#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2207413.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207413_Fobs loop_ _publ_author_name 'Choi, Ki-Young' 'Ryu, Haiil' 'Ko, Jaejung' 'Kang, Sang Ook' 'Han, Won-Sik' 'Suh, Il-Hwan' _publ_section_title ; catena-Poly[[[aquazinc(II)]-\m-6-[bis(2-pyridylmethyl)amino]caproato] perchlorate] ; _journal_coeditor_code AC6211 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2474 _journal_page_last m2476 _journal_volume 61 _journal_year 2005 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 15.9996 _cell_length_b 15.3187 _cell_length_c 16.7417 _exptl_crystal_F_000 2048.00 _reflns_d_resolution_high 0.7491 _[local]_cod_data_source_file ac6211Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kor534 in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 391.23 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 68517.55 70107.06 1320.68 o 4 0 0 135144.30 152318.20 3938.20 o 6 0 0 37594.71 36856.18 1000.14 o 8 0 0 20186.14 19252.39 569.68 o 10 0 0 658.54 513.15 84.79 o 12 0 0 860.97 833.32 114.03 o 14 0 0 161.61 247.40 95.84 o 16 0 0 326.98 246.10 103.47 o 18 0 0 2012.98 2204.64 211.98 o 20 0 0 25.08 -8.12 140.02 o 2 1 0 20244.42 19135.19 295.17 o 4 1 0 90151.70 92529.49 1219.96 o 6 1 0 11746.67 11677.98 209.31 o 8 1 0 442.43 485.99 44.60 o 10 1 0 34.19 81.39 46.40 o 12 1 0 1184.71 1367.81 97.71 o 14 1 0 1.75 33.25 62.04 o 16 1 0 1079.10 1326.21 117.75 o 18 1 0 383.49 295.11 89.54 o 20 1 0 0.49 24.96 94.93 o 0 2 0 153057.48 162409.80 4246.34 o 2 2 0 30120.03 32047.46 427.60 o 4 2 0 7270.75 7496.66 134.28 o 6 2 0 26028.77 25280.29 355.09 o 8 2 0 15249.94 15370.70 276.57 o 10 2 0 8011.97 8034.93 176.10 o 12 2 0 3563.57 3742.24 143.04 o 14 2 0 495.34 587.92 82.49 o 16 2 0 142.92 33.47 65.88 o 18 2 0 597.07 733.81 261.61 o 20 2 0 140.10 104.97 100.26 o 2 3 0 65417.89 69315.17 817.79 o 4 3 0 8324.35 7899.82 122.09 o 6 3 0 14356.47 14115.34 210.20 o 8 3 0 3985.26 4091.52 87.45 o 10 3 0 2049.78 1839.86 78.50 o 12 3 0 2225.24 2118.43 98.17 o 14 3 0 297.08 285.88 106.15 o 16 3 0 3371.38 3198.27 151.72 o 18 3 0 587.36 493.92 103.44 o 20 3 0 99.48 154.47 97.32 o 0 4 0 20131.76 19989.71 554.08 o 2 4 0 30331.29 33275.56 400.88 o 4 4 0 772.43 881.79 29.20 o 6 4 0 117.49 93.55 21.06 o 8 4 0 2028.54 1725.92 54.36 o 10 4 0 537.64 565.41 61.39 o 12 4 0 1014.61 1143.04 77.45 o 14 4 0 230.46 314.91 58.28 o 16 4 0 790.02 939.00 212.39 o 18 4 0 27.16 32.54 79.99 o 20 4 0 554.93 685.73 115.14 o 2 5 0 627.09 622.69 37.66 o 4 5 0 701.07 1004.88 32.41 o 6 5 0 20728.52 20828.31 367.07 o 8 5 0 12142.43 11325.11 168.51 o 10 5 0 10529.17 10873.78 185.83 o 12 5 0 2811.72 2632.92 146.78 o 14 5 0 4960.72 5351.08 134.72 o 16 5 0 729.11 712.89 68.15 o 18 5 0 287.71 243.25 92.45 o 20 5 0 322.19 208.71 107.04 o 0 6 0 5.57 48.24 38.01 o 2 6 0 447.33 477.11 22.28 o 4 6 0 106.79 151.21 19.33 o 6 6 0 13.13 15.63 19.66 o 8 6 0 916.74 766.70 43.06 o 10 6 0 5053.59 4835.32 95.97 o 12 6 0 514.34 625.52 73.53 o 14 6 0 1008.49 1026.43 91.59 o 16 6 0 317.47 275.00 59.11 o 18 6 0 309.76 439.33 76.74 o 20 6 0 9.60 -60.12 96.35 o 2 7 0 185.90 245.94 18.46 o 4 7 0 1097.17 1177.71 51.44 o 6 7 0 40.61 13.32 19.96 o 8 7 0 12837.98 13144.24 190.29 o 10 7 0 2490.42 2429.68 68.30 o 12 7 0 1999.02 2068.19 129.00 o 14 7 0 10348.50 10207.87 213.27 o 16 7 0 1146.10 1262.61 83.69 o 18 7 0 1836.56 1910.30 112.31 o 20 7 0 722.49 865.07 128.81 o 0 8 0 4803.95 4690.29 187.46 o 2 8 0 356.95 359.48 27.50 o 4 8 0 149.95 176.87 21.57 o 6 8 0 57.81 49.87 22.30 o 8 8 0 15.61 -8.54 24.28 o 10 8 0 452.12 423.55 40.17 o 12 8 0 531.41 405.01 63.58 o 14 8 0 461.40 471.57 74.66 o 16 8 0 234.92 103.19 57.30 o 18 8 0 124.76 144.98 63.83 o 2 9 0 487.72 556.52 34.28 o 4 9 0 4116.83 3876.61 71.61 o 6 9 0 7.36 10.64 23.13 o 8 9 0 4105.68 4107.93 85.71 o 10 9 0 292.45 327.88 39.50 o 12 9 0 419.69 403.90 51.25 o 14 9 0 2831.91 3049.59 105.94 o 16 9 0 313.81 126.48 57.06 o 18 9 0 59.16 143.15 87.74 o 0 10 0 6502.37 5819.90 235.21 o 2 10 0 8670.52 8805.36 166.52 o 4 10 0 614.88 572.55 30.43 o 6 10 0 666.20 686.18 38.73 o 8 10 0 1608.76 1777.63 67.95 o 10 10 0 177.07 177.23 42.83 o 12 10 0 2333.00 2427.64 96.34 o 14 10 0 71.81 67.26 65.55 o 16 10 0 932.88 1032.09 96.87 o 18 10 0 15.68 -90.42 90.42 o 2 11 0 316.77 284.27 112.16 o 4 11 0 42.96 34.77 38.21 o 6 11 0 668.32 740.45 156.19 o 8 11 0 2188.58 2120.19 115.05 o 10 11 0 205.85 152.25 52.28 o 12 11 0 88.95 196.08 75.77 o 14 11 0 40.41 -56.27 56.27 o 16 11 0 280.43 351.35 82.44 o 18 11 0 2.06 233.26 166.18 o 0 12 0 11192.84 10473.00 375.72 o 2 12 0 18245.49 17311.92 393.32 o 4 12 0 7098.22 7135.82 171.59 o 6 12 0 4493.97 4468.98 131.86 o 8 12 0 4962.58 5421.64 151.94 o 10 12 0 1293.78 1301.72 116.65 o 12 12 0 1699.34 1582.78 143.35 o 14 12 0 110.15 144.52 90.51 o 16 12 0 111.06 -41.81 95.33 o 2 13 0 2.63 31.61 51.19 o 4 13 0 2687.50 2901.93 111.59 o 6 13 0 20.58 -29.34 40.41 o 8 13 0 2391.88 2492.33 151.64 o 10 13 0 421.18 589.47 95.28 o 12 13 0 26.67 24.42 78.80 o 14 13 0 527.48 353.21 103.36 o 16 13 0 6.14 41.28 101.88 o 0 14 0 18068.57 17594.69 580.07 o 2 14 0 6208.65 5892.24 254.79 o 4 14 0 4650.99 4851.07 144.22 o 6 14 0 2813.58 2921.15 114.93 o 8 14 0 866.66 933.79 105.26 o 10 14 0 1157.90 1224.85 127.03 o 12 14 0 61.55 -75.98 75.98 o 14 14 0 178.98 163.07 99.59 o 2 15 0 736.61 740.33 84.01 o 4 15 0 309.13 318.70 60.62 o 6 15 0 341.44 283.39 117.56 o 8 15 0 831.98 691.02 106.21 o 10 15 0 1248.87 1568.98 139.84 o 12 15 0 619.85 507.91 113.22 o 14 15 0 755.31 728.12 124.41 o 0 16 0 598.94 500.32 118.91 o 2 16 0 6.81 -42.40 42.40 o 4 16 0 674.44 696.46 96.01 o 6 16 0 730.91 820.36 104.63 o 8 16 0 280.31 134.52 85.28 o 10 16 0 361.89 243.36 93.34 o 12 16 0 9.34 67.22 102.04 o 2 17 0 1284.53 1436.13 131.75 o 4 17 0 551.04 661.88 78.99 o 6 17 0 1070.77 873.51 115.65 o 8 17 0 1024.40 1120.92 128.89 o 10 17 0 714.19 619.24 218.08 o 0 18 0 506.80 506.00 133.04 o 2 18 0 453.41 571.42 80.21 o 4 18 0 79.23 66.89 64.59 o 6 18 0 133.65 113.61 88.78 o 8 18 0 0.39 -82.65 82.65 o 10 18 0 33.73 95.14 100.44 o 2 19 0 709.58 797.15 90.97 o 4 19 0 407.04 279.20 98.74 o 6 19 0 750.78 758.51 123.60 o 0 20 0 318.57 269.98 131.90 o 2 20 0 9.40 -21.50 81.30 o 4 20 0 13.90 -88.08 88.08 o 1 1 1 24666.77 27202.85 241.06 o 2 1 1 1620.70 1842.27 26.11 o 3 1 1 29443.98 31689.93 322.55 o 4 1 1 1312.06 1455.26 30.30 o 5 1 1 499.81 589.07 23.70 o 6 1 1 105.79 73.93 18.67 o 7 1 1 3854.29 3735.43 66.00 o 8 1 1 16200.63 16226.41 203.89 o 9 1 1 1296.50 1329.46 74.85 o 10 1 1 6681.61 6706.41 131.26 o 11 1 1 1287.55 1296.05 63.44 o 12 1 1 4690.46 4421.92 146.45 o 13 1 1 1872.64 2240.27 87.71 o 14 1 1 3477.21 3561.25 107.77 o 15 1 1 144.33 213.11 50.38 o 16 1 1 523.11 484.05 61.67 o 17 1 1 70.04 -5.22 50.13 o 18 1 1 1283.22 1298.51 100.20 o 19 1 1 154.79 153.15 63.44 o 20 1 1 346.29 397.48 75.73 o 21 1 1 143.28 116.16 66.72 o 0 2 1 17084.62 19169.46 230.78 o 1 2 1 10908.16 13737.79 124.00 o 2 2 1 2353.50 3078.27 34.43 o 3 2 1 7327.40 8507.18 83.70 o 4 2 1 30887.97 31625.50 325.60 o 5 2 1 711.76 1012.29 28.13 o 6 2 1 6766.09 7118.59 91.52 o 7 2 1 694.98 761.88 40.97 o 8 2 1 4459.52 4698.79 81.00 o 9 2 1 895.24 1008.87 42.18 o 10 2 1 1172.70 1274.20 49.10 o 11 2 1 56.72 71.37 31.63 o 12 2 1 93.30 178.81 42.19 o 13 2 1 481.78 684.30 91.11 o 14 2 1 374.59 271.87 50.77 o 15 2 1 420.08 382.20 57.46 o 16 2 1 39.45 16.67 48.78 o 17 2 1 3.82 -46.44 50.08 o 18 2 1 188.37 79.50 59.17 o 19 2 1 411.68 464.09 69.09 o 20 2 1 38.48 -53.95 65.88 o 21 2 1 6.58 -1.22 67.69 o 1 3 1 4011.59 4220.29 43.46 o 2 3 1 31640.43 32259.36 304.20 o 3 3 1 6895.66 6383.45 66.53 o 4 3 1 4769.04 5101.03 57.60 o 5 3 1 670.18 804.73 21.73 o 6 3 1 11684.83 13558.08 135.60 o 7 3 1 1461.33 1356.25 32.50 o 8 3 1 6728.73 7233.61 99.16 o 9 3 1 1505.54 1606.83 45.54 o 10 3 1 9365.82 9185.63 137.85 o 11 3 1 625.39 712.89 43.85 o 12 3 1 2403.31 2194.90 66.64 o 13 3 1 122.91 50.43 39.07 o 14 3 1 114.02 148.90 46.46 o 15 3 1 223.96 256.75 69.70 o 16 3 1 625.69 700.95 66.05 o 17 3 1 321.48 241.45 77.30 o 18 3 1 72.42 45.97 77.07 o 19 3 1 39.60 -57.28 58.29 o 20 3 1 147.97 227.47 71.47 o 21 3 1 41.69 65.43 64.93 o 0 4 1 285.13 454.78 38.77 o 1 4 1 13932.44 12822.31 124.76 o 2 4 1 6730.94 7305.09 70.39 o 3 4 1 11442.42 11697.92 113.77 o 4 4 1 3041.77 3102.95 41.17 o 5 4 1 2882.26 2782.67 40.45 o 6 4 1 27335.25 27430.48 256.27 o 7 4 1 990.10 1176.78 38.37 o 8 4 1 10221.27 10164.26 114.50 o 9 4 1 11968.76 11932.33 142.06 o 10 4 1 2272.77 2114.76 49.68 o 11 4 1 1411.08 1377.13 57.93 o 12 4 1 316.57 292.54 35.16 o 13 4 1 479.50 481.27 40.81 o 14 4 1 136.06 106.69 34.62 o 15 4 1 910.07 878.49 55.49 o 16 4 1 76.28 67.70 43.48 o 17 4 1 12.95 -5.07 54.63 o 18 4 1 0.74 -29.78 53.84 o 19 4 1 270.69 381.55 67.39 o 20 4 1 178.64 98.41 70.93 o 1 5 1 387.09 362.60 12.63 o 2 5 1 718.33 1072.77 20.54 o 3 5 1 3290.71 3011.60 37.86 o 4 5 1 211.61 117.94 12.90 o 5 5 1 4692.96 3810.27 50.05 o 6 5 1 969.04 1033.72 27.72 o 7 5 1 1214.60 1154.84 39.15 o 8 5 1 1.68 -11.55 14.83 o 9 5 1 135.25 97.99 19.28 o 10 5 1 2.12 -17.35 17.35 o 11 5 1 71.39 37.80 23.17 o 12 5 1 667.70 739.26 45.55 o 13 5 1 1592.31 1665.37 59.64 o 14 5 1 81.21 78.08 35.33 o 15 5 1 172.87 211.01 49.47 o 16 5 1 226.84 290.26 47.08 o 17 5 1 26.60 24.78 42.20 o 18 5 1 17.22 -5.02 46.78 o 19 5 1 41.55 40.32 63.57 o 20 5 1 54.67 30.29 68.21 o 0 6 1 5651.29 5415.00 103.36 o 1 6 1 1400.29 1297.81 25.62 o 2 6 1 14091.73 12881.92 130.54 o 3 6 1 571.45 698.85 19.17 o 4 6 1 23723.08 24161.72 215.19 o 5 6 1 1200.45 1268.72 27.54 o 6 6 1 14449.10 14530.62 139.99 o 7 6 1 3292.12 3321.56 50.89 o 8 6 1 1552.95 1513.19 37.02 o 9 6 1 4479.17 4612.26 66.74 o 10 6 1 1209.89 1168.64 36.77 o 11 6 1 5934.79 6007.97 103.08 o 12 6 1 582.56 666.56 43.88 o 13 6 1 2227.96 2301.39 67.48 o 14 6 1 3.39 -33.38 33.38 o 15 6 1 1968.84 2061.83 77.11 o 16 6 1 2.44 -34.25 34.25 o 17 6 1 1963.85 2037.55 72.55 o 18 6 1 21.50 -46.88 48.46 o 19 6 1 345.31 309.94 67.91 o 20 6 1 16.57 -49.60 65.97 o 1 7 1 2314.31 2313.90 41.64 o 2 7 1 1305.35 1393.15 28.69 o 3 7 1 508.62 540.02 17.95 o 4 7 1 313.20 268.77 16.47 o 5 7 1 3734.38 3723.73 57.45 o 6 7 1 831.05 1003.56 28.33 o 7 7 1 1180.73 1336.85 32.81 o 8 7 1 136.50 67.15 18.27 o 9 7 1 64.73 -17.10 17.10 o 10 7 1 497.56 529.99 29.47 o 11 7 1 125.77 93.83 25.12 o 12 7 1 4.79 -5.33 23.85 o 13 7 1 169.42 94.45 31.73 o 14 7 1 556.06 465.99 40.98 o 15 7 1 33.66 7.16 34.29 o 16 7 1 124.36 16.48 37.07 o 17 7 1 5.02 -37.61 37.61 o 18 7 1 86.09 76.25 42.16 o 19 7 1 9.77 84.09 58.14 o 20 7 1 49.53 -8.59 67.82 o 0 8 1 4745.74 4079.01 70.41 o 1 8 1 31.83 9.86 15.70 o 2 8 1 8008.69 7843.48 94.49 o 3 8 1 1.04 -9.49 10.52 o 4 8 1 11841.91 12259.90 119.98 o 5 8 1 32.25 22.75 13.65 o 6 8 1 7532.82 7563.63 85.03 o 7 8 1 6541.35 6522.41 78.49 o 8 8 1 190.81 113.08 20.01 o 9 8 1 430.64 477.46 31.18 o 10 8 1 1988.56 2060.17 50.90 o 11 8 1 5006.06 5147.61 80.35 o 12 8 1 230.33 289.50 33.75 o 13 8 1 745.32 765.46 45.33 o 14 8 1 88.34 46.60 33.39 o 15 8 1 734.09 643.66 46.69 o 16 8 1 69.28 31.64 37.13 o 17 8 1 605.49 589.06 51.76 o 18 8 1 48.07 2.24 42.73 o 19 8 1 33.40 -18.28 51.63 o 1 9 1 18444.53 18248.22 216.53 o 2 9 1 49.29 22.56 14.85 o 3 9 1 2995.94 2888.56 48.66 o 4 9 1 127.35 107.55 14.45 o 5 9 1 2345.50 2327.58 39.50 o 6 9 1 2378.90 2477.00 47.50 o 7 9 1 40.83 32.58 18.17 o 8 9 1 1611.32 1745.48 43.51 o 9 9 1 7.08 -4.78 19.81 o 10 9 1 71.89 57.96 25.06 o 11 9 1 282.71 321.69 33.59 o 12 9 1 2968.15 2907.53 68.91 o 13 9 1 84.67 41.26 32.10 o 14 9 1 2029.21 2254.83 70.57 o 15 9 1 1.45 -32.69 32.69 o 16 9 1 528.88 485.80 46.62 o 17 9 1 165.20 108.06 43.66 o 18 9 1 347.97 273.52 50.09 o 19 9 1 45.11 -35.94 55.19 o 0 10 1 333.85 427.45 52.84 o 1 10 1 464.70 340.60 26.47 o 2 10 1 1500.01 1616.23 62.31 o 3 10 1 2442.86 2355.12 39.72 o 4 10 1 1196.46 1123.58 34.99 o 5 10 1 4253.33 4192.25 59.76 o 6 10 1 1905.24 2007.14 39.56 o 7 10 1 1932.65 2076.32 43.43 o 8 10 1 872.74 892.83 39.87 o 9 10 1 34.87 1.67 22.42 o 10 10 1 1156.74 1229.48 43.23 o 11 10 1 455.93 540.79 39.16 o 12 10 1 157.68 123.12 35.38 o 13 10 1 25.19 -17.34 33.77 o 14 10 1 176.40 120.08 39.91 o 15 10 1 41.90 -18.04 42.05 o 16 10 1 0.67 -47.43 47.43 o 17 10 1 35.56 -13.55 50.52 o 18 10 1 22.58 -51.11 51.11 o 1 11 1 1844.91 1724.04 63.44 o 2 11 1 322.51 313.05 38.04 o 3 11 1 799.57 725.74 40.91 o 4 11 1 969.49 1190.91 50.08 o 5 11 1 5195.87 5320.67 87.89 o 6 11 1 4447.99 4542.55 116.10 o 7 11 1 192.21 190.65 30.04 o 8 11 1 3045.44 3061.30 68.27 o 9 11 1 2331.33 2505.72 65.38 o 10 11 1 1092.33 1130.86 55.81 o 11 11 1 2588.42 2910.41 103.21 o 12 11 1 2547.62 2915.57 95.57 o 13 11 1 136.04 59.14 39.88 o 14 11 1 645.07 606.26 57.07 o 15 11 1 189.96 142.55 47.64 o 16 11 1 485.11 458.51 64.23 o 17 11 1 152.60 33.19 61.95 o 0 12 1 241.74 241.56 53.61 o 1 12 1 3.89 -29.98 29.98 o 2 12 1 171.26 94.95 37.21 o 3 12 1 0.43 -25.44 25.44 o 4 12 1 38.64 8.90 27.87 o 5 12 1 343.47 349.41 38.43 o 6 12 1 436.90 433.91 40.29 o 7 12 1 2154.74 2405.80 72.23 o 8 12 1 284.83 277.06 42.96 o 9 12 1 43.31 49.87 40.11 o 10 12 1 175.89 112.09 49.28 o 11 12 1 258.11 89.74 50.53 o 12 12 1 120.31 119.19 54.96 o 13 12 1 5.23 -53.36 53.36 o 14 12 1 23.40 -56.30 56.30 o 15 12 1 0.53 46.86 63.89 o 16 12 1 39.31 -76.90 76.90 o 17 12 1 4.63 -64.91 64.91 o 1 13 1 7547.74 7458.02 190.15 o 2 13 1 309.41 294.93 42.80 o 3 13 1 2806.76 2851.56 74.64 o 4 13 1 352.46 376.96 39.94 o 5 13 1 2088.99 2239.61 71.20 o 6 13 1 857.83 723.96 48.80 o 7 13 1 683.90 693.90 57.56 o 8 13 1 1377.49 1582.18 88.27 o 9 13 1 547.21 430.43 58.08 o 10 13 1 2441.87 2986.14 121.12 o 11 13 1 151.53 108.62 53.32 o 12 13 1 1037.35 1167.69 129.43 o 13 13 1 11.32 -58.69 58.69 o 14 13 1 811.50 840.44 87.00 o 15 13 1 39.84 -65.03 65.29 o 16 13 1 396.11 216.82 134.71 o 0 14 1 200.41 137.48 60.11 o 1 14 1 633.02 743.50 58.63 o 2 14 1 1070.81 1084.89 79.99 o 3 14 1 267.26 287.22 37.17 o 4 14 1 1220.88 1276.95 58.52 o 5 14 1 58.32 17.07 34.72 o 6 14 1 742.85 800.27 51.62 o 7 14 1 453.92 409.99 54.79 o 8 14 1 183.31 110.84 50.08 o 9 14 1 3.50 -14.63 46.35 o 10 14 1 1.78 -24.89 49.66 o 11 14 1 309.80 232.94 58.49 o 12 14 1 11.84 -45.60 55.69 o 13 14 1 6.96 -59.04 59.04 o 14 14 1 61.59 -4.51 62.19 o 15 14 1 1.36 -63.80 63.80 o 1 15 1 455.81 370.14 50.87 o 2 15 1 38.09 12.78 39.22 o 3 15 1 1315.29 1509.80 64.33 o 4 15 1 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