 o
0 4 -9 4813.70 4525.70 82.91 o
2 4 -9 3031.60 2956.44 56.36 o
4 4 -9 1016.68 955.85 19.69 o
6 4 -9 4024.36 4097.39 75.76 o
8 4 -9 2715.92 2840.27 59.97 o
10 4 -9 1398.22 1417.79 40.51 o
12 4 -9 1709.82 1624.44 47.24 o
14 4 -9 1231.98 1235.78 37.44 o
-7 5 -9 1549.87 1583.53 64.16 o
-5 5 -9 1403.53 1445.77 33.27 o
-3 5 -9 618.18 671.42 17.72 o
-1 5 -9 259.55 245.18 8.02 o
1 5 -9 1599.30 1473.43 28.43 o
3 5 -9 71.68 65.60 3.84 o
5 5 -9 949.43 907.89 21.94 o
7 5 -9 3188.11 3278.09 89.67 o
9 5 -9 160.16 169.41 9.74 o
11 5 -9 591.52 618.39 22.82 o
13 5 -9 551.45 550.51 20.55 o
-6 6 -9 387.65 392.55 17.47 o
-4 6 -9 524.50 534.18 19.69 o
-2 6 -9 412.73 411.40 12.56 o
0 6 -9 955.62 911.31 19.49 o
2 6 -9 452.71 430.64 10.41 o
4 6 -9 132.25 128.78 7.76 o
6 6 -9 757.64 730.96 33.12 o
8 6 -9 272.18 297.93 19.91 o
10 6 -9 9.63 18.64 8.72 o
12 6 -9 463.99 474.98 20.01 o
-5 7 -9 62.87 64.05 8.89 o
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