#------------------------------------------------------------------------------ #$Date: 2016-04-03 00:17:54 +0300 (Sun, 03 Apr 2016) $ #$Revision: 180997 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/20/77/2207779.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2207779_Fobs loop_ _publ_author_name 'Xu, Zhi-Wei' 'Fu, Yun-Long' 'Ren, Jia-Lin' _publ_section_title ; Piperazinium(2+) hexaaquairon(II) bis(sulfate) ; _journal_coeditor_code HG6264 _journal_issue 1 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m161 _journal_page_last m162 _journal_volume 62 _journal_year 2006 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.284 _cell_angle_gamma 90.000 _cell_length_a 7.8345 _cell_length_b 9.3814 _cell_length_c 11.0965 _exptl_crystal_F_000 464.00 _reflns_d_resolution_high 0.7823 _cod_data_source_file hg6264Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' a11 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 156.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12990.30 12705.48 194.21 o 4 0 0 6860.95 6659.10 90.76 o 6 0 0 3950.00 4172.05 81.61 o 8 0 0 27.04 29.02 3.94 o 10 0 0 338.55 372.07 15.33 o 1 1 0 7.88 25.14 1.00 o 2 1 0 130.18 140.00 2.35 o 3 1 0 1779.81 1820.04 18.75 o 4 1 0 396.98 460.94 6.31 o 5 1 0 52.62 53.08 2.00 o 6 1 0 182.00 174.98 3.89 o 7 1 0 43.30 42.58 2.03 o 8 1 0 18.10 19.74 1.97 o 9 1 0 3.18 6.94 1.59 o 0 2 0 24498.47 17157.85 330.46 o 1 2 0 158.44 157.53 2.40 o 2 2 0 7910.75 8062.65 77.06 o 3 2 0 1.59 -0.32 0.52 o 4 2 0 5520.02 5727.68 55.84 o 5 2 0 250.27 228.89 4.32 o 6 2 0 2452.34 2409.12 26.02 o 7 2 0 336.75 343.82 9.32 o 8 2 0 337.42 344.76 7.81 o 9 2 0 6.63 9.97 1.48 o 1 3 0 1465.60 1429.29 17.35 o 2 3 0 44.03 52.40 1.60 o 3 3 0 637.51 704.99 8.70 o 4 3 0 121.02 129.35 3.00 o 5 3 0 72.70 69.04 2.34 o 6 3 0 270.16 265.69 6.17 o 7 3 0 258.11 256.75 6.35 o 8 3 0 117.00 123.08 4.43 o 9 3 0 113.65 114.39 4.49 o 0 4 0 803.01 912.03 21.08 o 1 4 0 486.66 471.57 7.52 o 2 4 0 4109.45 4022.94 38.76 o 3 4 0 252.96 258.49 6.06 o 4 4 0 2081.01 2170.65 23.38 o 5 4 0 261.96 268.66 5.15 o 6 4 0 842.23 805.40 12.96 o 7 4 0 110.85 123.53 6.22 o 8 4 0 749.27 729.41 13.18 o 9 4 0 24.94 31.28 3.14 o 1 5 0 171.30 149.15 4.97 o 2 5 0 293.71 294.94 8.55 o 3 5 0 143.89 123.58 2.67 o 4 5 0 322.55 348.91 5.15 o 5 5 0 246.06 218.70 4.56 o 6 5 0 33.84 37.42 3.12 o 7 5 0 299.52 291.20 9.53 o 8 5 0 192.80 207.11 6.59 o 9 5 0 83.69 91.04 4.12 o 0 6 0 1045.47 1027.55 25.67 o 1 6 0 7.79 8.22 1.77 o 2 6 0 1131.29 1108.67 26.47 o 3 6 0 180.70 181.61 5.88 o 4 6 0 344.64 348.29 6.80 o 5 6 0 160.20 157.67 4.00 o 6 6 0 261.00 263.33 6.41 o 7 6 0 8.24 10.07 1.30 o 8 6 0 158.40 151.31 4.48 o 1 7 0 1347.70 1465.33 27.13 o 2 7 0 201.76 199.35 6.93 o 3 7 0 906.75 898.66 14.03 o 4 7 0 126.80 121.63 6.42 o 5 7 0 971.63 924.85 15.35 o 6 7 0 162.56 161.96 4.39 o 7 7 0 55.67 54.22 2.57 o 8 7 0 149.89 165.14 4.76 o 0 8 0 1253.59 1202.65 31.38 o 1 8 0 269.98 248.43 9.80 o 2 8 0 30.99 28.63 3.17 o 3 8 0 28.42 31.16 3.40 o 4 8 0 83.24 83.67 4.85 o 5 8 0 140.28 136.83 5.19 o 6 8 0 157.30 150.34 5.52 o 7 8 0 31.56 30.88 2.87 o 1 9 0 848.78 881.83 18.68 o 2 9 0 72.09 65.53 4.63 o 3 9 0 460.39 453.00 12.30 o 4 9 0 1.29 2.60 1.67 o 5 9 0 347.01 343.62 19.67 o 6 9 0 149.59 153.01 7.97 o 0 10 0 1.65 -1.10 2.21 o 1 10 0 16.04 18.56 3.23 o 2 10 0 5.10 8.15 2.39 o 3 10 0 10.91 12.09 2.76 o 4 10 0 31.89 39.29 4.06 o 5 10 0 64.69 65.87 4.84 o 1 11 0 321.78 326.27 11.22 o 2 11 0 9.13 14.81 3.78 o 3 11 0 226.45 241.48 9.49 o -9 0 1 1.06 10.09 2.68 o -7 0 1 376.61 312.20 18.98 o -5 0 1 264.08 250.79 6.26 o -3 0 1 248.04 221.80 3.84 o -1 0 1 1875.91 1980.23 23.02 o 1 0 1 4396.47 5012.19 69.42 o 3 0 1 1079.55 971.71 15.08 o 5 0 1 7736.48 8108.31 177.25 o 7 0 1 2764.91 2775.95 42.13 o 9 0 1 1090.94 1059.43 28.58 o -9 1 1 0.61 4.20 1.21 o -8 1 1 1180.24 1132.54 61.28 o -7 1 1 14.67 12.42 2.01 o -6 1 1 3365.37 3289.67 43.46 o -5 1 1 2.52 2.37 0.59 o -4 1 1 2281.32 2216.78 22.86 o -3 1 1 3581.67 4012.32 35.51 o -2 1 1 2053.43 2222.21 21.54 o -1 1 1 247.61 283.46 4.87 o 0 1 1 247.01 284.17 7.31 o 1 1 1 467.33 505.98 9.13 o 2 1 1 9.90 13.06 0.93 o 3 1 1 477.48 502.91 6.30 o 4 1 1 1238.52 1267.24 14.04 o 5 1 1 104.24 100.03 4.33 o 6 1 1 49.44 39.81 1.83 o 7 1 1 0.93 1.49 0.80 o 8 1 1 8.85 8.16 1.33 o 9 1 1 19.08 22.32 2.18 o -9 2 1 2.54 2.28 1.05 o -8 2 1 160.64 157.01 5.04 o -7 2 1 1.97 2.94 0.99 o -6 2 1 230.27 207.99 11.82 o -5 2 1 7.49 4.33 0.73 o -4 2 1 0.11 0.35 0.71 o -3 2 1 1026.79 1033.24 11.51 o -2 2 1 1057.59 976.37 9.66 o -1 2 1 970.10 963.70 9.59 o 0 2 1 1433.70 1615.17 18.52 o 1 2 1 1568.39 1646.81 16.74 o 2 2 1 168.95 145.71 2.74 o 3 2 1 4798.92 4946.54 57.06 o 4 2 1 22.37 24.87 1.84 o 5 2 1 1981.44 1933.89 34.33 o 6 2 1 70.31 71.28 6.78 o 7 2 1 1175.39 1152.96 14.68 o 8 2 1 9.96 12.48 1.63 o 9 2 1 802.48 858.82 29.30 o -9 3 1 0.07 3.55 1.23 o -8 3 1 1225.92 1254.82 19.04 o -7 3 1 25.60 24.43 2.20 o -6 3 1 617.91 636.06 10.85 o -5 3 1 307.93 286.68 5.73 o -4 3 1 3226.17 3525.33 38.39 o -3 3 1 265.25 324.77 7.71 o -2 3 1 10176.64 9775.24 135.61 o -1 3 1 441.17 409.49 5.28 o 0 3 1 236.26 261.15 3.93 o 1 3 1 1140.79 1101.62 12.14 o 2 3 1 1330.38 1376.78 17.27 o 3 3 1 449.83 469.43 8.61 o 4 3 1 46.97 48.76 1.80 o 5 3 1 73.61 69.43 2.36 o 6 3 1 21.99 23.04 2.16 o 7 3 1 0.62 1.87 0.94 o 8 3 1 39.35 38.51 2.70 o 9 3 1 2.45 5.42 1.08 o -9 4 1 1.02 2.17 0.83 o -8 4 1 28.19 32.36 2.65 o -7 4 1 234.39 228.64 6.26 o -6 4 1 189.49 183.99 5.25 o -5 4 1 90.35 97.65 3.52 o -4 4 1 36.87 34.11 1.65 o -3 4 1 1230.83 1330.67 12.72 o -2 4 1 77.11 59.72 1.86 o -1 4 1 107.95 98.08 3.46 o 0 4 1 4.05 1.18 0.89 o 1 4 1 124.97 102.67 2.92 o 2 4 1 9.28 13.03 1.05 o 3 4 1 5529.80 5756.29 80.69 o 4 4 1 1159.61 1199.82 11.99 o 5 4 1 19.13 23.37 1.86 o 6 4 1 42.96 37.18 1.96 o 7 4 1 230.45 226.17 6.04 o 8 4 1 1.88 3.91 1.18 o 9 4 1 386.74 391.09 9.19 o -9 5 1 15.27 19.42 2.19 o -8 5 1 689.76 712.27 13.90 o -7 5 1 8.94 12.48 2.19 o -6 5 1 151.36 152.64 4.92 o -5 5 1 714.47 680.80 9.37 o -4 5 1 1734.77 1793.48 18.95 o -3 5 1 3406.02 3457.53 29.87 o -2 5 1 2700.58 2820.50 40.44 o -1 5 1 68.42 56.65 4.10 o 0 5 1 715.15 729.30 13.27 o 1 5 1 673.45 672.58 10.28 o 2 5 1 3241.94 3321.79 39.04 o 3 5 1 210.43 213.54 5.10 o 4 5 1 95.17 81.01 2.29 o 5 5 1 8.12 8.82 1.05 o 6 5 1 88.09 79.64 2.77 o 7 5 1 33.11 29.48 1.96 o 8 5 1 73.12 69.12 4.27 o 9 5 1 33.51 36.90 5.52 o -8 6 1 6.18 10.65 1.37 o -7 6 1 23.12 20.62 1.84 o -6 6 1 73.31 71.06 2.82 o -5 6 1 1.89 2.56 0.89 o -4 6 1 145.15 168.58 4.06 o -3 6 1 300.49 297.69 6.27 o -2 6 1 308.34 257.93 7.32 o -1 6 1 246.40 252.55 7.21 o 0 6 1 78.57 73.07 3.79 o 1 6 1 300.93 306.85 13.44 o 2 6 1 61.99 57.26 2.79 o 3 6 1 487.81 468.43 10.55 o 4 6 1 669.69 711.23 10.29 o 5 6 1 135.61 130.72 3.61 o 6 6 1 91.94 89.53 3.06 o 7 6 1 220.03 226.75 6.25 o 8 6 1 0.62 2.86 0.85 o -8 7 1 106.91 115.99 3.98 o -7 7 1 96.64 106.25 3.67 o -6 7 1 228.61 225.57 5.33 o -5 7 1 86.19 86.32 3.11 o -4 7 1 426.17 402.61 10.57 o -3 7 1 877.15 866.00 16.96 o -2 7 1 181.32 183.10 6.64 o -1 7 1 207.42 184.57 6.48 o 0 7 1 1416.99 1408.35 23.94 o 1 7 1 475.95 511.55 11.92 o 2 7 1 1745.30 1726.48 28.18 o 3 7 1 903.43 879.67 20.24 o 4 7 1 1133.72 1066.56 14.65 o 5 7 1 12.00 15.95 2.31 o 6 7 1 388.65 341.83 8.31 o 7 7 1 57.85 58.77 2.68 o 8 7 1 97.74 94.87 3.45 o -7 8 1 44.00 41.47 2.95 o -6 8 1 77.20 83.18 5.68 o -5 8 1 316.83 302.82 12.48 o -4 8 1 462.81 478.47 12.25 o -3 8 1 119.47 114.49 9.07 o -2 8 1 716.98 702.64 35.91 o -1 8 1 291.73 268.59 8.55 o 0 8 1 927.54 945.19 18.59 o 1 8 1 393.29 393.18 12.26 o 2 8 1 335.85 326.52 12.65 o 3 8 1 3.15 1.14 0.70 o 4 8 1 7.09 6.35 1.62 o 5 8 1 217.96 233.76 6.77 o 6 8 1 6.34 10.80 1.94 o 7 8 1 62.70 64.60 3.61 o -6 9 1 110.06 114.31 6.19 o -5 9 1 15.83 20.58 3.05 o -4 9 1 94.33 85.25 5.13 o -3 9 1 1.22 3.28 1.82 o -2 9 1 351.20 331.45 20.87 o -1 9 1 176.05 157.64 8.84 o 0 9 1 671.85 710.15 23.77 o 1 9 1 206.96 199.94 8.05 o 2 9 1 300.03 302.68 10.35 o 3 9 1 242.56 238.58 8.60 o 4 9 1 660.50 660.00 15.67 o 5 9 1 61.67 67.26 11.36 o 6 9 1 307.55 284.23 8.16 o -5 10 1 378.68 439.02 13.22 o -4 10 1 87.78 86.48 5.45 o -3 10 1 198.30 202.30 8.26 o -2 10 1 251.98 229.27 8.93 o -1 10 1 157.11 161.16 7.42 o 0 10 1 254.60 237.30 10.98 o 1 10 1 59.87 60.11 4.85 o 2 10 1 83.87 83.65 7.97 o 3 10 1 19.13 25.49 3.56 o 4 10 1 3.59 5.28 2.00 o 5 10 1 5.64 9.54 2.40 o -3 11 1 28.07 34.62 4.01 o -2 11 1 248.95 255.93 17.06 o -1 11 1 16.30 13.99 2.89 o 0 11 1 107.40 113.40 6.51 o 1 11 1 45.55 42.47 4.40 o 2 11 1 87.74 92.36 5.86 o 3 11 1 1.53 3.55 1.90 o -8 0 2 55.70 46.22 4.73 o -6 0 2 144.51 121.54 4.51 o -4 0 2 4.74 4.85 0.81 o -2 0 2 2767.71 2778.88 32.22 o 0 0 2 202.95 134.67 2.48 o 2 0 2 1.68 3.95 0.64 o 4 0 2 276.13 271.21 6.23 o 6 0 2 671.30 618.04 12.44 o 8 0 2 8.20 7.73 2.21 o -9 1 2 171.16 162.89 6.63 o -8 1 2 46.29 50.98 3.56 o -7 1 2 829.58 832.03 13.22 o -6 1 2 12.61 18.18 1.65 o -5 1 2 3209.75 3108.89 31.73 o -4 1 2 1.12 0.91 0.31 o -3 1 2 118.39 86.40 2.05 o -2 1 2 1198.97 1241.61 15.26 o -1 1 2 19660.20 19390.49 697.99 o 0 1 2 441.72 454.32 10.31 o 1 1 2 22711.16 22455.08 440.72 o 2 1 2 5492.72 5772.85 55.73 o 3 1 2 3724.16 3821.88 37.44 o 4 1 2 181.45 201.26 3.61 o 5 1 2 3927.36 4100.92 41.20 o 6 1 2 175.71 170.44 3.89 o 7 1 2 252.91 272.61 5.49 o 8 1 2 0.46 2.43 1.17 o 9 1 2 111.37 112.35 7.89 o -9 2 2 5.21 8.13 3.47 o -8 2 2 41.14 50.87 3.56 o -7 2 2 616.75 548.81 47.37 o -6 2 2 133.52 146.35 4.31 o -5 2 2 1230.15 1189.52 35.34 o -4 2 2 27.33 35.56 1.00 o -3 2 2 543.17 578.51 5.86 o -2 2 2 398.92 401.89 8.45 o -1 2 2 0.09 -0.17 0.51 o 0 2 2 123.44 130.39 5.30 o 1 2 2 3334.08 3365.17 72.29 o 2 2 2 43.30 32.53 1.00 o 3 2 2 153.74 141.50 2.39 o 4 2 2 6.78 6.65 1.55 o 5 2 2 36.35 40.79 1.80 o 6 2 2 126.11 123.55 3.36 o 7 2 2 464.67 441.36 7.49 o 8 2 2 58.16 58.85 3.85 o 9 2 2 7.92 8.20 2.68 o -9 3 2 191.04 210.51 7.93 o -8 3 2 136.66 137.15 4.83 o -7 3 2 946.89 927.51 14.91 o -6 3 2 7.50 13.37 1.73 o -5 3 2 2660.01 2688.45 32.79 o -4 3 2 87.79 92.63 2.31 o -3 3 2 6947.35 7089.78 104.74 o -2 3 2 2582.22 2717.85 41.78 o -1 3 2 3922.20 3780.59 34.40 o 0 3 2 436.12 437.92 5.76 o 1 3 2 1713.41 1559.61 31.48 o 2 3 2 2043.81 2206.57 23.12 o 3 3 2 2471.15 2533.00 36.76 o 4 3 2 21.86 16.65 2.07 o 5 3 2 1062.45 1051.12 18.29 o 6 3 2 607.32 611.33 9.06 o 7 3 2 795.53 799.74 23.09 o 8 3 2 2.63 5.05 2.05 o 9 3 2 62.37 59.63 5.84 o -9 4 2 68.14 83.93 5.84 o -8 4 2 203.05 195.90 6.07 o -7 4 2 198.51 195.31 5.77 o -6 4 2 823.64 781.95 12.95 o -5 4 2 36.22 42.66 2.46 o -4 4 2 102.56 74.41 2.98 o -3 4 2 17.09 15.51 2.13 o -2 4 2 222.67 219.40 3.88 o -1 4 2 178.03 207.34 4.54 o 0 4 2 649.75 650.93 8.27 o 1 4 2 34.93 25.71 1.54 o 2 4 2 8.38 9.58 2.09 o 3 4 2 72.70 77.92 1.73 o 4 4 2 13.93 18.73 1.17 o 5 4 2 42.48 48.55 1.75 o 6 4 2 56.96 53.77 5.76 o 7 4 2 101.61 93.96 3.69 o 8 4 2 150.85 140.94 9.31 o 9 4 2 106.90 108.55 8.20 o -9 5 2 128.71 139.20 5.31 o -8 5 2 54.98 57.63 3.78 o -7 5 2 249.86 247.80 6.78 o -6 5 2 164.83 163.61 5.16 o -5 5 2 843.85 890.67 14.13 o -4 5 2 173.96 186.12 4.10 o -3 5 2 3090.08 2956.50 31.88 o -2 5 2 8.66 12.70 1.73 o -1 5 2 668.90 657.61 10.48 o 0 5 2 2.81 3.16 0.97 o 1 5 2 2006.12 1954.38 24.24 o 2 5 2 1393.58 1343.75 14.11 o 3 5 2 940.77 894.41 10.15 o 4 5 2 1161.63 1183.38 12.17 o 5 5 2 308.59 290.77 7.39 o 6 5 2 271.27 269.68 4.81 o 7 5 2 744.57 715.47 13.95 o 8 5 2 82.53 84.24 7.10 o -8 6 2 21.42 19.76 1.92 o -7 6 2 47.81 42.92 2.53 o -6 6 2 278.61 245.26 5.46 o -5 6 2 41.47 42.78 2.55 o -4 6 2 1165.01 1108.87 16.59 o -3 6 2 162.51 141.43 5.36 o -2 6 2 400.21 393.56 24.53 o -1 6 2 17.68 26.43 6.39 o 0 6 2 811.40 800.30 16.14 o 1 6 2 0.71 1.92 0.86 o 2 6 2 275.13 266.28 6.05 o 3 6 2 192.60 184.81 4.32 o 4 6 2 188.24 167.31 4.39 o 5 6 2 315.15 309.75 7.16 o 6 6 2 384.78 359.68 6.49 o 7 6 2 60.34 58.49 3.29 o 8 6 2 62.47 52.53 5.52 o -8 7 2 20.17 21.88 2.34 o -7 7 2 6.72 12.27 3.02 o -6 7 2 53.32 48.86 2.99 o -5 7 2 129.04 139.65 4.48 o -4 7 2 60.84 58.05 3.95 o -3 7 2 7.10 8.14 2.01 o -2 7 2 714.96 682.41 14.41 o -1 7 2 268.12 244.42 7.54 o 0 7 2 30.53 27.28 2.95 o 1 7 2 1557.88 1510.60 25.26 o 2 7 2 519.59 526.24 9.87 o 3 7 2 145.98 149.76 4.19 o 4 7 2 517.40 508.31 12.46 o 5 7 2 326.47 313.33 7.61 o 6 7 2 49.27 51.46 3.10 o 7 7 2 203.82 193.82 6.16 o -7 8 2 87.38 81.33 6.23 o -6 8 2 165.05 140.26 6.46 o -5 8 2 17.51 18.77 2.90 o -4 8 2 781.39 770.29 19.90 o -3 8 2 12.26 15.64 2.56 o -2 8 2 526.30 526.55 19.71 o -1 8 2 70.84 62.03 4.18 o 0 8 2 729.38 786.09 25.85 o 1 8 2 512.52 517.23 12.64 o 2 8 2 455.16 468.60 11.80 o 3 8 2 344.70 331.35 6.81 o 4 8 2 358.91 357.28 13.12 o 5 8 2 281.83 289.51 7.61 o 6 8 2 239.72 254.82 7.25 o 7 8 2 307.66 318.25 8.49 o -6 9 2 0.02 0.09 1.39 o -5 9 2 19.60 29.98 8.12 o -4 9 2 9.96 8.53 2.40 o -3 9 2 16.91 19.98 3.05 o -2 9 2 205.18 214.60 18.40 o -1 9 2 78.60 70.60 4.69 o 0 9 2 185.50 168.61 7.50 o 1 9 2 7.80 5.12 2.04 o 2 9 2 4.20 3.09 2.92 o 3 9 2 39.07 47.98 3.52 o 4 9 2 64.46 67.03 4.35 o 5 9 2 197.03 206.70 12.70 o 6 9 2 46.94 60.41 5.54 o -5 10 2 1.40 2.89 1.55 o -4 10 2 240.44 257.13 9.66 o -3 10 2 71.73 66.68 5.05 o -2 10 2 713.11 717.90 36.43 o -1 10 2 21.44 18.77 3.23 o 0 10 2 555.52 591.74 17.17 o 1 10 2 235.97 217.55 13.82 o 2 10 2 431.39 448.54 16.05 o 3 10 2 171.05 180.21 7.75 o 4 10 2 250.85 256.46 9.32 o 5 10 2 43.16 59.32 4.56 o -3 11 2 7.16 10.44 2.51 o -2 11 2 0.88 3.65 1.73 o -1 11 2 9.66 17.79 5.28 o 0 11 2 84.61 96.75 14.59 o 1 11 2 42.60 47.92 4.65 o 2 11 2 19.02 18.35 3.23 o 3 11 2 58.44 69.61 5.02 o -9 0 3 571.22 574.25 20.25 o -7 0 3 1403.48 1402.79 33.94 o -5 0 3 474.19 471.96 8.88 o -3 0 3 2286.00 2296.74 27.44 o 1 0 3 4825.12 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