#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/76/2207688.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207688_Fobs loop_ _publ_author_name 'Linden, Anthony' 'Basu Baul, Tushar S.' 'Singh, Keisham S.' _publ_section_title ; catena-Poly[[tri-n-butyltin(IV)]-\m-2-{(E)-4-hydroxy-3-[(E)-4-methylphenyliminomethyl]phenyldiazenyl}benzoato-\k^2^O:O'] ; _journal_coeditor_code WN2001 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m2711 _journal_page_last m2713 _journal_volume 61 _journal_year 2005 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.137 _cell_angle_gamma 90.000 _cell_length_a 14.1439 _cell_length_b 9.9908 _cell_length_c 23.2964 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.7711 _[local]_cod_data_source_file wn2001Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TSBB-110 (L0436)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 237.34 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 24853.91 10302.05 6888.26 o 4 0 0 10137.71 9370.53 186.25 o 6 0 0 28995.47 31236.22 485.03 o 8 0 0 1336.09 1439.83 43.63 o 10 0 0 62.31 56.07 10.54 o 12 0 0 1722.07 1631.15 49.30 o 14 0 0 317.35 303.38 30.97 o 16 0 0 300.92 384.66 54.20 o 1 1 0 1834.97 1276.00 244.92 o 2 1 0 31.00 38.37 5.58 o 3 1 0 10319.40 10133.39 190.47 o 4 1 0 625.19 632.33 11.02 o 5 1 0 12076.61 11917.18 173.92 o 6 1 0 1363.47 1291.20 23.02 o 7 1 0 2600.93 2152.09 28.48 o 8 1 0 4240.35 4406.45 48.74 o 9 1 0 7412.10 7548.56 120.97 o 10 1 0 3864.26 3816.38 47.47 o 11 1 0 3994.82 4254.91 93.85 o 12 1 0 1275.45 1285.58 44.12 o 13 1 0 3247.48 3208.75 51.69 o 14 1 0 1017.70 1056.86 33.84 o 15 1 0 1090.39 1093.14 48.50 o 16 1 0 210.29 191.84 35.01 o 17 1 0 16.19 39.71 41.06 o 0 2 0 24580.56 23083.65 342.90 o 1 2 0 15735.86 16673.45 257.98 o 2 2 0 435.81 502.35 16.59 o 3 2 0 8447.48 7863.33 84.13 o 4 2 0 9.16 7.29 5.71 o 5 2 0 10143.33 9955.09 191.25 o 6 2 0 62.11 76.93 9.62 o 7 2 0 65.30 1015.96 188.99 o 8 2 0 4.77 38.76 9.69 o 9 2 0 54.71 48.54 10.27 o 10 2 0 170.25 139.39 14.20 o 11 2 0 1128.52 1127.08 26.88 o 12 2 0 333.29 285.70 16.70 o 13 2 0 46.73 74.37 30.04 o 14 2 0 74.23 63.27 22.71 o 15 2 0 493.27 488.89 30.31 o 16 2 0 32.36 53.18 38.88 o 17 2 0 561.81 490.17 72.42 o 1 3 0 117.47 112.02 6.83 o 2 3 0 4710.70 4703.20 60.04 o 3 3 0 19.44 5.59 3.47 o 4 3 0 884.00 752.28 22.36 o 5 3 0 1360.21 1254.46 21.42 o 6 3 0 2809.24 2540.94 29.76 o 7 3 0 1446.55 1457.73 20.64 o 8 3 0 2973.67 3116.54 40.83 o 9 3 0 2174.45 2092.97 32.84 o 10 3 0 6409.46 6634.77 128.95 o 11 3 0 10.58 26.91 10.81 o 12 3 0 1323.32 1277.05 28.66 o 13 3 0 500.16 545.85 27.90 o 14 3 0 497.39 494.86 30.82 o 15 3 0 251.59 227.06 38.74 o 16 3 0 337.47 285.25 50.38 o 17 3 0 22.91 88.77 51.31 o 0 4 0 12700.78 12134.32 170.37 o 1 4 0 1555.13 1523.11 18.93 o 2 4 0 13096.30 13456.20 191.04 o 3 4 0 56.44 58.48 8.99 o 4 4 0 18829.60 20257.35 215.48 o 5 4 0 706.31 710.77 23.15 o 6 4 0 1788.06 1825.13 27.93 o 7 4 0 177.60 177.81 9.34 o 8 4 0 1510.73 1478.53 31.28 o 9 4 0 7.08 15.70 12.21 o 10 4 0 776.13 691.15 18.19 o 11 4 0 335.25 330.97 17.82 o 12 4 0 919.83 769.42 34.00 o 13 4 0 31.33 -6.83 26.68 o 14 4 0 486.06 486.78 32.83 o 15 4 0 12.41 52.22 30.54 o 16 4 0 439.60 510.03 58.98 o 1 5 0 59.71 56.83 7.54 o 2 5 0 8252.40 8401.12 91.33 o 3 5 0 668.85 548.69 13.63 o 4 5 0 2313.66 2584.57 33.20 o 5 5 0 4416.60 4357.89 54.04 o 6 5 0 914.80 970.33 20.26 o 7 5 0 6885.12 7169.07 99.10 o 8 5 0 1824.51 1724.70 31.55 o 9 5 0 8578.16 8952.49 111.78 o 10 5 0 305.94 348.30 16.08 o 11 5 0 2410.83 2434.10 48.13 o 12 5 0 29.03 84.08 20.38 o 13 5 0 3583.76 3840.21 102.42 o 14 5 0 88.96 169.67 41.45 o 15 5 0 1493.93 1507.81 75.92 o 16 5 0 0.91 13.33 50.89 o 0 6 0 7028.55 6789.68 115.43 o 1 6 0 11592.67 11927.11 121.03 o 2 6 0 2377.64 2527.68 43.73 o 3 6 0 7545.93 7858.66 88.59 o 4 6 0 4799.40 5034.22 54.01 o 5 6 0 6084.79 6448.89 85.13 o 6 6 0 1967.56 2002.12 40.59 o 7 6 0 674.41 692.64 17.81 o 8 6 0 12.36 25.77 11.02 o 9 6 0 233.77 189.66 14.53 o 10 6 0 75.14 53.28 13.87 o 11 6 0 1.63 -16.14 16.14 o 12 6 0 15.61 -10.25 36.47 o 13 6 0 163.85 61.99 44.78 o 14 6 0 52.96 105.73 39.56 o 15 6 0 321.54 350.17 54.42 o 1 7 0 192.91 187.48 11.84 o 2 7 0 3504.59 3491.57 53.27 o 3 7 0 75.46 81.57 8.68 o 4 7 0 1123.58 1128.07 20.30 o 5 7 0 1329.29 1401.57 50.36 o 6 7 0 5040.49 5241.93 82.94 o 7 7 0 160.59 196.40 22.94 o 8 7 0 4540.72 4689.59 70.44 o 9 7 0 187.31 210.57 21.50 o 10 7 0 1912.31 1897.47 42.18 o 11 7 0 78.12 86.48 24.16 o 12 7 0 2001.37 2102.01 77.15 o 13 7 0 135.50 92.21 43.01 o 14 7 0 1268.65 1260.09 87.59 o 0 8 0 5840.21 5829.01 113.00 o 1 8 0 2225.20 2266.20 37.30 o 2 8 0 4929.06 5087.21 168.31 o 3 8 0 1642.65 1707.62 28.58 o 4 8 0 1488.58 1442.59 24.47 o 5 8 0 107.35 117.68 13.93 o 6 8 0 1637.76 1766.58 45.52 o 7 8 0 346.67 312.47 16.36 o 8 8 0 1655.41 1494.39 56.65 o 9 8 0 210.02 123.27 18.09 o 10 8 0 0.69 -23.07 24.59 o 11 8 0 2.69 -31.11 31.11 o 12 8 0 195.76 243.53 39.08 o 13 8 0 23.65 -16.14 36.83 o 1 9 0 198.64 164.63 18.92 o 2 9 0 142.93 121.42 17.88 o 3 9 0 1647.07 1671.74 38.68 o 4 9 0 5.69 60.18 31.72 o 5 9 0 2388.32 2494.94 45.61 o 6 9 0 185.57 197.11 22.55 o 7 9 0 2673.68 2763.69 58.03 o 8 9 0 10.46 66.79 32.96 o 9 9 0 4077.92 4345.59 116.93 o 10 9 0 161.47 145.85 62.56 o 11 9 0 2294.82 2197.51 83.97 o 12 9 0 64.20 35.01 61.45 o 0 10 0 1304.91 1340.00 55.12 o 1 10 0 392.93 421.53 22.91 o 2 10 0 1634.38 1597.92 38.07 o 3 10 0 480.33 445.47 32.58 o 4 10 0 983.29 1027.79 41.16 o 5 10 0 276.24 218.85 20.70 o 6 10 0 618.37 617.34 28.84 o 7 10 0 580.38 518.20 40.49 o 8 10 0 195.23 148.28 39.43 o 9 10 0 22.60 41.69 26.07 o 10 10 0 8.14 -33.00 33.00 o 11 10 0 7.35 38.45 61.73 o 1 11 0 5.81 -24.92 24.92 o 2 11 0 28.06 -19.30 22.60 o 3 11 0 105.08 132.28 46.99 o 4 11 0 933.34 902.65 45.22 o 5 11 0 46.88 67.88 34.50 o 6 11 0 1094.41 1082.87 58.76 o 7 11 0 123.74 116.01 34.80 o 8 11 0 1591.47 1616.41 110.43 o 9 11 0 349.57 387.53 75.37 o 0 12 0 1026.00 794.82 239.20 o 1 12 0 2774.51 3106.51 435.07 o 2 12 0 254.89 267.37 59.85 o 3 12 0 396.19 391.25 42.35 o 4 12 0 151.54 255.31 61.51 o 5 12 0 838.29 790.06 92.09 o 6 12 0 138.06 46.44 83.92 o -17 0 1 811.53 819.54 117.80 o -15 0 1 191.15 279.39 45.02 o -13 0 1 62.85 57.03 16.29 o -11 0 1 712.47 687.58 29.77 o -9 0 1 4578.55 4845.15 75.67 o -7 0 1 26162.16 27696.12 429.01 o -5 0 1 35013.04 35150.57 596.68 o -3 0 1 39547.53 41210.99 1351.28 o 3 0 1 56330.98 54775.59 1203.25 o 5 0 1 14239.48 14139.02 294.59 o 7 0 1 1175.79 1182.23 34.32 o 9 0 1 111.45 127.67 10.98 o 11 0 1 2973.98 3118.53 107.31 o 13 0 1 1782.18 1661.63 60.73 o 15 0 1 1409.21 1463.10 75.26 o 17 0 1 395.14 245.78 55.75 o -17 1 1 168.37 191.86 47.44 o -16 1 1 478.52 435.18 51.04 o -15 1 1 870.71 913.40 56.08 o -14 1 1 2355.71 2197.37 80.56 o -13 1 1 1559.18 1568.90 64.20 o -12 1 1 1011.75 1064.40 31.54 o -11 1 1 1738.01 1659.65 37.96 o -10 1 1 7326.33 7648.62 109.29 o -9 1 1 1784.55 1924.19 76.49 o -8 1 1 10861.56 11828.36 234.21 o -7 1 1 54.39 131.48 10.83 o -6 1 1 16405.19 16749.94 283.29 o -5 1 1 3521.73 3524.63 46.08 o -4 1 1 3259.79 3450.63 43.70 o -3 1 1 134.46 202.98 20.12 o -2 1 1 34754.74 27208.27 3133.69 o -1 1 1 4691.22 1985.83 554.84 o 1 1 1 5670.48 3058.26 617.09 o 2 1 1 7.72 10.98 1.90 o 3 1 1 9659.92 9268.20 582.37 o 4 1 1 12688.43 11892.99 383.87 o 5 1 1 15909.57 16180.75 275.74 o 6 1 1 14919.69 14370.25 246.38 o 7 1 1 2767.04 3309.87 253.26 o 8 1 1 7072.74 7412.31 102.72 o 9 1 1 6199.35 6426.97 107.54 o 10 1 1 3469.78 3603.83 95.53 o 11 1 1 1513.08 1522.65 42.41 o 12 1 1 2653.49 2764.07 42.37 o 13 1 1 776.57 761.06 21.77 o 14 1 1 774.71 756.99 31.06 o 15 1 1 359.83 381.29 32.83 o 16 1 1 361.61 339.63 41.55 o 17 1 1 28.18 43.21 46.40 o -17 2 1 52.65 89.59 49.16 o -16 2 1 302.38 306.88 68.67 o -15 2 1 49.64 43.23 26.63 o -14 2 1 77.52 82.31 28.08 o -13 2 1 1591.83 1411.29 66.23 o -12 2 1 661.98 570.87 28.20 o -11 2 1 251.75 237.94 15.66 o -10 2 1 3233.65 3030.64 70.13 o -9 2 1 434.19 425.83 14.81 o -8 2 1 3223.06 3219.37 38.24 o -7 2 1 1155.35 1282.08 21.91 o -6 2 1 9743.24 9790.13 124.67 o -5 2 1 1998.80 2076.97 40.72 o -4 2 1 11760.02 11033.07 145.04 o -3 2 1 124.11 120.21 7.19 o -2 2 1 1486.35 1502.70 18.50 o -1 2 1 11605.62 11712.93 125.26 o 1 2 1 924.64 956.29 15.02 o 2 2 1 3298.96 3194.33 36.91 o 3 2 1 0.86 -1.00 2.59 o 4 2 1 801.38 702.60 14.35 o 5 2 1 1882.74 1837.84 38.79 o 6 2 1 1952.64 1828.62 24.77 o 7 2 1 1583.11 1688.14 33.20 o 8 2 1 698.31 580.53 16.69 o 9 2 1 63.27 63.55 8.25 o 10 2 1 275.68 312.45 14.84 o 11 2 1 6.64 43.84 11.66 o 12 2 1 1955.35 1872.76 40.21 o 13 2 1 46.79 53.78 20.72 o 14 2 1 1114.65 1134.44 41.14 o 15 2 1 31.92 10.71 25.20 o 16 2 1 548.56 576.85 50.11 o 17 2 1 13.93 7.60 48.80 o -17 3 1 13.61 -50.12 50.12 o -16 3 1 226.15 221.37 110.23 o -15 3 1 1341.45 1462.32 58.20 o -14 3 1 392.49 488.30 29.20 o -13 3 1 2821.83 2893.69 82.59 o -12 3 1 735.66 729.29 24.00 o -11 3 1 11.38 27.43 11.99 o -10 3 1 671.97 720.61 32.25 o -9 3 1 1274.17 1196.13 23.61 o -8 3 1 1947.00 1987.02 34.19 o -7 3 1 2387.68 2336.12 88.06 o -6 3 1 1056.40 1039.14 21.11 o -5 3 1 2479.75 2258.71 50.28 o -4 3 1 1632.36 1651.04 49.21 o -3 3 1 368.37 393.45 10.97 o -2 3 1 0.34 -0.63 3.63 o -1 3 1 11.79 6.77 5.23 o 0 3 1 61.25 86.97 3.98 o 1 3 1 4.70 4.47 4.02 o 2 3 1 2.65 27.50 8.75 o 3 3 1 9698.94 9222.14 142.50 o 4 3 1 1265.81 1334.11 18.20 o 5 3 1 10883.93 11099.87 139.19 o 6 3 1 869.64 857.30 16.41 o 7 3 1 390.74 303.52 12.54 o 8 3 1 1562.60 1454.34 21.67 o 9 3 1 6614.29 6429.55 104.93 o 10 3 1 3551.86 3503.57 48.22 o 11 3 1 2826.69 3017.47 45.58 o 12 3 1 270.51 334.57 21.66 o 13 3 1 1401.71 1369.01 40.20 o 14 3 1 486.57 506.64 52.07 o 15 3 1 384.58 317.13 41.16 o 16 3 1 46.66 26.97 107.50 o 17 3 1 2.28 -44.51 44.51 o -16 4 1 36.71 10.86 46.94 o -15 4 1 591.18 589.09 49.71 o -14 4 1 5.98 8.35 32.15 o -13 4 1 0.22 -11.25 20.98 o -12 4 1 0.00 -10.60 14.03 o -11 4 1 685.26 563.46 41.71 o -10 4 1 756.16 705.13 22.28 o -9 4 1 1495.39 1437.11 27.71 o -8 4 1 176.92 196.46 11.98 o -7 4 1 3463.49 3635.05 71.74 o -6 4 1 2152.01 2262.27 33.38 o -5 4 1 21935.02 23228.78 295.11 o -4 4 1 4056.70 4194.77 63.34 o -3 4 1 8676.12 8311.09 83.89 o -2 4 1 1558.88 1529.75 22.24 o -1 4 1 25973.98 26171.22 249.95 o 0 4 1 66.78 56.63 5.54 o 1 4 1 7897.38 7766.88 81.23 o 2 4 1 198.09 211.76 10.04 o 3 4 1 6811.59 6566.24 77.13 o 4 4 1 191.39 316.41 10.90 o 5 4 1 6137.34 6020.88 78.29 o 6 4 1 290.71 239.53 12.58 o 7 4 1 564.64 523.36 21.72 o 8 4 1 898.02 843.71 18.62 o 9 4 1 150.34 174.48 17.11 o 10 4 1 172.22 171.72 12.60 o 11 4 1 1356.45 1318.76 28.65 o 12 4 1 4.03 6.56 22.30 o 13 4 1 273.59 280.31 33.76 o 14 4 1 187.56 181.05 38.48 o 15 4 1 700.12 702.81 62.25 o 16 4 1 160.78 227.25 53.45 o -16 5 1 793.24 628.26 80.50 o -15 5 1 74.96 92.06 40.44 o -14 5 1 2485.98 2520.28 150.00 o -13 5 1 265.07 368.57 78.33 o -12 5 1 3031.94 2997.43 68.23 o -11 5 1 305.39 303.23 17.91 o -10 5 1 6315.93 6744.88 83.88 o -9 5 1 1276.51 1275.78 25.89 o -8 5 1 3878.47 3988.13 77.75 o -7 5 1 1496.34 1541.60 30.54 o -6 5 1 10597.48 11099.89 177.36 o -5 5 1 575.34 942.04 41.47 o -4 5 1 3331.02 3503.85 60.97 o -3 5 1 898.87 1012.39 18.70 o -2 5 1 1519.34 1763.72 24.96 o -1 5 1 383.54 389.54 8.32 o 0 5 1 1657.82 1658.86 75.35 o 1 5 1 5.93 5.21 5.30 o 2 5 1 6828.27 6911.19 70.91 o 3 5 1 4.21 14.24 6.00 o 4 5 1 3837.33 3616.92 54.72 o 5 5 1 890.21 919.21 17.39 o 6 5 1 11231.21 11903.76 154.40 o 7 5 1 1666.21 1741.12 28.20 o 8 5 1 7156.27 7212.32 116.39 o 9 5 1 145.34 217.32 16.90 o 10 5 1 2828.76 2902.93 41.81 o 11 5 1 24.21 21.85 13.55 o 12 5 1 3056.13 3139.83 82.68 o 13 5 1 172.47 207.46 33.26 o 14 5 1 949.93 869.96 74.42 o 15 5 1 38.48 130.37 48.22 o 16 5 1 387.04 393.02 63.32 o -15 6 1 84.98 71.54 46.71 o -14 6 1 240.78 289.74 51.62 o -13 6 1 43.58 51.04 31.03 o -12 6 1 16.73 18.99 72.75 o -11 6 1 43.10 57.28 19.57 o -10 6 1 61.75 83.09 14.12 o -9 6 1 23.28 21.13 11.97 o -8 6 1 1067.68 1052.34 28.53 o -7 6 1 1475.41 1503.42 37.36 o -6 6 1 4100.38 4415.78 57.55 o -5 6 1 3738.93 4026.00 65.62 o -4 6 1 4765.28 4640.32 54.43 o -3 6 1 1447.24 1435.41 31.06 o -2 6 1 4934.90 4976.87 50.74 o -1 6 1 7086.12 7330.03 81.20 o 0 6 1 12835.29 13488.04 142.13 o 1 6 1 2740.33 2637.84 33.58 o 2 6 1 9436.55 9952.40 106.96 o 3 6 1 5924.81 6366.13 72.04 o 4 6 1 7564.18 7768.53 82.10 o 5 6 1 987.08 996.45 23.60 o 6 6 1 138.41 149.12 11.74 o 7 6 1 696.57 636.96 18.03 o 8 6 1 127.40 99.71 10.84 o 9 6 1 160.04 154.69 13.96 o 10 6 1 53.09 21.05 13.66 o 11 6 1 142.81 92.84 18.29 o 12 6 1 760.48 612.65 42.14 o 13 6 1 64.09 133.18 43.56 o 14 6 1 794.12 866.15 57.04 o 15 6 1 212.45 122.37 54.86 o -15 7 1 821.51 830.45 84.72 o -14 7 1 0.29 3.27 65.72 o -13 7 1 887.72 825.71 72.58 o -12 7 1 170.88 125.14 33.36 o -11 7 1 2785.06 2679.80 64.39 o -10 7 1 303.81 295.78 20.80 o -9 7 1 7203.47 7698.52 107.90 o -8 7 1 122.77 107.19 14.85 o -7 7 1 2110.62 2213.28 42.10 o -6 7 1 293.40 311.62 17.06 o -5 7 1 3005.68 3016.95 41.99 o -4 7 1 56.49 59.33 8.58 o -3 7 1 117.66 130.86 8.85 o -2 7 1 1.04 -9.97 9.97 o -1 7 1 1615.69 1713.61 31.73 o 0 7 1 67.80 95.29 12.27 o 1 7 1 2054.07 1942.67 29.63 o 2 7 1 208.33 205.05 10.09 o 3 7 1 5540.65 5760.19 73.25 o 4 7 1 28.56 44.69 9.09 o 5 7 1 4232.44 4243.52 71.35 o 6 7 1 423.54 408.50 16.89 o 7 7 1 6339.76 6532.52 91.37 o 8 7 1 217.30 181.41 15.30 o 9 7 1 1544.09 1415.06 50.73 o 10 7 1 63.23 47.21 23.52 o 11 7 1 1304.84 1391.00 101.97 o 12 7 1 25.00 110.33 32.60 o 13 7 1 1264.52 1267.79 108.55 o 14 7 1 147.72 153.98 47.88 o -14 8 1 161.92 57.41 56.74 o -13 8 1 6.15 -10.03 52.56 o -12 8 1 0.80 2.06 47.73 o -11 8 1 36.65 0.07 31.56 o -10 8 1 148.08 127.68 28.16 o -9 8 1 538.42 415.85 27.73 o -8 8 1 16.53 -3.38 14.98 o -7 8 1 1350.70 1368.82 31.15 o -6 8 1 1749.93 1809.47 41.69 o -5 8 1 3662.83 3825.82 55.98 o -4 8 1 670.23 693.14 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215.91 180.77 65.07 o -10 1 28 598.17 665.33 67.43 o -9 1 28 572.62 595.44 50.63 o -8 1 28 795.92 833.62 55.18 o -7 1 28 320.61 360.72 41.88 o -6 1 28 540.58 475.09 40.05 o -5 1 28 443.84 479.04 40.20 o -4 1 28 143.24 106.89 28.57 o -3 1 28 24.19 49.80 34.28 o -2 1 28 95.24 108.87 30.21 o -1 1 28 3.44 17.22 31.21 o 0 1 28 46.11 26.74 32.63 o 1 1 28 17.30 5.89 33.92 o 2 1 28 14.80 70.60 38.23 o -10 2 28 104.81 184.91 53.46 o -9 2 28 86.37 116.83 47.01 o -8 2 28 13.50 -17.61 34.02 o -7 2 28 465.68 467.65 49.62 o -6 2 28 38.52 92.33 35.50 o -5 2 28 319.68 289.88 34.76 o -4 2 28 29.75 45.41 28.82 o -3 2 28 713.80 786.65 58.73 o -2 2 28 28.59 30.65 30.35 o -1 2 28 1167.30 1271.28 51.81 o 0 2 28 30.83 -25.93 35.98 o 1 2 28 194.93 166.60 38.66 o -9 3 28 877.32 809.20 63.74 o -8 3 28 557.42 555.13 50.72 o -7 3 28 98.51 55.99 58.80 o -6 3 28 516.21 492.05 48.55 o -5 3 28 78.69 44.05 31.02 o -4 3 28 221.11 178.71 34.19 o -3 3 28 48.50 -28.14 31.82 o -2 3 28 5.07 -29.85 29.85 o -1 3 28 13.31 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