#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/74/2207406.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207406_Fobs loop_ _publ_author_name 'Cao, Qian-Yong' 'Huang, Li-Qun' 'Wang, Zhong-Wei' 'Yang, Chang-Jian' 'Gao, Xi-Cun' _publ_section_title ; Tris[4-(3-methyl-4-oxo-1-phenyl-4,5-dihydro-1H-pyrazol-4-ylidene)isobutanolato-\k^2^O,O']bis(triphenylphosphine oxide-\kO)europium(III) ; _journal_coeditor_code XU6061 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2414 _journal_page_last m2415 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.890 _cell_angle_gamma 90.000 _cell_length_a 13.3872 _cell_length_b 23.1865 _cell_length_c 23.1299 _exptl_crystal_F_000 2968.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file xu6061Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 50802E in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 498.45 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17463.61 17988.25 467.98 o 4 0 0 56709.44 56151.18 985.18 o 6 0 0 15292.45 15973.69 401.16 o 8 0 0 2316.64 2647.54 230.12 o 10 0 0 6212.50 5712.20 447.85 o 12 0 0 5037.34 4563.78 539.64 o 14 0 0 3498.61 3458.23 549.02 o 16 0 0 1377.15 794.90 536.77 o 1 1 0 136162.25 142581.84 2293.29 o 2 1 0 17021.54 17315.07 321.91 o 3 1 0 1760.81 1666.27 119.35 o 4 1 0 2979.78 3075.05 95.71 o 5 1 0 358.16 162.84 81.74 o 6 1 0 1670.71 1734.85 170.51 o 7 1 0 332.89 233.54 82.25 o 8 1 0 20335.04 20030.61 367.76 o 9 1 0 4172.69 3874.64 181.18 o 10 1 0 8243.74 8099.41 313.33 o 11 1 0 928.73 836.48 148.41 o 12 1 0 381.23 525.54 155.60 o 13 1 0 2212.30 2117.14 324.13 o 14 1 0 1750.69 1152.09 328.82 o 15 1 0 334.53 48.77 313.39 o 16 1 0 8.78 -64.30 349.30 o 17 1 0 234.09 92.46 409.76 o 0 2 0 7386.41 7245.87 217.61 o 1 2 0 4228.74 4670.55 116.80 o 2 2 0 86.16 120.20 36.36 o 3 2 0 35258.55 36502.05 483.48 o 4 2 0 2153.92 2088.29 114.55 o 5 2 0 752.08 894.89 76.82 o 6 2 0 0.53 -51.77 63.58 o 7 2 0 41415.69 42753.68 698.98 o 8 2 0 786.08 706.77 103.70 o 9 2 0 17364.09 16369.48 343.21 o 10 2 0 622.73 440.67 123.09 o 11 2 0 2215.30 2140.71 185.04 o 12 2 0 93.34 -8.10 149.23 o 13 2 0 2869.00 1988.58 364.56 o 14 2 0 42.86 97.28 281.21 o 15 2 0 166.00 351.26 476.99 o 16 2 0 132.03 -139.00 379.20 o 17 2 0 130.42 -463.52 852.30 o 1 3 0 18661.08 19482.36 596.67 o 2 3 0 18881.78 18395.61 362.20 o 3 3 0 1926.74 1961.33 77.05 o 4 3 0 26.42 4.76 50.94 o 5 3 0 42215.18 42650.80 576.24 o 6 3 0 1429.44 1468.92 102.92 o 7 3 0 6480.35 6991.37 303.84 o 8 3 0 2057.36 1983.85 139.05 o 9 3 0 1455.80 1181.60 135.07 o 10 3 0 659.33 580.38 132.72 o 11 3 0 1994.57 1888.33 181.19 o 12 3 0 1751.32 1406.56 357.94 o 13 3 0 4042.15 3821.88 382.71 o 14 3 0 102.31 -178.30 258.75 o 15 3 0 537.79 -109.57 453.48 o 16 3 0 83.53 -500.91 333.94 o 17 3 0 1093.72 954.74 439.14 o 0 4 0 1189.56 891.95 107.80 o 1 4 0 23056.44 24577.76 783.64 o 2 4 0 69993.17 73334.21 1237.61 o 3 4 0 2666.00 2714.35 108.30 o 4 4 0 4202.84 3605.24 128.92 o 5 4 0 9184.45 9346.07 200.72 o 6 4 0 12388.50 12151.88 249.29 o 7 4 0 100.72 44.84 78.14 o 8 4 0 244.33 196.07 95.06 o 9 4 0 130.00 130.94 124.37 o 10 4 0 667.07 360.16 121.96 o 11 4 0 25.50 -195.39 130.26 o 12 4 0 3599.56 3327.52 350.93 o 13 4 0 1.16 85.02 322.66 o 14 4 0 2706.44 2722.27 384.40 o 15 4 0 202.40 -479.88 319.92 o 16 4 0 1401.19 1403.83 425.63 o 1 5 0 13181.26 12912.48 301.44 o 2 5 0 8969.51 9560.78 293.60 o 3 5 0 81.39 18.95 53.37 o 4 5 0 19254.21 18506.89 344.35 o 5 5 0 7745.61 7948.19 188.34 o 6 5 0 20146.86 20523.33 355.69 o 7 5 0 471.88 441.47 94.03 o 8 5 0 7791.90 7299.73 219.17 o 9 5 0 69.81 -15.50 108.34 o 10 5 0 9919.64 9803.32 281.38 o 11 5 0 2012.84 1958.90 186.69 o 12 5 0 4744.40 4958.39 417.13 o 13 5 0 1037.18 1303.77 366.14 o 14 5 0 528.37 441.09 454.60 o 15 5 0 650.77 678.82 361.74 o 16 5 0 1.42 -140.08 385.87 o 0 6 0 17152.53 16593.55 536.77 o 1 6 0 884.18 832.11 77.45 o 2 6 0 25666.55 26577.17 437.30 o 3 6 0 9327.96 7854.86 197.29 o 4 6 0 7764.64 7429.52 200.18 o 5 6 0 52599.62 54330.38 728.69 o 6 6 0 694.31 686.08 93.62 o 7 6 0 6657.44 6344.37 289.40 o 8 6 0 62.99 -24.17 94.04 o 9 6 0 22361.22 21605.26 421.47 o 10 6 0 450.53 406.01 133.38 o 11 6 0 1503.00 1739.52 255.35 o 12 6 0 949.21 1028.20 387.38 o 13 6 0 1047.53 781.89 387.33 o 14 6 0 15.23 -10.21 447.72 o 15 6 0 409.39 124.98 349.59 o 16 6 0 531.90 -26.01 499.00 o 1 7 0 58157.17 59883.09 872.43 o 2 7 0 8586.03 9025.44 180.75 o 3 7 0 17831.49 17820.90 365.99 o 4 7 0 14234.89 13739.34 297.28 o 5 7 0 9608.26 10063.47 260.27 o 6 7 0 324.03 238.93 88.69 o 7 7 0 628.64 669.85 132.28 o 8 7 0 2232.35 2232.64 161.45 o 9 7 0 1432.49 1453.86 156.77 o 10 7 0 39.49 161.45 130.26 o 11 7 0 4169.22 4634.89 253.25 o 12 7 0 928.39 792.31 226.48 o 13 7 0 3926.09 4082.26 333.58 o 14 7 0 177.07 27.42 317.98 o 15 7 0 1517.46 1683.34 567.78 o 16 7 0 69.29 55.78 555.78 o 0 8 0 13044.56 12458.22 639.44 o 1 8 0 48.94 76.88 52.50 o 2 8 0 22236.17 22226.77 342.49 o 3 8 0 4082.51 4237.24 146.03 o 4 8 0 328.20 15.58 101.15 o 5 8 0 26472.83 28244.07 515.18 o 6 8 0 3340.93 3454.80 162.56 o 7 8 0 6258.33 6131.85 223.74 o 8 8 0 1077.40 875.08 130.65 o 9 8 0 5988.90 6005.57 230.13 o 10 8 0 170.55 172.93 136.83 o 11 8 0 428.58 379.71 179.32 o 12 8 0 3295.07 3559.66 440.01 o 13 8 0 41.69 96.00 224.10 o 14 8 0 561.94 342.92 442.47 o 15 8 0 3.21 -595.05 476.74 o 16 8 0 1478.69 1924.71 619.56 o 1 9 0 3736.81 3811.73 165.24 o 2 9 0 252.30 112.70 63.96 o 3 9 0 568.77 202.65 87.83 o 4 9 0 52439.09 53959.59 871.97 o 5 9 0 159.48 78.11 92.34 o 6 9 0 19514.29 18382.48 357.00 o 7 9 0 1583.52 1219.11 319.58 o 8 9 0 18545.67 18484.34 388.29 o 9 9 0 939.32 810.52 179.29 o 10 9 0 7484.12 7516.17 331.38 o 11 9 0 160.17 635.23 204.21 o 12 9 0 28.60 351.88 214.97 o 13 9 0 229.41 -53.01 257.58 o 14 9 0 485.46 108.05 460.23 o 15 9 0 9.21 449.22 545.27 o 16 9 0 3.80 301.65 580.54 o 0 10 0 70296.13 73283.21 1933.47 o 1 10 0 60.68 79.13 64.39 o 2 10 0 2996.02 2865.15 121.77 o 3 10 0 10738.59 10846.21 408.74 o 4 10 0 12726.58 13473.68 321.22 o 5 10 0 9529.87 8750.70 370.37 o 6 10 0 681.75 729.20 198.84 o 7 10 0 5530.67 6083.04 218.81 o 8 10 0 242.03 102.96 117.80 o 9 10 0 12405.49 12509.96 333.80 o 10 10 0 785.85 614.77 159.38 o 11 10 0 660.99 403.13 217.21 o 12 10 0 1086.57 1258.31 445.92 o 13 10 0 205.92 604.50 314.50 o 14 10 0 1208.06 1406.70 533.27 o 15 10 0 327.99 -155.83 484.74 o 16 10 0 391.18 670.59 587.79 o 1 11 0 29446.95 28761.83 472.91 o 2 11 0 98.43 -12.99 75.35 o 3 11 0 33830.91 33698.71 600.20 o 4 11 0 1128.41 1233.22 151.77 o 5 11 0 8828.62 9723.75 285.62 o 6 11 0 91.90 43.73 107.64 o 7 11 0 1677.84 1700.22 157.89 o 8 11 0 149.87 75.91 129.08 o 9 11 0 188.02 103.99 137.93 o 10 11 0 129.03 -161.96 143.02 o 11 11 0 3403.36 3648.03 390.19 o 12 11 0 191.27 28.25 276.07 o 13 11 0 2558.03 3584.09 876.31 o 14 11 0 51.45 -93.55 461.98 o 15 11 0 1064.62 630.57 525.51 o 0 12 0 5853.64 5943.02 240.55 o 1 12 0 199.59 62.53 91.71 o 2 12 0 6053.55 6225.63 184.71 o 3 12 0 8694.36 8522.73 230.62 o 4 12 0 4158.70 4466.23 208.33 o 5 12 0 2330.13 2346.76 208.15 o 6 12 0 115.96 26.80 120.28 o 7 12 0 10610.54 10762.33 295.56 o 8 12 0 39.64 -233.13 155.42 o 9 12 0 2529.29 3146.81 219.71 o 10 12 0 467.03 32.54 177.11 o 11 12 0 4328.40 5117.12 443.87 o 12 12 0 1779.06 1880.76 465.73 o 13 12 0 2201.25 3007.81 753.38 o 14 12 0 949.84 693.35 524.26 o 15 12 0 83.86 327.41 553.53 o 1 13 0 3625.62 3340.39 210.98 o 2 13 0 4831.70 4501.52 182.21 o 3 13 0 47.68 62.92 96.67 o 4 13 0 14608.83 14903.86 323.21 o 5 13 0 2353.39 2497.28 232.11 o 6 13 0 12483.51 11806.17 344.12 o 7 13 0 1637.16 1346.89 153.75 o 8 13 0 8853.27 8768.14 283.99 o 9 13 0 102.08 -132.50 165.62 o 10 13 0 6226.55 6863.23 323.70 o 11 13 0 363.18 123.56 263.01 o 12 13 0 1519.50 1916.86 376.12 o 13 13 0 41.38 358.87 329.54 o 14 13 0 946.53 1603.30 589.54 o 15 13 0 1.07 -88.79 547.77 o 0 14 0 19493.81 18256.38 488.27 o 1 14 0 71.11 -50.43 95.76 o 2 14 0 9703.18 9687.91 249.21 o 3 14 0 1219.02 1229.58 141.23 o 4 14 0 399.08 380.09 141.50 o 5 14 0 9330.32 9829.27 317.89 o 6 14 0 3794.64 3738.80 238.26 o 7 14 0 1530.39 1430.21 257.34 o 8 14 0 17.67 66.91 161.53 o 9 14 0 2759.88 2862.59 360.78 o 10 14 0 492.17 374.26 212.74 o 11 14 0 634.02 794.75 440.85 o 12 14 0 521.08 366.88 431.84 o 13 14 0 535.65 485.27 360.51 o 14 14 0 1561.79 1597.55 582.29 o 15 14 0 6.10 -382.44 528.51 o 1 15 0 41922.36 40590.04 618.58 o 2 15 0 4467.11 3801.91 210.84 o 3 15 0 149.65 111.81 107.69 o 4 15 0 236.76 191.36 158.30 o 5 15 0 8783.68 8737.34 306.44 o 6 15 0 2295.77 2177.19 213.04 o 7 15 0 31.76 38.34 184.93 o 8 15 0 37.12 63.03 166.11 o 9 15 0 145.29 29.20 189.87 o 10 15 0 157.11 33.63 280.64 o 11 15 0 1062.59 1081.35 317.96 o 12 15 0 79.55 -10.71 315.79 o 13 15 0 3118.87 3616.44 486.36 o 14 15 0 0.84 171.92 383.41 o 0 16 0 22031.00 22006.37 588.40 o 1 16 0 4986.65 5230.40 199.68 o 2 16 0 1172.70 1060.59 167.06 o 3 16 0 3415.34 2775.25 214.04 o 4 16 0 448.05 242.61 209.64 o 5 16 0 3654.98 3861.84 294.22 o 6 16 0 881.67 943.56 233.72 o 7 16 0 12098.91 11560.51 481.01 o 8 16 0 2135.27 2035.51 388.04 o 9 16 0 7252.55 7296.19 355.49 o 10 16 0 44.05 -63.99 307.28 o 11 16 0 1238.87 1823.50 374.59 o 12 16 0 723.45 388.54 338.48 o 13 16 0 486.31 956.64 394.57 o 14 16 0 459.18 540.07 413.48 o 1 17 0 2069.96 2133.14 205.63 o 2 17 0 2177.17 1936.77 199.87 o 3 17 0 1753.57 1621.38 205.87 o 4 17 0 3340.88 2888.35 457.35 o 5 17 0 20.52 66.20 196.98 o 6 17 0 2395.22 2452.36 297.05 o 7 17 0 550.82 262.11 233.21 o 8 17 0 13027.53 12705.61 499.41 o 9 17 0 128.26 82.20 210.37 o 10 17 0 1946.89 2465.83 547.27 o 11 17 0 279.23 180.39 483.37 o 12 17 0 1506.51 1403.08 398.85 o 13 17 0 48.35 -349.16 368.06 o 0 18 0 28088.21 28280.15 1114.56 o 1 18 0 0.40 -163.17 195.01 o 2 18 0 6375.01 5940.39 281.26 o 3 18 0 179.99 -14.05 161.16 o 4 18 0 862.16 1302.97 254.24 o 5 18 0 225.29 304.90 216.44 o 6 18 0 2104.62 2292.54 297.65 o 7 18 0 591.25 62.27 229.83 o 8 18 0 306.22 -88.91 187.26 o 9 18 0 216.19 438.44 220.47 o 10 18 0 1272.76 1327.99 348.54 o 11 18 0 85.20 148.58 341.47 o 12 18 0 1326.01 2084.62 433.98 o 13 18 0 191.26 582.34 435.07 o 1 19 0 10420.24 10278.27 473.28 o 2 19 0 42.14 237.57 215.86 o 3 19 0 2705.84 2596.30 646.95 o 4 19 0 1875.35 1523.11 293.06 o 5 19 0 2098.30 2429.27 316.52 o 6 19 0 1084.79 865.17 268.56 o 7 19 0 110.30 618.65 256.59 o 8 19 0 1085.68 1203.40 399.29 o 9 19 0 713.70 917.20 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557.39 o 3 22 0 402.95 1035.08 461.73 o 4 22 0 6300.95 6592.10 498.17 o 5 22 0 11.07 274.02 270.63 o 6 22 0 607.14 810.06 303.45 o 7 22 0 16.74 -110.46 280.76 o 8 22 0 7.41 4.69 240.05 o 9 22 0 226.97 732.15 417.46 o 10 22 0 186.40 -21.76 431.84 o 11 22 0 148.42 168.62 387.84 o 1 23 0 2843.17 3127.24 398.61 o 2 23 0 37.79 -137.31 273.72 o 3 23 0 1059.29 1216.51 335.15 o 4 23 0 1457.81 1135.33 341.68 o 5 23 0 1061.70 1284.86 718.86 o 6 23 0 2562.84 2813.97 546.77 o 7 23 0 2.38 -123.81 312.91 o 8 23 0 1372.40 1111.35 304.54 o 9 23 0 19.89 -339.72 323.48 o 10 23 0 1531.85 1952.01 1078.66 o 0 24 0 457.60 1069.03 476.99 o 1 24 0 3.60 93.11 299.29 o 2 24 0 512.56 888.94 341.77 o 3 24 0 2315.08 2264.31 543.40 o 4 24 0 399.76 244.52 326.80 o 5 24 0 2795.11 3069.73 405.55 o 6 24 0 3.16 -86.94 300.25 o 7 24 0 2756.73 2533.85 711.98 o 8 24 0 72.22 317.36 371.52 o 9 24 0 3224.71 3658.91 511.08 o 10 24 0 107.95 460.22 408.81 o 1 25 0 2768.49 2655.65 436.99 o 2 25 0 145.81 270.31 320.05 o 3 25 0 2345.18 2531.67 539.52 o 4 25 0 2770.66 2371.95 360.33 o 5 25 0 208.24 300.97 317.63 o 6 25 0 77.32 178.55 338.37 o 7 25 0 38.08 -58.41 356.51 o 8 25 0 1062.47 743.33 372.30 o 9 25 0 98.72 102.55 539.02 o 0 26 0 3984.02 4878.44 715.11 o 1 26 0 93.26 -123.55 367.94 o 2 26 0 1931.89 2230.60 421.59 o 3 26 0 5.47 -153.99 595.80 o 4 26 0 1600.93 2420.27 332.37 o 5 26 0 57.93 648.50 334.81 o 6 26 0 397.66 102.02 355.50 o 7 26 0 483.78 201.32 389.51 o 8 26 0 0.22 -443.47 480.99 o 1 27 0 524.31 275.11 373.36 o 2 27 0 515.68 920.76 738.49 o 3 27 0 818.65 564.06 398.14 o 4 27 0 1261.41 1056.64 375.08 o 5 27 0 190.04 7.39 346.55 o 6 27 0 1389.45 1044.57 511.26 o 7 27 0 55.31 714.11 532.52 o 0 28 0 494.07 899.20 646.57 o 1 28 0 22.37 -155.93 420.24 o 2 28 0 170.41 -122.97 422.10 o 3 28 0 1062.15 759.05 1008.88 o 4 28 0 262.89 -17.82 366.25 o 5 28 0 1124.08 823.41 536.27 o 1 29 0 2230.13 663.58 632.07 o 2 29 0 10.41 988.24 680.84 o 3 29 0 1567.31 1058.53 703.35 o -17 0 1 0.85 -7.25 544.77 o -15 0 1 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